CN106726920A - A kind of moisturizing astringent and preparation method thereof - Google Patents
A kind of moisturizing astringent and preparation method thereof Download PDFInfo
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- CN106726920A CN106726920A CN201611168771.7A CN201611168771A CN106726920A CN 106726920 A CN106726920 A CN 106726920A CN 201611168771 A CN201611168771 A CN 201611168771A CN 106726920 A CN106726920 A CN 106726920A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention provides a kind of moisturizing astringent and preparation method thereof.In terms of the percentage by weight of the moisturizing astringent, the moisturizing astringent includes following components：The oil-dispersing property emollient of parcel and/or the oil-soluble emollient of parcel：1 15%, preferably 3 12%；Water soluble humectants：5 40%, preferably 8 31%；Water-soluble thickener：0.05 0.5%, preferably 0.08 0.3%；Skin conditioning agent：0.1 5%, preferably 0.3 3%；Solubilizer：0.05 0.8%, preferably 0.05 0.5%；PH adjusting agent：0.001 0.2%, preferably 0.005 0.1%；Water：45 93%, preferably 55 88%.The moisturizing astringent contains the oil-dispersing property emollient of parcel and/or the oil-soluble emollient of parcel, not only causes the texture that there is moisturizing astringent soft sense of touch, silk to slide, additionally it is possible to reduce the sticky sense of toner.
Description
Technical field
The present invention relates to a kind of moisturizing astringent and preparation method thereof, belongs to cosmetic field.
Background technology
With economy, the increasingly improvement of living standard, the basis maintenance of skin has turned into a part for daily life, moisturizing
It is one of most important function in skin protection cosmetics.Skin it is delicate, plentiful, whether beautiful it is critical only that it is aqueous in skin
Amount, the important channel of moisture of skin is to maintain using moisture-keeping cosmetics.Contain moisturizing in so-called moisture-keeping cosmetics, i.e. cosmetics the inside
Composition, the water content that keratoderma can be kept certain can increase moisture of skin, humidity, to recover the gloss and elasticity of skin.
Toner in the market mainly has based on transparent type and emulsifying.Transparent type toner, mainly uses sweet
The material with moisture absorption aquation such as oil, butanediol, high molecular weight water soluble polymer carries out moisturizing, and this kind of material had from week
The function that collarette border absorbs water, therefore under conditions of relative humidity is high, the moistening effect to skin is fine.But transparent type
Toner is very low in relative humidity, and cold is dried, windy weather, can be absorbed water from skin inner layer, and makes skin drier,
Cutaneous normal function, simultaneously because with the addition of high molecular polymer, has obvious sticky sense when smearing.
Due to the addition of grease in emulsifying toner, product appearance is translucent or milky, is protected by grease
It is wet, closed film can be formed in skin surface, so that transepidermal water loss (TEWL) is reduced, while can also prevent skin from being absorbed from the external world
Moisture.Its shortcoming is excessively greasy, is only suitable for extremely dry skin or is used in bone-dry winter.
The content of the invention
Problems to be solved by the invention
It is an object of the invention to provide a kind of moisturizing astringent and preparation method thereof, the moisturizing astringent is not only caused
Moisturizing astringent has the texture that soft sense of touch, silk are slided, additionally it is possible to reduce the sticky sense of toner.
The scheme for solving problem
The present invention provides a kind of moisturizing astringent, wherein, it is in terms of the percentage by weight of the moisturizing astringent including following
Component：
The oil-dispersing property emollient of parcel and/or the oil-soluble emollient of parcel：1-15%, preferably 3-12%；
Water soluble humectants：5-40%, preferably 8-31%；
Water-soluble thickener：0.05-0.5%, preferably 0.08-0.3%；
Skin conditioning agent：0.1-5%, preferably 0.3-3%；
Solubilizer：0.05-0.8%, preferably 0.05-0.5%；
PH adjusting agent：0.001-0.2%, preferably 0.005-0.1%；
Water：45-93%, preferably 55-88%.
