CN110279630A

CN110279630A - A kind of sugarcane vinegar is taken a shower packet and preparation method thereof

Info

Publication number: CN110279630A
Application number: CN201910682673.2A
Authority: CN
Inventors: 郑凤锦; 陈赶林; 李志春; 林波; 方晓纯; 孙健
Original assignee: Guangxi Zhuang Nationality Autonomous Region Academy of Agricultural Sciences
Current assignee: Guangxi Zhuang Nationality Autonomous Region Academy of Agricultural Sciences
Priority date: 2019-07-26
Filing date: 2019-07-26
Publication date: 2019-09-27
Anticipated expiration: 2039-07-26
Also published as: CN110279630B

Abstract

The present invention provides a kind of sugarcane vinegar and takes a shower packet and preparation method thereof, it is related to bath article technical field, sugarcane vinegar of the invention is taken a shower to wrap and is made of the raw material of following parts by weight: 8-10 parts of passion fruit branch, 10-15 parts of lychee leaf, 8-12 parts of honeysuckle, bluegrass 5-8 parts red, 2-3 parts of sea salt, 2-3 parts of common four-o' clock leaf, 6-10 parts of Fructus Aurantii, 7-14 parts of composite essential oil and 18-25 parts of sugarcane vinegar；Sugarcane vinegar of the invention takes a shower packet for putting into shower container before shower, release anti-inflammation components and weight reducing action component can be dissolved, sterilizing can be carried out to the skin of user, improve body defenses external world harmful microbe ability, promote skin blood circulation, unfold pore, effective component is promoted to absorb, has the function of sweating weight reducing, perfume body, anti-inflammatory, warming up；And this product is easy to use, is suitble to crowd extensive.

Description

A kind of sugarcane vinegar is taken a shower packet and preparation method thereof

[technical field]

The present invention relates to bath article technical fields, and in particular to a kind of sugarcane vinegar is taken a shower packet and preparation method thereof.

[background technique]

" shower " has a bath, and can remove sweat mixed with dirt greasy dirt, eliminate fatigue, relaxing tendons and activating collaterals, improves sleep, raising skin new old generation Thank function and premunition.The mode of bathing includes rushing bath and bathing.

Current city life rhythm is fast, and busy life often makes people dog-tired, because bathing with warm rapidly Body and mind excludes vivotoxin, improves skin care efficiency, alleviates eye strain, pore dirt is cleared off, easily removing body angle The effects of matter, many people can select to bath to eliminate fatigue, calm nerves.

But simple baths it will be seen that it is played the role of being very small.Therefore, it is necessary to one kind to bath with washing one's hair Bath packet is used for the shower packet bathed by its effect currently on the market and is divided into two major classes to reinforce the beneficial effect bathed, and one It is the shower packet based on cleaning skin, increase body note, another kind is medicinal shower packet, and either cleaning is taken a shower to wrap and be washed one's hair with medicinal Bath packet, will the stringent characteristic according to component adjust application method, existing showers, which is wrapped, to be had the disadvantage that 1. mostly by chemical industry Product preparation, therefore always remain more chemical component, to be easy to damage skin；2. utilization rate is not high, bubble Skin is extremely limited to the absorption of shower packet effective component during bath；3. effect is single and using effect is bad.

Based on this, the present invention provides a kind of shower packet containing sugarcane vinegar.

[summary of the invention]

In view of this, of the invention is sweet the purpose of the present invention is to provide a kind of sugarcane vinegar shower packet and preparation method thereof Sugarcane vinegar takes a shower packet for putting into shower container before shower, can dissolve and discharge anti-inflammation components and weight reducing action component, can Sterilizing is carried out to the skin of user, improves body defenses external world harmful microbe ability, promotes skin blood circulation, Unfold pore, effective component is promoted to absorb.

In order to solve the above-mentioned technical problem, present invention employs the following technical solutions:

A kind of sugarcane vinegar shower packet, the sugarcane vinegar are taken a shower to wrap and be made of the raw material of following parts by weight: passion fruit branch 8-10 Part, 10-15 parts of lychee leaf, 8-12 parts of honeysuckle, bluegrass 5-8 parts red, 2-3 parts of sea salt, 2-3 parts of common four-o' clock leaf, 6-10 parts of Fructus Aurantii, 7-14 parts and sugarcane vinegar 18-25 parts of composite essential oil.

In the present invention, further, the sugarcane vinegar is taken a shower to wrap and is made of the raw material of following parts by weight: 9 parts of passion fruit branch, 12 parts of lychee leaf, 10 parts of honeysuckle, 6 parts of red bluegrass, 2 parts of sea salt, 2 parts of common four-o' clock leaf, 8 parts of Fructus Aurantii, 10 parts of essential oil and sugarcane vinegar 22 parts.

In the present invention, further, the composite essential oil is made of the raw material of following parts by weight: 6-12 parts of menthol, reed 4-9 parts of luxuriant growth, 5-10 parts of ginger and 3-8 parts of tea seed.

