CN106588175A - Shrimp culture ecological fertilizer water paste - Google Patents
Shrimp culture ecological fertilizer water paste Download PDFInfo
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- CN106588175A CN106588175A CN201611021578.0A CN201611021578A CN106588175A CN 106588175 A CN106588175 A CN 106588175A CN 201611021578 A CN201611021578 A CN 201611021578A CN 106588175 A CN106588175 A CN 106588175A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F1/00—Fertilisers made from animal corpses, or parts thereof
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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Abstract
The invention discloses shrimp culture ecological fertilizer water paste, which is prepared from the following ingredients in parts by weight: 1 to 50 parts of fish and shrimp protein hydrolysate, 1 to 50 parts of oyster shell powder slurry, 1 to 30 parts of urea, 1 to 5 parts of monoammonium phosphate, 1 to 5 parts of magnesium sulfate, 1 to 3 parts of ferrous sulfate and 0.1 to 2 parts of potassium chloride. The aquatic product processing wastes of oyster shell, shrimp heads and shells, waste fish juice and sugar factory molasses are used as major raw materials for processing; the obtained shrimp culture ecological fertilizer water paste contains various rich biological active peptide, active calcium, amino acid and chitosan nutrients; various ecological factors of a water body can be balanced; the growth and the breeding of beneficial algae and beneficial plankton are promoted; a great number of palatable living baits are provided for shrimps; through water quality and pond micro-ecological environment improvement, good living environment and survival conditions are provided for the shrimps.
Description
Technical field
The present invention relates to technical field of aquaculture, it is more particularly related to a kind of prawn culturing ecology rich water
Cream.
Background technology
China is the big country of global aquaculture first, accounts for more than the 70% of world's aquaculture total amount.China's sea water
With inland aquaculture area summation up to 1.1 hundred million mu, wherein prawn culturing area occupies up to 3,000,000 mu in national economy for cultivation
Critical role.In recent years, with the fast development and the popularity application of cultivation science and technology of national economy, China's Aquatic product is made
The level of production of aquaculture is greatly improved.
Find that the outbreak main inducing of prawn virus disease is that prawn is improper by the research for a long time to prawn culturing process
What shelling was caused.At present, effective Therapeutic Method is still lacked to prawn's virus, generally believes and keep and optimize good cultivation life
State environment, carries out the preferable outlet that healthy aquaculture is that shrimp culture industry walks out virosiss predicament.Therefore, prawn virus disease is prevented
Control and still rely mainly on prevention, take the way of " anti-overweighting is controlled, and preventing and treating is combined ".Therefore, the preventing and treating of prawn virus disease, except from not
Viruliferous high-quality health young shrimp does seed shrimp, reduces from source outside the vertical transmission of virosiss.Also it is exactly in prawn culturing
During, maintain the aqueous bio factor (such as algae, mushroom) and the dynamic equilibrium of physical and chemical factor (pH value, dissolved oxygen) and whole
The ecological balance of individual water body, allows algal bloom, by the photosynthesis of algae itself, makes the dissolved oxygen in water on the shrimp pool, prawn
Create cleaning, a good growing environment.
At present conventional rich water method has inorganic fat water, fertilizer rich water, bean milk rich water, chemical fertilizer water preparation rich water etc..
In general, inorganic fertilizer rich water, fertilizer rich water, bean milk rich water effect it is poor, and the rich water of current chemical fertilizer water preparation imitate
Fruit is also uneven, and price is of a relatively high.Therefore, in production practices, especially rich water is often run at the cultivation initial stage
The problems such as difficult or rich water high cost.
The content of the invention
It is an object of the invention to solve at least the above, and provide the advantage that at least will be described later.
It is a still further object of the present invention to provide a kind of prawn culturing ecology Fertilizer water paste, using aquatic products processing garbage Concha Ostreae
Shell, prawn head Crusta Penaeus seu Panulirus, useless anchovy sauce and sugar refinery molasses are processed for primary raw material, and the prawn culturing ecology Fertilizer water paste for obtaining is rich in more
Kind of biologically active peptide, activated calcium, aminoacid and shitosan nutrient, can balance the various ecological factors of water body, promote beneficial algae and
Beneficial planktonic growth and breeding, for prawn substantial amounts of agreeable to the taste biological feed is provided, and by improving the micro- life of water quality and pond
State environment, is that prawn sets up a good living environment and conditions of existence.