Moisturizing astringent of the invention, wherein, the oil-dispersing property emollient of the parcel includes：Polydimethylsiloxanes
Alkane (and) deionized water (glycerine) pentadiene alcohol (and) Dimethicone/Vinyl Dimethicone cross-linked polymer
(and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM, octyl group polymethyl siloxane (and) deionized water is (sweet
Oil) butanediol (and) cetearyl Dimethicone Crosspolymer (and) card ripple (and) Phenoxyethanol (and) aminomethyl
Propyl alcohol (and) one or two in EDETATE SODIUM；Preferably, the oil-soluble emollient of the parcel includes：Trifluoro propyl diformazan
Radical siloxane (and) water (and) glycerine (and) pentadiene alcohol (and) amodimethicones (and) card ripple (and) Phenoxyethanol
(and) NaOH (and) EDETATE SODIUM, ring five dimethyl silicone polymer (and) water (and) glycerine (and) butanediol (and) poly- diformazan
One or two in radical siloxane (and) card ripple (and) Phenoxyethanol (and) aminomethyl propanol (and) EDETATE SODIUM.
Moisturizing astringent of the invention, wherein, the water soluble humectants include：Glycerine, propane diols, ethanol, fourth
One or more, excellent in glycol, glycine betaine, panthenol, PEG/PPG-17/6 copolymers, glycerin polyether -26, Sodium Hyaluronate
Elect in glycerine, ethanol, butanediol, Sodium Hyaluronate one or more as.
Moisturizing astringent of the invention, wherein, the water-soluble thickener includes：Acrylic acid (ester) class/C10-30
Alkylol acrylamide acid esters cross-linked polymer, hydroxyethyl cellulose, xanthans, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate
One or more in copolymer, Carbomer, AVC；Preferably acrylic acid
In (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, Carbomer, AVC
One or more.
Moisturizing astringent of the invention, wherein, the skin conditioning agent includes：Flos Chrysanthemi water, oat peptide, lanatechead saussurea herb with flower
Extract, radix ampelopsis root extract, European horse-chestnut seed extract, bladder-wrack extract, tea extract, hydrolyzed milk protein,
One or more in undaria pinnitafida extract；Preferably Flos Chrysanthemi water, oat peptide, Herba Saussureae Involueratae extract, hydrolysed milk egg
One or more in white.
Moisturizing astringent of the invention, wherein, the solubilizer includes：Polysorbate -20, PEG-40 hydrogenation castors
One or more in sesame oil, PPG-26- butylol polyethers -26, preferably polysorbate -20, PEG-40 hydrogenated castors
One or two in oil.
Moisturizing astringent of the invention, wherein, the pH adjusting agent includes：Citric acid, sodium lactate, NaOH,
One or more in potassium hydroxide, triethanolamine, aminomethyl propanol, arginine；Preferably NaOH, aminomethyl third
One or more in alcohol, arginine.
Moisturizing astringent of the invention, wherein, the moisturizing astringent also includes：One kind in preservative, essence
Or two kinds；Preferably, the preservative includes：Chlorphenesin, pungent glycol, Phenoxyethanol, methyl hydroxybenzoate, pentanediol, phenmethylol
In one or more, one or more in preferably pungent glycol, Phenoxyethanol, methyl hydroxybenzoate, pentanediol；It is preferred that
, in terms of the percentage by weight of the moisturizing astringent, the preservative addition is 0.05-1.5%, preferably 0.1-
1.2%；It is highly preferred that the addition of the essence is 0.01-0.2%, preferably 0.01-0.12%.
The present invention also provides a kind of preparation method of moisturizing astringent of the invention, including：The moisturizing is made up
The step of each component of water mixes.
The method according to the invention, wherein, comprise the following steps：
Deionized water is placed in reaction vessel, water soluble humectants, water-soluble thickener is added, is stirred and heated to
75-85 DEG C of dissolving is complete；
48-55 DEG C is cooled to, adds the oil-dispersing property emollient of parcel and/or the oil-soluble of parcel to moisten in reaction vessel
Skin agent, dispersed with stirring is uniform；
42-47.9 DEG C is cooled to, skin conditioning agent, solubilizer, optionally pH adjusting agent, anti-corrosion are added in reaction vessel
Agent, optionally essence, stir；
36-41.9 DEG C of filtering is cooled to, moisturizing astringent is prepared.
