CN106538640A - A kind of Pesticidal combination for killing fragrant-flowered garlic maggot and preparation method thereof - Google Patents

A kind of Pesticidal combination for killing fragrant-flowered garlic maggot and preparation method thereof Download PDF

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CN106538640A
CN106538640A CN201610962248.5A CN201610962248A CN106538640A CN 106538640 A CN106538640 A CN 106538640A CN 201610962248 A CN201610962248 A CN 201610962248A CN 106538640 A CN106538640 A CN 106538640A
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parts
folium
radix
fragrant
killing
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袁国防
李洪
孙明
王亮
宋辉
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Qingdao Haizhixing Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/02Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention belongs to field of agricultural production technologies, more particularly to a kind of Pesticidal combination for killing fragrant-flowered garlic maggot, further relate to a kind of preparation method of above-mentioned Pesticidal combination.The Pesticidal combination is prepared from by each component of following parts by weight:21 parts of Exocarpium Citrulli, 22 parts of Folium Mori, 20 parts of Semen Cucurbitae, 27 parts of Herba Lophatheri, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 21 parts of Semen Hydnocarpi, 17 parts of Herba Hydrocotyleses, 18 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 14 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 15 parts of Pericarpium Granati, 8 parts of Radix Rosae Normaliss, 9 parts of Fructus Zanthoxyli, 3 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 2 parts of Folium Crataegi, 22 parts of Folium Allii tuberosi stem.It is an advantage of the invention that environmental protection, having good insecticidal effect to fragrant-flowered garlic maggot.

Description

A kind of Pesticidal combination for killing fragrant-flowered garlic maggot and preparation method thereof
Technical field
The invention belongs to field of agricultural production technologies, more particularly to a kind of Pesticidal combination for killing fragrant-flowered garlic maggot, also relate to And a kind of above-mentioned preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot.
Background technology
Fragrant-flowered garlic maggot, belongs to the liliaceous vegetables such as Diptera, eye Sciaridae, main harm Folium Allii tuberosi, Herba Alii fistulosi, Bulbus Allii Cepae, Herba Alii fistulosi, Bulbus Allii, Also Caulis et Folium Lactucae sativae, green vegetable, Herba Apii graveolentis etc. are endangered once in a while, are distributed in Beijing, Tianjin, Shandong, Shanxi, Liaoning, Jiangxi, Ningxia, the Inner Mongol, Zhejiang The ground such as river, Taiwan, are one of primary pests of allium vegetables.Worm state has adult, ovum, larva, pupa, is gathered in Folium Allii tuberosi with larva The bulb of underground part and tender stem cause harm.Newly hatched larvae is first caused harm the upper end of Folium Allii tuberosi leaf sheath base and bulb.Spring, Qiu Liangji The young stem of Folium Allii tuberosi of mainly causing harm causes rotten, makes fragrant-flowered garlic leaf withered and yellow and dead.The downward activity of summer larva is eaten into into bulb, and severe one bulb is rotten Rotten, whole pier Folium Allii tuberosi is dead.
Fragrant-flowered garlic maggot is that for common pest and disease damage in Folium Allii tuberosi production, fragrant-flowered garlic maggot larva is gathered in underground, bores the pseudobulb of food Folium Allii tuberosi, fragrant-flowered garlic After dish is aggrieved, gently then affect commodity value, it is heavy then cause ground blade it is thin and weak it is withered and yellow, wilt and rot or even dead in flakes, greatly Compromise the interests of fragrant-flowered garlic agriculture.More than the medicine of the specialty preventing and treating fragrant-flowered garlic maggot that at present fragrant-flowered garlic agriculture is adopted with phoxim (organophosphorus insecticide) and Based on chlopyrifos, although two kinds of pesticide are the insecticides of national approved applications, but due to the interior suction and trophophase of Folium Allii tuberosi it is short Characteristic, Folium Allii tuberosi is not up to safety interval of pesticide pollution when gathering in, and fragrant-flowered garlic agriculture cannot be also obtained using the quantity and frequency of such medicine To effective control.As the administration of such pesticide, fragrant-flowered garlic maggot are also increasingly stronger to the resistance of pesticide, fragrant-flowered garlic agriculture is forced to go to apply in violation of rules and regulations more High poison, more effective pesticide form vicious cycle, cause Folium Allii tuberosi pesticide residues exceeded, a lot of " malicious Folium Allii tuberosi " events occur, seriously Person's even threat to life.In order to solve this problem, related researcher develops the biological preparation of some preventing and treating fragrant-flowered garlic maggots, so And these biological preparation effects are not so good as chemical pesticide, it is impossible to promote on a large scale and application.Therefore, develop a kind of environmental protection and The Insecticidal combinations group of good disinsection effect has important market prospect.