In the present invention, further, the composite essential oil obtains by the following method:

(1) tea seed is carried out being crushed to 30-50 mesh, then carries out supercritical CO₂Extraction, the oil that will be obtained by extraction Rouge carries out water-oil separating, removes water layer, carries out molecular distillation at being 100-140 DEG C in temperature by obtained crude oil, obtains oil tea Seed oil；

(2) take aloe be added with its etc. quality distilled water, be then put into fractionating device, carried out under the conditions of 60-85 DEG C Fractionation is extracted, and extract is obtained；It is extracted to the sodium chloride for obtaining the quality such as addition in extract, then filters to take oil reservoir, Up to aloe essential oil；

(3) it is handled after cleaning ginger by saline solution soaking sterilization, is then crushed to 20-50 mesh, is subsequently placed in hair Ferment ferments 24-48 hours at a temperature of filling 75-80 DEG C inherent, forms ginger fermentation material；Ginger fermentation material is sent into extraction kettle, It is extracted through first time extraction and second, collects and merge the CO containing extract₂, through first time parsing separation and parse for second Separation is collected separating liquid A and separating liquid B and is merged, obtains oil of ginger crude product, oil of ginger crude product is stirred under water bath condition, into Oil is mutually filtered by vacuum in row water-oil separating, and collection obtains ginger essential oil；

(4) ginger essential oil obtained by aloe essential oil obtained by step (2) and step (3) is mixed, is heated up to 60-70 DEG C, and Camellia seed oil is added in whipping process, forms mixed liquor, is then allowed to stand, so that the temperature of mixed liquor is down to room temperature, then add Menthol, and stir 45-55 minutes, obtain the composite essential oil.

In the present invention, further, the sugarcane vinegar obtains by the following method:

1) it squeezes sugar-cane juice: sugarcane is squeezed, and flip sugarcane juice liquid level foam, stand, it is spare to obtain sugar-cane juice；

2) fermented pretreatment: pure water is added into sugar-cane juice obtained by step 1), pol is adjusted to 10-12Brix, is obtained To sugarcane liquid；Then 0.3-0.5 times of weight of sugarcane liquid of purslane is added in sugarcane liquid, obtains mixture A；Purslane is adding 30-40 mesh is first crushed to before entering；

3) one time fermentation: the mixture A that step 2) obtains is transferred in sealed fermenting tank, is then added in the fermenter The grape wine schlempe for accounting for the belt leather fermentation of mixture A mass 10-15%, ferments under the conditions of 25-30 DEG C to the alcohol of fermentation liquid Degree reaches 8-10% (v/v), stops fermentation, obtains mixture B；Wherein, the grape wine schlempe of belt leather fermentation is by belt leather grape And after making grape wine required raw material mixed fermentation 30-120 days, filter residue that finished product is separated by solid-liquid separation；

4) secondary fermentation: mixture B obtained by step 3) is accessed into the acetic acid bacteria activated according to 12% inoculum concentration, is being sent out Ferment temperature is fermented 8-10 days under conditions of being 25-35 DEG C, obtains mixture C；

5) it filters: mixture C obtained by step 4) being filtered by filter press technique, sugarcane vinegar can be obtained in sterilization treatment.

The present invention also provides a kind of preparation methods of sugarcane vinegar shower packet, include the following steps:

A. it prepares Plant Powder: passion fruit branch, honeysuckle, red bluegrass, common four-o' clock leaf being cleaned into removal of impurities, it is aqueous to be dried to material Amount is lower than 10%, was then crushed to 80-100 mesh, it is spare to obtain Plant Powder；

B. it preparing Fructus Aurantii powder: flesh is removed into Fructus Aurantii chopping, the alcohol reflux of the 70-80% then measured with 5-7 times extracts 2 times, 1-2 hours every time, obtained Fructus Aurantii extracting solution is concentrated under reduced pressure, the medicinal extract that relative density is 1.2-1.3 is obtained, by medicinal extract It is dried to obtain Fructus Aurantii powder spare；

C. lychee leaf is handled: being taken bottle-green lychee leaf and is accounted for the calcium carbonate and Zhan Lizhi of lychee leaf weight 0.2-0.5% The quartz sand of leaf weight 0.05-0.1%, co-grinding obtain lychee leaf powder, by lychee leaf powder pressure be 0.12-0.16MPa, Temperature is 110-128 DEG C, and acidity hydrolyzes 3-4h under conditions of being 1.0-1.6%；Hydrolyzate is then obtained by filtration, controls hydrolyzate Temperature is 40-50 DEG C, 95% alcohol is added, ligninase and cellulase react 1 hour, then by hydrolyzate be warming up to 83 DEG C into Row enzyme deactivation 10min；After enzyme deactivation then amylase, protease are added in hydrolyzate, then passes through control to 45 DEG C for cooling hydrolyzate The centrifugal rotational speed of centrifuge processed separates chlorophyll and mother liquor, by controlling the temperature and ambient humidity of dryer, makes in chlorophyll Moisture evaporation, obtain lychee leaf chlorophyll product；

D. it the processing of sea salt: takes sea salt to crush to obtain sea salt powder, was then crushed to 80-100 mesh again, it is thin to obtain sea salt Powder is spare；

E. mixing granulation: Plant Powder, Fructus Aurantii powder, lychee leaf chlorophyll are mixed, sugarcane vinegar and composite essential oil are subsequently added into It mixes, and is placed in centrifugal granulator and first sprays alcohol master batch, until master batch forms dried for standby after larger particles, as take a shower Particle；

F. packed: to be sealed bath granules are packed into non-woven bag by the amount of 110-140g/ packet obtained by step d again, i.e., Obtain the sugarcane vinegar shower packet.

