CN105439640A - Transmutation glaze and preparation method thereof - Google Patents
Transmutation glaze and preparation method thereof Download PDFInfo
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- CN105439640A CN105439640A CN201410493797.3A CN201410493797A CN105439640A CN 105439640 A CN105439640 A CN 105439640A CN 201410493797 A CN201410493797 A CN 201410493797A CN 105439640 A CN105439640 A CN 105439640A
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Abstract
The invention relates to a transmutation glaze comprising the following components by the weight fraction: 49-53 parts of opal, 18-21 parts of purple knar clay, 14-17 parts of apatite, 3-5 parts of talc, 9-11 parts of feldspar, 0.6-1.2 parts of lasurite, 4-6 parts of iron oxide red, 14-16 parts of rutile, 10-15 parts of malachite, 3-5 parts of cobalt oxide, and 1-2 parts of zinc oxide. A prepared transmutation ceramic product has a dark red glaze surface, has a blue water drop-shaped pattern in a distribution manner, and is bright in color and luster, stronger in decorative effect, and good in thermal stability.
Description
Technical field
The present invention relates to ceramic glaze technical field, more specifically, relate to a kind of furnace transmutation glaze and preparation method thereof.
Background technology
Furnace transmutation glaze, as the term suggests, be that beyond thought glaze chromatic effect has appearred in implements in sintering process.Containing multiple pigmentation element in kiln, through oxidation or reductive action, porcelain may present unexpected glaze chromatic effect after kiln discharge.Because furnace transmutation glaze occurs for accidentally, form is special, and people do not know again its principle, only knows roasting process change in kiln and obtains, therefore being referred to as " furnace transmutation glaze ".Common saying has " transmutation is unparalleled ", just refers to changing unpredictably of furnace transmutation glaze, unique.That is familiar with furnace transmutation glaze along with people gos deep into, and the beauty of defect of transmutation also obtains liking of people gradually, the defect that kiln fire causes to glaze paint, and see and allow people enjoy endless aftertastes long afterwards on the contrary, in multicoloured coloured glaze, furnace transmutation glaze porcelain seems very unique and marvellous.In recent years, furnace transmutation glaze price commercially also starts to go up gradually.
As everyone knows, can there is a series of very complicated physical and chemical changes in porcelain in sintering process, especially will produce different transmutation effects, the impact being subject to formula, technique etc. is larger, therefore, the manufacture difficulty of furnace transmutation glaze is high, and current transmutation effect is also less.
Summary of the invention
The object of this invention is to provide a kind of furnace transmutation glaze, its glaze paint is garnet, and is distributed with in blue drops pattern, bright in colour.
Another object of the present invention is to provide a kind of preparation method of described furnace transmutation glaze.
The object of the invention is achieved by the following technical programs:
A kind of furnace transmutation glaze is provided, be made up of each component of following weight fraction: 49 ~ 53 parts, opal, camwood knag 18 ~ 21 parts, 14 ~ 17 parts, phosphatic rock, 3 ~ 5 parts, talcum, feldspar 9 ~ 11 parts, oriental lapis 0.6 ~ 1.2 part, iron oxide red 4 ~ 6 parts, rutile 14 ~ 16 parts, malachite 10 ~ 15 parts, cobalt oxide 3 ~ 5 parts, 1 ~ 2 part, zinc oxide.
Preferably, described furnace transmutation glaze is made up of each component of following weight fraction: 51 parts, opal, camwood knag 19 parts, 16 parts, phosphatic rock, 4 parts, talcum, feldspar 11 parts, oriental lapis 0.7 part, iron oxide red 4.5 parts, rutile 14.5 parts, malachite 13 parts, cobalt oxide 3.5 parts, 1.8 parts, zinc oxide.
Present invention also offers the preparation method of described furnace transmutation glaze, comprise the following steps:
S1. starting material are got by weight ratio, to expect: ball: the ratio of water=1:1.7 ~ 2.3:0.5 ~ 0.7 enters ball milling, obtains glaze slip;
S2. by the glazing on base substrate of the glaze slip of S1 gained;
S3. enter kiln oxydizing flame to fire, in 3h, make firing temperature be raised to 320 DEG C; Firing temperature is risen to 850 DEG C by continuation oxydizing flame in 2h again, insulation 40 ~ 50min; Then in 1h, firing temperature is risen to 1050 DEG C with reducing flame, insulation 30 ~ 45min; Firing temperature is risen to 1230 DEG C by continuation reducing flame in 1.5h again, insulation 20 ~ 30min; Finally in 30min, firing temperature is dropped to 1050 DEG C, insulation 3 ~ 4h, naturally cools to room temperature.