The content of the invention
An object of the present invention is to provide a kind of Pesticidal combination for killing fragrant-flowered garlic maggot, its environmental protection, to fragrant-flowered garlic maggot There is good insecticidal effect.
In order to solve above-mentioned technical problem, the present invention is employed the following technical solutions:A kind of parasite killing group for killing fragrant-flowered garlic maggot Compound, is prepared from by each component of following parts by weight:Exocarpium Citrulli 21-27 parts, Folium Mori 20-25 parts, Semen Cucurbitae 18-25 parts, Herba Lophatheri 20-27 parts, Rhizoma Dryopteris Crassirhizomatiss 17-24 parts, morning glory 18-21 parts, Semen Hydnocarpi 15-21 parts, Herba Hydrocotyleses 14-20 part, Folium Eriobotryae Leaf 16-21 parts, Radix Tripterygii Wilfordii 12-17 parts, Radix et Caulis Opuntiae Dillenii 11-18 parts, sulfur 9-12 parts, Pericarpium Granati 11-15 parts, Radix Rosae Normaliss 8-14 parts, Fructus Zanthoxyli 7-10 parts, Fructus Quisqualis 3-5 parts, Cortex Meliae 2-3 parts, Folium Artemisiae Argyi 4-6 parts, Folium Crataegi 1-4 parts, Folium Allii tuberosi stem 20-25 parts.
Preferably, the Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:West 21 parts of melon skin, 22 parts of Folium Mori, 20 parts of Semen Cucurbitae, 27 parts of Herba Lophatheri, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, Semen Hydnocarpi 21 part, day 17 parts of Herba Coriandri, 18 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 14 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 15 parts of Pericarpium Granati, 8 parts of Radix Rosae Normaliss, Fructus Zanthoxyli 9 Part, 3 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 2 parts of Folium Crataegi, 22 parts of Folium Allii tuberosi stem.
Preferably, the Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:West 21 parts of melon skin, 20 parts of Folium Mori, 25 parts of Semen Cucurbitae, 25 parts of Herba Lophatheri, 20 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, Semen Hydnocarpi 18 part, day 20 parts of Herba Coriandri, 21 parts of Folium Eriobotryae, 14 parts of Radix Tripterygii Wilfordii, 18 parts of Radix et Caulis Opuntiae Dillenii, 9 parts of sulfur, 11 parts of Pericarpium Granati, 12 parts of Radix Rosae Normaliss, Fructus Zanthoxyli 7 Part, 5 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 1 part of Folium Crataegi, 24 parts of Folium Allii tuberosi stem.
Preferably, the Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:West 22 parts of melon skin, 25 parts of Folium Mori, 21 parts of Semen Cucurbitae, 21 parts of Herba Lophatheri, 18 parts of Rhizoma Dryopteris Crassirhizomatiss, 18 parts of morning glory, Semen Hydnocarpi 15 part, day 15 parts of Herba Coriandri, 16 parts of Folium Eriobotryae, 17 parts of Radix Tripterygii Wilfordii, 16 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 14 parts of Pericarpium Granati, 14 parts of Radix Rosae Normaliss, Fructus Zanthoxyli 8 parts, 4 parts of Fructus Quisqualis, 2 parts of Cortex Meliae, 4 parts of Folium Artemisiae Argyi, 3 parts of Folium Crataegi, 24 parts of Folium Allii tuberosi stem.
Preferably, the Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:West 24 parts of melon skin, 21 parts of Folium Mori, 20 parts of Semen Cucurbitae, 24 parts of Herba Lophatheri, 24 parts of Rhizoma Dryopteris Crassirhizomatiss, 18 parts of morning glory, Semen Hydnocarpi 16 part, day 16 parts of Herba Coriandri, 18 parts of Folium Eriobotryae, 12 parts of Radix Tripterygii Wilfordii, 15 parts of Radix et Caulis Opuntiae Dillenii, 11 parts of sulfur, 11 parts of Pericarpium Granati, 11 parts of Radix Rosae Normaliss, Fructus Zanthoxyli 8 parts, 5 parts of Fructus Quisqualis, 2 parts of Cortex Meliae, 5 parts of Folium Artemisiae Argyi, 4 parts of Folium Crataegi, 23 parts of Folium Allii tuberosi stem.
