CN105218164A - Copper red furnace transmutation glaze and by its copper red furnace transmutation glaze ceramic prepared and preparation method - Google Patents
Copper red furnace transmutation glaze and by its copper red furnace transmutation glaze ceramic prepared and preparation method Download PDFInfo
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Abstract
The present invention relates to a kind of copper red furnace transmutation glaze and by its copper red furnace transmutation glaze ceramic prepared and preparation method, belong to ceramic technology field.This copper red furnace transmutation glaze comprises the following component according to weight parts: glaze formula basestocks: nepheline syenite 34-35 part, calcium carbonate 20-22 part, barium carbonate 3-4 part, zinc oxide 2-3 part, magnesiumcarbonate 1-2 part, kaolin 26-27 part, nano silicon oxide 9.5-10.5 part, chromogenic reagent: Quilonum Retard 1.8-2.5 part, bone ash 2-4 part, copper carbonate 2-4 part.The ceramic using this copper red furnace transmutation glaze to fire has more bright-coloured redness, and glaze color distribution is even, and yield rate is high.
Description
Technical field
The invention belongs to ceramic technology field, be specifically related to a kind of copper red furnace transmutation glaze and by its copper red furnace transmutation glaze ceramic prepared and preparation method.
Background technology
Rough flambe is loved by the people since ancient times, and be famousr and precious a kind of glaze, in the Ming Dynasty, mid-term was once once lost, and it is red to change burning alum.What in rough flambe, color was the most bright-coloured will count ox-blood glaze, namely general rough flambe is chromogenic reagent with copper-containing substance, through reducing the red glaze fired, its materials and the quality of firing condition to glaze are key, as long as materials are slightly different or deviation, will cause reduction not exclusively, even cause the phenomenons such as glaze blackout, greening.Bright-coloured copper red is always more rare, pursue by people.And generally can burn out the composition of raw materials of the good rough flambe of quality and technique is not all disclosed, the rough flambe burnt out according to the glaze of existing rough flambe not only color effects is not good, what have even can produce the defects such as glaze color distribution inequality, the surperficial generation pin hole of glaze, even if add the auxiliary agents such as stablizer again to fire in glaze, above deficiency is also difficult to avoid, and studies carefully its major cause or the formula of glaze is unreasonable and the condition setting of reduction when firing is unreasonable.Therefore, the research of the glaze of rough flambe and exploration are had great importance.
Summary of the invention
The object of the invention is to solve the deficiencies in the prior art, and provide a kind of copper red furnace transmutation glaze and by its copper red furnace transmutation glaze ceramic prepared and preparation method, the ceramic using this copper red furnace transmutation glaze to fire has more bright-coloured redness, and glaze color distribution is even, and yield rate is high.
The present invention adopts following technical scheme:
Copper red furnace transmutation glaze, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 34-35 part, calcium carbonate 20-22 part, barium carbonate 3-4 part, zinc oxide 2-3 part, magnesiumcarbonate 1-2 part, kaolin 26-27 part, nano silicon oxide 9.5-10.5 part, chromogenic reagent: Quilonum Retard 1.8-2.5 part, bone ash 2-4 part, copper carbonate 2-4 part.
Described copper red furnace transmutation glaze, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 34.67 parts, 21.26 parts, calcium carbonate, barium carbonate 3.56 parts, 2.93 parts, zinc oxide, 1.45 parts, magnesiumcarbonate, kaolin 26.06 parts, nano silicon oxide 10.07 parts, chromogenic reagent: Quilonum Retard 2 parts, 3 parts, bone ash, copper carbonate 3 parts.
Prepare the method for copper red furnace transmutation glaze ceramic with described copper red furnace transmutation glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 50%-55% carries out ball milling, is milled to mixture particle and crosses 200-250 mesh sieve, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 39 °-40 ° of degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glaze thickness is 1.2-1.5mm, dry, obtains ceramic first product;
Step 4, reduction is fired: fired by step 3 gained ceramic first product, be warming up to 865-875 DEG C, keep carbon monoxide volumetric concentration in kiln to be 3%-3.5%, constant temperature fires 35-45min, after continuing to be warming up to 1260-1270 DEG C, carbon monoxide volumetric concentration in kiln is kept to be 1%-1.5%, constant temperature fires 20-30min, rear cooling down, obtains described copper red furnace transmutation glaze ceramic.
