CN106490072A - A kind of botanical pesticide of preventing and treating buprestid beetle and preparation method thereof - Google Patents
A kind of botanical pesticide of preventing and treating buprestid beetle and preparation method thereof Download PDFInfo
- Publication number
- CN106490072A CN106490072A CN201610927037.8A CN201610927037A CN106490072A CN 106490072 A CN106490072 A CN 106490072A CN 201610927037 A CN201610927037 A CN 201610927037A CN 106490072 A CN106490072 A CN 106490072A
- Authority
- CN
- China
- Prior art keywords
- extract
- parts
- herba
- preparation
- seu caulis
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/46—Stemonaceae [Stemona family], e.g. croomia
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：80 100 parts of 5 15 parts of Radix seu Caulis Derridis Trifoliatae extract, 4 12 parts of Herba Eupatorii Odorati extract, 39 parts of Radix Stemonae extract, 26 parts of Herba Convallariae extract, 8 14 parts of tea tree oil, 26 parts of attractant, 25 parts of surfactant, 35 parts of antifreezing agent, 13 parts of preservative and water.The botanical pesticide drug effect of the present invention is high, with low cost, be easily obtained, and effective ingredient is natural materials, is easier to be decomposed into after administration innocuous substance, environmentally safe, noresidue, nuisanceless；It is unlikely to deteriorate during storage, is a kind of safe and efficient compositionss for killing buprestid beetle, with promotion prospect.
Description
Technical field
The present invention relates to a kind of botanical pesticide and its method, more particularly, to a kind of botanical pesticide of preventing and treating buprestid beetle
And its preparation side.
Background technology
Buprestid beetle is commonly called as blistering worm, scale worm, category coleoptera, Buprestidae.Larva moth food branch cortex, is had stream by harm
Glue, bark explosion when causing harm serious, or even cause whole strain withered, very harmful to fruit tree.At present, for the pesticide system of buprestid beetle
Agent mostly is chemical pesticide, and the application of chemical pesticide has caused extremely serious harm to the mankind and other biologies, and plant
Source pesticide, refer to directly utilize or extract the root of plant, stem, leaf, flower, really, seed etc. or made using its secondary metabolites
There is the active substance of parasite killing or bactericidal action, therefore a kind of botanical pesticide for being specifically designed for buprestid beetle of necessary exploitation.
The Chinese patent of Application No. 2015105487371, discloses a kind of transplanted plantlet buprestid beetle pest control method,
Carry out as follows：（1）Bayer 71628 is pressed 1 with water：After the ratio of 600-800 is uniformly mixed, common soil is added to stir
Mix to pasty state；（2）The soil of the pasty state containing Bayer 71628 is wrapped in after transplanting with the thickness of 15-20mm, growing way recovers poor
On branch, parcel positioning is carried out using rubbish cloth then；（3）Every 1-2 days, the soil being wrapped on nursery stock is carried out squirting one
Secondary, every 8-10 days, carry out spraying water once to the soil being wrapped on nursery stock, the liquid medicine is by 1：The ratio of 600-800
Carry out mixed uniformly Bayer 71628 and water, the present invention can long-time effectively preventing buprestid beetle insect pest, effectively prevent Ji Ding
Pests recurrent exerbation.The Chinese patent of Application No. 2013106227175, discloses a kind of botanical pesticide, composition of raw materials
Including baicalin, Oleum Bulbus Allii, matrine, Fructus Cnidii, Carboxymethyl cellulose sodium, Fructus Carpesii, fulvic acid and modified starch；The plant
The component ratio of source pesticide is as follows：0. 1%-0. 25% of baicalin, 0. 6%-0. 8% of Oleum Bulbus Allii, matrine 7%-56%, Fructus Cnidii
0. 2%-0. 5%, Carboxymethyl cellulose sodium 14%-30%, 0. 1%-0. 25% of Fructus Carpesii, 15% yellow humic acid solution 10- of mass percent
30%, modified starch 2-5%, the invention proportioning are simple, easy to use, with botanical material as major ingredient, the botanical pesticide of preparation,
Pollution level is little.
Present in above-mentioned patent, problem is：
（1）The chemical pesticide for synthesis that preventing and treating buprestid beetle adopts in patent one, after granting on trees, although can prevent and treat lucky fourth
Worm, but the chemical composition for synthesizing easily accumulation on trees, not only pollute environment, and the health to the mankind have potential prestige
The side of body.
（2）Although employing botanical material in patent two as effective insecticidal constituent of pesticide, and it is not directed specifically to
Buprestid beetle is prevented and treated.
Content of the invention
In view of this, the purpose of the present invention is for the deficiencies in the prior art, there is provided a kind of plant source of preventing and treating buprestid beetle
Pesticide and preparation method thereof, solves the problems, such as currently without the botanical pesticide for specially preventing and treating buprestid beetle.
For reaching above-mentioned purpose, the present invention is employed the following technical solutions：
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：Radix seu Caulis Derridis Trifoliatae extract 5-15 parts, Herba Eupatorii Odorati are carried
Take thing 4-12 parts, Radix Stemonae extract 3-9 parts, Herba Convallariae extract 2-6 parts, tea tree oil 8-14 parts, attractant 2-6 parts, surface activity
Agent 2-5 parts, antifreezing agent 3-5 parts, preservative 1-3 parts and water 80-100 parts.
Preferably, the botanical pesticide of described preventing and treating buprestid beetle, including the raw material of following weight portion：Radix seu Caulis Derridis Trifoliatae extract 10
Part, 8 parts of Herba Eupatorii Odorati extract, 6 parts of Radix Stemonae extract, 4 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, surface activity
90 parts of 3 parts of agent, 4 parts of antifreezing agent, 2 parts of preservative and water.
Preferably, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 60-80 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby
With；Radix seu Caulis Derridis Trifoliatae powder is taken, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：3-7 adds volume fraction for the ethanol solution of 70-90%,
Ultrasound 4-8h at 30-40 DEG C, supersonic frequency 20-40KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, after vacuum drying i.e.
