CN109554226A - A kind of preparation method of Rosa Damascana - Google Patents
A kind of preparation method of Rosa Damascana Download PDFInfo
- Publication number
- CN109554226A CN109554226A CN201710872568.6A CN201710872568A CN109554226A CN 109554226 A CN109554226 A CN 109554226A CN 201710872568 A CN201710872568 A CN 201710872568A CN 109554226 A CN109554226 A CN 109554226A
- Authority
- CN
- China
- Prior art keywords
- rose
- rosa damascana
- added
- roseleaf
- stoste
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
A kind of preparation method of Rosa Damascana, comprising the following specific steps (1) hand picking is fresh, and the roseleaf without small holes caused by worms or breakage；(2) 12% salt water of roseleaf is impregnated rose 3~5 hours；(3) it uses 8% salt water to impregnate again 1 hour the rose in step (2), then carries out vacreation；(4) roseleaf after vacreation in step (3) is put into container, distilled water is added and is stirred to obtain rose paste with blender；(5) rose paste in step (4) is put into boiler, first passes through direct steam heating to 85 DEG C, then use indirect steam heating instead to boiling, its condensate liquid is introduced into oil water separator progress water-oil separating and obtains Rosa Damascana stoste.
Description
Technical field
The invention belongs to daily chemical products related fieldss, and in particular to a kind of preparation method of Rosa Damascana.
Background technique
Rose is known as spending middle queen, and Rosa Damascana is the essential oil extracted after fresh rose flower is taken in the morning, about
The flower of five tons of weights can only extract two pounds of attar of rose, so being the essential oil of most expensive in the world, referred to as " after essential oil ".
The essential oil secreted out of in rose is the space between cells for being present in rose with small drop-wise, plays the hormonal angle of life
Color, can help rose adapt to around environment, resist the disease and insect pest.Rosa Damascana includes kind of the chemical substance more than 300, it
More thorough with fragrance volatilizing, the features such as no plant gelatinous precipitate are the rare advanced concentration essence in the world.Rosa Damascana is rich in
Vitamin C, carrotene, vitamin B and vitamin K.Rosa Damascana is Pure natural plant essential oil, mainly there is following functions: can be pierced
Sharp anterior lobe of cerebrum secrets out of that interior coffee is eliminated and brain coffee eliminates two kinds of hormone, makes spirit that the state of the most comfortable be presented；With antibacterial, anti-convulsion
Contraction is sterilized, is promoted the sexual maturity, purifying, is calm, mending body and other effects；Effect that is strong and shrinking capilary；Mood is smoothed, calm nerves are tight
And pressure；It keeps off infection, treatment skin adjusts endocrine, promotes human physiology and psychology activity.
Summary of the invention
It is an object of the invention to aiming at the shortcomings in the prior art, provide a kind of preparation method of Rosa Damascana.
In order to realize the present invention, using following technical scheme: a kind of preparation method of Rosa Damascana, including walk in detail below
It is rapid:
(1) hand picking is fresh, and the roseleaf without small holes caused by worms or breakage；
(2) 12% salt water of roseleaf is impregnated rose 3~5 hours；
(3) it uses 8% salt water to impregnate again 1 hour the rose in step (2), then carries out vacreation；
(4) roseleaf after vacreation in step (3) is put into container, distilled water is added and is stirred with blender
It mixes to obtain rose paste；
(5) rose paste in step (4) is put into boiler, first passes through direct steam heating to 85 DEG C, then used instead indirectly
It is steam heated to boiling, its condensate liquid is introduced into oil water separator progress water-oil separating and obtains Rosa Damascana stoste；
(6) lemon acid for adjusting pH value is added in the Rosa Damascana stoste obtained in step (5) to 3.6~4.7, is added 0.15%
After acid cellulose enzyme reaction 45 minutes, 0.22% pectase and 0.13% compound protein enzyme reaction 40 minutes are added；
(7) it takes the middle resulting Rosa Damascana stoste of reaction of step (6) to be put into 5 liters of fermentor, 1.2% glucose is added,
1.3% yeast extract, 0.8% tryptone, and pH to 6.2, reaction 28 are adjusted with 1mol/L phosphate buffer
85 DEG C of inactivations are heated to after hour.
Further, the rose stoste of the enzymatic hydrolysis and fermentation carries out constant flow filtering in sheet frame or utilizes ceramic membrane mistake
Filter, is concentrated in 30L Rotary Evaporators under 0.1Mpa pressure after filtering, and 6% alcohol is added up to rose after 800 times of concentration
Rare essential oil.
The utility model has the advantages that the present invention can delicate skin, bright color, reply the youth, moisturize the skin, releive, maintenance；It prevents
Pachylosis makes skin wet, softness, flexible, protection skin health.
Specific embodiment
Embodiment: a kind of preparation method of Rosa Damascana, comprising the following specific steps
(1) hand picking is fresh, and the roseleaf without small holes caused by worms or breakage；
(2) 12% salt water of roseleaf is impregnated rose 3~5 hours；
(3) it uses 8% salt water to impregnate again 1 hour the rose in step (2), then carries out vacreation；
(4) roseleaf after vacreation in step (3) is put into container, distilled water is added and is stirred with blender
It mixes to obtain rose paste；
(5) rose paste in step (4) is put into boiler, first passes through direct steam heating to 85 DEG C, then used instead indirectly
It is steam heated to boiling, its condensate liquid is introduced into oil water separator progress water-oil separating and obtains Rosa Damascana stoste；
(6) lemon acid for adjusting pH value is added in the Rosa Damascana stoste obtained in step (5) to 3.6~4.7, is added 0.15%
After acid cellulose enzyme reaction 45 minutes, 0.22% pectase and 0.13% compound protein enzyme reaction 40 minutes are added；
(7) it takes the middle resulting Rosa Damascana stoste of reaction of step (6) to be put into 5 liters of fermentor, 1.2% glucose is added,
1.3% yeast extract, 0.8% tryptone, and pH to 6.2, reaction 28 are adjusted with 1mol/L phosphate buffer
85 DEG C of inactivations are heated to after hour.
The rose stoste of the enzymatic hydrolysis and fermentation carries out constant flow filtering in sheet frame or using ceramic membrane filter, after filtering
It is concentrated in 30L Rotary Evaporators under 0.1Mpa pressure, 6% alcohol is added up to Rosa Damascana after 800 times of concentration.