Preferably, glaze slip fineness described in S1 is that 10000-hole sieve tails over 0.06 ~ 0.09%.
Preferably, enameling method described in S2 is leaching glaze.
Preferably, the glazed thickness of glazing described in S2 is 0.3 ~ 1.6mm.
Compared with prior art, the present invention has following beneficial effect:
The invention provides a kind of furnace transmutation glaze, its glaze paint is garnet, and is distributed with in blue drops pattern, bright in colour, and decorative effect is comparatively strong, and Heat stability is good.
Embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of furnace transmutation glaze, be made up of each component of following weight fraction: 51 parts, opal, camwood knag 19 parts, 16 parts, phosphatic rock, 4 parts, talcum, feldspar 11 parts, oriental lapis 0.7 part, iron oxide red 4.5 parts, rutile 14.5 parts, malachite 13 parts, cobalt oxide 3.5 parts, 1.8 parts, zinc oxide.
Embodiment 2
Present embodiment discloses a kind of furnace transmutation glaze, be made up of each component of following weight fraction: 52 parts, opal, camwood knag 20 parts, 15 parts, phosphatic rock, 5 parts, talcum, feldspar 10 parts, oriental lapis 0.8 part, iron oxide red 5 parts, rutile 15 parts, malachite 11 parts, cobalt oxide 4 parts, 1 part, zinc oxide.
Embodiment 3
Present embodiment discloses a kind of furnace transmutation glaze, be made up of each component of following weight fraction: 49 parts, opal, camwood knag 21 parts, 14 parts, phosphatic rock, 3 parts, talcum, feldspar 9 parts, oriental lapis 1 part, iron oxide red 6 parts, rutile 14 parts, malachite 10 parts, cobalt oxide 5 parts, 2 parts, zinc oxide.
Embodiment 4
The components by weight percent of Example 1,2,3 any embodiment prepares furnace transmutation glaze, and preparation process is as follows:
S1. get starting material by weight ratio, to expect: ball: the ratio of water=1:2:0.6 enters ball milling, obtains glaze slip, glaze slip fineness controls to tail over 0.06% at 10000-hole sieve;
S2. the glaze slip of S1 gained is adopted on base substrate the glazing of leaching glaze mode, glazed thickness is 1.5mm;
S3. enter kiln oxydizing flame to fire, in 3h, make firing temperature be raised to 320 DEG C; Firing temperature is risen to 850 DEG C by continuation oxydizing flame in 2h again, insulation 40min; Then in 1h, firing temperature is risen to 1050 DEG C with reducing flame, insulation 45min; Firing temperature is risen to 1230 DEG C by continuation reducing flame in 1.5h again, insulation 20min; Finally in 30min, firing temperature is dropped to 1050 DEG C, insulation 3h, naturally cools to room temperature, obtains kiln-transformation ceramic product product.
Products obtained therefrom glaze paint is garnet, and is distributed with in blue drops pattern, bright in colour, and decorative effect is comparatively strong, and thermostability is at 180 DEG C to 20 DEG C heat exchanges flawless.
Embodiment 5
The components by weight percent of Example 1,2,3 any embodiment prepares furnace transmutation glaze, and preparation process is as follows:
S1. get starting material by weight ratio, to expect: ball: the ratio of water=1:1.8:0.7 enters ball milling, obtains glaze slip, glaze slip fineness controls to tail over 0.08% at 10000-hole sieve;
S2. the glaze slip of S1 gained is adopted on base substrate the glazing of leaching glaze mode, glazed thickness is 1.2mm;
S3. enter kiln oxydizing flame to fire, in 3h, make firing temperature be raised to 320 DEG C; Firing temperature is risen to 850 DEG C by continuation oxydizing flame in 2h again, insulation 45min; Then in 1h, firing temperature is risen to 1050 DEG C with reducing flame, insulation 35min; Firing temperature is risen to 1230 DEG C by continuation reducing flame in 1.5h again, insulation 25min; Finally in 30min, firing temperature is dropped to 1050 DEG C, insulation 3.5h, naturally cools to room temperature, obtains kiln-transformation ceramic product product.