In order to realize these purposes of the invention and further advantage, there is provided a kind of prawn culturing ecology Fertilizer water paste,
Including the component of following parts by weight：
Fish and shrimp protein hydrolyzate 1-50 parts, Concha Ostreae slurry 1-50 part, carbamide 1-30 parts, MAP 1-5 parts, magnesium sulfate
1-5 parts, ferrous sulfate 1-3 parts and potassium chloride 0.1-2 parts；
Wherein, the preparation method of the fish and shrimp slurry is comprised the following steps：
Step one, by processing fish flour when squeeze out useless anchovy sauce concentration after, be obtained fish slurry, it is standby；
Step 2, the leftover bits and pieces prawn head that aquatic products processing is obtained, Crusta Penaeus seu Panulirus are squeezed, and shrimp slurry is obtained, standby；
Step 3, by obtained fish slurry and shrimp slurry in mass ratio be 1-5:1-5 mixes, and after stirring, pH value is adjusted
To 6.5-7.5, fish and shrimp slurry is obtained, it is standby；
Step 4, to obtained fish and shrimp slurry in add quality be fish and shrimp starch quality 1-2 ‰ by mass ratio be 1:2 fat
After the compound enzyme that enzyme and protease are mixed, after hydrolyzing 8 hours at a temperature of 50 DEG C, 85-90 DEG C is warming up to, enzyme denaturing 10-
15 minutes, obtain final product the fish and shrimp protein hydrolyzate；
The preparation method of the Concha Ostreae slurry is：Under agitation, oyster shell powder is immersed in into the salt that mass fraction is 8%
In aqueous acid after 48 hours, add the sodium hydrate aqueous solution that mass fraction is 8% to adjust pH value to 7, that is, be obtained described male
Oyster shells is starched.
Preferably, in described prawn culturing ecology Fertilizer water paste, the prawn culturing ecology Fertilizer water paste includes following heavy
The component of amount number：
40 parts of fish and shrimp protein hydrolyzate, 30 parts of Concha Ostreae slurry, 20 parts of carbamide, 4 parts of MAP, 3 parts of magnesium sulfate, sulphuric acid
Ferrous 2 parts and 1 part of potassium chloride.
Preferably, in described prawn culturing ecology Fertilizer water paste, also including the component of following parts by weight：
Seafood shell 1-20 parts.
Preferably, in described prawn culturing ecology Fertilizer water paste, the seafood shell be cycle of sixty years shell, the clam shell, scallop shell,
Any one or a few in extra large melon seed cases, Concha meretricis seu cyclinae shell, oyster shell and blood clam shell.
A kind of preparation method of prawn culturing ecology Fertilizer water paste, comprises the following steps：
Step a, the seafood shell powder of 1-20 weight portions is immersed in 40-60 weight portions containing whiterot fungi, Bacillus licheniformis,
In the water of Paenibacillus polymyxa and bacillus acidophilus, first temperature be 20-35 DEG C, air humidity be 70-85% bottom fermentations 48
After hour, then temperature be 35-40 DEG C, air humidity be 80-90% bottom fermentations 24 hours, be dried afterwards, first with 200 when being dried
DEG C/heating rate of h by room temperature to 300 DEG C, then again room temperature dropped to by 300 DEG C with the rate of temperature fall of 80 DEG C/h, circulate
After 2-3 time, fermentation seafood shell powder is obtained；
Step b, by step a it is obtained fermentation seafood shell powder, the fish and shrimp protein hydrolyzate of 1-50 weight portions and 1-50 weight
After the Concha Ostreae slurry mix homogeneously of amount part, carbamide, the MAP of 1-5 weight portions, the 1-5 weight portions of 1-30 weight portions are added
Magnesium sulfate, the ferrous sulfate of 1-3 weight portions and 0.1-2 weight portions potassium chloride, mix homogeneously obtains final product prawn culturing life
State Fertilizer water paste.
