CN105268993A - 一种制备片状纳米银粉的方法 - Google Patents
一种制备片状纳米银粉的方法 Download PDFInfo
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- CN105268993A CN105268993A CN201510815965.0A CN201510815965A CN105268993A CN 105268993 A CN105268993 A CN 105268993A CN 201510815965 A CN201510815965 A CN 201510815965A CN 105268993 A CN105268993 A CN 105268993A
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- Prior art keywords
- silver
- salt
- ferrous
- silver powder
- surfactant
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 title claims abstract description 31
- 238000000034 method Methods 0.000 title claims abstract description 24
- 239000000843 powder Substances 0.000 title abstract description 4
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 claims abstract description 13
- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical group [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 claims abstract description 12
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 10
- 239000004094 surface-active agent Substances 0.000 claims abstract description 9
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims abstract description 6
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims abstract description 6
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims abstract description 6
- 229910001961 silver nitrate Inorganic materials 0.000 claims abstract description 6
- IMBKASBLAKCLEM-UHFFFAOYSA-L ferrous ammonium sulfate (anhydrous) Chemical group [NH4+].[NH4+].[Fe+2].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O IMBKASBLAKCLEM-UHFFFAOYSA-L 0.000 claims abstract description 4
- 239000007864 aqueous solution Substances 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims description 11
- 238000002360 preparation method Methods 0.000 abstract description 13
- 238000006243 chemical reaction Methods 0.000 abstract description 11
- 229910000359 iron(II) sulfate Inorganic materials 0.000 abstract description 5
- 230000035484 reaction time Effects 0.000 abstract description 4
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 abstract description 3
- 239000002202 Polyethylene glycol Substances 0.000 abstract description 3
- 229920001223 polyethylene glycol Polymers 0.000 abstract description 3
- 239000012266 salt solution Substances 0.000 abstract description 3
- 239000011790 ferrous sulphate Substances 0.000 abstract description 2
- 235000003891 ferrous sulphate Nutrition 0.000 abstract description 2
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- CQLFBEKRDQMJLZ-UHFFFAOYSA-M silver acetate Chemical compound [Ag+].CC([O-])=O CQLFBEKRDQMJLZ-UHFFFAOYSA-M 0.000 abstract description 2
- 229940071536 silver acetate Drugs 0.000 abstract description 2
- YPNVIBVEFVRZPJ-UHFFFAOYSA-L silver sulfate Chemical compound [Ag+].[Ag+].[O-]S([O-])(=O)=O YPNVIBVEFVRZPJ-UHFFFAOYSA-L 0.000 abstract description 2
- 229910000367 silver sulfate Inorganic materials 0.000 abstract description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 abstract 1
- 229940010514 ammonium ferrous sulfate Drugs 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 6
- 229920003081 Povidone K 30 Polymers 0.000 description 6
- 238000006722 reduction reaction Methods 0.000 description 6
- SURQXAFEQWPFPV-UHFFFAOYSA-L iron(2+) sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Fe+2].[O-]S([O-])(=O)=O SURQXAFEQWPFPV-UHFFFAOYSA-L 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 3
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 229910052709 silver Inorganic materials 0.000 description 3
- 239000004332 silver Substances 0.000 description 3
- 239000012279 sodium borohydride Substances 0.000 description 3
- 229910000033 sodium borohydride Inorganic materials 0.000 description 3
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical group OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002135 nanosheet Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000001291 vacuum drying Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 description 1