Further, the described method preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze, wherein said biscuit of ceramics adopts potter's clay fire and obtain.
Further, the described method preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze, wherein the rotating speed of ball milling described in step one is 400-450r/min.
The copper red furnace transmutation glaze ceramic that a kind of method that the present invention also provides copper red furnace transmutation glaze to prepare copper red furnace transmutation glaze ceramic is obtained.
Compared with prior art, its beneficial effect is in the present invention:
The present invention is by studying intensively copper red furnace transmutation glaze glaze, ceramic journey can be made after obtaining a kind of firing compared with the glaze of hunting pink, this glaze is not only bright-colored, and color distribution is even, and glaze surface is moist, smooth uniform, in addition, the yield rate of the copper red furnace transmutation glaze ceramic fired according to the inventive method can reach more than 90%, therefore, the present invention has good market outlook, is suitable for applying on a large scale.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention.
embodiment 1
Copper red furnace transmutation glaze, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 34.67 parts, 21.26 parts, calcium carbonate, barium carbonate 3.56 parts, 2.93 parts, zinc oxide, 1.45 parts, magnesiumcarbonate, kaolin 26.06 parts, nano silicon oxide 10.07 parts, chromogenic reagent: Quilonum Retard 2 parts, 3 parts, bone ash, copper carbonate 3 parts.
Prepare the method for copper red furnace transmutation glaze ceramic with described copper red furnace transmutation glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 50% carries out ball milling, is milled to mixture particle and crosses 250 mesh sieves, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 40 ° degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glaze thickness is 1.4mm, dry, obtains ceramic first product;
Step 4, reduction is fired: fired by step 3 gained ceramic first product, be warming up to 870 DEG C, keep carbon monoxide volumetric concentration in kiln to be 3.2%, constant temperature fires 40min, after continuing to be warming up to 1270 DEG C, carbon monoxide volumetric concentration in kiln is kept to be 1.3%, constant temperature fires 25min, rear cooling down, obtains described copper red furnace transmutation glaze ceramic.
embodiment 2
Copper red furnace transmutation glaze, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 34 parts, 20 parts, calcium carbonate, barium carbonate 3 parts, 2 parts, zinc oxide, 1 part, magnesiumcarbonate, kaolin 26 parts, nano silicon oxide 9.5 parts, chromogenic reagent: Quilonum Retard 1.8 parts, 2 parts, bone ash, copper carbonate 2 parts.
Prepare the method for copper red furnace transmutation glaze ceramic with described copper red furnace transmutation glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 50% carries out ball milling, is milled to mixture particle and crosses 200 mesh sieves, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 39 ° degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glaze thickness is 1.2mm, dry, obtains ceramic first product;
Step 4, reduction is fired: fired by step 3 gained ceramic first product, be warming up to 865 DEG C, keep carbon monoxide volumetric concentration in kiln to be 3%, constant temperature fires 35min, after continuing to be warming up to 1260 DEG C, carbon monoxide volumetric concentration in kiln is kept to be 1%, constant temperature fires 30min, rear cooling down, obtains described copper red furnace transmutation glaze ceramic.
embodiment 3
Copper red furnace transmutation glaze, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 35 parts, 22 parts, calcium carbonate, barium carbonate 4 parts, 3 parts, zinc oxide, 2 parts, magnesiumcarbonate, kaolin 27 parts, nano silicon oxide 10.5 parts, chromogenic reagent: Quilonum Retard 2.5 parts, 4 parts, bone ash, copper carbonate 4 parts.