In conclusion by adopting the above-described technical solution, the present invention is include at least the following beneficial effects:

1. sugarcane vinegar of the invention is taken a shower, packet uses passion fruit branch, lychee leaf, honeysuckle, red bluegrass, sea salt, common four-o' clock leaf The effect of Fructus Aurantii, composite essential oil and sugarcane vinegar are raw material, science and effectively by honeysuckle dispelling wind-heat, removing summer-heat blood poison, it is compound The effect of essential oil unfolds pore, sorbefacient special role, and sugarcane vinegar bactericidal antiphlogistic effect and Fructus Aurantii are reduced weight combines, In bathing experience, by impregnating in the aqueous solution containing nutriment, human skin can absorb small molecule nutriment, from And sterilizing is carried out to the skin of user, pore is opened by sugarcane vinegar, Fructus Aurantii promotes blood circulation, by red bluegrass, sea Salt and common four-o' clock leaf combine, and further sterilize to skin, have good effect to all kinds of skin diseases such as treatment psoriasis, and Body defenses external world harmful microbe ability is improved, fundamentally improves immunity of organisms, and the compounding of component can promote It is recycled into skin blood, unfolds pore, effective component is promoted to absorb, there is good health-care efficacy.The pure day of raw material of the present invention So, nontoxic, non-stimulated, smell faint scent, and using there is no any method and temporal limitations, it is convenient and practical, it is suitble to crowd Extensively.

Contain Fructus Aurantii in packet 2. sugarcane vinegar of the invention is taken a shower, and the synephrine contained in Fructus Aurantii has lipolytic work With, when bathing, synephrine is absorbed by skin, into each pore of body, can stimulate sympathetic activation, directly burn, Consumption is stored at intracorporal fat, reduces appetite and achievees the purpose that eat less.

3. it has been found that human body is extremely limited to the drug absorption effect in water of bathing during bathing, this be by There is one layer of barrier in skin surface, affects to extraneous absorption, the primary absorption pathway of skin is to infiltrate through corneocyte, Through epidermis, other each layers reach corium and are absorbed again, and sugarcane vinegar is added in the application, cooperate menthol, can effectively soften skin The cuticula on surface, and sugarcane vinegar molecular weight is small, good penetrability is easy to be absorbed by the skin, and cooperates the aloe essential oil of the application, can So that skin layers water content increases, moisture retention is played, thus enhance the absorbability of skin, furthermore, sugarcane vinegar can sterilize Anti-inflammatory, and mild safety, go deep into lesion of going directly inside skin, cooperate ginger essential oil, can boost metabolism, reinforce bactericidal antiphlogistic Effect, the mild nursing of the tea seed essential oil of cooperation make skin be in state in the pink of condition.

4. the present invention is in the extraction process of ginger essential oil, after ginger powder is crushed to suitable partial size first, destroy The cell wall of ginger refines its particle, and essential oil is more easier to extract, and makes dry matter in ginger by storing sth. in a cellar fermentation And the content of essential oil tends towards stability, and the nutritional ingredient in ginger is made to ferment, concentration synthesizes new important chemical component, leads to The extraction and parsing for crossing secondary different pressures, avoid the use of high pressure, and extraction time is short, improves production efficiency, obtain Oil of ginger crude yield it is high, be conducive to subsequent purifying.

5. the present invention, using the chlorophyll extracted in lychee leaf as one of the component for packet of taking a shower, chlorophyll is a kind of good Natural pigment, and have refreshing and detoxicating, moisturizing, resist the effects of radiation, be present in one of green plants it is unique and Important nutriment cooperates with the plant essence liquid phase of the application, can be improved the stability of product.

[specific embodiment]

The following examples can help those skilled in the art that the present invention is more fully understood, but cannot be with any Mode limits the present invention.

Embodiment 1

It takes a shower to wrap the present embodiment provides a kind of sugarcane vinegar and be made of the raw material of following parts by weight: 8 parts of passion fruit branch, lychee leaf 10 parts, 8 parts of honeysuckle, 5 parts of red bluegrass, 2 parts of sea salt, 2 parts of common four-o' clock leaf, 6 parts of Fructus Aurantii, 7 parts of composite essential oil and 18 parts of sugarcane vinegar； Wherein, composite essential oil is made of the raw material of following parts by weight: 6 parts of menthol, 4 parts of aloe, 5 parts of ginger and 3 parts of tea seed.