Preferably, the Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:West 25 parts of melon skin, 24 parts of Folium Mori, 18 parts of Semen Cucurbitae, 25 parts of Herba Lophatheri, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, Semen Hydnocarpi 20 part, day 18 parts of Herba Coriandri, 20 parts of Folium Eriobotryae, 17 parts of Radix Tripterygii Wilfordii, 16 parts of Radix et Caulis Opuntiae Dillenii, 9 parts of sulfur, 12 parts of Pericarpium Granati, 9 parts of Radix Rosae Normaliss, Fructus Zanthoxyli 10 Part, 3 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 5 parts of Folium Artemisiae Argyi, 1 part of Folium Crataegi, 20 parts of Folium Allii tuberosi stem.
Preferably, the Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:West 27 parts of melon skin, 22 parts of Folium Mori, 21 parts of Semen Cucurbitae, 22 parts of Herba Lophatheri, 19 parts of Rhizoma Dryopteris Crassirhizomatiss, 21 parts of morning glory, Semen Hydnocarpi 17 part, day 14 parts of Herba Coriandri, 19 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 11 parts of Radix et Caulis Opuntiae Dillenii, 12 parts of sulfur, 11 parts of Pericarpium Granati, 14 parts of Radix Rosae Normaliss, Fructus Zanthoxyli 9 parts, 5 parts of Fructus Quisqualis, 2 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 3 parts of Folium Crataegi, 21 parts of Folium Allii tuberosi stem.
Each raw material components Nantural non-toxic of the present invention, the Folium Allii tuberosi of the edible Pesticidal combination for having sprayed the present invention are not interfered with People's is healthy, in addition Pesticidal combination ecological, environmental protective of the invention, will not contaminated soil, it is also pollution-free to environment.This In invention, by Exocarpium Citrulli, Folium Mori, Semen Cucurbitae, Herba Lophatheri, Rhizoma Dryopteris Crassirhizomatiss, morning glory, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Thunder God Rattan, Radix et Caulis Opuntiae Dillenii, sulfur, Pericarpium Granati, Radix Rosae Normaliss, Fructus Zanthoxyli, Fructus Quisqualis, Cortex Meliae, Folium Artemisiae Argyi, Folium Crataegi are with above-mentioned specific proportioning group When being combined, there is good insecticidal effect to fragrant-flowered garlic maggot.The Folium Crataegi and Folium Allii tuberosi stem of addition proper proportion can improve the present invention Pesticidal combination abnormal smells from the patient, can lure that fragrant-flowered garlic maggot stings the Pesticidal combination of the food present invention into, and then be conducive to making the parasite killing of the present invention Compositionss preferably play insecticidal action.Additionally, the Pesticidal combination of the present invention has no toxic side effect to Folium Allii tuberosi, Folium Allii tuberosi is not affected Normal growth.
The invention also discloses a kind of preparation method of above-mentioned fragrant-flowered garlic maggot Pesticidal combination, which comprises the following steps:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Usage and dosage:The clear water for killing 400-500 times of weight of the Pesticidal combination of fragrant-flowered garlic maggot of the present invention is diluted Afterwards, it is directed at Folium Allii tuberosi rhizome portion to use along ridge sprinkling irrigation medicine liquid spray, the parasite killing group of the present invention of every mu of Folium Allii tuberosi administration 0.05-0.1kg Compound.
The preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot of the present invention is simple, and preparation process will not be to environment Bring pollution.In preparation method, the effect that each raw material components are ground respectively is advantageous for into above-mentioned each component follow-up anti- It is fully contacted in answering, is conducive to fully reacting between each component, to give full play to interaction.By Folium Mori, Semen Cucurbitae, phyllostachys nigra (lodd.ex lindl.) munro var.henonis (miff.) spapf et rendle Leaf, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis mix after under condition of different temperatures repeatedly immersion or The effect of decoction is fully to separate out the effective ingredient in above-mentioned each component, is conducive to the abundant reaction between each component, is conducive to Drug effect is improved, and improves the stimulation of medicine so as to which the not growth to Folium Allii tuberosi has a negative impact.By Rhizoma Dryopteris Crassirhizomatiss, Melia azedarach L. The soaking in rice vinegar effect of 12 hours of skin, Folium Artemisiae Argyi is that the cell for making Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae, Folium Artemisiae Argyi softens, and is conducive to follow-up In decoction step, and immersion process after Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae, Folium Artemisiae Argyi and rice vinegar haptoreaction, be conducive to improving insecticidal effect; The purpose dried is to reduce the rice vinegar that remains in medicine, to reduce stimulation of the rice vinegar to Folium Allii tuberosi, it is to avoid Folium Allii tuberosi growth is produced not Profit affects.The dip operation of step (4) can be conducive to the precipitation of effective ingredient and react to each other;Decoct can fully it is fried it is effective into Point, drug effect is improved, and the rice vinegar remained in making medicine fully volatilizees, to reduce the adverse effect that rice vinegar is grown to Folium Allii tuberosi.By west It is to become cell that melon skin, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli mix the preservation effect of 12 hours in being put into ultra cold storage freezer It is crisp, the effective ingredient in Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli is preferably leached in being conducive to subsequent step.Step Suddenly the operation purpose of (6) is the effective ingredient in each component is fully leached, and makes fully to react between each component.Step (7), in, the purpose of ultrasonic Treatment is made obtained by decoction liquor obtained by sulfur, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Decoction liquor, the soak obtained by step (6) more fully mixes and reacts.
Compared with prior art, the beneficial effects of the present invention is:
(1) each raw material components Nantural non-toxic of the invention, the Folium Allii tuberosi of the edible Pesticidal combination for having sprayed the present invention will not Affect that people's is healthy, in addition Pesticidal combination ecological, environmental protective of the invention, will not contaminated soil, to environment also without dirt Dye.In the present invention, by Exocarpium Citrulli, Folium Mori, Semen Cucurbitae, Herba Lophatheri, Rhizoma Dryopteris Crassirhizomatiss, morning glory, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix et Caulis Opuntiae Dillenii, sulfur, Pericarpium Granati, Radix Rosae Normaliss, Fructus Zanthoxyli, Fructus Quisqualis, Cortex Meliae, Folium Artemisiae Argyi, Folium Crataegi are specifically matched somebody with somebody with above-mentioned During than combining, there is good insecticidal effect to fragrant-flowered garlic maggot.The Folium Crataegi and Folium Allii tuberosi stem of addition proper proportion can improve this The abnormal smells from the patient of the Pesticidal combination of invention, can lure that fragrant-flowered garlic maggot stings the Pesticidal combination of the food present invention into, and then be conducive to making the present invention's Pesticidal combination preferably plays insecticidal action.Additionally, the Pesticidal combination of the present invention has no toxic side effect to Folium Allii tuberosi, fragrant-flowered garlic is not affected The normal growth of dish.
(2) preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot of the invention is simple, and preparation process will not be right Environment brings pollution.In preparation method, the effect that each raw material components are ground respectively is advantageous for into above-mentioned each component rear It is fully contacted in continuous reaction, is conducive to fully reacting between each component, to give full play to interaction.By Folium Mori, Semen Cucurbitae, light Folium Bambusae, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis soak after mixing under condition of different temperatures repeatedly Or the effect for decocting is fully to separate out the effective ingredient in above-mentioned each component, is conducive to the abundant reaction between each component, favorably In raising drug effect, and improve the stimulation of medicine so as to which the not growth to Folium Allii tuberosi has a negative impact.By Rhizoma Dryopteris Crassirhizomatiss, hardship The soaking in rice vinegar effect of 12 hours of chinaberry skin, Folium Artemisiae Argyi is that the cell for making Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae, Folium Artemisiae Argyi softens, and is conducive to follow-up Decoction step, and in immersion process after Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae, Folium Artemisiae Argyi and rice vinegar haptoreaction, be conducive to improving parasite killing effect Really;The purpose dried is to reduce the rice vinegar that remains in medicine, to reduce stimulation of the rice vinegar to Folium Allii tuberosi, it is to avoid Folium Allii tuberosi growth is produced Adverse effect.The dip operation of step (4) can be conducive to the precipitation of effective ingredient and react to each other;Decocting can be fully fried effective Composition, improves drug effect, and the rice vinegar remained in making medicine fully volatilizees, to reduce the adverse effect that rice vinegar is grown to Folium Allii tuberosi.Will It is to make cell that Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli mix the preservation effect of 12 hours in being put into ultra cold storage freezer Become fragile, in being conducive to subsequent step, preferably leach the effective ingredient in Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli. The operation purpose of step (6) is the effective ingredient in each component is fully leached, and makes fully to react between each component.Step (7), in, the purpose of ultrasonic Treatment is made obtained by decoction liquor obtained by sulfur, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Decoction liquor, the soak obtained by step (6) more fully mixes and reacts.