The effect of invention
In moisturizing astringent of the invention, the moisture of skin can be pinned with depth, even in the relatively low ring of relative humidity
In border, skin moisture also can be for a long time kept, make skin that water shortage will not be dried because of the influence of environment, so as to keep skin for a long time
The moisture of skin and moist degree, and improve skin elasticity.Further, moisturizing astringent of the invention can also reduce cosmetic
The sticky sense of water.
Brief description of the drawings
Fig. 1 is the moisture growth rate curve of the moisturizing astringent that embodiment 1, embodiment 7 and comparative example 1 are prepared
Figure.
Specific embodiment
The present invention provides a kind of moisturizing astringent, wherein, it is in terms of the percentage by weight of the moisturizing astringent including following
Component：The oil-dispersing property emollient of parcel and/or oil-soluble emollient, water soluble humectants, water-soluble thickener, the skin of parcel
Skin conditioner, solubilizer, pH adjusting agent and water.
The oil-dispersing property emollient of parcel of the invention, is a kind of elastomer silicone of parcel, is easily disperseed in water,
And stability is strong.Enable that elastomer silicone is applied in toner, not only further function as the effect of moisturizing, also have
There is skin sense to moisten and soft and smooth silty sense.The oil-soluble emollient of parcel of the invention, is a kind of silicone oil of parcel, is preferably wrapped up
Fluorosilicon oil, it is same easily to disperse in water, and stability is strong.Enable that fluorosilicon oil is applied in toner, and have
The absorbability of good sebum grease, so that toner has the effect of dumb light.
Moisturizing astringent of the invention, wherein, the oil-dispersing property emollient and/or the oil-soluble of parcel of the parcel
The addition of emollient is 1-15%, preferably 3-12%；When the oil-dispersing property emollient and/or the oil-soluble profit of parcel of parcel
When the addition of skin agent is less than 1%, the moist moistening effect of moisturizing astringent for preparing is poor, when addition is more than 15%
When, the comparing for preparing moisturizing astringent is greasy and relatively costly.
In some specific embodiments, the oil-dispersing property emollient addition of the parcel is 2-8%, the oil of parcel
Dissolubility emollient addition is 2-4%, can further improve moistening effect.
Preferably, the oil-dispersing property emollient of the parcel includes：Dimethyl silicone polymer (and) deionized water (glycerine)
Pentadiene alcohol (and) Dimethicone/Vinyl Dimethicone cross-linked polymer (and) card ripple (and) Phenoxyethanol
(and) NaOH (and) EDETATE SODIUM, octyl group polymethyl siloxane (and) deionized water (glycerine) butanediol (and) cetearyl alcohol
In base Dimethicone Crosspolymer (and) card ripple (and) Phenoxyethanol (and) aminomethyl propanol (and) EDETATE SODIUM
One or two；Preferably, the oil-soluble emollient of the parcel includes：Trifluoro propyl dimethyl siloxane (and) water (and) sweet
Oil (and) pentadiene alcohol (and) amodimethicones (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDTA bis-
Sodium, ring five dimethyl silicone polymer (and) water (and) glycerine (and) butanediol (and) dimethyl silicone polymer (and) card ripple (and) benzene
One or two in oxyethanol (and) aminomethyl propanol (and) EDETATE SODIUM.
Dimethyl silicone polymer (and) deionized water (glycerine) pentadiene alcohol (and) dimethyl silicone polymer in the present invention/
Vinyl dimethicone cross polymer (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM, its
In fact be a kind of composition of parcel, be one kind include dimethyl silicone polymer, glycerine, pentadiene alcohol, dimethyl silicone polymer/
Vinyl dimethicone cross polymer, card ripple, Phenoxyethanol, NaOH, EDETATE SODIUM and deionized water
Composition.
Trifluoro propyl dimethyl siloxane (and) water (and) glycerine (and) pentadiene alcohol (and) amino diformazan in the present invention
Radical siloxane (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM, it is also a kind of composition of parcel, be
One kind includes trifluoro propyl dimethyl siloxane, water, glycerine, pentadiene alcohol, amodimethicones, card ripple, benzene oxygen second
The composition of alcohol, NaOH and EDETATE SODIUM.