The present embodiment also provides the method for preparing a kind of above-mentioned sugarcane vinegar shower packet, comprising the following steps:

(1) composite essential oil is prepared

(1) tea seed is carried out being crushed to 30 meshes, then carries out supercritical CO₂Extraction, the grease that will be obtained by extraction Water-oil separating is carried out, water layer is removed, molecular distillation is carried out at being 100 DEG C in temperature by obtained crude oil, obtains camellia seed oil；

(2) take aloe be added with its etc. quality distilled water, be then put into fractionating device, be fractionated under the conditions of 60 DEG C It extracts, obtains extract；Extracted to the sodium chloride of quality such as obtaining being added in extract, then filter to take oil reservoir to get Aloe essential oil；

(3) it is handled after cleaning ginger by saline solution soaking sterilization, is then crushed to 20 meshes, be subsequently placed in fermentation and fill It ferments 24 hours at a temperature of 75 DEG C inherent, forms ginger fermentation material；Ginger fermentation material is sent into extraction kettle, is extracted for the first time It takes and second extracts, collect and merge the CO containing extract₂, separate, collect through first time parsing separation and second of parsing Separating liquid A and separating liquid B merges, and obtains oil of ginger crude product, oil of ginger crude product is stirred under water bath condition, carries out grease point From, to oil be mutually filtered by vacuum, collect obtain ginger essential oil；

(4) ginger essential oil obtained by aloe essential oil obtained by step (2) and step (3) is mixed, is heated up to 60 DEG C, and stirring Camellia seed oil is added in the process, forms mixed liquor, is then allowed to stand, so that the temperature of mixed liquor is down to room temperature, then add peppermint Brain, and stir 45 minutes, obtain the composite essential oil.

(2) sugarcane vinegar is prepared

2) fermented pretreatment: pure water is added into sugar-cane juice obtained by step 1), pol is adjusted to 10Brix, is obtained sweet Sugarcane liquid；Then the purslane of 0.3 times of sugarcane liquid weight is added in sugarcane liquid, obtains mixture A；Purslane first powder before addition It is broken to 30 mesh；

3) one time fermentation: the mixture A that step 2) obtains is transferred in sealed fermenting tank, is then added in the fermenter The grape wine schlempe of the belt leather fermentation of mixture A mass 10% is accounted for, the alcoholic strength to ferment under the conditions of 25 DEG C to fermentation liquid reaches 8% (v/v) stops fermentation, obtains mixture B；Wherein, the grape wine schlempe of belt leather fermentation is by belt leather grape and brewing Portugal Needed for grape wine after raw material mixed fermentation 30 days, filter residue that finished product is separated by solid-liquid separation；

4) secondary fermentation: mixture B obtained by step 3) is accessed into the acetic acid bacteria activated according to 12% inoculum concentration, is being sent out Ferment temperature is fermented 8 days under conditions of being 25 DEG C, obtains mixture C；

(3) preparation sugarcane vinegar, which is taken a shower, wraps

A. it prepares Plant Powder: passion fruit branch, honeysuckle, red bluegrass, common four-o' clock leaf being cleaned into removal of impurities, it is aqueous to be dried to material Amount is lower than 10%, was then crushed to 80 meshes, it is spare to obtain Plant Powder；

B. it prepares Fructus Aurantii powder: flesh is removed into Fructus Aurantii chopping, then with the 70% alcohol reflux extraction of 5 times of amounts 2 times, every time 1 Hour, obtained Fructus Aurantii extracting solution is concentrated under reduced pressure, the medicinal extract that relative density is 1.2 is obtained, medicinal extract is dried It is spare to Fructus Aurantii powder；

C. lychee leaf is handled: being taken bottle-green lychee leaf and is accounted for the calcium carbonate of lychee leaf weight 0.2% and account for lychee leaf weight The quartz sand of amount 0.05%, co-grinding obtains lychee leaf powder, in pressure is 0.12MPa by lychee leaf powder, and temperature is 110 DEG C, Acidity hydrolyzes 3h under conditions of being 1.0%；Hydrolyzate is then obtained by filtration, control hydrolyzate temperature is 40 DEG C, and 95% wine is added Essence, ligninase and cellulase react 1 hour, and hydrolyzate is then warming up to 83 DEG C of progress enzyme deactivation 10min；Cooling water after enzyme deactivation Liquid is solved to 45 DEG C, amylase, protease are then added in hydrolyzate, then passes through the centrifugal rotational speed of control centrifuge, separation Chlorophyll and mother liquor evaporate the moisture in chlorophyll, obtain lychee leaf leaf by controlling the temperature and ambient humidity of dryer Green element product；

D. it the processing of sea salt: takes sea salt to crush to obtain sea salt powder, was then crushed to 80 meshes again, it is standby to obtain sea salt fine powder With；

F. packed: to be sealed again by bath granules are packed into non-woven bag by the amount of 110g/ packet obtained by step d to get institute State sugarcane vinegar shower packet.

Embodiment 2

It takes a shower to wrap the present embodiment provides a kind of sugarcane vinegar and be made of the raw material of following parts by weight: 9 parts of passion fruit branch, lychee leaf 12 parts, 10 parts of honeysuckle, 6 parts of red bluegrass, 2 parts of sea salt, 2 parts of common four-o' clock leaf, 8 parts of Fructus Aurantii, 10 parts of essential oil and 22 parts of sugarcane vinegar；Its In, composite essential oil is made of the raw material of following parts by weight: 8 parts of menthol, 7 parts of aloe, 7 parts of ginger and 6 parts of tea seed.