Obtain Radix seu Caulis Derridis Trifoliatae extract；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 60-80 mesh, obtains Stemona Root, standby；Take the Radix Stemonae
Powder, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：3-7 adds volume fraction for the ethanol solution of 70-90%, at 20-40 DEG C
Lower ultrasonic 4-8h, supersonic frequency 20-40KHz collect Radix Stemonae extracting solution, are concentrated into without alcohol taste, obtain final product the Radix Stemonae and carry after vacuum drying
Take thing.
Preferably, the preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 70-90 mesh, obtains Herba Eupatorii Odorati
Powder, standby；Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：5-9, is 70-90%'s with volume fraction
Ethanol solution reflux, extract, 4-6 time, merges Herba Eupatorii Odorati extracting solution and is concentrated into without alcohol taste, be then vacuum dried, obtain final product Herba Eupatorii Odorati
Extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 70-90 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae
Powder, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：5-9, with ethanol solution reflux, extract, 4-6 that volume fraction is 70-90%
Secondary, merge Herba Convallariae extracting solution and be concentrated into without alcohol taste, be then vacuum dried, obtain final product Herba Convallariae extract.
Preferably, the attractant is the one kind in Oleum sesami, Oleum Arachidis hypogaeae semen, sucrose and brown sugar；
The one kind of the surfactant for dodecylbenzene sodium sulfonate, wooden sodium sulfonate, cocinic acid and polysorbas20；
The antifreezing agent be glycerol, 2-Butoxyethyl acetate and 1, the one kind in 2 one dichloroethanes；
The preservative is the one kind in sodium benzoate, potassium sorbate, hydroquinone and salicylic acid.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 40-60min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 20- again
40min, obtains oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, obtain final product product after homogenization 30-60min again.
Preferably, the homogenization is carried out under 20-25PMa.
The invention has the beneficial effects as follows：
The botanical pesticide drug effect of the present invention is high, with low cost, easily prepared, and effective ingredient is natural materials, after administration
It is easier to be decomposed into innocuous substance, environmentally safe, noresidue, nuisanceless；Be unlikely to deteriorate during storage, be a kind of safety,
The efficient compositionss for killing buprestid beetle, with promotion prospect, specifically have following some：
（1）The botanical pesticide component diversification of the present invention, makes that insect is more difficult to develop immunity to drugs, and wherein Radix seu Caulis Derridis Trifoliatae belongs to pulse family liana
Plant, is one of three great tradition pesticide plants, and acrid in the mouth is warm in nature, very toxic, can be used for treatment and controls eczema, and Fengshi Guanjie swells and ache, and falls
Beat to swell and ache etc. and disease and wipe out the flies and mosquitoes, paroxysmal abdominal pain occurs after poisoning, nausea, vomiting, paroxysmal general spasticity, muscle are shaken
Quiver, breathing slows down, last respiratory center paralysis and dead.Modern study shows, in Radix seu Caulis Derridis Trifoliatae containing rotenone, Radix seu Caulis Derridis Trifoliatae ketone derivatives,
Terpenoid and aliphatic category compound, wherein rotenone can suppress mitochondrial respiratory chain, cause insect dyspnea and convulsions occur
Deng breathing decorum obstacle, be slow in action, paralysis and dead, insect is had strong tag and stomach poison function, can effectively prevent and treat aphid
The various pests such as worm, hawkmoth, three-spotted plusia are matched somebody with somebody by worm, red spider, aleyrodid, leafhopper, army, while plant growth can also be promoted.
Herba Eupatorii Odorati, is herbaceos perennial, and rhizome is sturdy, originates in Central America, finds in Yunnan Province of China south within 1934,
Now be distributed in the ground such as TaiWan, China, Guangdong, be global invasive species, reproductive capacity is extremely strong, be a kind of have emulative harmful
Species, are listed in for 2003 by the Chinese government《Chinese Invasive Alien Species list》.Taste micro-pungent, warm in nature, slightly poisonous, with dissipating blood stasis
The effect of detumescence, hemostasis, parasite killing, for treating treating swelling and pain by traumatic injury, traumatic hemorrhage, non-irrigated hirudinea bite haemophilia, sore swollen toxin etc.
Disease；Modern study shows in Herba Eupatorii Odorati containing flavonoid, half terpenoid and steroid, Herba Eupatorii Odorati extract to Pieris rapae,
The various pests such as diamondback moth larvae have strong repellent action, insecticidal and antifungal effect, while other are planted can also to suppress periphery
The growth of thing.
The Radix Stemonae, sweet in the mouth warm in nature, hardship, the Radix Stemonae contain multiple alkaloids, (-)-Stemoninine, Stemonidine, isostemonidine, the former Radix Stemonae
Alkali, stenine alkali, sinostemonine etc., can nourishing the lung to keep the adverse QI downward cough-relieving, desinsection and delousion coughs for new chronic cough, pulmonary tuberculosis cough, pertussis；Outward
There is killing action with to mosquitos and flies larva, head louse, clothing louse and Cimex bedbug etc.；Radix Astragali sweet in the mouth, slightly warm in nature enter lung, spleen channel, containing the Radix Astragali
Glycoside I, II, daucosterol, β-Palmic acid, sucrose etc.；Consolidating superficial resistance, inducing diuresis to remove edema, poison holding, granulation promoting effect are defended with benefit, can be used to control
Treatment spontaneous perspiration, night sweat, arthralgia due to stagnation of blood, edema, carbuncle are not burst or are burst and do not receive long, proctoptosis, deficiency of vital energy blood prostration.
Herba Convallariae, mountain valley Bulbus Lilii, Canterburybells is uniquely planted in Lily of the valley, and sweet in the mouth, hardship are warm in nature, poisonous, have heart tonifying, profit
The effect of urine, it is usually used in congestive heart failure, atrial fibrillation, the left heart failure caused by hypertension and nephritis, modern times grind
Study carefully and show, containing the bioactive ingredients such as convallatoxin, Convallatoxol, Herba Convallariae toxogen glycoside in Herba Convallariae, can cause anorexia, sialorrhea,
The symptoms of digestive tract such as Nausea and vomiting, while Herba Convallariae also has broad-spectrum sterilization performance, can suppress tulase, Diplococcus pneumoniae, Fructus Vitis viniferae
The growth and breeding of the various bacterias such as coccus.