Preferably, in the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the seafood shell powder
For：
Seafood shell is soaked after 2-4 hours in the potassium permanganate solution that mass fraction is 0.001%, is taken out, with clearly
Water is rinsed 2-3 time, after drying, is put in the dilute hydrochloric acid solution that mass fraction is 10-20% and is soaked 12-24 hours, then by pH
Value is adjusted to 6-7, after standing 6-8 hours, is taken out, and is rinsed 2-3 time with clear water, after drying, is crushed, and 40-60 mesh sieves is crossed, in 200-
Dry after 3-4 hours at 300 DEG C, obtain final product the seafood shell powder.
Preferably, in the preparation method of described prawn culturing ecology Fertilizer water paste, brown rot fungus, lichens in step a
The initial clump count of bacillus cereuss, Paenibacillus polymyxa and bacillus acidophilus in water is respectively 400-600CFU/mL, 600-
1200CFU/mL, 500-1000CFU/mL and 800-1200CFU/mL.
Preferably, in the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the oyster shell powder
Comprise the following steps：
Step A, Concha Ostreae clear water is rinsed well after, dry, be put in the dilute hydrochloric acid that mass fraction is 12% soak
After 12-24 hours, take out, rinsed well with clear water, dry, be put into the hydroxide that the mass fraction that temperature is 35-45 DEG C is 8%
Soak in sodium solution after 12-24 hours, take out, rinsed well with clear water, dry, it is standby；
Step B, using infrared ray to processed in step A Concha Ostreae irradiation 2-3 hours after, Concha Ostreae is placed in into 800-
2-3 hours are calcined at a temperature of 900 DEG C, is crushed, cross 60-80 mesh sieves, Concha Ostreae just powder is obtained, it is standby；
Step C, by obtained Concha Ostreae in step B, just powder is put in the ethanol solution that volume fraction is 50-60% and soaks
After 2-3 hours, it is evaporated, that is, the oyster shell powder is obtained.
The present invention at least includes following beneficial effect：
The present invention is primary raw material research and development using aquatic products processing garbage Concha Ostreae, prawn head Crusta Penaeus seu Panulirus, anchovy sauce and sugar refinery molasses
Prawn culturing ecology Fertilizer water paste, the garbage for rationally being produced using aquatic products processing, with very big economic worth.
The prawn culturing ecology Fertilizer water paste of the present invention improves the beneficial planktonic quality and quantity in pond comprehensively, keeps good
Good water colour, cuts off pathogenic main Water Factors, so as to reduce the generation of prawn disease, promotes prawn to grow up healthy and sound, and improves prawn
Rate of growth and survival rate, increase yield.
The present invention uses Concha Ostreae, because oyster shell powder inside has the plurality of duct for interconnecting, with very
Strong hydrophilic and absorbability, can adsorb ammoniacal nitrogen, nitrite nitrogen, hydrogen sulfide and harmful microorganism etc., can not only be net
Change water quality, moreover it is possible to improve Dissolved Oxygen in Water content.
The further advantage of the present invention, target and feature embody part by description below, and part will also be by this
The research of invention and practice and be understood by the person skilled in the art.
Specific embodiment
With reference to embodiment, the present invention is described in further detail, to make those skilled in the art with reference to description
Word can be implemented according to this.
<Embodiment 1>
A kind of prawn culturing ecology Fertilizer water paste, including the component of following parts by weight：
1 part of fish and shrimp protein hydrolyzate, 1 part of Concha Ostreae slurry, 1 part of carbamide, 1 part of MAP, 1 part of magnesium sulfate, sulphuric acid are sub-
0.1 part of 1 part of ferrum and potassium chloride；
Wherein, the preparation method of the fish and shrimp slurry is comprised the following steps：
Step one, by processing fish flour when squeeze out useless anchovy sauce concentration after, be obtained fish slurry, it is standby；
Step 2, the leftover bits and pieces prawn head that aquatic products processing is obtained, Crusta Penaeus seu Panulirus are squeezed, and shrimp slurry is obtained, standby；
Step 3, by obtained fish slurry and shrimp slurry in mass ratio be 1:5 mixing, after stirring, by pH value adjust to
6.5, fish and shrimp slurry is obtained, it is standby；
Step 4, to obtained fish and shrimp slurry in add quality be fish and shrimp starch quality 1 ‰ by mass ratio be 1:2 lipase
After the compound enzyme mixed with protease, at a temperature of 50 DEG C after hydrolysis 8 hours, 90 DEG C are warming up to, enzyme denaturing 15 minutes, i.e.,
Obtain the fish and shrimp protein hydrolyzate；
The preparation method of the Concha Ostreae slurry is：Under agitation, oyster shell powder is immersed in into the salt that mass fraction is 8%
In aqueous acid after 48 hours, add the sodium hydrate aqueous solution that mass fraction is 8% to adjust pH value to 7, that is, be obtained described male
Oyster shells is starched.