(1) composite essential oil is prepared

(1) tea seed is carried out being crushed to 40 meshes, then carries out supercritical CO₂Extraction, the grease that will be obtained by extraction Water-oil separating is carried out, water layer is removed, molecular distillation is carried out at being 120 DEG C in temperature by obtained crude oil, obtains camellia seed oil；

(2) take aloe be added with its etc. quality distilled water, be then put into fractionating device, be fractionated under the conditions of 72 DEG C It extracts, obtains extract；Extracted to the sodium chloride of quality such as obtaining being added in extract, then filter to take oil reservoir to get Aloe essential oil；

(3) it is handled after cleaning ginger by saline solution soaking sterilization, is then crushed to 35 meshes, be subsequently placed in fermentation and fill It ferments 36 hours at a temperature of 77 DEG C inherent, forms ginger fermentation material；Ginger fermentation material is sent into extraction kettle, is extracted for the first time It takes and second extracts, collect and merge the CO containing extract₂, separate, collect through first time parsing separation and second of parsing Separating liquid A and separating liquid B merges, and obtains oil of ginger crude product, oil of ginger crude product is stirred under water bath condition, carries out grease point From, to oil be mutually filtered by vacuum, collect obtain ginger essential oil；

(4) ginger essential oil obtained by aloe essential oil obtained by step (2) and step (3) is mixed, is heated up to 65 DEG C, and stirring Camellia seed oil is added in the process, forms mixed liquor, is then allowed to stand, so that the temperature of mixed liquor is down to room temperature, then add peppermint Brain, and stir 50 minutes, obtain the composite essential oil.

(2) sugarcane vinegar is prepared

2) fermented pretreatment: pure water is added into sugar-cane juice obtained by step 1), pol is adjusted to 11Brix, is obtained sweet Sugarcane liquid；Then the purslane of 0.4 times of sugarcane liquid weight is added in sugarcane liquid, obtains mixture A；Purslane first powder before addition It is broken to 35 mesh；

3) one time fermentation: the mixture A that step 2) obtains is transferred in sealed fermenting tank, is then added in the fermenter The grape wine schlempe of the belt leather fermentation of mixture A mass 12% is accounted for, the alcoholic strength to ferment under the conditions of 27 DEG C to fermentation liquid reaches 9% (v/v) stops fermentation, obtains mixture B；Wherein, the grape wine schlempe of belt leather fermentation is by belt leather grape and brewing Portugal Needed for grape wine after raw material mixed fermentation 60 days, filter residue that finished product is separated by solid-liquid separation；

4) secondary fermentation: mixture B obtained by step 3) is accessed into the acetic acid bacteria activated according to 12% inoculum concentration, is being sent out Ferment temperature is fermented 9 days under conditions of being 30 DEG C, obtains mixture C；

(3) preparation sugarcane vinegar, which is taken a shower, wraps

A. it prepares Plant Powder: passion fruit branch, honeysuckle, red bluegrass, common four-o' clock leaf being cleaned into removal of impurities, it is aqueous to be dried to material Amount is lower than 10%, was then crushed to 90 meshes, it is spare to obtain Plant Powder；

B. it prepares Fructus Aurantii powder: flesh is removed into Fructus Aurantii chopping, 75% alcohol reflux then measured with 6 times extracts 2 times, each 1- 2 hours, obtained Fructus Aurantii extracting solution is concentrated under reduced pressure, obtains the medicinal extract that relative density is 1.2, medicinal extract is dried It is spare to Fructus Aurantii powder；

C. lychee leaf is handled: being taken bottle-green lychee leaf and is accounted for the calcium carbonate of lychee leaf weight 0.4% and account for lychee leaf weight The quartz sand of amount 0.07%, co-grinding obtains lychee leaf powder, in pressure is 0.14MPa by lychee leaf powder, and temperature is 119 DEG C, Acidity hydrolyzes 3.5h under conditions of being 1.3%；Hydrolyzate is then obtained by filtration, control hydrolyzate temperature is 45 DEG C, is added 95% Alcohol, ligninase and cellulase react 1 hour, and hydrolyzate is then warming up to 83 DEG C of progress enzyme deactivation 10min；It is cooling after enzyme deactivation Then amylase, protease is added to 45 DEG C in hydrolyzate in hydrolyzate, then by the centrifugal rotational speed of control centrifuge, divide The moisture in chlorophyll is evaporated, lychee leaf is obtained by controlling the temperature and ambient humidity of dryer from chlorophyll and mother liquor Chlorophyll product；

D. it the processing of sea salt: takes sea salt to crush to obtain sea salt powder, was then crushed to 90 meshes again, it is standby to obtain sea salt fine powder With；

F. packed: to be sealed again by bath granules are packed into non-woven bag by the amount of 125g/ packet obtained by step d to get institute State sugarcane vinegar shower packet.

Embodiment 3

It takes a shower to wrap the present embodiment provides a kind of sugarcane vinegar and be made of the raw material of following parts by weight: 10 parts of passion fruit branch, lichee 15 parts of leaf, 12 parts of honeysuckle, 8 parts of red bluegrass, 3 parts of sea salt, 3 parts of common four-o' clock leaf, 10 parts of Fructus Aurantii, 14 parts of composite essential oil and sugarcane vinegar 25 parts；Wherein, composite essential oil is made of the raw material of following parts by weight: 12 parts of menthol, 9 parts of aloe, 10 parts of ginger and tea seed 8 Part.