Therefore the botanical pesticide of one's duty invention, add first buprestid beetle is had strong tag and stomach poison function fish
Rattan and the Herba Eupatorii Odorati with strong repellent action and bacteriostasis, then add containing multiple alkaloids the Radix Stemonae, desinsection and delousion,
On this basis, finally add the Herba Convallariae with broad-spectrum sterilization performance, four compoundings are added, and synergism effectively can be killed
Buprestid beetle.
（2）Herba Eupatorii Odorati as China's ecosystem in a kind of invasive species, endanger especially severe, be also universally acknowledged
Pernicious poisonous weeds.It can secrete and help to change material, squeeze eciophyte, make grassland lose value, affect tree growth and
Update；Meanwhile, its leaf has the toxic compounds such as toxin, can cause scytitiss and the anaphylactic disease of people, eat tender leaf by mistake
Dizziness, vomiting, poultry, domestic animal and Fish can be caused to eat by mistake, there is the ecosystem of China huge potential
Threat.The present invention using Herba Eupatorii Odorati as a kind of raw material, through processing its effective ingredient as one of component for killing buprestid beetle,
Resource reasonable employment is achieved, is turned waste into wealth, with the meaning that promotes the use of.
（3）It is dodecylbenzene sodium sulfonate, wooden sodium sulfonate, coconut palm to add surfactant in the botanical pesticide of the present invention
Seed oil acid and one kind of polysorbas20, above-mentioned several surfactants are nonionic surfactant, its in pesticide not with from
Sub- state is present, the botanical pesticide for therefore preparing, and the stability of active component is high, in Pesticide use overshoot is difficult to receive
The impact that strong electrolyte is present, is not easy to be affected by acid, alkali, and the compatibility is good, and dissolubility is good, excellent in stability.
（4）In the botanical pesticide preparation process of the present invention, one side Radix seu Caulis Derridis Trifoliatae extract and Radix Stemonae extract are using ultrasound
Extractive technique, the strong cavitation effect and mechanical vibration produced using ultrasound wave effectively accelerate Radix seu Caulis Derridis Trifoliatae powder and Stemona Root
In effective ingredient rapidly enter in etoh solvent solution, therefore preparation method of the invention not only effectively shortens Radix seu Caulis Derridis Trifoliatae and hundred
Ask during the extraction in portion, and significantly increase the dissolution rate of effective ingredient in Radix seu Caulis Derridis Trifoliatae and the Radix Stemonae, improve Radix seu Caulis Derridis Trifoliatae and the Radix Stemonae
Utilization rate, reduces production cost.
Specific embodiment
With reference to specific embodiment, the invention will be further described.
Embodiment 1
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：5 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
12 parts of thing, 3 parts of Radix Stemonae extract, 6 parts of Herba Convallariae extract, 8 parts of tea tree oil, 6 parts of attractant, 2 parts of surfactant, antifreezing agent 5
Part, 100 parts of 1 part of preservative and water, wherein attractant is Oleum sesami, and surfactant is dodecylbenzene sodium sulfonate, antifreezing agent
For glycerol, preservative is sodium benzoate.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 60 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：3 addition volume fractions are 90% ethanol solution, surpass at 40 DEG C
Sound 8h, supersonic frequency 20KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, obtain final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 60 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：3 add the ethanol solution that volume fractions are 90%, ultrasound 8h at 20 DEG C to surpass
Acoustic frequency 20KHz, collects Radix Stemonae extracting solution, is concentrated into without alcohol taste, obtains final product Radix Stemonae extract after vacuum drying.
The preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 70 mesh, obtains Herba Eupatorii Odorati powder, standby；
Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：5, carried with the ethanol solution backflow that volume fraction is 70%
Take 6 times, merge Herba Eupatorii Odorati extracting solution and be concentrated into without alcohol taste, be then vacuum dried, obtain final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 70 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae powder
End, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：9, with the ethanol solution reflux, extract, that volume fraction is 70% 4 times, merge bell
Blue extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Convallariae extract.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 60min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 20min again, obtains
Oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, again under 20PMa after homogenization 30min i.e.
Obtain product.
Embodiment 2
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：15 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
4 parts of thing, 9 parts of Radix Stemonae extract, 2 parts of Herba Convallariae extract, 14 parts of tea tree oil, 2 parts of attractant, 5 parts of surfactant, antifreezing agent 3
80 parts of part, 3 parts of preservative and water, wherein attractant are Oleum Arachidis hypogaeae semen, and surfactant is wooden sodium sulfonate, and antifreezing agent is ethylene glycol
Monobutyl ether acetate, preservative are potassium sorbate.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 80 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：7 addition volume fractions are 70% ethanol solution, surpass at 30 DEG C
Sound 4h, supersonic frequency 40KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, obtain final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 80 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：7 add the ethanol solution that volume fractions are 70%, ultrasound 4h at 40 DEG C to surpass
Acoustic frequency 40KHz, collects Radix Stemonae extracting solution, is concentrated into without alcohol taste, obtains final product Radix Stemonae extract after vacuum drying.
The preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 90 mesh, obtains Herba Eupatorii Odorati powder, standby；
Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：5, carried with the ethanol solution backflow that volume fraction is 90%
Take 6 times, merge Herba Eupatorii Odorati extracting solution and be concentrated into without alcohol taste, be then vacuum dried, obtain final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 90 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae powder
End, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：5, with the ethanol solution reflux, extract, that volume fraction is 90% 6 times, merge bell
Blue extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Convallariae extract.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 40min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 40min again, obtains
Oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, again under 25PMa after homogenization 60min i.e.
Obtain product.
Embodiment 3
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：10 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
8 parts of thing, 6 parts of Radix Stemonae extract, 4 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant, antifreezing agent 4
90 parts of part, 2 parts of preservative and water, wherein attractant are sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one dichloros
Ethane, preservative are hydroquinone.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 70 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：5 addition volume fractions are 80% ethanol solution, surpass at 35 DEG C
Sound 6h, supersonic frequency 30KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, obtain final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 70 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：5 add the ethanol solution that volume fractions are 80%, ultrasound 6h at 30 DEG C to surpass
Acoustic frequency 30KHz, collects Radix Stemonae extracting solution, is concentrated into without alcohol taste, obtains final product Radix Stemonae extract after vacuum drying.