Claims (2)
1. a kind of preparation method of Rosa Damascana, which is characterized in that comprising the following specific steps
(1) hand picking is fresh, and the roseleaf without small holes caused by worms or breakage；
(2) 12% salt water of roseleaf is impregnated rose 3~5 hours；
(3) it uses 8% salt water to impregnate again 1 hour the rose in step (2), then carries out vacreation；
(4) roseleaf after vacreation in step (3) is put into container, distilled water is added and is stirred with blender
It mixes to obtain rose paste；
(5) rose paste in step (4) is put into boiler, first passes through direct steam heating to 85 DEG C, then used instead indirectly
It is steam heated to boiling, its condensate liquid is introduced into oil water separator progress water-oil separating and obtains Rosa Damascana stoste；
(6) lemon acid for adjusting pH value is added in the Rosa Damascana stoste obtained in step (5) to 3.6~4.7, is added 0.15%
After acid cellulose enzyme reaction 45 minutes, 0.22% pectase and 0.13% compound protein enzyme reaction 40 minutes are added；
(7) it takes the middle resulting Rosa Damascana stoste of reaction of step (6) to be put into 5 liters of fermentor, 1.2% glucose is added,
1.3% yeast extract, 0.8% tryptone, and pH to 6.2, reaction 28 are adjusted with 1mol/L phosphate buffer
85 DEG C of inactivations are heated to after hour.
2. a kind of preparation method of Rosa Damascana according to claim 1, which is characterized in that the rose of the enzymatic hydrolysis and fermentation
Flower stoste is carried out in sheet frame constant flow filtering or utilize ceramic membrane filter, after filtering under 0.1Mpa pressure 30L rotary evaporation
It is concentrated in instrument, 6% alcohol is added up to Rosa Damascana after 800 times of concentration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710872568.6A CN109554226A (en) | 2017-09-25 | 2017-09-25 | A kind of preparation method of Rosa Damascana |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710872568.6A CN109554226A (en) | 2017-09-25 | 2017-09-25 | A kind of preparation method of Rosa Damascana |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109554226A true CN109554226A (en) | 2019-04-02 |
Family
ID=65863060
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710872568.6A Pending CN109554226A (en) | 2017-09-25 | 2017-09-25 | A kind of preparation method of Rosa Damascana |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109554226A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112662476A (en) * | 2020-12-30 | 2021-04-16 | 小金县夹金山清多香野生资源开发有限责任公司 | Extraction method of rose essential oil with high oil yield |
| CN114806714A (en) * | 2022-02-11 | 2022-07-29 | 安徽盛世百川农林科技发展有限公司 | Rose essential oil extraction method |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4301251A (en) * | 1979-02-07 | 1981-11-17 | Rumyantseva Galina N | Process for producing rose oil |
| US20020158015A1 (en) * | 1999-07-13 | 2002-10-31 | Danisco A/S | Process for separating essential oils from an essential oil-containing material |
| CN102776072A (en) * | 2012-07-09 | 2012-11-14 | 广州市澳键丰泽生物科技有限公司 | Method for preparing rose essential oil |
| CN105820879A (en) * | 2015-01-05 | 2016-08-03 | 达金兰 | Preparation method of rose essential oil |
| CN105969528A (en) * | 2016-06-14 | 2016-09-28 | 云南金大康农业科技有限公司 | Extracting method for rose essential oil |
| CN106281700A (en) * | 2016-08-16 | 2017-01-04 | 重庆雅香美源生态农业科技有限公司 | The extraction of Flos Rosae Rugosae quintessence oil and processing method |
-
2017
- 2017-09-25 CN CN201710872568.6A patent/CN109554226A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4301251A (en) * | 1979-02-07 | 1981-11-17 | Rumyantseva Galina N | Process for producing rose oil |
| US20020158015A1 (en) * | 1999-07-13 | 2002-10-31 | Danisco A/S | Process for separating essential oils from an essential oil-containing material |
| CN102776072A (en) * | 2012-07-09 | 2012-11-14 | 广州市澳键丰泽生物科技有限公司 | Method for preparing rose essential oil |
| CN105820879A (en) * | 2015-01-05 | 2016-08-03 | 达金兰 | Preparation method of rose essential oil |
| CN105969528A (en) * | 2016-06-14 | 2016-09-28 | 云南金大康农业科技有限公司 | Extracting method for rose essential oil |
| CN106281700A (en) * | 2016-08-16 | 2017-01-04 | 重庆雅香美源生态农业科技有限公司 | The extraction of Flos Rosae Rugosae quintessence oil and processing method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112662476A (en) * | 2020-12-30 | 2021-04-16 | 小金县夹金山清多香野生资源开发有限责任公司 | Extraction method of rose essential oil with high oil yield |
| CN114806714A (en) * | 2022-02-11 | 2022-07-29 | 安徽盛世百川农林科技发展有限公司 | Rose essential oil extraction method |
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Application publication date: 20190402 |