Octyl group polymethyl siloxane (and) deionized water (glycerine) butanediol (and) cetearyl poly- two in the present invention
Methylsiloxane cross-linked polymer (and) card ripple (and) Phenoxyethanol (and) aminomethyl propanol (and) EDETATE SODIUM, it is also a kind of bag
The composition wrapped up in, is that one kind includes octyl group polymethyl siloxane, deionized water, butanediol, cetearyl poly dimethyl silicon
Oxygen alkane cross-linked polymer, card ripple, Phenoxyethanol, aminomethyl propanol, the composition of EDETATE SODIUM.
Ring five dimethyl silicone polymer (and) water (and) glycerine (and) butanediol (and) polydimethylsiloxanes in the present invention
Alkane (and) card ripple (and) Phenoxyethanol (and) aminomethyl propanol (and) EDETATE SODIUM, it is also a kind of composition of parcel, it is a kind of
Include ring five dimethyl silicone polymer, water, glycerine, butanediol, dimethyl silicone polymer, card ripple, Phenoxyethanol, aminomethyl third
The composition of alcohol, EDETATE SODIUM.
Moisturizing astringent of the invention, wherein, the addition of the water soluble humectants is 5-40%, preferably 8-
31%；When the addition of water soluble humectants is less than 5%, the moistening effect of preparation-obtained moisturizing astringent is poor, works as water
When the addition of dissolubility NMF is more than 40%, preparation-obtained moisturizing astringent is sticky, and relatively costly.Preferably, institute
Stating water soluble humectants includes：It is glycerine, propane diols, ethanol, butanediol, glycine betaine, panthenol, PEG/PPG-17/6 copolymers, sweet
In oily polyethers -26, Sodium Hyaluronate, tremella polysaccharides one or more, preferably glycerine, ethanol, butanediol, hyaluronic acid
In sodium, tremella polysaccharides one or more.
Moisturizing astringent of the invention, wherein, the addition of the water-soluble thickener is 0.05-0.5%, preferably
It is 0.08-0.3%.When the addition of water-soluble thickener is less than 0.05%, the suspension of preparation-obtained moisturizing astringent
Power is bad, and when the addition of water-soluble thickener is more than 0.5%, the spreadability of preparation-obtained moisturizing astringent is poor.It is excellent
Selection of land, the water-soluble thickener includes：Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, ethoxy are fine
Dimension element, xanthans, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, Carbomer, acryloyldimethyl taurine
One or more in ammonium/VP copolymers.
Preferably, the water-soluble thickener includes：Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymerics
One or more in thing, Carbomer, AVC.Wherein, acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymer has good thickening capabilities with preferably resistance to ionic after neutralization, can increase
Plus the stability of product, there is provided the skin sense of water profit.
Moisturizing astringent of the invention, wherein, the addition of the skin conditioning agent is 0.1-5%, preferably
0.3-3%；When the addition of skin conditioning agent is less than 0.1%, effect of preparation-obtained moisturizing astringent conditioning skin
Difference, when the addition of the skin conditioning agent is more than 5%, the cost of preparation-obtained moisturizing astringent is greatly increased.
Preferably, the skin conditioning agent includes：Flos Chrysanthemi water, oat peptide, Herba Saussureae Involueratae extract, radix ampelopsis root extract,
One kind in European horse-chestnut seed extract, bladder-wrack extract, tea extract, hydrolyzed milk protein, undaria pinnitafida extract
Or it is two or more；It is highly preferred that the skin conditioning agent includes：Flos Chrysanthemi water, oat peptide, Herba Saussureae Involueratae extract, hydrolysed milk
One or more in albumen.Wherein, hydrolyzed milk protein can increase the life of collagenous fibres in human body, elastomer
Into making skin more charm.
Moisturizing astringent of the invention, wherein, the addition of the solubilizer is 0.05-0.8%, preferably
0.05-0.5%；When the addition of the solubilizer is less than 0.05%, the solubilising power of the moisturizing astringent for preparing is poor,
Transparency is poor, and when the addition of the solubilizer is more than 0.8%, the excitant of the moisturizing astringent for preparing is larger
(because solubilizer belongs to surfactant, with certain excitant).Preferably, the solubilizer includes：Polysorbate-
20th, in Cremophor RH40, PPG-26- butylol polyethers -26 one or more, preferably polysorbate -20,
One or two in Cremophor RH40.