Wherein, the preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 80 mesh, obtains Herba Eupatorii Odorati powder,
Standby；Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：7, returned with the ethanol solution that volume fraction is 80%
Stream is extracted 5 times, is merged Herba Eupatorii Odorati extracting solution and is concentrated into without alcohol taste, is then vacuum dried, obtains final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 80 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae powder
End, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：7, with the ethanol solution reflux, extract, that volume fraction is 80% 5 times, merge bell
Blue extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Convallariae extract.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 50min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 30min again, obtains
Oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, again under 23PMa after homogenization 50min i.e.
Obtain product.
Embodiment 4
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：10 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
8 parts of thing, 6 parts of Radix Stemonae extract, 4 parts of Herba Convallariae extract, 3 parts of Azuritum, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant,
90 parts of 4 parts of antifreezing agent, 2 parts of preservative and water, wherein attractant are sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2
One dichloroethanes, preservative are hydroquinone, and Azuritum is the powder of 500 mesh of particle diameter.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 70 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：5 addition volume fractions are 80% ethanol solution, surpass at 35 DEG C
Sound 6h, supersonic frequency 30KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, obtain final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 70 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：5 add the ethanol solution that volume fractions are 80%, ultrasound 6h at 30 DEG C to surpass
Acoustic frequency 30KHz, collects Radix Stemonae extracting solution, is concentrated into without alcohol taste, obtains final product Radix Stemonae extract after vacuum drying.
Wherein, the preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 80 mesh, obtains Herba Eupatorii Odorati powder,
Standby；Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：7, returned with the ethanol solution that volume fraction is 80%
Stream is extracted 5 times, is merged Herba Eupatorii Odorati extracting solution and is concentrated into without alcohol taste, is then vacuum dried, obtains final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 80 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae powder
End, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：7, with the ethanol solution reflux, extract, that volume fraction is 80% 5 times, merge bell
Blue extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Convallariae extract.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 50min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 30min again, obtains
Oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, again under 23PMa after homogenization 50min i.e.
Obtain product.
Embodiment 5
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：7 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
7 parts of thing, 4 parts of Radix Stemonae extract, 5 parts of Herba Convallariae extract, 12 parts of tea tree oil, 3 parts of attractant, 4 parts of surfactant, antifreezing agent 3
100 parts of part, 1 part of preservative and water, wherein attractant are brown sugar, and surfactant is polysorbas20, and antifreezing agent is butyl glycol ether
Acetate, preservative are salicylic acid.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 60 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：4 addition volume fractions are 80% ethanol solution, surpass at 30 DEG C
Sound 7h, supersonic frequency 20KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, obtain final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 80 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：6 add the ethanol solution that volume fractions are 80%, ultrasound 5h at 20 DEG C to surpass
Acoustic frequency 40KHz, collects Radix Stemonae extracting solution, is concentrated into without alcohol taste, obtains final product Radix Stemonae extract after vacuum drying.
Wherein, the preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 70 mesh, obtains Herba Eupatorii Odorati powder,
Standby；Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：6, returned with the ethanol solution that volume fraction is 70%
Stream is extracted 6 times, is merged Herba Eupatorii Odorati extracting solution and is concentrated into without alcohol taste, is then vacuum dried, obtains final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 90 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae powder
End, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：8, with the ethanol solution reflux, extract, that volume fraction is 70% 6 times, merge bell
Blue extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Convallariae extract.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 40min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 40min again, obtains
Oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, again under 24PMa after homogenization 40min i.e.
Obtain product.
Embodiment 6
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：9 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
6 parts of thing, 8 parts of Radix Stemonae extract, 3 parts of Herba Convallariae extract, 10 parts of tea tree oil, 5 parts of attractant, 2 parts of surfactant, antifreezing agent 5
Part, 85 parts of 3 parts of preservative and water, wherein attractant is Oleum Arachidis hypogaeae semen, and surfactant is wooden sodium sulfonate, and antifreezing agent is the third three
Alcohol, preservative are potassium sorbate.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 70 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：6 addition volume fractions are 90% ethanol solution, surpass at 40 DEG C
Sound 5h, supersonic frequency 30KHz collect Radix seu Caulis Derridis Trifoliatae extracting solution, are concentrated into without alcohol taste, obtain final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 60 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：5 add the ethanol solution that volume fractions are 70%, ultrasound 5h at 30 DEG C to surpass
Acoustic frequency 30KHz, collects Radix Stemonae extracting solution, is concentrated into without alcohol taste, obtains final product Radix Stemonae extract after vacuum drying.
Wherein, the preparation method of the Herba Eupatorii Odorati extract is to take Herba Eupatorii Odorati herb to be crushed to 80 mesh, obtains Herba Eupatorii Odorati powder,
Standby；Herba Eupatorii Odorati powder is taken, is counted by solid-to-liquid ratio as 1 with Herba Eupatorii Odorati powder quality：8, returned with the ethanol solution that volume fraction is 70%
Stream is extracted 4 times, is merged Herba Eupatorii Odorati extracting solution and is concentrated into without alcohol taste, is then vacuum dried, obtains final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 70 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae powder
End, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：6, with the ethanol solution reflux, extract, that volume fraction is 90% 5 times, merge bell
Blue extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Convallariae extract.
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle, comprises the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 50min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 20min again, obtains
Oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, again under 22PMa after homogenization 50min i.e.
Obtain product.
Embodiment 7
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：11 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
10 parts of thing, 7 parts of Radix Stemonae extract, 3 parts of Herba Convallariae extract, 9 parts of tea tree oil, 2 parts of attractant, 5 parts of surfactant, antifreezing agent 4
95 parts of part, 2 parts of preservative and water, wherein attractant are sucrose, and surfactant is dodecylbenzene sodium sulfonate, and antifreezing agent is second
Glycol monobutyl ether acetate, preservative are salicylic acid.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is identical with the preparation method of Radix seu Caulis Derridis Trifoliatae extract in embodiment 5；
The preparation method of the Radix Stemonae extract is identical with the preparation method of Radix Stemonae extract in embodiment 3.
