CN105601110B - Black silver drop reduction furnace transmutation glaze and the black silver drop prepared with it restore transmutation glazed pottery ceramic products and preparation method - Google Patents
Black silver drop reduction furnace transmutation glaze and the black silver drop prepared with it restore transmutation glazed pottery ceramic products and preparation method Download PDFInfo
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- CN105601110B CN105601110B CN201610022907.7A CN201610022907A CN105601110B CN 105601110 B CN105601110 B CN 105601110B CN 201610022907 A CN201610022907 A CN 201610022907A CN 105601110 B CN105601110 B CN 105601110B
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/04—Frit compositions, i.e. in a powdered or comminuted form containing zinc
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Abstract
Reduction furnace transmutation glaze is dripped the present invention relates to a kind of black silver and restores transmutation glazed pottery ceramic products and preparation method with the black silver drop of its preparation, belongs to ceramic technology field.Black silver drop reduction furnace transmutation glaze includes the following component according to mass fraction meter: 33-36 parts of nepheline syenite, 18-22 parts of precipitated calcium carbonate, 4-6 parts of barium carbonate, 2-4 parts of zinc oxide, 1-3 parts of magnesium carbonate, 9-12 parts of kaolin, waste old ceramics biscuit processing material 14-18 parts, 8-12 parts of quartz, 2-6 parts of bone ash, 2-8 parts of manganese oxide, 2-7 parts of copper oxide.Glazing techniques of the present invention are simple and easy, can effectively improve production efficiency；Black silver drop reduction transmutation glazed pottery ceramic products obtained have pitch-black glaze, low-key, and use silver drop decoration, more aobvious noble quality atmosphere, and be fired according to the method for the present invention, the yield rate of ceramic product is higher by up to 92% or more, is suitble to production domestic ceramics and decorative porcelain.
Description
Technical field
The invention belongs to ceramic technology fields, and in particular to a kind of black silver drop reduction furnace transmutation glaze and the black with its preparation
Silver drop reduction transmutation glazed pottery ceramic products and preparation method.
Background technique
Glaze is the glassy thin layer for being covered on billet surface, and smooth surface is glossy, and is not easy to be stained with waterproof
Dirty performance, not only can be improved the physical property of ceramic body, can also enhance the appearance of beautification ceramic.Black glaze has
There is the glaze of black glossy, general black glaze is both needed in high temperature firing, and black glaze is favored due to its glaze colours uniqueness by common people.
When furnace transmutation glaze, that is, porcelain is burnt into kiln, due in glaze containing there are many pigmentation element, through oxidation or reduction,
Unexpected glaze colours effect is showed after kiln discharge, since its glaze colours is unexpected, form is special, and people do not know its principle again,
Only know and changes in roasting process in kiln and obtain, therefore referred to as " transmutation ", common saying has " transmutation is unparalleled " to call it to change unpredictably, an only nothing
Two.Due to the uniqueness of furnace transmutation glaze and extensive market prospects, people have also put into more and more concerns to furnace transmutation glaze.And it wants
It fires that a kind of glaze colours is special and unique furnace transmutation glaze, needs to spend a large amount of manpower and material resources, and the yield rate of furnace transmutation glaze
It is universal relatively low.Although the current report in relation to black glaze is more, the relevant report of black silver drop furnace transmutation glaze yet there are no.
Such as application No. is 200710193874.3 Chinese patents to disclose a kind of system of black glaze gold drip glaze and products thereof
Make method, although disclosing the production method of black glaze gold drop glaze that one kind is fired at relatively high temperatures and products thereof, the glaze
Make bottom with black, is decorated with golden yellow, wide adaptability, thermal stability is good, but the glazing techniques of the glaze are comparatively laborious, need
Upper inside and outside glaze respectively, causes certain inconvenience to production, furthermore also poor strong according to the yield rate of product made from its production method
People's will.
Summary of the invention
The purpose of the present invention is to solve the deficiencies in the prior art, and provide a kind of black silver drop reduction furnace transmutation glaze and use
Its black silver prepared drop reduction transmutation glazed pottery ceramic products and preparation method, black silver drop reduction furnace transmutation glaze have pitch-black glaze
Face, low-key, silver drop decoration, more aobvious noble quality atmosphere and are fired according to the method for the present invention, the yield rate of ceramic product compared with
Height is suitble to domestic ceramics and decorative porcelain.