Moisturizing astringent of the invention, wherein, the addition of pH adjusting agent is 0.001-0.2%, preferably
0.005-0.1%, when the addition of pH adjusting agent is less than 0.001%, the pH of preparation-obtained moisturizing astringent is too high, when
When the addition of pH adjusting agent is more than 0.2%, the pH of moisturizing astringent is too low, and the pH of moisturizing astringent is too high or too low to skin
Skin is irritant.Preferably, the pH adjusting agent includes：Citric acid, sodium lactate, NaOH, potassium hydroxide, three ethanol
One or more in amine, aminomethyl propanol, arginine；It is highly preferred that the pH adjusting agent includes：NaOH, ammonia
One or more in methylpropanol, arginine.
Moisturizing astringent of the invention, wherein, the moisturizing astringent also includes：One kind in preservative, essence
Or two kinds；Preferably, the preservative includes：Chlorphenesin, pungent glycol, Phenoxyethanol, methyl hydroxybenzoate, pentanediol, phenmethylol
In one or more, one or more in preferably pungent glycol, Phenoxyethanol, methyl hydroxybenzoate, pentanediol.
Preferably, in terms of the percentage by weight of the moisturizing astringent, the preservative addition is 0.05-1.5%, excellent
Elect 0.1-1.2%, more preferably more preferably 0.2-1.0%, 0.3-0.6% as；It is highly preferred that the addition of the essence
It is 0.01-0.2% to measure, preferably 0.01-0.12%.
Moisturizing astringent of the invention, wherein, the addition of water is 45-93%, preferably 55-88%.
The present invention also provides a kind of preparation method of moisturizing astringent of the invention, and it includes：By the moisturizing
The step of each component of adornment water mixes.
Specifically, the method according to the invention, comprises the following steps：
Deionized water is placed in reaction vessel, water soluble humectants, water-soluble thickener and preservative, stirring is added
And it is complete to be heated to 75-85 DEG C of dissolving；
48-55 DEG C is cooled to, adds the oil-dispersing property emollient of parcel and/or the oil-soluble of parcel to moisten in reaction vessel
Skin agent, dispersed with stirring is uniform；
42-47.9 DEG C is cooled to, skin conditioning agent, solubilizer, pH adjusting agent, preservative, perfume (or spice) are added in reaction vessel
Essence, stirs；
36-41.9 DEG C of filtering is cooled to, moisturizing astringent is prepared.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.It is unreceipted specific in embodiment
Condition person, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or the unreceipted production firm person of instrument, are
Can by city available from conventional products.
In embodiment, dimethyl silicone polymer (and) deionized water (glycerine) pentadiene alcohol (and) dimethyl silicone polymer/
Vinyl dimethicone cross polymer (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM
Manufacturer is UnSil Co., and Ltd, production code member is CES-1104；
Trifluoro propyl dimethyl siloxane (and) water (and) glycerine (and) pentadiene alcohol (and) amodimethicones
The manufacturer of (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM is UnSil Co., and Ltd, product is compiled
Number be CES-3401.
Embodiment 1-7
According to the content (number) of each component of embodiment 1-7 in table 1 below and table 2, and prepare as steps described below
Moisturizing astringent I-VII.
The preparation method of moisturizing astringent I-VII is as follows：
Step 1), deionized water is placed in reaction vessel, add water soluble humectants, water-soluble thickener and anti-corrosion
Agent (methyl hydroxybenzoate), is stirred and heated to 80 DEG C of dissolvings complete；
Step 2), 50 DEG C are cooled to, the oil-dispersing property emollient of parcel and/or the oil soluble of parcel are added in reaction vessel
Property emollient, dispersed with stirring is uniform；
Step 3), 45 DEG C are cooled to, skin conditioning agent, solubilizer, pH adjusting agent, preservative are added in reaction vessel
(Phenoxyethanol, pentanediol), essence, stir；
Step 4), 38 DEG C of filterings are cooled to, prepare moisturizing astringent.
Comparative example 1-2
According to the content (number) of each component of comparative example 1-2 in table 2 below, and moisturizing is prepared as steps described below
Adornment water VIII-IX.