In described prawn culturing ecology Fertilizer water paste, also including the component of following parts by weight：
1 part of seafood shell.
In described prawn culturing ecology Fertilizer water paste, the seafood shell be cycle of sixty years shell, the clam shell, scallop shell, extra large melon seed cases,
Any one or a few in Concha meretricis seu cyclinae shell, oyster shell and blood clam shell.
A kind of preparation method of prawn culturing ecology Fertilizer water paste, comprises the following steps：
Step a, the seafood shell powder of 1 weight portion is immersed in 40 weight portions containing whiterot fungi, Bacillus licheniformis, glue class
In the water of bacillus cereuss and bacillus acidophilus, first temperature be 20 DEG C, after air humidity is 70% bottom fermentation 48 hours, then in temperature
Spend and be 80% bottom fermentation 24 hours for 35 DEG C, air humidity, be dried afterwards, first with the heating rate of 200 DEG C/h by room when being dried
Temperature is warmed up to 300 DEG C, then with the rate of temperature fall of 80 DEG C/h drops to room temperature by 300 DEG C again, after circulation 2 times, fermentation seafood is obtained
Shell powder；
Step b, by obtained fermentation seafood shell powder in step a, the fish and shrimp protein hydrolyzate of 1 weight portion and 1 weight portion
After Concha Ostreae slurry mix homogeneously, carbamide, the MAP of 1 weight portion, the magnesium sulfate of 1 weight portion, 1 weight of 1 weight portion is added
The ferrous sulfate of amount part and the potassium chloride of 0.1 weight portion, mix homogeneously, obtain final product the prawn culturing ecology Fertilizer water paste.
In the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the seafood shell powder is：
After seafood shell is soaked 2 hours in the potassium permanganate solution that mass fraction is 0.001%, take out, use clear water
Rinse 2 times, after drying, be put in the dilute hydrochloric acid solution that mass fraction is 10% and soak 12 hours, then pH value is adjusted to 6,
After standing 6 hours, take out, rinsed 2 times with clear water, after drying, crush, cross 40 mesh sieves, after drying 3 hours at 200 DEG C, obtain final product institute
State seafood shell powder.
In the preparation method of described prawn culturing ecology Fertilizer water paste, brown rot fungus in step a, Bacillus licheniformis,
The initial clump count of Paenibacillus polymyxa and bacillus acidophilus in water is respectively 400CFU/mL, 600CFU/mL, 500CFU/
ML and 800CFU/mL.
In the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the oyster shell powder includes following step
Suddenly：
Step A, Concha Ostreae clear water is rinsed well after, dry, be put in the dilute hydrochloric acid that mass fraction is 12% soak
After 12 hours, take out, rinsed well with clear water, dry, be put into the sodium hydroxide solution that the mass fraction that temperature is 35 DEG C is 8%
After middle immersion 12 hours, take out, rinsed well with clear water, dry, it is standby；
Step B, the Concha Ostreae that processed in step A is irradiated 2 hours using infrared ray after, Concha Ostreae is placed in into 800 DEG C
At a temperature of calcine 2 hours, crush, cross 60 mesh sieves, Concha Ostreae just powder is obtained, it is standby；
Step C, by obtained Concha Ostreae in step B just powder to be put into immersion 2 in the ethanol solution that volume fraction is 50% little
Shi Hou, is evaporated, that is, the oyster shell powder is obtained.