The present invention adopts the following technical scheme:
Black silver drop reduction furnace transmutation glaze, including the following component according to mass fraction meter: 33-36 part of nepheline syenite, gently
18-22 parts of matter calcium carbonate, 4-6 parts of barium carbonate, 2-4 parts of zinc oxide, 1-3 parts of magnesium carbonate, 9-12 parts of kaolin, waste old ceramics biscuit
Processing material 14-18 parts, 8-12 parts of quartz, 2-6 parts of bone ash, 2-8 parts of manganese oxide, 2-7 parts of copper oxide.
Further, the described black silver drop reduction furnace transmutation glaze, wherein waste old ceramics biscuit processing material by with
Lower method obtains: waste old ceramics biscuit being crushed to 200-300 mesh, polyvinyl alcohol is added afterwards, stirs evenly, in 0.5-0.8MPa
Lower briquet, after be crushed to graininess to get waste old ceramics biscuit processing expect, wherein the polyvinyl alcohol and waste old ceramics that are added
The mass ratio of biscuit is 1:5 ~ 1:9.
Further, black silver drop reduction furnace transmutation glaze, including the following component according to mass fraction meter: nepheline
35 parts of orthoclase, 20.26 parts of precipitated calcium carbonate, 4.56 parts of barium carbonate, 2.93 parts of zinc oxide, 1.45 parts of magnesium carbonate, kaolin
10.06 parts, 16 parts of waste old ceramics biscuit processing material, quartzy 10.07 parts, 3 parts of bone ash, 5 parts of manganese oxide, 5 parts of copper oxide.
The method that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products is dripped with the black silver, including as follows
Step:
Ball milling of stocking up: step 1 according to the weight proportion, gets nepheline syenite, precipitated calcium carbonate, barium carbonate, oxygen ready
Change zinc, magnesium carbonate, kaolin, waste old ceramics biscuit and handle material, quartz, bone ash, manganese oxide, copper oxide, above-mentioned each raw material is mixed
It closes uniformly, obtains mixture, add water in mixture, be sieved after ball milling, obtain ball milling material；
Glaze slip production: ball milling material obtained by step 1 is adjusted to 37-38 Baume degrees, stirs evenly, obtain glaze slurry by step 2；
Step 3 soaks glaze: the biscuit of ceramics baked in advance being immersed in glaze slurry obtained by step 2 and carries out glazing, must be made pottery
Ceramic products first product；
Step 4 is fired: ceramic first product obtained by step 3 being fired in reducing atmosphere, specific firing is such as
Under: it is warming up to 405-415 DEG C in 2h, continues to heat up, 650-660 DEG C is warming up in 2h, continues to heat up, is warming up in 2h
960-970 DEG C, continue to heat up, then is warming up to 1150-1155 DEG C with the heating rate of 1-1.3 DEG C/min, then with 0.5-1 DEG C/min
Heating rate be warming up to 1265-1275 DEG C, keep the temperature 1h, drip reduction transmutation glazed pottery porcelain to natural cooling to get the black silver
Product.
Further, described that the side that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products is dripped with black silver
Method wherein crosses 200-250 mesh after ball milling in step 1.
Further, described that the side that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products is dripped with black silver
Method, wherein the biscuit of ceramics is Red Stone Ware or cosmetic soil biscuit.
The present invention also provides a kind of black silver drop reduction transmutation glazed pottery made from the black silver drop reduction furnace transmutation glaze
Ceramic products.
Compared with prior art, the present invention has the advantages that:
The present invention utilize waste old ceramics biscuit material, by being reprocessed to waste old ceramics biscuit material, afterwards with other glaze
Enamel frit makeing is starched after cooperation mixing, by soaking after glaze mode carries out glazing, through reductive firing can get Hei Seyin drop reduction furnace transmutation glaze,
Glazing techniques are simple and easy, can effectively improve production efficiency；In addition, dripping reduction transmutation glazed pottery according to black silver produced by the present invention
Ceramic products have pitch-black glaze, low-key, and are decorated using silver drop, and more aobvious noble quality atmosphere first uses in sintering procedure
Be rapidly heated in a short time, then reduce heating rate and slowly heat up, after continue growing heating rate heating, it is rear to reduce heating again
Rate is to slowly warm up to 1150-1155 DEG C, then is warming up to 1265-1275 DEG C with the heating rate of 0.5-1 DEG C/min, keeps the temperature 1h,
So that glaze is formed pitch-black glaze between heating cooling and make silver drop that crystallization be precipitated, to ensure that the uniqueness and beauty of glaze
Property, and be fired according to the method for the present invention, the yield rate of ceramic product is higher, and up to 92% or more, it is suitble to the daily pottery of production
Porcelain and decorative porcelain.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example is merely to illustrate the present invention, and it should not be regarded as limiting this hair
Bright range.