Specific embodiment
Below example facilitates a better understanding of the present invention, but does not limit the present invention.Experiment in following embodiments Method, if no special instructions, is conventional method.
Embodiment 1
A kind of Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:Exocarpium Citrulli 21 Part, 22 parts of Folium Mori, 20 parts of Semen Cucurbitae, 27 parts of Herba Lophatheri, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 21 parts of Semen Hydnocarpi, Herba Hydrocotyleses 17 Part, 18 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 14 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 15 parts of Pericarpium Granati, 8 parts of Radix Rosae Normaliss, 9 parts of Fructus Zanthoxyli, make 3 parts of gentleman, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 2 parts of Folium Crataegi, 22 parts of Folium Allii tuberosi stem.
The above-mentioned preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot is as follows:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Embodiment 2
A kind of Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:Exocarpium Citrulli 21 Part, 20 parts of Folium Mori, 25 parts of Semen Cucurbitae, 25 parts of Herba Lophatheri, 20 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 18 parts of Semen Hydnocarpi, Herba Hydrocotyleses 20 Part, 21 parts of Folium Eriobotryae, 14 parts of Radix Tripterygii Wilfordii, 18 parts of Radix et Caulis Opuntiae Dillenii, 9 parts of sulfur, 11 parts of Pericarpium Granati, 12 parts of Radix Rosae Normaliss, 7 parts of Fructus Zanthoxyli, make 5 parts of gentleman, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 1 part of Folium Crataegi, 24 parts of Folium Allii tuberosi stem.
The above-mentioned preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot is as follows:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Embodiment 3
A kind of Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:Exocarpium Citrulli 22 Part, 25 parts of Folium Mori, 21 parts of Semen Cucurbitae, 21 parts of Herba Lophatheri, 18 parts of Rhizoma Dryopteris Crassirhizomatiss, 18 parts of morning glory, 15 parts of Semen Hydnocarpi, Herba Hydrocotyleses 15 Part, 16 parts of Folium Eriobotryae, 17 parts of Radix Tripterygii Wilfordii, 16 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 14 parts of Pericarpium Granati, 14 parts of Radix Rosae Normaliss, 8 parts of Fructus Zanthoxyli, make 4 parts of gentleman, 2 parts of Cortex Meliae, 4 parts of Folium Artemisiae Argyi, 3 parts of Folium Crataegi, 24 parts of Folium Allii tuberosi stem.
The above-mentioned preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot is as follows:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Embodiment 4
A kind of Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:Exocarpium Citrulli 24 Part, 21 parts of Folium Mori, 20 parts of Semen Cucurbitae, 24 parts of Herba Lophatheri, 24 parts of Rhizoma Dryopteris Crassirhizomatiss, 18 parts of morning glory, 16 parts of Semen Hydnocarpi, Herba Hydrocotyleses 16 Part, 18 parts of Folium Eriobotryae, 12 parts of Radix Tripterygii Wilfordii, 15 parts of Radix et Caulis Opuntiae Dillenii, 11 parts of sulfur, 11 parts of Pericarpium Granati, 11 parts of Radix Rosae Normaliss, 8 parts of Fructus Zanthoxyli, make 5 parts of gentleman, 2 parts of Cortex Meliae, 5 parts of Folium Artemisiae Argyi, 4 parts of Folium Crataegi, 23 parts of Folium Allii tuberosi stem.
The above-mentioned preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot is as follows:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Embodiment 5
A kind of Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:Exocarpium Citrulli 25 Part, 24 parts of Folium Mori, 18 parts of Semen Cucurbitae, 25 parts of Herba Lophatheri, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 20 parts of Semen Hydnocarpi, Herba Hydrocotyleses 18 Part, 20 parts of Folium Eriobotryae, 17 parts of Radix Tripterygii Wilfordii, 16 parts of Radix et Caulis Opuntiae Dillenii, 9 parts of sulfur, 12 parts of Pericarpium Granati, 9 parts of Radix Rosae Normaliss, 10 parts of Fructus Zanthoxyli, make 3 parts of gentleman, 3 parts of Cortex Meliae, 5 parts of Folium Artemisiae Argyi, 1 part of Folium Crataegi, 20 parts of Folium Allii tuberosi stem.