(1) composite essential oil is prepared

(1) tea seed is carried out being crushed to 50 meshes, then carries out supercritical CO₂Extraction, the grease that will be obtained by extraction Water-oil separating is carried out, water layer is removed, molecular distillation is carried out at being 140 DEG C in temperature by obtained crude oil, obtains camellia seed oil；

(2) take aloe be added with its etc. quality distilled water, be then put into fractionating device, be fractionated under the conditions of 85 DEG C It extracts, obtains extract；Extracted to the sodium chloride of quality such as obtaining being added in extract, then filter to take oil reservoir to get Aloe essential oil；

(3) it is handled after cleaning ginger by saline solution soaking sterilization, is then crushed to 50 meshes, be subsequently placed in fermentation and fill It ferments 48 hours at a temperature of 80 DEG C inherent, forms ginger fermentation material；Ginger fermentation material is sent into extraction kettle, is extracted for the first time It takes and second extracts, collect and merge the CO containing extract₂, separate, collect through first time parsing separation and second of parsing Separating liquid A and separating liquid B merges, and obtains oil of ginger crude product, oil of ginger crude product is stirred under water bath condition, carries out grease point From, to oil be mutually filtered by vacuum, collect obtain ginger essential oil；

(4) ginger essential oil obtained by aloe essential oil obtained by step (2) and step (3) is mixed, is heated up to 70 DEG C, and stirring Camellia seed oil is added in the process, forms mixed liquor, is then allowed to stand, so that the temperature of mixed liquor is down to room temperature, then add peppermint Brain, and stir 55 minutes, obtain the composite essential oil.

(2) sugarcane vinegar is prepared

2) fermented pretreatment: pure water is added into sugar-cane juice obtained by step 1), pol is adjusted to 12Brix, is obtained sweet Sugarcane liquid；Then the purslane of 0.5 times of sugarcane liquid weight is added in sugarcane liquid, obtains mixture A；Purslane first powder before addition It is broken to 40 mesh；

3) one time fermentation: the mixture A that step 2) obtains is transferred in sealed fermenting tank, is then added in the fermenter The grape wine schlempe of the belt leather fermentation of mixture A mass 15% is accounted for, the alcoholic strength to ferment under the conditions of 30 DEG C to fermentation liquid reaches 10% (v/v) stops fermentation, obtains mixture B；Wherein, the grape wine schlempe of belt leather fermentation is by belt leather grape and brewing Needed for grape wine after raw material mixed fermentation 120 days, filter residue that finished product is separated by solid-liquid separation；

4) secondary fermentation: mixture B obtained by step 3) is accessed into the acetic acid bacteria activated according to 12% inoculum concentration, is being sent out Ferment temperature is fermented 10 days under conditions of being 35 DEG C, obtains mixture C；

(3) preparation sugarcane vinegar, which is taken a shower, wraps

A. it prepares Plant Powder: passion fruit branch, honeysuckle, red bluegrass, common four-o' clock leaf being cleaned into removal of impurities, it is aqueous to be dried to material Amount is lower than 10%, is then crushed to and sieves with 100 mesh sieve, it is spare to obtain Plant Powder；

B. it prepares Fructus Aurantii powder: flesh is removed into Fructus Aurantii chopping, then with the 80% alcohol reflux extraction of 7 times of amounts 2 times, every time 2 Hour, obtained Fructus Aurantii extracting solution is concentrated under reduced pressure, the medicinal extract that relative density is 1.3 is obtained, medicinal extract is dried It is spare to Fructus Aurantii powder；

C. lychee leaf is handled: being taken bottle-green lychee leaf and is accounted for the calcium carbonate of lychee leaf weight 0.5% and account for lychee leaf weight The quartz sand of amount 0.1%, co-grinding obtains lychee leaf powder, in pressure is 0.16MPa by lychee leaf powder, temperature is 128 DEG C, acid Degree hydrolyzes 4h under conditions of being 1.6%；Hydrolyzate is then obtained by filtration, control hydrolyzate temperature is 50 DEG C, 95% alcohol of addition, Ligninase and cellulase react 1 hour, and hydrolyzate is then warming up to 83 DEG C of progress enzyme deactivation 10min；Cooling hydrolysis after enzyme deactivation Then amylase, protease is added to 45 DEG C in liquid in hydrolyzate, then by the centrifugal rotational speed of control centrifuge, separate leaf Green element and mother liquor evaporate the moisture in chlorophyll, it is green to obtain lychee leaf leaf by controlling the temperature and ambient humidity of dryer Plain product；

D. it the processing of sea salt: takes sea salt to crush to obtain sea salt powder, is then crushed to and sieves with 100 mesh sieve again, obtain sea salt fine powder It is spare；

F. packed: to be sealed again by bath granules are packed into non-woven bag by the amount of 140g/ packet obtained by step d to get institute State sugarcane vinegar shower packet.

Compliance test result

It takes a shower in order to further illustrate the present invention the practical value of packet, does following comparative testing: five groups below comparative test It takes a shower the characteristic of packet, wherein slimming effect, moistening effect are all made of " ++++" " +++ ", and " ++ " "+" indicates that its effect is poor Not；By collection trier, the feedback after carries out Contrast on effect to anti-inflammatory anti-itch effect；Allergy rate is that user allergy occurs Shape crowd accounts for the percentage of user, and allergic symptom includes redness, itch or bleb.