Embodiment 1
Black silver drop reduction furnace transmutation glaze, including the following component according to mass fraction meter: 35 parts of nepheline syenite, lightweight carbon
20.26 parts of sour calcium, 4.56 parts of barium carbonate, 2.93 parts of zinc oxide, 1.45 parts of magnesium carbonate, 10.06 parts of kaolin, waste old ceramics biscuit
16 parts of processing material, quartzy 10.07 parts, 3 parts of bone ash, 5 parts of manganese oxide, 5 parts of copper oxide.The wherein waste old ceramics biscuit processing material
It is obtained by following methods: waste old ceramics biscuit being crushed to 300 mesh, polyvinyl alcohol is added afterwards, stirs evenly, under 0.6MPa
Briquet, after be crushed to graininess to get waste old ceramics biscuit processing expect, wherein be added polyvinyl alcohol and waste old ceramics element
The mass ratio of base is 1:8.
The method that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products is dripped with the black silver, including as follows
Step:
Ball milling of stocking up: step 1 according to the weight proportion, gets nepheline syenite, precipitated calcium carbonate, barium carbonate, oxygen ready
Change zinc, magnesium carbonate, kaolin, waste old ceramics biscuit and handle material, quartz, bone ash, manganese oxide, copper oxide, above-mentioned each raw material is mixed
It closes uniformly, obtains mixture, add water in mixture, 250 meshes are crossed after ball milling, obtain ball milling material；
Glaze slip production: ball milling material obtained by step 1 is adjusted to 38 Baume degrees, stirs evenly, obtain glaze slurry by step 2；
Step 3 soaks glaze: the biscuit of ceramics baked in advance being immersed in glaze slurry obtained by step 2 and carries out glazing, must be made pottery
Ceramic products first product, wherein the biscuit of ceramics is Red Stone Ware biscuit；
Step 4 is fired: ceramic first product obtained by step 3 being fired in reducing atmosphere, specific firing is such as
Under: it is warming up to 410 DEG C in 2h, continues to heat up, 655 DEG C are warming up in 2h, continues to heat up, 965 DEG C are warming up in 2h, continues
Heating, then 1152 DEG C are warming up to the heating rate of 1.1 DEG C/min, then be warming up to 1270 DEG C with the heating rate of 0.8 DEG C/min,
1h is kept the temperature, drips reduction transmutation glazed pottery ceramic products to natural cooling to get the black silver.
Reduction its yield rate of transmutation glazed pottery ceramic products is dripped up to 95% according to black silver made from the present embodiment, makes glaze
With three-dimensional sense.
Embodiment 2
Black silver drop reduction furnace transmutation glaze, including the following component according to mass fraction meter: 33 parts of nepheline syenite, lightweight carbon
18 parts of sour calcium, 4 parts of barium carbonate, 2 parts of zinc oxide, 1 part of magnesium carbonate, 9 parts of kaolin, 14 parts of waste old ceramics biscuit processing material, quartz 8
Part, 2 parts of bone ash, 2 parts of manganese oxide, 2 parts of copper oxide.Wherein the waste old ceramics biscuit processing material is obtained by following methods: will
Waste old ceramics biscuit is crushed to 200 mesh, and polyvinyl alcohol is added afterwards, stirs evenly, the briquet under 0.5MPa, after be crushed to
It is granular to expect to get the processing of waste old ceramics biscuit, wherein the mass ratio of the polyvinyl alcohol and waste old ceramics biscuit that are added is 1:5.