The preparation method of moisturizing astringent VIII-IX is as follows：
Step 1), deionized water is placed in reaction vessel, add water soluble humectants, water-soluble thickener and anti-corrosion
Agent (methyl hydroxybenzoate), is stirred and heated to 80 DEG C of dissolvings complete；
Step 2), 45 DEG C are cooled to, skin conditioning agent, solubilizer, pH adjusting agent, preservative are added in reaction vessel
(Phenoxyethanol, pentanediol), essence, stir；
Step 3), 38 DEG C of filterings are cooled to, prepare moisturizing astringent.
Table 1
Table 2
Using effect is tested
Moisturizing astringent I, the moisturizing astringent V-VI and the and of comparative example 1 prepared from embodiment 1, embodiment 5-6
The moisturizing astringent VIII-IX that comparative example 2 is prepared carries out the test of consumer's experience.It is 28 with 60 average ages
The consumer in year is estimated for object.Appraisal procedure is that selection is as follows to projects preference degree (whether liking) in 1-9 points
It is shown：
Test result is as shown in table 3：
Table 3
| Test content | Embodiment 1 | Embodiment 5 | Embodiment 6 | Comparative example 1 | Comparative example 2 |
| Product appearance | 8.5 | 8.2 | 8.0 | 8.0 | 8.0 |
| Silk smooth felling | 9.0 | 8.5 | 8.2 | 7.5 | 7.2 |
| Sticky sense | 8.8 | 8.5 | 8.3 | 8.0 | 7.8 |
| Moisten degree | 9.0 | 8.0 | 8.2 | 7.0 | 7.2 |
| Salubrious degree | 8.5 | 8.2 | 8.0 | 7.5 | 7.0 |
| Moisture retention | 9.0 | 8.5 | 8.3 | 8.0 | 8.1 |
As can be seen from Table 3：The moisturizing astringent of the embodiment of the present application 1,5,6 is the oil-dispersing property emollient containing parcel
And/or moisturizing astringent I, V, VI of the oil-soluble emollient of parcel, its using effect is substantially better than comparative example 1 and comparative example 2
Moisturizing astringent VIII-IX.In addition, carrying out using effect survey to the moisturizing astringent II-IV that embodiment 2-4 is prepared
Examination, the moisturizing astringent II-IV that embodiment 2-4 is prepared possesses equally good use result.
Moisture content of skin is tested
Choose 20~35 years old tested volunteer 19 of women, wherein more than 30 years old 3,20~30 years old 16.Choose upper arm
Two symmetrical regions of inner side, respectively as control group and the test zone of test group, in the environment (temperature 22 of constant temperature and humidity
DEG C, humidity 55%) tested, test the moisture of skin.Test group is obtained from embodiment 1 and embodiment 7 are prepared
Moisturizing astringent I and VII, the moisturizing astringent VIII that control group is prepared from comparative example 1, the two is under the same conditions
Do same test.Moisture test period is 3.5 hours, at interval of test in 30 minutes once.
Tested using capacitance method principle, moisture measurement probe vertical is pressed in tested skin surface, probe top
A segment distance is pushed back, there is a spring to make probe top keep the pressure of 0.16N to be pressed in skin surface 1 second inside probe, measured
Humidity measurements (Moisture Measurement Value, MMV).The humidity measurements are between 0~150.
The skin of Medial upper arm is cleaned, volunteer sits quietly 0.5 in the environment of constant temperature and humidity (22 DEG C of temperature, humidity 55%)
After hour, carry out two initial humidities of test zone using skinanalysis apparatus (German CK, Cutometer MPA580) and measure
The measurement of value.After 0.5 hour, then moisturizing prepared by the embodiment 1 and embodiment 7 for smearing equivalent in two test zones respectively
The moisturizing astringent VIII that adornment water I and VII is prepared with comparative example 1, and two humidity measurements in region are tested, interval time point
Wei 0.5 hour, 1 hour, 1.5 hours, 2 hours, 2.5 hours, 3 hours, 3.5 hours.Every subject is measured in test group
With the skin moisture content in control group region, each test data is recorded.The humidity that the result of skin moisture content passes through setting
Measured value is represented.
Each test data is subtracted the change of the initial humidity measured value as period humidity measurements, then divided by initial
Humidity measurements are to draw skin moisture content growth rate, as shown in table 4, table 5 and table 6.
Skin moisture content Growth Rate Calculation formula is：
Skin moisture content growth rate %=(MMVt-MMV0)/MMV0× 100%
Wherein, MMV0：The initial humidity measured value of skin before smearing；
MMVt：The humidity measurements of t period skins after smearing.