- 238000001069 Raman spectroscopy Methods 0.000 description 1
- -1 Silver salt Silver nitrate Silver nitrate Silver nitrate Silver sulfate Silver acetate Chemical compound 0.000 description 1
- ZLXPLDLEBORRPT-UHFFFAOYSA-M [NH4+].[Fe+].[O-]S([O-])(=O)=O Chemical group [NH4+].[Fe+].[O-]S([O-])(=O)=O ZLXPLDLEBORRPT-UHFFFAOYSA-M 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 238000000498 ball milling Methods 0.000 description 1
- 239000000090 biomarker Substances 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000004377 microelectronic Methods 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 230000010512 thermal transition Effects 0.000 description 1
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 description 1
- 229940038773 trisodium citrate Drugs 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Abstract
Description
实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | |
银盐 | 硝酸银 | 硝酸银 | 硝酸银 | 硫酸银 | 醋酸银 |
表面活性剂 | PVP-K30 | PEG-10000 | SDS | PVP-K30 | CTAB |
亚铁盐 | 六水合硫酸亚铁铵 | 七水合硫酸亚铁 | 六水合硫酸亚铁铵 | 七水合硫酸亚铁 | 六水合硫酸亚铁铵 |
实施例1 | 实施例6 | 实施例7 | 实施例8 | 实施例9 | 实施例10 | 实施例11 | |
硝酸银 | 0.20g | 0.20g | 0.20g | 0.20g | 2.00g | 2.00g | 2.00g |
PVP-K30 | 0.04g | 0.01g | 0.02g | 0.40g | 0.10g | 0.04g | 0.40g |
六水合硫酸亚铁铵 | 0.40g | 0.80g | 0.20g | 0.10g | 2.00g | 4.00g | 7.00g |
反应温度 | 60℃ | 40℃ | 20℃ | 50℃ | 80℃ | 0℃ | 60℃ |
反应时间 | 30min | 28min | 35min | 30min | 32min | 25min | 30min |
Claims (1)
Priority Applications (1)
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CN201510815965.0A CN105268993B (zh) | 2012-11-29 | 2012-11-29 | 一种制备片状纳米银粉的方法 |
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CN201510815965.0A CN105268993B (zh) | 2012-11-29 | 2012-11-29 | 一种制备片状纳米银粉的方法 |
CN201210500911.1A CN102974837B (zh) | 2012-11-29 | 2012-11-29 | 片状纳米银粉的制备方法 |
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CN201210500911.1A Division CN102974837B (zh) | 2012-11-29 | 2012-11-29 | 片状纳米银粉的制备方法 |
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CN105268993A true CN105268993A (zh) | 2016-01-27 |
CN105268993B CN105268993B (zh) | 2019-01-25 |
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CN201510815965.0A Active CN105268993B (zh) | 2012-11-29 | 2012-11-29 | 一种制备片状纳米银粉的方法 |
CN201210500911.1A Active CN102974837B (zh) | 2012-11-29 | 2012-11-29 | 片状纳米银粉的制备方法 |
CN201510819711.6A Active CN105290420B (zh) | 2012-11-29 | 2012-11-29 | 制备片状纳米银粉的方法 |
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CN201210500911.1A Active CN102974837B (zh) | 2012-11-29 | 2012-11-29 | 片状纳米银粉的制备方法 |
CN201510819711.6A Active CN105290420B (zh) | 2012-11-29 | 2012-11-29 | 制备片状纳米银粉的方法 |
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Cited By (2)
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CN108655414A (zh) * | 2018-06-11 | 2018-10-16 | 合肥学院 | 一种快速宏量制备二维Ag微纳米材料的简易方法 |
CN111496269A (zh) * | 2020-05-21 | 2020-08-07 | 广州大学附属中学 | 一种纳米银及其制备方法和应用 |
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JP5763869B2 (ja) * | 2013-06-25 | 2015-08-12 | 化研テック株式会社 | 薄片状銀粉、導電性ペースト、および薄片状銀粉の製造方法 |
CN103521777A (zh) * | 2013-10-11 | 2014-01-22 | 南京邮电大学 | 制备不同形貌的二维银纳米片的方法 |
KR101618093B1 (ko) * | 2014-03-17 | 2016-05-09 | 주식회사 상보 | 도전막 형성을 위한 유연 기판용 전도성 페이스트 조성물 및 이의 제조방법 |
CN104551007A (zh) * | 2015-01-13 | 2015-04-29 | 山东大学 | 一种可大量制备银纳米片的方法 |
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CN108655414A (zh) * | 2018-06-11 | 2018-10-16 | 合肥学院 | 一种快速宏量制备二维Ag微纳米材料的简易方法 |
CN111496269A (zh) * | 2020-05-21 | 2020-08-07 | 广州大学附属中学 | 一种纳米银及其制备方法和应用 |
Also Published As
Publication number | Publication date |
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CN102974837A (zh) | 2013-03-20 |
CN105290420A (zh) | 2016-02-03 |
CN105268993B (zh) | 2019-01-25 |
CN105290420B (zh) | 2017-11-21 |
CN102974837B (zh) | 2016-01-06 |
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