<Embodiment 2>
A kind of prawn culturing ecology Fertilizer water paste, including the component of following parts by weight：
25 parts of fish and shrimp protein hydrolyzate, 25 parts of Concha Ostreae slurry, 15 parts of carbamide, 2 parts of MAP, 2 parts of magnesium sulfate, sulphuric acid
Ferrous 2 parts and 1 part of potassium chloride；
Wherein, the preparation method of the fish and shrimp slurry is comprised the following steps：
Step one, by processing fish flour when squeeze out useless anchovy sauce concentration after, be obtained fish slurry, it is standby；
Step 2, the leftover bits and pieces prawn head that aquatic products processing is obtained, Crusta Penaeus seu Panulirus are squeezed, and shrimp slurry is obtained, standby；
Step 3, by obtained fish slurry and shrimp slurry in mass ratio be 1:1 mixing, after stirring, pH value is adjusted to 7,
Prepared fish and shrimp slurry, it is standby；
Step 4, to obtained fish and shrimp slurry in add quality be fish and shrimp starch quality 1.5 ‰ by mass ratio be 1:2 fat
After the compound enzyme that enzyme and protease are mixed, at a temperature of 50 DEG C after hydrolysis 8 hours, 90 DEG C are warming up to, enzyme denaturing 15 minutes,
Obtain final product the fish and shrimp protein hydrolyzate；
The preparation method of the Concha Ostreae slurry is：Under agitation, oyster shell powder is immersed in into the salt that mass fraction is 8%
In aqueous acid after 48 hours, add the sodium hydrate aqueous solution that mass fraction is 8% to adjust pH value to 7, that is, be obtained described male
Oyster shells is starched.
In described prawn culturing ecology Fertilizer water paste, also including the component of following parts by weight：
10 parts of seafood shell.
In described prawn culturing ecology Fertilizer water paste, the seafood shell be cycle of sixty years shell, the clam shell, scallop shell, extra large melon seed cases,
Any one or a few in Concha meretricis seu cyclinae shell, oyster shell and blood clam shell.
A kind of preparation method of prawn culturing ecology Fertilizer water paste, comprises the following steps：
Step a, the seafood shell powder of 10 weight portions is immersed in 50 weight portions containing whiterot fungi, Bacillus licheniformis, glue more
In the water of series bacillus and bacillus acidophilus, first temperature be 30 DEG C, after air humidity is 80% bottom fermentation 48 hours, then
Temperature is 38 DEG C, air humidity is 85% bottom fermentation 24 hours, is dried afterwards, when being dried first with the heating rate of 200 DEG C/h by
Room temperature to 300 DEG C, then with the rate of temperature fall of 80 DEG C/h drops to room temperature by 300 DEG C again, after circulation 2 times, fermentation sea is obtained
Fresh shell powder；
Step b, by obtained fermentation seafood shell powder, the fish and shrimp protein hydrolyzate of 25 weight portions and 25 weight portions in step a
Concha Ostreae slurry mix homogeneously after, add the carbamide of 15 weight portions, the MAP of 2 weight portions, the magnesium sulfate of 2 weight portions, 2
The potassium chloride of the ferrous sulfate of weight portion and 1 weight portion, mix homogeneously obtains final product the prawn culturing ecology Fertilizer water paste.
In the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the seafood shell powder is：
After seafood shell is soaked 3 hours in the potassium permanganate solution that mass fraction is 0.001%, take out, use clear water
Rinse 2 times, after drying, be put in the dilute hydrochloric acid solution that mass fraction is 15% and soak 18 hours, then pH value is adjusted to 7,
After standing 7 hours, take out, rinsed 3 times with clear water, after drying, crush, cross 50 mesh sieves, after drying 4 hours at 250 DEG C, obtain final product institute
State seafood shell powder.
In the preparation method of described prawn culturing ecology Fertilizer water paste, brown rot fungus in step a, Bacillus licheniformis,
The initial clump count of Paenibacillus polymyxa and bacillus acidophilus in water is respectively 500CFU/mL, 900CFU/mL, 750CFU/
ML and 1000CFU/mL.