The above-mentioned preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot is as follows:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Embodiment 6
A kind of Pesticidal combination for killing fragrant-flowered garlic maggot, is prepared from by each component of following parts by weight:Exocarpium Citrulli 27 Part, 22 parts of Folium Mori, 21 parts of Semen Cucurbitae, 22 parts of Herba Lophatheri, 19 parts of Rhizoma Dryopteris Crassirhizomatiss, 21 parts of morning glory, 17 parts of Semen Hydnocarpi, Herba Hydrocotyleses 14 Part, 19 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 11 parts of Radix et Caulis Opuntiae Dillenii, 12 parts of sulfur, 11 parts of Pericarpium Granati, 14 parts of Radix Rosae Normaliss, 9 parts of Fructus Zanthoxyli, make 5 parts of gentleman, 2 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 3 parts of Folium Crataegi, 21 parts of Folium Allii tuberosi stem.
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed Even, in mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire at 20-30 DEG C 20-30 minutes are boiled, after being cooled to room temperature, is soaked 50-60 minutes under 50-60 DEG C of water bath condition, is then cooked by slow fire 20-30 Minute, filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight phase Same rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature After 12 hours, 20-30 minutes are cooked by slow fire, filter to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C Preservation 12 hours, takes out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to recovering into the blending ingredients of room temperature, addition is heavy The clear water for 9 times of blending ingredients gross weight is measured, after putting in agitator with the rotating speed concussion 8h of 120r/min, 70-80 DEG C of water-bath Under the conditions of soak 30-40 minutes, cross 80 mesh sieves take soak;
(7) by obtained by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), step (4) Soak obtained by decoction liquor, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C of conditions Under be concentrated into relative density for 45 DEG C when 1.15~1.18, it is bottled, obtain final product.
Experimental result
Testing was carried out in Qingdao of Shandong province Jiangzhou Chinese chive field in October, 2015, the life of 4 years fragrant-flowered garlic ages, and fragrant-flowered garlic maggot over the years occurs It is universal and uniform.The cultivation condition (soil types, fertilising, growing stage, seeding row spacing etc.) of all experimental plots and Folium Allii tuberosi growing way It is homogeneous and consistent with local cultivation step.
The Pesticidal combination for killing fragrant-flowered garlic maggot of embodiment of the present invention 1- embodiment 6 is clear with 500 times of weight respectively After water dilution, alignment Folium Allii tuberosi rhizome portion is used along ridge sprinkling irrigation medicine liquid spray, the parasite killing of the present invention of every mu of Folium Allii tuberosi administration 0.08kg Compositionss.Each embodiment setting two is parallel.
Survival insect population investigation:2 days before medicine and after medicine, 4 days, investigated after 6 days respectively and dig 5 caves (pier) in each group experimental field Folium Allii tuberosi, inside and outside statistics bulb, fragrant-flowered garlic maggot number living, calculates Revision insect recluced rate.
The insecticidal effect for killing the Pesticidal combination of fragrant-flowered garlic maggot of 1 embodiment of the present invention 1- embodiment 6 of table
Test result indicate that, the Pesticidal combination of the present invention has good insecticidal action to fragrant-flowered garlic maggot.
The above is only the preferred embodiment of the present invention, it should be pointed out that:For the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvement can also be made, these improvement should be regarded as the guarantor of the present invention Shield scope.

Claims (8)

1. a kind of Pesticidal combination for killing fragrant-flowered garlic maggot, it is characterised in that:It is prepared from by each component of following parts by weight: Exocarpium Citrulli 21-27 parts, Folium Mori 20-25 parts, Semen Cucurbitae 18-25 parts, Herba Lophatheri 20-27 parts, Rhizoma Dryopteris Crassirhizomatiss 17-24 parts, morning glory 18-21 parts, Semen Hydnocarpi 15-21 parts, Herba Hydrocotyleses 14-20 part, Folium Eriobotryae 16-21 parts, Radix Tripterygii Wilfordii 12-17 parts, Radix et Caulis Opuntiae Dillenii 11-18 Part, sulfur 9-12 parts, Pericarpium Granati 11-15 parts, Radix Rosae Normaliss 8-14 parts, Fructus Zanthoxyli 7-10 parts, Fructus Quisqualis 3-5 parts, Cortex Meliae 2-3 parts, Folium Artemisiae Argyi 4-6 parts, Folium Crataegi 1-4 parts, Folium Allii tuberosi stem 20-25 parts.