Table 4
Table 5
Table 6
Fig. 1 is the moisturizing astringent VIII that moisturizing astringent I and VII prepared by embodiment 1 and 7 is prepared with comparative example 1
The curve map of the growth rate change of moisture content of skin.Embodiment 1 and embodiment 7 can be seen that by table 4, table 5 and table 6 and Fig. 1
Moisturizing astringent I compared with VII comparative example 1 preparation moisturizing astringent VIII moisture growth rate it is higher, moisturizing astringent 1
The moisture growth rate of the moisturizing astringent I of preparation is most notable.Therefore, prepared using containing embodiments of the invention 1 and embodiment 7
Moisturizing astringent I and VII, even if in the relatively low environment of relative humidity, remaining able to enduringly pin the moisture of skin, flesh
Skin can for a long time keep more water content, so that skin water profit is plentiful.
In addition, carrying out using effect test, embodiment 2-6 systems to the moisturizing astringent II-VI that embodiment 2-6 is prepared
The standby moisturizing astringent II-VI for obtaining, even if in the relatively low environment of relative humidity, remaining able to enduringly pin the water of skin
Point, skin can for a long time keep more water content, so that skin water moistens plentiful result.
Claims (10)
1. a kind of moisturizing astringent, it is characterised in that in terms of the percentage by weight of the moisturizing astringent, including following components：
The oil-dispersing property emollient of parcel and/or the oil-soluble emollient of parcel：1-15%, preferably 3-12%；
Water soluble humectants：5-40%, preferably 8-31%；
Water-soluble thickener：0.05-0.5%, preferably 0.08-0.3%；
Skin conditioning agent：0.1-5%, preferably 0.3-3%；
Solubilizer：0.05-0.8%, preferably 0.05-0.5%；
PH adjusting agent：0.001-0.2%, preferably 0.005-0.1%；
Water：45-93%, preferably 55-88%.
2. moisturizing astringent according to claim 1, it is characterised in that the oil-dispersing property emollient of the parcel includes：
Dimethyl silicone polymer (and) deionized water (glycerine) pentadiene alcohol (and) dimethyl silicone polymer/vinylpolydimethyl silica
Alkane cross-linked polymer (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM, octyl group polymethyl siloxane (and)
Deionized water (glycerine) butanediol (and) cetearyl Dimethicone Crosspolymer (and) card ripple (and) benzene oxygen second
One or two in alcohol (and) aminomethyl propanol (and) EDETATE SODIUM；
Preferably, the oil-soluble emollient of the parcel includes：Trifluoro propyl dimethyl siloxane (and) water (and) glycerine (and)
Pentadiene alcohol (and) amodimethicones (and) card ripple (and) Phenoxyethanol (and) NaOH (and) EDETATE SODIUM, ring five
Dimethyl silicone polymer (and) water (and) glycerine (and) butanediol (and) dimethyl silicone polymer (and) card ripple (and) Phenoxyethanol
One or two in (and) aminomethyl propanol (and) EDETATE SODIUM.
3. moisturizing astringent according to claim 1 and 2, it is characterised in that the water soluble humectants include：Glycerine,
One in propane diols, ethanol, butanediol, glycine betaine, panthenol, PEG/PPG-17/6 copolymers, glycerin polyether -26, Sodium Hyaluronate
Kind or it is two or more, preferably in glycerine, ethanol, butanediol, Sodium Hyaluronate one or more.
4. the moisturizing astringent according to claim any one of 1-3, it is characterised in that the water-soluble thickener includes：
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, hydroxyethyl cellulose, xanthans, hydroxy-ethyl acrylate/the third
In alkene acyl dimethyltaurine sodium copolymer, Carbomer, AVC one or two with
On；Preferably acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, Carbomer, acryloyldimethyl taurine
One or more in ammonium/VP copolymers.
5. the moisturizing astringent according to claim any one of 1-4, it is characterised in that the skin conditioning agent includes：It is female
Chrysanthemum water, oat peptide, Herba Saussureae Involueratae extract, radix ampelopsis root extract, European horse-chestnut seed extract, bladder-wrack extract, tealeaves
One or more in extract, hydrolyzed milk protein, undaria pinnitafida extract；Preferably Flos Chrysanthemi water, oat peptide, saussurea involucrata
One or more in flower extract, hydrolyzed milk protein.