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 2；
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 5.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 6
With.
Embodiment 8
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：13 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati are extracted
9 parts of thing, 5 parts of Radix Stemonae extract, 2 parts of Herba Convallariae extract, 13 parts of tea tree oil, 3 parts of attractant, 3 parts of surfactant, antifreezing agent 3
90 parts of part, 1 part of preservative and water, wherein attractant are brown sugar, and surfactant is dodecylbenzene sodium sulfonate, and antifreezing agent is third
Triol, preservative are sodium benzoate.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is identical with the preparation method of Radix seu Caulis Derridis Trifoliatae extract in embodiment 2；
The preparation method of the Radix Stemonae extract is identical with the preparation method of Radix Stemonae extract in embodiment 1.
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 4；
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 6.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 5
With.
Comparative example 1
Comparative example 1 is substantially the same manner as Example 3, and difference is to carry without Radix seu Caulis Derridis Trifoliatae in the formula of botanical pesticide in comparative example 1
Take thing.
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：13 parts of Herba Eupatorii Odorati extract, the Radix Stemonae
10 parts of extract, 8 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant, 4 parts of antifreezing agent, preservative 2
Part and 90 parts of water, wherein attractant is sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one dichloroethanes, preservative
For hydroquinone.
The preparation method of the Radix Stemonae extract is identical with the preparation method of Radix Stemonae extract in embodiment 3.
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 3；
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 3.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 3
With.
Comparative example 2
Comparative example 1 is substantially the same manner as Example 3, and difference is in comparative example 1 in the formula of botanical pesticide without Herba Eupatorii Odorati
Extract.
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：13 parts of Radix seu Caulis Derridis Trifoliatae extract, the Radix Stemonae are carried
Take 9 parts of thing, 6 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant, 4 parts of antifreezing agent, 2 parts of preservative
With 90 parts of water, wherein attractant is sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one dichloroethanes, and preservative is
Hydroquinone.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is identical with the preparation method of Radix seu Caulis Derridis Trifoliatae extract in embodiment 3；
The preparation method of the Radix Stemonae extract is identical with the preparation method of Radix Stemonae extract in embodiment 3.
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 3.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 3
With.
Comparative example 3
Comparative example 1 is substantially the same manner as Example 3, and difference is to carry without the Radix Stemonae in the formula of botanical pesticide in comparative example 1
Take thing.
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：12 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati
10 parts of extract, 6 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant, 4 parts of antifreezing agent, preservative 2
Part and 90 parts of water, wherein attractant is sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one dichloroethanes, preservative
For hydroquinone.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is identical with the preparation method of Radix seu Caulis Derridis Trifoliatae extract in embodiment 3；
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 3；
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 3.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 3
With.
Comparative example 4
Comparative example 1 is substantially the same manner as Example 3, and difference is to carry without Herba Convallariae in the formula of botanical pesticide in comparative example 1
Take thing.
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：12 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati
9 parts of extract, 7 parts of Radix Stemonae extract, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant, 4 parts of antifreezing agent, preservative 2
Part and 90 parts of water, wherein attractant is sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one dichloroethanes, preservative
For hydroquinone.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is identical with the preparation method of Radix seu Caulis Derridis Trifoliatae extract in embodiment 3；
The preparation method of the Radix Stemonae extract is identical with the preparation method of Radix Stemonae extract in embodiment 3.
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 3；
The preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle is identical with the preparation method of botanical pesticide in embodiment 3.
Comparative example 5
Comparative example 1 is substantially the same manner as Example 3, and difference is in comparative example 1 in the formula of botanical pesticide to live without surface
Property agent.
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：10 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati
8 parts of extract, 6 parts of Radix Stemonae extract, 4 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, 4 parts of antifreezing agent, preservative 2
Part and 90 parts of water, wherein attractant is sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one dichloroethanes, preservative
For hydroquinone.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is identical with the preparation method of Radix seu Caulis Derridis Trifoliatae extract in embodiment 3；
The preparation method of the Radix Stemonae extract is identical with the preparation method of Radix Stemonae extract in embodiment 3.
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 3；
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 3.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 3
With.
Comparative example 6
Comparative example 6 is substantially the same manner as Example 3, and difference is in comparative example 6 prepared by Radix seu Caulis Derridis Trifoliatae extract and Radix Stemonae extract
Shi Caiyong decocting cooking methods.
A kind of botanical pesticide of preventing and treating buprestid beetle, including the raw material of following weight portion：10 parts of Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati
8 parts of extract, 6 parts of Radix Stemonae extract, 4 parts of Herba Convallariae extract, 11 parts of tea tree oil, 4 parts of attractant, 3 parts of surfactant, antifreeze
90 parts of 4 parts of agent, 2 parts of preservative and water, wherein attractant are sucrose, and surfactant is cocinic acid, and antifreezing agent is 1,2 one two
Ethyl chloride, preservative are hydroquinone.
Wherein, the preparation method of the Radix seu Caulis Derridis Trifoliatae extract is to take derris root to be crushed to 70 mesh, obtains Radix seu Caulis Derridis Trifoliatae powder, standby；Take
Radix seu Caulis Derridis Trifoliatae powder, is counted by solid-to-liquid ratio as 1 with Radix seu Caulis Derridis Trifoliatae powder quality：10 are extracted 3 times using decocting cooking method, collect Radix seu Caulis Derridis Trifoliatae extracting solution, dense
Radix seu Caulis Derridis Trifoliatae extract is obtained final product after being vacuum dried after contracting；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 70 mesh, obtains Stemona Root, standby；Take Radix Stemonae powder
End, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：10 are carried using decocting cooking method
Take 3 times, collect Radix Stemonae extracting solution, after being vacuum dried after concentration, obtain final product Radix Stemonae extract.
The preparation method of the Herba Eupatorii Odorati extract is identical with the preparation method of Herba Eupatorii Odorati extract in embodiment 3；
The preparation method of the Herba Convallariae extract is identical with the preparation method of Herba Convallariae extract in embodiment 3.