The application method of shower packet are as follows: will take a shower before shower and wrap investment water temperature to impregnate 5 points in 45 DEG C of shower container Person on probation baths after clock, and the time of bathing is 30 minutes, and the number on probation of every kind of packet of taking a shower is 20 people, wherein every group has 5 People has different degrees of dermatitis symptom, and test period was five week.Experimental result is as shown in table 1:

First group: cooperating mode described above to bath using the shower packet in the embodiment of the present invention 2；

Second group: removing this raw material of sugarcane vinegar, other modes are identical as first group；

Third group: removing this raw material of Fructus Aurantii, and other modes are identical as first group；

4th group: self-control composite essential oil is changed to Kneipp/ valerian hops water solubility and bathed and bathes essential oil, other modes with First group identical；

5th group: the step of lychee leaf is handled modification are as follows: take lychee leaf to crush to obtain lychee leaf powder, it is spare；Its other party Formula is identical as first group.

Table 1

As can be seen from Table 1, from the stability of product, the 5th group of product is unstable, this shows that chlorophyll influences The stability of the stability of product, the product of Determination of Chlorophyll is preferable.From allergy rate, essential oil is changed to essential oil on the market In the case of, there is relatively large number of allergic phenomena, be since derived essential oil on the market is not mild enough, it is quick containing chemical substance Sense skin does not tolerate, 4 allergic phenomenas of the 5th group of appearance, it is believed that caused since product is unstable；Come from weight-reducing effect It sees, 2 product slimming effect of the embodiment of the present invention is good, and the slimming effect of third group is poor, and bathing can be improved metabolism, promotes It perspires, therefore has certain fat-reducing effect, but after joined Fructus Aurantii of the invention, the synephrine contained, which has, to reduce fat Effect, and equally including Fructus Aurantii component second group and the 4th group of slimming effect be not so good as first group, show that two groups of ingredients exist Weight reducing aspect has significant synergistic effect, this is because human body is extremely limited to the drug absorption effect in water of bathing, this be by There is one layer of barrier in skin surface, affects to extraneous absorption, essential oil and sugarcane vinegar can speed up skin to nutritional ingredient It absorbs, when bathing, synephrine is absorbed by skin, into each pore of body, can be stimulated sympathetic activation, directly be fired Burning, consumption are stored at intracorporal fat, reduce appetite and achieve the purpose that eat less；For moistening effect, the 4th group of moistening effect It is worst, illustrate composite essential oil of the invention can moisturizing, promote drug absorption simultaneously repair skin barrier, make skin moisture It keeps, not easily runs off, show moist, tender, smooth effect；For sterilizing and itch-relieving effect, first group of effect is best, table Present antipruritic effect is good, and dermatitis patients are washed one's hair bath pruritus degree and mitigated at once, and the erythema after three days on skin becomes smaller, after two weeks Fundamental sensation is less than pruritis, and the erythema on skin subsides completely, and has lacked second group of sugarcane vinegar, although subtracting after shower Light itch, but not persistently, this is because second group of shower packet can only realize surface disinfection, and can not deep layer anti-inflammatory, the After essential oil is changed to essential oil on the market by four groups, it is also able to achieve bactericidal antiphlogistic, but the period is long, illustrates that the essential oil of the application can promote Into skin absorption of drugs.To sum up, each index is that first group of corresponding product effect is best, is optimum test group.Meanwhile The probability that allergic symptom occurs in product of the present invention user is 0, this shows reasonable recipe of the present invention, and additive is safe and reliable, tool There is good application prospect.

Although above the present invention is described in detail with a general description of the specific embodiments, On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause This, these modifications or improvements, fall within the scope of the claimed invention without departing from theon the basis of the spirit of the present invention.

Claims

The packet 1. a kind of sugarcane vinegar is taken a shower, which is characterized in that the sugarcane vinegar is taken a shower to wrap and is made of the raw material of following parts by weight: hundred is fragrant 8-10 parts of fruit branch, 10-15 parts of lychee leaf, 8-12 parts of honeysuckle, bluegrass 5-8 parts red, 2-3 parts of sea salt, 2-3 parts of common four-o' clock leaf, trifoliate orange 6-10 parts of shell, 7-14 parts of composite essential oil and 18-25 parts of sugarcane vinegar.
The packet 2. a kind of sugarcane vinegar according to claim 1 is taken a shower, which is characterized in that the sugarcane vinegar takes a shower packet by following heavy Measure the raw material composition of part: 9 parts of passion fruit branch, 12 parts of lychee leaf, 10 parts of honeysuckle, 6 parts of red bluegrass, 2 parts of sea salt, common four-o' clock leaf 2 Part, 8 parts of Fructus Aurantii, 10 parts of essential oil and 22 parts of sugarcane vinegar.
The packet 3. a kind of sugarcane vinegar according to claim 1 is taken a shower, which is characterized in that the composite essential oil is by following parts by weight Raw material composition: 6-12 parts of menthol, 4-9 parts of aloe, 5-10 parts of ginger and 3-8 parts of tea seed.
The packet 4. a kind of sugarcane vinegar according to claim 3 is taken a shower, which is characterized in that the composite essential oil is by the following method It obtains:

(1) tea seed is carried out being crushed to 30-50 mesh, then carries out supercritical CO₂Extraction, by the grease being obtained by extraction into Row water-oil separating removes water layer, carries out molecular distillation at being 100-140 DEG C in temperature by obtained crude oil, obtains camellia seed oil；