In the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the oyster shell powder includes following step
Suddenly：
Step A, Concha Ostreae clear water is rinsed well after, dry, be put in the dilute hydrochloric acid that mass fraction is 12% soak
After 18 hours, take out, rinsed well with clear water, dry, be put into the sodium hydroxide solution that the mass fraction that temperature is 40 DEG C is 8%
After middle immersion 18 hours, take out, rinsed well with clear water, dry, it is standby；
Step B, the Concha Ostreae that processed in step A is irradiated 2 hours using infrared ray after, Concha Ostreae is placed in into 850 DEG C
At a temperature of calcine 2 hours, crush, cross 70 mesh sieves, Concha Ostreae just powder is obtained, it is standby；
Step C, by obtained Concha Ostreae in step B just powder to be put into immersion 3 in the ethanol solution that volume fraction is 55% little
Shi Hou, is evaporated, that is, the oyster shell powder is obtained.
<Embodiment 3>
A kind of prawn culturing ecology Fertilizer water paste, including the component of following parts by weight：
50 parts of fish and shrimp protein hydrolyzate, 50 parts of Concha Ostreae slurry, 30 parts of carbamide, 5 parts of MAP, 5 parts of magnesium sulfate, sulphuric acid
Ferrous 3 parts and 2 parts of potassium chloride；
Wherein, the preparation method of the fish and shrimp slurry is comprised the following steps：
Step one, by processing fish flour when squeeze out useless anchovy sauce concentration after, be obtained fish slurry, it is standby；
Step 2, the leftover bits and pieces prawn head that aquatic products processing is obtained, Crusta Penaeus seu Panulirus are squeezed, and shrimp slurry is obtained, standby；
Step 3, by obtained fish slurry and shrimp slurry in mass ratio be 5:1 mixing, after stirring, by pH value adjust to
7.5, fish and shrimp slurry is obtained, it is standby；
Step 4, add in obtained fish and shrimp slurry quality be fish and shrimp starch quality 2 ‰ by the lipase that mass ratio is 2 and
After the compound enzyme that protease is mixed, after hydrolyzing 8 hours at a temperature of 50 DEG C, 90 DEG C are warming up to, enzyme denaturing 15 minutes is obtained final product
The fish and shrimp protein hydrolyzate；
The preparation method of the Concha Ostreae slurry is：Under agitation, oyster shell powder is immersed in into the salt that mass fraction is 8%
In aqueous acid after 48 hours, add the sodium hydrate aqueous solution that mass fraction is 8% to adjust pH value to 7, that is, be obtained described male
Oyster shells is starched.
In described prawn culturing ecology Fertilizer water paste, also including the component of following parts by weight：
20 parts of seafood shell.
In described prawn culturing ecology Fertilizer water paste, the seafood shell be cycle of sixty years shell, the clam shell, scallop shell, extra large melon seed cases,
Any one or a few in Concha meretricis seu cyclinae shell, oyster shell and blood clam shell.
A kind of preparation method of prawn culturing ecology Fertilizer water paste, comprises the following steps：
Step a, the seafood shell powder of 20 weight portions is immersed in 60 weight portions containing whiterot fungi, Bacillus licheniformis, glue more
In the water of series bacillus and bacillus acidophilus, first temperature be 35 DEG C, after air humidity is 85% bottom fermentation 48 hours, then
Temperature is 40 DEG C, air humidity is 90% bottom fermentation 24 hours, is dried afterwards, when being dried first with the heating rate of 200 DEG C/h by
Room temperature to 300 DEG C, then with the rate of temperature fall of 80 DEG C/h drops to room temperature by 300 DEG C again, after circulation 3 times, fermentation sea is obtained
Fresh shell powder；
Step b, by obtained fermentation seafood shell powder, the fish and shrimp protein hydrolyzate of 50 weight portions and 50 weight portions in step a
Concha Ostreae slurry mix homogeneously after, add the carbamide of 30 weight portions, the MAP of 5 weight portions, the magnesium sulfate of 5 weight portions, 3
The potassium chloride of the ferrous sulfate of weight portion and 2 weight portions, mix homogeneously obtains final product the prawn culturing ecology Fertilizer water paste.