The preparation method phase of the preparation method of the botanical pesticide of above-mentioned preventing and treating buprestid beetle and botanical pesticide in embodiment 3
With.
Physicochemical property is tested
Physicochemical property observation and detection are carried out to the botanical pesticide that embodiment 1-8 and comparative example 1-6 are prepared, including outer
Sight, stability of emulsion, low-temperature stability, heat stability and transparency temperature scope, Physico-chemical tests the results are shown in Table 1, wherein according to finger
Mark is required：
Outward appearance：Qualified product is transparent or the homogeneous liquid of similar transparent in storage period outward appearance；
Stability of emulsion：With 342mg/L standard hard waters by microemulsion diluted sample after, at 20 DEG C stand 30min, observe outward appearance
Situation, is such as suspended without oily or precipitation of solid material, keeps pellucidity, and can be mixed with water in any proportion, be considered as emulsion steady
Fixed；
Low-temperature stability：Microemulsion does not produce irreversible caking in low temperature or muddiness is considered as qualified, therefore carries out ice freeze-thaw
Change test.Take botanical pesticide about 30mL to be mounted in the ground glass stoppered bottle of clear, colorless, measure after sealing in -10-0 DEG C of refrigerator
Cold preservation, takes out after 24h, places at room temperature, observes visual condition, if caking or research of chaotic phenomenon die down, can recover transparent
State is then qualified；
Heat stability：Sample is loaded after sealing in ampere bottle, be placed in 54 ± 2 DEG C of calorstat and store 14 days, it is desirable to outward appearance
Keep homogeneous phase transparent, if there is layering, after shaking at room temperature resilient analyze for qualified, then after heat storage effective into
Divide content, and calculate effective ingredient resolution ratio, resolution ratio≤10% is considered as qualified.The resolution ratio (X) of effective ingredient is counted as the following formula
Calculate：X=[（Active constituent content after active constituent content-heat storage before heat storage）Active constituent content before the storage of/heat] × 100%.
Insect killing effect test
The botanical pesticide of preventing and treating buprestid beetle prepared by embodiment 1-8 and comparative example 1-7 is respectively with water according to 1:1000 matter
Amount proportioning mixing, obtains medicinal liquid, and insect killing effect test the results are shown in Table 2.
Test method is according to People's Republic of China's agricultural industry criteria《Farm-chemical indoor determination test rule》Parasite killing
In agent NYT 1154.6-2006, the dip method of the 6th part is carried out.Two kinds, ten speckle buprestid beetle for buprestid beetle and six stars are lucky
The medicinal liquid that Tintinnid, each embodiment or comparative example are prepared processes each kind 60, and processing method is that target pest is immersed medicine
In liquid after 20s, unnecessary medicinal liquid is drawn with filter paper, test worm is transferred under normal condition and is raised, and arranged without botanical pesticide
The aqueous solution of medicinal liquid as a control group, processes 48h statistic record test worm The dead quantities and calculates mortality rate and corrected mortality.
Mortality rate（%）=dead test worm number/total test worm number × 100%
Corrected mortality（%）=（Mortality rate-control mortality rate）/（1- compares mortality rate）×100%
Physicochemical property test result table 1 and insect killing effect test result table 2 from above-described embodiment 1-8：The system of the present invention
The botanical pesticide of the standby preventing and treating buprestid beetle for obtaining is transparent, homogeneous liquid, and stability of emulsion and low-temperature stability meet mark
In standard, and heat stabilization test, effective ingredient resolution ratio is 2%-6%, and its equal physics and chemistry not only conforms with relevant national standard, pin
Dip method test is carried out to two kinds, the ten speckle buprestid beetle and six star buprestid beetles of buprestid beetle, as a result shows that ten speckle buprestid beetles are dead
Rate and corrected mortality are respectively 85.00%-95.00%, 84.75%-94.92%, six star buprestid beetle mortality rates and corrected mortality
Respectively 86.67%-96.67%, 86.21%-96.55%, illustrate that the botanical pesticide of the present invention is excellent for buprestid beetle prevention effect
Different, orientation killing action is produced to buprestid beetle, while effective insecticidal constituent of botanical pesticide comes from plant original in nature
Material, it is to avoid insecticide causes to endanger to natural environment and ecological balance using substantial amounts of organic agricultural chemicals in currently available technology
Evil, is easier to be decomposed into after administration innocuous substance, environmentally safe, noresidue, nuisanceless；It is unlikely to deteriorate during storage, is
A kind of safe and efficient compositionss for killing buprestid beetle, with promotion prospect.
In conjunction with Tables 1 and 2, from embodiment 4 and embodiment 3：With the addition of in the formula of 4 botanical pesticide of embodiment suitable
The Azuritum of amount, Azuritum are called Piao Qing, are natural copper sulfate, are the Ore of carbonate mineral chessy copper, monoclinic system, generally
In pelletized form, the block such as the kidney shape, dispersion shape, earthy or the surface of other copper mines is coated in, in navy blue, with improving eyesight, relieving convulsion, kill
Effect of worm, can be used for treat wind heat conjunctival congestion, pain, puckery itch, a lot of secretion in the eye is red rotten, wind syndrome of head, infantile convulsion, the disease such as migratory arthralgia.Imitated by parasite killing
Fruit understands that, after adding appropriate Azuritum, the insecticidal effect of the botanical pesticide of preparation increases, and this is due to adding Azuritum
Afterwards, Azuritum can strengthen insecticidal effect with the effective ingredient collaboration in medicine.
In conjunction with Tables 1 and 2, from embodiment 3 and comparative example 1, comparative example 2, comparative example 3 and comparative example 4, comparative example 1-
Eliminate Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, hundred step extracts or Herba Convallariae extract in 4 formula respectively, prepare
Botanical pesticide substantially reduces for the insecticidal effect of buprestid beetle, the preventing and treating botanical pesticide of this explanation present invention, is carried with Radix seu Caulis Derridis Trifoliatae
Thing, Herba Eupatorii Odorati extract, Radix Stemonae extract and Herba Convallariae extract are taken as effective ingredient, to have strong tagging to buprestid beetle
Based on the Radix seu Caulis Derridis Trifoliatae extract of stomach poison function and the Herba Eupatorii Odorati extract with strong repellent action and bacteriostasis, first
First to buprestid beetle formed tag and stomach toxicity effect so that buprestid beetle is slow in action, eating difficulties, then add contain multiple biologies
The Radix Stemonae extract of alkali, forms to buprestid beetle and further injures, finally Herba Convallariae extract of the interpolation with broad-spectrum sterilization performance, and four
Person's compounding is added, and synergism kills the excellent effect of buprestid beetle.