(2) take aloe be added with its etc. quality distilled water, be then put into fractionating device, be fractionated under the conditions of 60-85 DEG C It extracts, obtains extract；Extracted to the sodium chloride of quality such as obtaining being added in extract, then filter to take oil reservoir to get Aloe essential oil；

(3) it is handled after cleaning ginger by saline solution soaking sterilization, is then crushed to 20-50 mesh, be subsequently placed in fermentation and fill It ferments 24-48 hours at a temperature of inherent 75-80 DEG C, forms ginger fermentation material；Ginger fermentation material is sent into extraction kettle, through the Single extraction and second of extraction, collect and merge the CO containing extract₂, through first time parsing separation and second of parsing point From, it collects separating liquid A and separating liquid B and merges, obtain oil of ginger crude product, oil of ginger crude product is stirred under water bath condition, progress Oil is mutually filtered by vacuum in water-oil separating, and collection obtains ginger essential oil；

(4) ginger essential oil obtained by aloe essential oil obtained by step (2) and step (3) is mixed, is heated up to 60-70 DEG C, and stirring Camellia seed oil is added in the process, forms mixed liquor, is then allowed to stand, so that the temperature of mixed liquor is down to room temperature, then add peppermint Brain, and stir 45-55 minutes, obtain the composite essential oil.
The packet 5. a kind of sugarcane vinegar according to claim 1 is taken a shower, which is characterized in that the sugarcane vinegar obtains by the following method It arrives:

1) it squeezes sugar-cane juice: sugarcane is squeezed, and flip sugarcane juice liquid level foam, stand, it is spare to obtain sugar-cane juice；

2) fermented pretreatment: pure water is added into sugar-cane juice obtained by step (1), pol is adjusted to 10-12Brix, is obtained sweet Sugarcane liquid；Then 0.3-0.5 times of weight of sugarcane liquid of purslane is added in sugarcane liquid, obtains mixture A；Purslane is before addition First it is crushed to 30-40 mesh；

3) one time fermentation: the mixture A that step 2) obtains is transferred in sealed fermenting tank, then in the fermenter be added account for it is mixed The grape wine schlempe of the belt leather fermentation of object A mass 10-15% is closed, the alcoholic strength to ferment under the conditions of 25-30 DEG C to fermentation liquid reaches To 8-10% (v/v), stops fermentation, obtain mixture B；

4) secondary fermentation: mixture B obtained by step (3) is accessed into the acetic acid bacteria activated according to 12% inoculum concentration, is being fermented Temperature is fermented 8-10 days under conditions of being 25-35 DEG C, obtains mixture C；

5) it filters: mixture C obtained by step (4) being filtered by filter press technique, sugarcane vinegar can be obtained in sterilization treatment.
The preparation method of packet 6. a kind of sugarcane vinegar according to claim 1-5 is taken a shower, which is characterized in that the system Preparation Method includes the following steps:

A. it prepares Plant Powder: passion fruit branch, honeysuckle, red bluegrass, common four-o' clock leaf being cleaned into removal of impurities, it is low to be dried to material moisture In 10%, it was then crushed to 80-100 mesh, it is spare to obtain Plant Powder；

B. it prepares Fructus Aurantii powder: flesh is removed into Fructus Aurantii chopping, the alcohol reflux extraction of the 70-80% then measured with 5-7 times 2 times, every time 1-2 hours, obtained Fructus Aurantii extracting solution is concentrated under reduced pressure, obtains the medicinal extract that relative density is 1.2-1.3, medicinal extract is carried out It is spare to be dried to obtain Fructus Aurantii powder；

C. lychee leaf is handled: being taken bottle-green lychee leaf and is accounted for the calcium carbonate of lychee leaf weight 0.2-0.5% and account for lychee leaf weight The quartz sand of 0.05-0.1% is measured, co-grinding obtains lychee leaf powder, in pressure is 0.12-0.16MPa, temperature by lychee leaf powder It is 110-128 DEG C, acidity hydrolyzes 3-4h under conditions of being 1.0-1.6%；Hydrolyzate is then obtained by filtration, controls hydrolyzate temperature It is 40-50 DEG C, 95% alcohol, ligninase and cellulase is added and reacts 1 hour, hydrolyzate is then warming up to 83 DEG C and is gone out Enzyme 10min；After enzyme deactivation then amylase, protease is added to 45 DEG C in cooling hydrolyzate in hydrolyzate, then by control from The centrifugal rotational speed of scheming separates chlorophyll and mother liquor, by controlling the temperature and ambient humidity of dryer, makes the water in chlorophyll Divide evaporation, obtains lychee leaf chlorophyll product；

D. it the processing of sea salt: takes sea salt to crush to obtain sea salt powder, was then crushed to 80-100 mesh again, it is standby to obtain sea salt fine powder With；

E. mixing granulation: Plant Powder, Fructus Aurantii powder, lychee leaf chlorophyll are mixed, and are subsequently added into sugarcane vinegar and composite essential oil mixes, And be placed in centrifugal granulator and first spray alcohol master batch, until master batch forms dried for standby, as bath granules after larger particles；

F. packed: to be sealed again by bath granules are packed into non-woven bag by the amount of 110-140g/ packet obtained by step d to get institute State sugarcane vinegar shower packet.