2. the Pesticidal combination for killing fragrant-flowered garlic maggot according to claim 1, it is characterised in that:It is described for killing fragrant-flowered garlic maggot Pesticidal combination, be prepared from by each component of following parts by weight:It is 21 parts of Exocarpium Citrulli, 22 parts of Folium Mori, 20 parts of Semen Cucurbitae, light 27 parts of Folium Bambusae, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 21 parts of Semen Hydnocarpi, 17 parts of Herba Hydrocotyleses, 18 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 14 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 15 parts of Pericarpium Granati, 8 parts of Radix Rosae Normaliss, 9 parts of Fructus Zanthoxyli, 3 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 2 parts of Folium Crataegi, 22 parts of Folium Allii tuberosi stem.
3. the Pesticidal combination for killing fragrant-flowered garlic maggot according to claim 1, it is characterised in that:It is described for killing fragrant-flowered garlic maggot Pesticidal combination, be prepared from by each component of following parts by weight:It is 21 parts of Exocarpium Citrulli, 20 parts of Folium Mori, 25 parts of Semen Cucurbitae, light 25 parts of Folium Bambusae, 20 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 18 parts of Semen Hydnocarpi, 20 parts of Herba Hydrocotyleses, 21 parts of Folium Eriobotryae, 14 parts of Radix Tripterygii Wilfordii, 18 parts of Radix et Caulis Opuntiae Dillenii, 9 parts of sulfur, 11 parts of Pericarpium Granati, 12 parts of Radix Rosae Normaliss, 7 parts of Fructus Zanthoxyli, 5 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 6 parts of Folium Artemisiae Argyi, 1 part of Folium Crataegi, 24 parts of Folium Allii tuberosi stem.
4. the Pesticidal combination for killing fragrant-flowered garlic maggot according to claim 1, it is characterised in that:It is described for killing fragrant-flowered garlic maggot Pesticidal combination, be prepared from by each component of following parts by weight:It is 22 parts of Exocarpium Citrulli, 25 parts of Folium Mori, 21 parts of Semen Cucurbitae, light 21 parts of Folium Bambusae, 18 parts of Rhizoma Dryopteris Crassirhizomatiss, 18 parts of morning glory, 15 parts of Semen Hydnocarpi, 15 parts of Herba Hydrocotyleses, 16 parts of Folium Eriobotryae, 17 parts of Radix Tripterygii Wilfordii, 16 parts of Radix et Caulis Opuntiae Dillenii, 10 parts of sulfur, 14 parts of Pericarpium Granati, 14 parts of Radix Rosae Normaliss, 8 parts of Fructus Zanthoxyli, 4 parts of Fructus Quisqualis, 2 parts of Cortex Meliae, Folium Artemisiae Argyi 4 Part, 3 parts of Folium Crataegi, 24 parts of Folium Allii tuberosi stem.
5. the Pesticidal combination for killing fragrant-flowered garlic maggot according to claim 1, it is characterised in that:It is described for killing fragrant-flowered garlic maggot Pesticidal combination, be prepared from by each component of following parts by weight:It is 24 parts of Exocarpium Citrulli, 21 parts of Folium Mori, 20 parts of Semen Cucurbitae, light 24 parts of Folium Bambusae, 24 parts of Rhizoma Dryopteris Crassirhizomatiss, 18 parts of morning glory, 16 parts of Semen Hydnocarpi, 16 parts of Herba Hydrocotyleses, 18 parts of Folium Eriobotryae, 12 parts of Radix Tripterygii Wilfordii, 15 parts of Radix et Caulis Opuntiae Dillenii, 11 parts of sulfur, 11 parts of Pericarpium Granati, 11 parts of Radix Rosae Normaliss, 8 parts of Fructus Zanthoxyli, 5 parts of Fructus Quisqualis, 2 parts of Cortex Meliae, Folium Artemisiae Argyi 5 Part, 4 parts of Folium Crataegi, 23 parts of Folium Allii tuberosi stem.
6. the Pesticidal combination for killing fragrant-flowered garlic maggot according to claim 1, it is characterised in that:It is described for killing fragrant-flowered garlic maggot Pesticidal combination, be prepared from by each component of following parts by weight:It is 25 parts of Exocarpium Citrulli, 24 parts of Folium Mori, 18 parts of Semen Cucurbitae, light 25 parts of Folium Bambusae, 17 parts of Rhizoma Dryopteris Crassirhizomatiss, 20 parts of morning glory, 20 parts of Semen Hydnocarpi, 18 parts of Herba Hydrocotyleses, 20 parts of Folium Eriobotryae, 17 parts of Radix Tripterygii Wilfordii, 16 parts of Radix et Caulis Opuntiae Dillenii, 9 parts of sulfur, 12 parts of Pericarpium Granati, 9 parts of Radix Rosae Normaliss, 10 parts of Fructus Zanthoxyli, 3 parts of Fructus Quisqualis, 3 parts of Cortex Meliae, 5 parts of Folium Artemisiae Argyi, 1 part of Folium Crataegi, 20 parts of Folium Allii tuberosi stem.