In the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the seafood shell powder is：
After seafood shell is soaked 4 hours in the potassium permanganate solution that mass fraction is 0.001%, take out, use clear water
Rinse 3 times, after drying, be put into mass fraction be 10-20% dilute hydrochloric acid solution in soak 24 hours, then by pH value adjust to
7, after standing 8 hours, take out, rinsed 3 times with clear water, after drying, crush, 40-60 mesh sieves are crossed, after drying 4 hours at 300 DEG C,
Obtain final product the seafood shell powder.
In the preparation method of described prawn culturing ecology Fertilizer water paste, brown rot fungus in step a, Bacillus licheniformis,
The initial clump count of Paenibacillus polymyxa and bacillus acidophilus in water be respectively 600CFU/mL, 1200CFU/mL,
1000CFU/mL and 1200CFU/mL.
In the preparation method of described prawn culturing ecology Fertilizer water paste, the preparation method of the oyster shell powder includes following step
Suddenly：
Step A, Concha Ostreae clear water is rinsed well after, dry, be put in the dilute hydrochloric acid that mass fraction is 12% soak
After 24 hours, take out, rinsed well with clear water, dry, be put into the sodium hydroxide solution that the mass fraction that temperature is 45 DEG C is 8%
After middle immersion 24 hours, take out, rinsed well with clear water, dry, it is standby；
Step B, the Concha Ostreae that processed in step A is irradiated 3 hours using infrared ray after, Concha Ostreae is placed in into 900 DEG C
At a temperature of calcine 3 hours, crush, cross 80 mesh sieves, Concha Ostreae just powder is obtained, it is standby；
Step C, by obtained Concha Ostreae in step B just powder to be put into immersion 3 in the ethanol solution that volume fraction is 60% little
Shi Hou, is evaporated, that is, the oyster shell powder is obtained.
Although embodiment of the present invention is disclosed as above, it is not restricted to listed in description and embodiment
With, it can be applied to completely various suitable the field of the invention, for those skilled in the art, can be easily
Other modification is realized, therefore under the general concept limited without departing substantially from claim and equivalency range, the present invention is not limited
In specific details and shown here as the embodiment with description.
Claims (8)
1. a kind of prawn culturing ecology Fertilizer water paste, it is characterised in that including the component of following parts by weight：
Fish and shrimp protein hydrolyzate 1-50 parts, Concha Ostreae slurry 1-50 part, carbamide 1-30 parts, MAP 1-5 parts, magnesium sulfate 1-5
Part, ferrous sulfate 1-3 parts and potassium chloride 0.1-2 parts；
Wherein, the preparation method of the fish and shrimp slurry is comprised the following steps：
Step one, by processing fish flour when squeeze out useless anchovy sauce concentration after, be obtained fish slurry, it is standby；
Step 2, the leftover bits and pieces prawn head that aquatic products processing is obtained, Crusta Penaeus seu Panulirus are squeezed, and shrimp slurry is obtained, standby；
Step 3, by obtained fish slurry and shrimp slurry in mass ratio be 1-5:1-5 mix, after stirring, by pH value adjust to
6.5-7.5, is obtained fish and shrimp slurry, standby；
Step 4, to obtained fish and shrimp slurry in add quality be fish and shrimp starch quality 1-2 ‰ by mass ratio be 1:2 lipase and
After the compound enzyme that protease is mixed, after hydrolyzing 8 hours at a temperature of 50 DEG C, 85-90 DEG C, enzyme denaturing 10-15 point is warming up to
Clock, obtains final product the fish and shrimp protein hydrolyzate；
The preparation method of the Concha Ostreae slurry is：Under agitation, oyster shell powder is immersed in into the hydrochloric acid water that mass fraction is 8%
In solution after 48 hours, add the sodium hydrate aqueous solution that mass fraction is 8% to adjust pH value to 7, that is, the Concha Ostreae is obtained
Slurry.
2. prawn culturing as claimed in claim 1 ecology Fertilizer water paste, it is characterised in that the prawn culturing ecology Fertilizer water paste bag
Include the component of following parts by weight：
40 parts of fish and shrimp protein hydrolyzate, 30 parts of Concha Ostreae slurry, 20 parts of carbamide, 4 parts of MAP, 3 parts of magnesium sulfate, ferrous sulfate
2 parts and 1 part of potassium chloride.