Prepare the method for copper red furnace transmutation glaze ceramic with described copper red furnace transmutation glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 55% carries out ball milling, is milled to mixture particle and crosses 220 mesh sieves, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 39 ° degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glaze thickness is 1.5mm, dry, obtains ceramic first product;
Step 4, reduction is fired: fired by step 3 gained ceramic first product, be warming up to 875 DEG C, keep carbon monoxide volumetric concentration in kiln to be 3.5%, constant temperature fires 35min, after continuing to be warming up to 1270 DEG C, carbon monoxide volumetric concentration in kiln is kept to be 1.5%, constant temperature fires 20min, rear cooling down, obtains described copper red furnace transmutation glaze ceramic.
The copper red furnace transmutation glaze ceramic obtained according to glaze formula described in embodiment 1 to 3 and preparation method all has bright-coloured copper red look, and color distribution is even, glaze surface is moist, smooth uniform, and yield rate all can reach more than 90%, wherein, the yield rate of embodiment 1 can reach 95%, can be considered most preferred embodiment.
The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (6)
1. copper red furnace transmutation glaze, it is characterized in that, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 34-35 part, calcium carbonate 20-22 part, barium carbonate 3-4 part, zinc oxide 2-3 part, magnesiumcarbonate 1-2 part, kaolin 26-27 part, nano silicon oxide 9.5-10.5 part, chromogenic reagent: Quilonum Retard 1.8-2.5 part, bone ash 2-4 part, copper carbonate 2-4 part.
2. copper red furnace transmutation glaze according to claim 1, it is characterized in that, comprise the following component according to weight parts: glaze formula basestocks: nepheline syenite 34.67 parts, 21.26 parts, calcium carbonate, barium carbonate 3.56 parts, 2.93 parts, zinc oxide, 1.45 parts, magnesiumcarbonate, kaolin 26.06 parts, nano silicon oxide 10.07 parts, chromogenic reagent: Quilonum Retard 2 parts, 3 parts, bone ash, copper carbonate 3 parts.
3. prepare the method for copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze described in claim 1, it is characterized in that, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 50%-55% carries out ball milling, is milled to mixture particle and crosses 200-250 mesh sieve, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 39 °-40 ° of degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glaze thickness is 1.2-1.5mm, dry, obtains ceramic first product;
Step 4, reduction is fired: fired by step 3 gained ceramic first product, be warming up to 865-875 DEG C, keep carbon monoxide volumetric concentration in kiln to be 3%-3.5%, constant temperature fires 35-45min, after continuing to be warming up to 1260-1270 DEG C, carbon monoxide volumetric concentration in kiln is kept to be 1%-1.5%, constant temperature fires 20-30min, rear cooling down, obtains described copper red furnace transmutation glaze ceramic.
4. copper red furnace transmutation glaze according to claim 3 prepares the method for copper red furnace transmutation glaze ceramic, it is characterized in that, described biscuit of ceramics adopts potter's clay fire and obtain.
5. copper red furnace transmutation glaze according to claim 3 prepares the method for copper red furnace transmutation glaze ceramic, it is characterized in that, the rotating speed of ball milling described in step one is 400-450r/min.
6. the copper red furnace transmutation glaze ceramic that the method that copper red furnace transmutation glaze according to claim 3 prepares copper red furnace transmutation glaze ceramic obtains.
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| CN105731799A (en) * | 2016-01-14 | 2016-07-06 | 福建省泉州得盛集团有限公司 | Copper red reduction transmutation glaze, copper red reduction transmutation glaze ceramic product and preparation method thereof |
| CN106082670A (en) * | 2016-06-22 | 2016-11-09 | 德化县太阳鸟工艺品有限公司 | Foaming glaze and the glaze foamed ceramic made of it |
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| CN105601110B (en) * | 2016-01-14 | 2019-04-09 | 福建省泉州得盛集团有限公司 | Black silver drop reduction furnace transmutation glaze and the black silver drop prepared with it restore transmutation glazed pottery ceramic products and preparation method |
| CN105601110A (en) * | 2016-01-14 | 2016-05-25 | 福建省泉州得盛集团有限公司 | Black silver drop reduced transmutation glaze, black silver drop reduced transmutation glaze ceramic product prepared using same and preparation method |
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