In conjunction with Tables 1 and 2, from embodiment 3 and comparative example 5, surfactant in the formula of comparative example 5, comparative example 5
The stability of emulsion and low-temperature stability of the product for preparing substantially reduces, and effective ingredient resolution ratio is raised, and pin
The mortality rate and corrected mortality of ten speckle buprestid beetles and six star buprestid beetles are substantially reduced, surface activity in this explanation present invention
The presence of agent so that the botanical pesticide of preparation, the stability of active component are high, are difficult by forceful electric power solution in Pesticide use overshoot
The impact that matter is present, is not easy to be affected by acid, alkali, and the compatibility is good, and dissolubility is good, excellent in stability, is therefore directed to buprestid beetle
Good disinsection effect.
In conjunction with Tables 1 and 2, from embodiment 3 and comparative example 6, Radix seu Caulis Derridis Trifoliatae extract and Radix Stemonae extract system in comparative example 6
After being carried out using decocting cooking method when standby, the product for preparing reduces for the insecticidal effect of buprestid beetle, in this explanation embodiment 3
Radix seu Caulis Derridis Trifoliatae extract and Radix Stemonae extract adopt ultrasound assisted extraction technique, effectively accelerate in Radix seu Caulis Derridis Trifoliatae powder and Stemona Root effective into
Point rapidly enter in etoh solvent solution, ask during the extraction for not only effectively shortening Radix seu Caulis Derridis Trifoliatae and the Radix Stemonae, and significantly increase fish
The dissolution rate of effective ingredient in rattan and the Radix Stemonae, improves the utilization rate of Radix seu Caulis Derridis Trifoliatae and the Radix Stemonae, reduces production cost, for lucky fourth
The insecticide efficiency of worm is significantly improved.
Finally illustrate, only in order to technical scheme to be described and unrestricted, this area is common for above example
Other modifications or equivalent that technical staff is made to technical scheme, without departing from technical solution of the present invention
Spirit and scope, all should cover in the middle of scope of the presently claimed invention.
Claims (7)
1. a kind of preventing and treating buprestid beetle botanical pesticide, it is characterised in that including the raw material of following weight portion：Radix seu Caulis Derridis Trifoliatae extract 5-
15 parts, Herba Eupatorii Odorati extract 4-12 parts, Radix Stemonae extract 3-9 parts, Herba Convallariae extract 2-6 parts, tea tree oil 8-14 parts, attractant 2-
6 parts, surfactant 2-5 parts, antifreezing agent 3-5 parts, preservative 1-3 parts and water 80-100 parts.
2. according to claim 1 preventing and treating buprestid beetle botanical pesticide, it is characterised in that including the original of following weight portion
Material：10 parts of Radix seu Caulis Derridis Trifoliatae extract, 8 parts of Herba Eupatorii Odorati extract, 6 parts of Radix Stemonae extract, 4 parts of Herba Convallariae extract, 11 parts of tea tree oil, lure
90 parts of 4 parts of agent, 3 parts of surfactant, 4 parts of antifreezing agent, 2 parts of preservative and water.
3. according to claim 1 and 2 preventing and treating buprestid beetle botanical pesticide, it is characterised in that：The Radix seu Caulis Derridis Trifoliatae extract
Preparation method be to take derris root to be crushed to 60-80 mesh, obtain Radix seu Caulis Derridis Trifoliatae powder, standby；Radix seu Caulis Derridis Trifoliatae powder is taken, in terms of Radix seu Caulis Derridis Trifoliatae powder quality
It is 1 by solid-to-liquid ratio：3-7 adds volume fraction for the ethanol solution of 70-90%, ultrasound 4-8h, supersonic frequency 20- at 30-40 DEG C
40KHz, collects Radix seu Caulis Derridis Trifoliatae extracting solution, is concentrated into without alcohol taste, obtains final product Radix seu Caulis Derridis Trifoliatae extract after vacuum drying；
The preparation method of the Radix Stemonae extract is to take Radix Stemonae herb to be crushed to 60-80 mesh, obtains Stemona Root, standby；Take the Radix Stemonae
Powder, is counted by solid-to-liquid ratio as 1 with Stemona Root quality：3-7 adds volume fraction for the ethanol solution of 70-90%, at 20-40 DEG C
Lower ultrasonic 4-8h, supersonic frequency 20-40KHz collect Radix Stemonae extracting solution, are concentrated into without alcohol taste, obtain final product the Radix Stemonae and carry after vacuum drying
Take thing.
4. according to claim 1 and 2 preventing and treating buprestid beetle botanical pesticide, it is characterised in that：The Herba Eupatorii Odorati is extracted
The preparation method of thing is to take Herba Eupatorii Odorati herb to be crushed to 70-90 mesh, obtains Herba Eupatorii Odorati powder, standby；Herba Eupatorii Odorati powder is taken, with aircraft
Careless powder quality meter is 1 by solid-to-liquid ratio：5-9, with the ethanol solution reflux, extract, that volume fraction is 70-90% 4-6 time, merges and flies
Machine grass extracting solution is simultaneously concentrated into without alcohol taste, is then vacuum dried, is obtained final product Herba Eupatorii Odorati extract；
The preparation method of the Herba Convallariae extract is to take Herba Convallariae herb to be crushed to 70-90 mesh, obtains Herba Convallariae powder, standby；Take Herba Convallariae
Powder, is counted by solid-to-liquid ratio as 1 with Herba Convallariae powder quality：5-9, with ethanol solution reflux, extract, 4-6 that volume fraction is 70-90%
Secondary, merge Herba Convallariae extracting solution and be concentrated into without alcohol taste, be then vacuum dried, obtain final product Herba Convallariae extract.