3. prawn culturing as claimed in claim 1 ecology Fertilizer water paste, it is characterised in that also including the group of following parts by weight
Point：
Seafood shell 1-20 parts.
4. prawn culturing as claimed in claim 1 ecology Fertilizer water paste, it is characterised in that the seafood shell is cycle of sixty years shell, razor clam
Any one or a few in shell, scallop shell, extra large melon seed cases, Concha meretricis seu cyclinae shell, oyster shell and blood clam shell.
5. a kind of preparation method of prawn culturing as claimed in claim 3 ecology Fertilizer water paste, it is characterised in that including following step
Suddenly：
Step a, the seafood shell powder of 1-20 weight portions is immersed in 40-60 weight portions containing whiterot fungi, Bacillus licheniformis, glue more
In the water of series bacillus and bacillus acidophilus, first temperature be 20-35 DEG C, air humidity be 70-85% bottom fermentations 48 hours
Afterwards, then temperature be 35-40 DEG C, air humidity be 80-90% bottom fermentations 24 hours, be dried afterwards, first with 200 DEG C/h when being dried
Heating rate by room temperature to 300 DEG C, then again room temperature dropped to by 300 DEG C with the rate of temperature fall of 80 DEG C/h, circulate 2-3 time
Afterwards, fermentation seafood shell powder is obtained；
Step b, by obtained fermentation seafood shell powder, the fish and shrimp protein hydrolyzate of 1-50 weight portions and 1-50 weight portions in step a
Concha Ostreae slurry mix homogeneously after, add 1-30 weight portions carbamide, the MAP of 1-5 weight portions, the sulfur of 1-5 weight portions
The potassium chloride of sour magnesium, the ferrous sulfate of 1-3 weight portions and 0.1-2 weight portions, mix homogeneously obtains final product the prawn culturing Eco-fertilizer
Water cream.
6. the preparation method of prawn culturing as claimed in claim 5 ecology Fertilizer water paste, it is characterised in that the seafood shell powder
Preparation method is：
Seafood shell is soaked after 2-4 hours in the potassium permanganate solution that mass fraction is 0.001%, is taken out, rushed with clear water
Wash 2-3 time, after drying, be put in the dilute hydrochloric acid solution that mass fraction is 10-20% and soak 12-24 hours, then adjust pH value
Save to 6-7, after standing 6-8 hours, take out, rinsed 2-3 time with clear water, after drying, crush, 40-60 mesh sieves are crossed, in 200-300
Dry after 3-4 hours at DEG C, obtain final product the seafood shell powder.
7. the preparation method of prawn culturing as claimed in claim 5 ecology Fertilizer water paste, it is characterised in that brown in step a
The initial clump count of rotten bacterium, Bacillus licheniformis, Paenibacillus polymyxa and bacillus acidophilus in water is respectively 400-
600CFU/mL, 600-1200CFU/mL, 500-1000CFU/mL and 800-1200CFU/mL.
8. the preparation method of prawn culturing as claimed in claim 5 ecology Fertilizer water paste, it is characterised in that the oyster shell powder
Preparation method is comprised the following steps：
Step A, Concha Ostreae clear water is rinsed well after, dry, be put in the dilute hydrochloric acid that mass fraction is 12% and soak 12-24
After hour, take out, rinsed well with clear water, dry, be put into the sodium hydroxide that the mass fraction that temperature is 35-45 DEG C is 8% molten
Soak in liquid after 12-24 hours, take out, rinsed well with clear water, dry, it is standby；
Step B, using infrared ray to processed in step A Concha Ostreae irradiation 2-3 hours after, Concha Ostreae is placed in into 800-900
2-3 hours are calcined at a temperature of DEG C, is crushed, cross 60-80 mesh sieves, Concha Ostreae just powder is obtained, it is standby；
Step C, by obtained Concha Ostreae in step B, just powder is put into that to soak 2-3 in the ethanol solution that volume fraction is 50-60% little
Shi Hou, is evaporated, that is, the oyster shell powder is obtained.
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