The method that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products is dripped with the black silver, including as follows
Step:
Ball milling of stocking up: step 1 according to the weight proportion, gets nepheline syenite, precipitated calcium carbonate, barium carbonate, oxygen ready
Change zinc, magnesium carbonate, kaolin, waste old ceramics biscuit and handle material, quartz, bone ash, manganese oxide, copper oxide, above-mentioned each raw material is mixed
It closes uniformly, obtains mixture, add water in mixture, 200 meshes are crossed after ball milling, obtain ball milling material；
Glaze slip production: ball milling material obtained by step 1 is adjusted to 37 Baume degrees, stirs evenly, obtain glaze slurry by step 2；
Step 3 soaks glaze: the biscuit of ceramics baked in advance being immersed in glaze slurry obtained by step 2 and carries out glazing, must be made pottery
Ceramic products first product, wherein the biscuit of ceramics is cosmetic soil biscuit；
Step 4 is fired: ceramic first product obtained by step 3 being fired in reducing atmosphere, specific firing is such as
Under: it is warming up to 405 DEG C in 2h, continues to heat up, 650 DEG C are warming up in 2h, continues to heat up, 960 DEG C are warming up in 2h, continues
Heating, then 1150 DEG C are warming up to the heating rate of 1 DEG C/min, then be warming up to 1265 DEG C with the heating rate of 0.5 DEG C/min, it protects
Warm 1h drips reduction transmutation glazed pottery ceramic products to natural cooling to get the black silver.
Reduction its yield rate of transmutation glazed pottery ceramic products is dripped up to 93% according to black silver made from the present embodiment, makes glaze
With three-dimensional sense.
Embodiment 3
Black silver drop reduction furnace transmutation glaze, including the following component according to mass fraction meter: 36 parts of nepheline syenite, lightweight carbon
22 parts of sour calcium, 6 parts of barium carbonate, 4 parts of zinc oxide, 3 parts of magnesium carbonate, 12 parts of kaolin, 18 parts of waste old ceramics biscuit processing material, quartz
12 parts, 6 parts of bone ash, 8 parts of manganese oxide, 7 parts of copper oxide.Wherein the waste old ceramics biscuit processing material is obtained by following methods:
Waste old ceramics biscuit is crushed to 250 mesh, polyvinyl alcohol is added afterwards, stirs evenly, the briquet under 0.8MPa, after be crushed to
Graininess is expected to get the processing of waste old ceramics biscuit, wherein the mass ratio of the polyvinyl alcohol and waste old ceramics biscuit that are added is 1:9.
The method that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products is dripped with the black silver, including as follows
Step:
Ball milling of stocking up: step 1 according to the weight proportion, gets nepheline syenite, precipitated calcium carbonate, barium carbonate, oxygen ready
Change zinc, magnesium carbonate, kaolin, waste old ceramics biscuit and handle material, quartz, bone ash, manganese oxide, copper oxide, above-mentioned each raw material is mixed
It closes uniformly, obtains mixture, add water in mixture, 250 meshes are crossed after ball milling, obtain ball milling material；
Glaze slip production: ball milling material obtained by step 1 is adjusted to 38 Baume degrees, stirs evenly, obtain glaze slurry by step 2；
Step 3 soaks glaze: the biscuit of ceramics baked in advance being immersed in glaze slurry obtained by step 2 and carries out glazing, must be made pottery
Ceramic products first product, wherein the biscuit of ceramics is Red Stone Ware biscuit；
Step 4 is fired: ceramic first product obtained by step 3 being fired in reducing atmosphere, specific firing is such as
Under: it is warming up to 415 DEG C in 2h, continues to heat up, 660 DEG C are warming up in 2h, continues to heat up, 970 DEG C are warming up in 2h, continues
Heating, then 1155 DEG C are warming up to the heating rate of 1.3 DEG C/min, then be warming up to 1275 DEG C with the heating rate of 1 DEG C/min, it protects
Warm 1h drips reduction transmutation glazed pottery ceramic products to natural cooling to get the black silver.
Reduction its yield rate of transmutation glazed pottery ceramic products is dripped up to 92% according to black silver made from the present embodiment, makes glaze
With three-dimensional sense.
It should be understood by those skilled in the art that the present invention is not limited to the above embodiments, above-described embodiment and explanation
It is merely illustrated the principles of the invention described in book, without departing from the spirit and scope of the present invention, the present invention also has
Various changes and modifications, these changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention
It is defined by the appending claims and its equivalent thereof.