5. according to claim 1 and 2 preventing and treating buprestid beetle botanical pesticide, it is characterised in that：The attractant is sesame
One kind in Oleum Sesami, Oleum Arachidis hypogaeae semen, sucrose and brown sugar；
The one kind of the surfactant for dodecylbenzene sodium sulfonate, wooden sodium sulfonate, cocinic acid and polysorbas20；
The antifreezing agent be glycerol, 2-Butoxyethyl acetate and 1, the one kind in 2 one dichloroethanes；
The preservative is the one kind in sodium benzoate, potassium sorbate, hydroquinone and salicylic acid.
6. a kind of preparation method of the botanical pesticide of the preventing and treating buprestid beetle as described in any one of claim 1-5, its feature exists
In comprising the following steps：
（1）Prepare oil phase：After Radix seu Caulis Derridis Trifoliatae extract, Herba Eupatorii Odorati extract, Radix Stemonae extract, Herba Convallariae extract and tea tree oil are mixed
Homogenization 40-60min, is subsequently adding attractant, surfactant, antifreezing agent and preservative homogenization 20- again
40min, obtains oil-phase solution；
（2）Water oil mixing：To step（1）In oil-phase solution in add water, obtain final product product after homogenization 30-60min again.
7. according to claim 6 preventing and treating buprestid beetle botanical pesticide preparation method, it is characterised in that the homogenizing
Process is carried out under 20-25PMa.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610927037.8A CN106490072A (en) | 2016-10-31 | 2016-10-31 | A kind of botanical pesticide of preventing and treating buprestid beetle and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610927037.8A CN106490072A (en) | 2016-10-31 | 2016-10-31 | A kind of botanical pesticide of preventing and treating buprestid beetle and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106490072A true CN106490072A (en) | 2017-03-15 |
Family
ID=58318674
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610927037.8A Pending CN106490072A (en) | 2016-10-31 | 2016-10-31 | A kind of botanical pesticide of preventing and treating buprestid beetle and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106490072A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111357779A (en) * | 2018-12-26 | 2020-07-03 | 西北农林科技大学 | Lure for preventing and controlling Chinese prickly ash and Giardia and preparation method thereof |
| CN114467966A (en) * | 2022-03-03 | 2022-05-13 | 安徽蓝田农业开发有限公司 | Composite herbicide containing bensulfuron-methyl, pyrazosulfuron-ethyl and cafenstrole and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101218910A (en) * | 2007-01-11 | 2008-07-16 | 深圳职业技术学院 | Eupatorium herb microemulsion and method for producing the same |
| CN105532763A (en) * | 2015-12-16 | 2016-05-04 | 郑晓锋 | Traditional Chinese medicine pesticide |
-
2016
- 2016-10-31 CN CN201610927037.8A patent/CN106490072A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101218910A (en) * | 2007-01-11 | 2008-07-16 | 深圳职业技术学院 | Eupatorium herb microemulsion and method for producing the same |
| CN105532763A (en) * | 2015-12-16 | 2016-05-04 | 郑晓锋 | Traditional Chinese medicine pesticide |
Non-Patent Citations (2)
| Title |
|---|
| 吴学民: "《农药制剂加工实验 第二版》", 31 August 2014, 化学工业出版社 * |
| 肖放: "《医巫闾山地区野生植物原色图鉴》", 30 September 2015, 中国林业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111357779A (en) * | 2018-12-26 | 2020-07-03 | 西北农林科技大学 | Lure for preventing and controlling Chinese prickly ash and Giardia and preparation method thereof |
| CN114467966A (en) * | 2022-03-03 | 2022-05-13 | 安徽蓝田农业开发有限公司 | Composite herbicide containing bensulfuron-methyl, pyrazosulfuron-ethyl and cafenstrole and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103689017B (en) | A kind of composite plant source pesticide and preparation method thereof | |
| CN103931686B (en) | A kind of botanical pesticide and its preparation method and application | |
| CN105532755A (en) | Novel plant source insecticide for fruit trees, preparation method and application thereof | |
| CN103535389B (en) | Plant source fruit tree insecticide | |
| CN105379771A (en) | Plant-derived pesticide and its preparation method and use | |
| CN102754667B (en) | High-efficiency composite botanical pesticide | |
| CN105594765A (en) | Environment-friendly pesticide | |
| CN103609618A (en) | Tea pollution-free pesticide | |
| CN103548895A (en) | Botanical vegetable insecticide | |
| CN102217659B (en) | Botanical pesticide and its preparation method and use | |
| CN101427692B (en) | Plant pesticide and preparation method thereof | |
| CN101258861A (en) | Use of southernwood extract as plant growth regulator and adverse-resistant agent | |
| CN106259516A (en) | A kind of acaricide and preparation method thereof | |
| CN104098405B (en) | Micro-fertilizer of Chelating state having desinsection concurrently and preparation method thereof | |
| CN103598266B (en) | Non-polluted pesticide with pure traditional Chinese medicinal components, as well as preparation method and application thereof | |
| CN106614806A (en) | Biological pesticide for vegetables and preparation method thereof | |
| CN106490072A (en) | A kind of botanical pesticide of preventing and treating buprestid beetle and preparation method thereof | |
| CN102626114A (en) | Disease-curing insecticidal plant nutrient solution with pure traditional Chinese medicinal formula, and making method thereof | |
| CN1218645C (en) | Chinese herbal medicine pesticide and sterilizer and its preparing method | |
| CN103340216A (en) | Pollution-free pesticide microcapsule suspending preparation and preparation method thereof | |
| CN102485002A (en) | Application of burdock extract in harmful citrus mite controlling | |
| CN106490077A (en) | A kind of botanical pesticide for urban greening project and preparation method thereof | |
| CN105994431A (en) | Efficient and lasting termite control preparation and preparation method thereof | |
| CN106259515A (en) | A kind of mango insecticide and preparation method thereof | |
| CN106490073A (en) | A kind of botanical pesticide of preventing and treating bollworm and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170315 |
|
| RJ01 | Rejection of invention patent application after publication |