7. the Pesticidal combination for killing fragrant-flowered garlic maggot according to claim 1, it is characterised in that:It is described for killing fragrant-flowered garlic maggot Pesticidal combination, be prepared from by each component of following parts by weight:It is 27 parts of Exocarpium Citrulli, 22 parts of Folium Mori, 21 parts of Semen Cucurbitae, light 22 parts of Folium Bambusae, 19 parts of Rhizoma Dryopteris Crassirhizomatiss, 21 parts of morning glory, 17 parts of Semen Hydnocarpi, 14 parts of Herba Hydrocotyleses, 19 parts of Folium Eriobotryae, 15 parts of Radix Tripterygii Wilfordii, 11 parts of Radix et Caulis Opuntiae Dillenii, 12 parts of sulfur, 11 parts of Pericarpium Granati, 14 parts of Radix Rosae Normaliss, 9 parts of Fructus Zanthoxyli, 5 parts of Fructus Quisqualis, 2 parts of Cortex Meliae, Folium Artemisiae Argyi 6 Part, 3 parts of Folium Crataegi, 21 parts of Folium Allii tuberosi stem.
8. the preparation method for killing the Pesticidal combination of fragrant-flowered garlic maggot any one of a kind of claim 1-7, its feature It is:Comprise the following steps:
(1) above-mentioned each component is weighed according to proportioning, and grind respectively, it is standby;
(2) Folium Mori, Semen Cucurbitae, Herba Lophatheri, Semen Hydnocarpi, Herba Hydrocotyleses, Folium Eriobotryae, Radix Tripterygii Wilfordii, Radix Rosae Normaliss, Fructus Quisqualis are mixed, to In mixture, addition weight is 20 times of total weight of the mixture of clear water, after soaking 12 hours, is cooked by slow fire 20- at 20-30 DEG C 30 minutes, after being cooled to room temperature, soak 50-60 minutes under 50-60 DEG C of water bath condition, be then cooked by slow fire 20-30 minutes, Filter to take gained decoction liquor;
(3) Rhizoma Dryopteris Crassirhizomatiss, Cortex Meliae and Folium Artemisiae Argyi are mixed, adds weight and horse Rhizoma Osmundae, Cortex Meliae, Folium Artemisiae Argyi gross weight identical Rice vinegar, after soaking 12 hours, dries;
(4) clear water for adding in thing that weight is 18 times that dry thing gross weight to drying obtained by step (3), soak at room temperature 12 are little Shi Hou, is cooked by slow fire 20-30 minutes, filters to take gained decoction liquor;
(5) Exocarpium Citrulli, morning glory, Radix et Caulis Opuntiae Dillenii, Pericarpium Granati, Fructus Zanthoxyli are mixed, sealing is put in ultra cold storage freezer, -80 DEG C of preservations 12 hours, take out;
(6) recover to room temperature after the blending ingredients obtained by step (5), to addition weight is recovered into the blending ingredients of room temperature be The clear water of 9 times of blending ingredients gross weight, is shaken after 8h with the rotating speed of 120r/min in putting agitator, 70-80 DEG C of water bath condition Lower immersion 30-40 minutes, cross 80 mesh sieves and take soak;
(7) by the decoction liquor obtained by the sulfur for grinding, Folium Crataegi, Folium Allii tuberosi stem and step (2), the decoction obtained by step (4) Soak obtained by liquid, step (6) is mixed, and is put in ultrasonic oscillator, ultrasonic Treatment 30 minutes;
(8) by the blending ingredients obtained by step (7) pressure be -0.06~-0.08Mpa, temperature be 40~45 DEG C under the conditions of it is dense It is reduced to 1.15~1.18 when relative density is 45 DEG C, it is bottled, obtain final product.
CN201610962248.5A 2016-10-28 2016-10-28 A kind of Pesticidal combination for killing fragrant-flowered garlic maggot and preparation method thereof Withdrawn CN106538640A (en)

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