Claims (5)
1. dripping the method that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products with black silver, which is characterized in that packet
Include following steps:
Step 1, ball milling of stocking up: according to the weight proportion, get ready nepheline syenite, precipitated calcium carbonate, barium carbonate, zinc oxide,
Magnesium carbonate, kaolin, waste old ceramics biscuit handle material, quartz, bone ash, manganese oxide, copper oxide, above-mentioned each raw material are mixed equal
It is even, mixture is obtained, is added water in mixture, is sieved after ball milling, ball milling material is obtained；
Glaze slip production: ball milling material obtained by step 1 is adjusted to 37-38 Baume degrees, stirs evenly, obtain glaze slurry by step 2；
Step 3 soaks glaze: the biscuit of ceramics baked in advance being immersed in glaze slurry obtained by step 2 and carries out glazing, obtains ceramic system
Product first product；
Step 4 is fired: ceramic first product obtained by step 3 being fired in reducing atmosphere, specific firing is as follows: 2h
It is inside warming up to 405-415 DEG C, continues to heat up, 650-660 DEG C is warming up in 2h, continues to heat up, 960-970 is warming up in 2h
DEG C, continue to heat up, then be warming up to 1150-1155 DEG C with the heating rate of 1-1.3 DEG C/min, then with the heating of 0.5-1 DEG C/min
Rate is warming up to 1265-1275 DEG C, keeps the temperature 1h, drips reduction transmutation glazed pottery ceramic products to natural cooling to get the black silver；
Wherein, the black silver drop reduction furnace transmutation glaze includes the following component according to mass fraction meter: nepheline syenite 33-36
Part, 18-22 parts of precipitated calcium carbonate, 4-6 parts of barium carbonate, 2-4 parts of zinc oxide, 1-3 parts of magnesium carbonate, 9-12 parts of kaolin, waste and old pottery
Porcelain biscuit processing material 14-18 parts, 8-12 parts of quartz, 2-6 parts of bone ash, 2-8 parts of manganese oxide, 2-7 parts of copper oxide；
The waste old ceramics biscuit processing material is obtained by following methods: waste old ceramics biscuit is crushed to 200-300 mesh, it is rear to add
Enter polyvinyl alcohol, stir evenly, the briquet under 0.5-0.8MPa, after be crushed to graininess to get waste old ceramics biscuit at
Reason material, wherein the mass ratio of the polyvinyl alcohol and waste old ceramics biscuit that are added is 1:5 ~ 1:9.
2. according to claim 1 prepare black silver drop reduction transmutation glazed pottery ceramic products with black silver drop reduction furnace transmutation glaze
Method, which is characterized in that the black silver drop reduction furnace transmutation glaze includes the following component according to mass fraction meter: nepheline syenite
35 parts, 20.26 parts of precipitated calcium carbonate, 4.56 parts of barium carbonate, 2.93 parts of zinc oxide, 1.45 parts of magnesium carbonate, 10.06 parts of kaolin,
16 parts of waste old ceramics biscuit processing material, quartzy 10.07 parts, 3 parts of bone ash, 5 parts of manganese oxide, 5 parts of copper oxide.
3. dripping the side that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products with black silver according to claim 1
Method, which is characterized in that cross 200-250 mesh in step 1 after ball milling.
4. dripping the side that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products with black silver according to claim 1
Method, which is characterized in that the biscuit of ceramics is Red Stone Ware or cosmetic soil biscuit.
5. dripping the side that reduction furnace transmutation glaze prepares black silver drop reduction transmutation glazed pottery ceramic products with black silver by described in claim 1
The drop reduction transmutation glazed pottery ceramic products of black silver made from method.
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| CN106082670B (en) * | 2016-06-22 | 2018-12-11 | 德化县太阳鸟工艺品有限公司 | Foam glaze and the glaze paint foamed ceramic with its production |
| CN107540224A (en) * | 2016-06-24 | 2018-01-05 | 江西省康舒陶瓷有限公司 | A kind of animal bone Application way and heat-resistant porcelain glaze material formula |
| CN109095884B (en) * | 2018-08-29 | 2021-06-15 | 巫贵豪 | Process for preparing cup |
| CN110818259A (en) * | 2019-12-10 | 2020-02-21 | 醴陵市良盛陶瓷制造有限公司 | Dark devitrification reaction black glaze and preparation method thereof |
| CN111875344B (en) * | 2020-06-28 | 2022-07-08 | 卓瑶养 | Black-bottom silver drop building cup firing process |
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| CN105152685B (en) * | 2015-10-19 | 2017-05-10 | 福建省德化县华茂陶瓷有限公司 | Matte metal glaze, matte metal glaze ceramic product prepared from same and preparation method of matte metal glaze ceramic product |
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| CN104478484A (en) * | 2014-11-18 | 2015-04-01 | 福建省德化协发光洋陶器有限公司 | Preparation method for black or white spotted glaze slurry |
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