6. the moisturizing astringent according to claim any one of 1-5, it is characterised in that the solubilizer includes：Poly- sorb
One or more in alcohol ester -20, Cremophor RH40, PPG-26- butylol polyethers -26, preferably polysorbate
One or two in ester -20, Cremophor RH40.
7. the moisturizing astringent according to claim any one of 1-6, it is characterised in that the pH adjusting agent includes：Lemon
One or more in acid, sodium lactate, NaOH, potassium hydroxide, triethanolamine, aminomethyl propanol, arginine；It is preferred that
For one or more in NaOH, aminomethyl propanol, arginine.
8. the moisturizing astringent according to claim any one of 1-7, it is characterised in that the moisturizing astringent also includes：
One or two in preservative, essence；Preferably, the preservative includes：Chlorphenesin, pungent glycol, Phenoxyethanol, oxybenzene
In methyl esters, pentanediol, phenmethylol one or more, in preferably pungent glycol, Phenoxyethanol, methyl hydroxybenzoate, pentanediol
One or more；Preferably, in terms of the percentage by weight of the moisturizing astringent, the preservative addition is 0.05-
1.5%, preferably 0.1-1.2%；It is highly preferred that the addition of the essence is 0.01-0.2%, preferably 0.01-
0.12%.
9. the preparation method of a kind of moisturizing astringent according to claim any one of 1-8, it is characterised in that including：Will
The step of each component of the moisturizing astringent mixes.
10. method according to claim 9, it is characterised in that comprise the following steps：
Deionized water is placed in reaction vessel, water soluble humectants, water-soluble thickener is added, 75-85 is stirred and heated to
DEG C dissolving is complete；
48-55 DEG C is cooled to, the oil-dispersing property emollient of parcel and/or the oil-soluble moisturizing of parcel are added in reaction vessel
Agent, dispersed with stirring is uniform；
Be cooled to 42-47.9 DEG C, in reaction vessel add skin conditioning agent, solubilizer, pH adjusting agent, optionally preservative,
Optionally essence, stirs；
36-41.9 DEG C of filtering is cooled to, moisturizing astringent is prepared.
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107485598A (en) * | 2017-08-30 | 2017-12-19 | 广州市科能化妆品科研有限公司 | A kind of pearl toner of thickening certainly and preparation method thereof |
| CN107535495A (en) * | 2017-10-27 | 2018-01-05 | 陕西省石油化工研究设计院 | A kind of wide spectrum daily chemical products anticorrosion and bactericidal agent |
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| CN108125852A (en) * | 2017-12-29 | 2018-06-08 | 广州慈康生物科技有限公司 | Extremely strong essence lotion of a kind of water moisture feeling and preparation method thereof |
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| CN110101627A (en) * | 2019-06-18 | 2019-08-09 | 杭州悦萱堂化妆品有限公司 | A kind of essence dew and preparation method thereof with suspension microballon |
| CN111437222A (en) * | 2020-02-26 | 2020-07-24 | 广东省粤企产业创新研究院 | Toner composition, preparation method thereof and toner |
| CN113476344A (en) * | 2021-07-05 | 2021-10-08 | 广州市百好博有限公司 | Cosmetic composition, cosmetic, oil-in-water lip glaze and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150272861A1 (en) * | 2014-03-28 | 2015-10-01 | Nusil Technology Llc | Dispersions containing encapsulated materials and compositions using same |
| CN105456176A (en) * | 2015-12-29 | 2016-04-06 | 广州市科能化妆品科研有限公司 | Emulsion cream and preparing method thereof |
-
2016
- 2016-12-16 CN CN201611168771.7A patent/CN106726920B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150272861A1 (en) * | 2014-03-28 | 2015-10-01 | Nusil Technology Llc | Dispersions containing encapsulated materials and compositions using same |
| CN105456176A (en) * | 2015-12-29 | 2016-04-06 | 广州市科能化妆品科研有限公司 | Emulsion cream and preparing method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 杨继生: "《表面活性剂原理与应用》", 31 December 2012, 东南大学出版社 * |
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