Products obtained therefrom glaze paint is garnet, and is distributed with in blue drops pattern, bright in colour, and decorative effect is comparatively strong, and thermostability is at 180 DEG C to 20 DEG C heat exchanges flawless.
Embodiment 6
The components by weight percent of Example 1,2,3 any embodiment prepares furnace transmutation glaze, and preparation process is as follows:
S1. get starting material by weight ratio, to expect: ball: the ratio of water=1:2.1:0.6 enters ball milling, obtains glaze slip, glaze slip fineness controls to tail over 0.07% at 10000-hole sieve;
S2. the glaze slip of S1 gained is adopted on base substrate the glazing of leaching glaze mode, glazed thickness is 1.4mm;
S3. enter kiln oxydizing flame to fire, in 3h, make firing temperature be raised to 320 DEG C; Firing temperature is risen to 850 DEG C by continuation oxydizing flame in 2h again, insulation 50min; Then in 1h, firing temperature is risen to 1050 DEG C with reducing flame, insulation 40min; Firing temperature is risen to 1230 DEG C by continuation reducing flame in 1.5h again, insulation 30min; Finally in 30min, firing temperature is dropped to 1050 DEG C, insulation 3h, naturally cools to room temperature, obtains kiln-transformation ceramic product product.
Products obtained therefrom glaze paint is garnet, and is distributed with in blue drops pattern, bright in colour, and decorative effect is comparatively strong, and thermostability is at 180 DEG C to 20 DEG C heat exchanges flawless.
Claims (6)
1. a furnace transmutation glaze, is characterized in that, is made up of each component of following weight fraction: 49 ~ 53 parts, opal, camwood knag 18 ~ 21 parts, 14 ~ 17 parts, phosphatic rock, 3 ~ 5 parts, talcum, feldspar 9 ~ 11 parts, oriental lapis 0.6 ~ 1.2 part, iron oxide red 4 ~ 6 parts, rutile 14 ~ 16 parts, malachite 10 ~ 15 parts, cobalt oxide 3 ~ 5 parts, 1 ~ 2 part, zinc oxide.
2. furnace transmutation glaze according to claim 1, is characterized in that, is made up of each component of following weight fraction: 51 parts, opal, camwood knag 19 parts, 16 parts, phosphatic rock, 4 parts, talcum, feldspar 11 parts, oriental lapis 0.7 part, iron oxide red 4.5 parts, rutile 14.5 parts, malachite 13 parts, cobalt oxide 3.5 parts, 1.8 parts, zinc oxide.
3. the preparation method of furnace transmutation glaze according to claim 1 or 2, is characterized in that, comprise the following steps:
S1. starting material are got by weight ratio, to expect: ball: the ratio of water=1:1.7 ~ 2.3:0.5 ~ 0.7 enters ball milling, obtains glaze slip;
S2. by the glazing on base substrate of the glaze slip of S1 gained;
S3. enter kiln oxydizing flame to fire, in 3h, make firing temperature be raised to 320 DEG C; Firing temperature is risen to 850 DEG C by continuation oxydizing flame in 2h again, insulation 40 ~ 50min; Then in 1h, firing temperature is risen to 1050 DEG C with reducing flame, insulation 30 ~ 45min; Firing temperature is risen to 1230 DEG C by continuation reducing flame in 1.5h again, insulation 20 ~ 30min; Finally in 30min, firing temperature is dropped to 1050 DEG C, insulation 3 ~ 4h, naturally cools to room temperature.
4. the preparation method of furnace transmutation glaze according to claim 3, it is characterized in that, glaze slip fineness described in S1 is that 10000-hole sieve tails over 0.06 ~ 0.09%.
5. the preparation method of furnace transmutation glaze according to claim 3, is characterized in that, enameling method described in S2 is leaching glaze.
6. the preparation method of furnace transmutation glaze according to claim 3, it is characterized in that, the glazed thickness of glazing described in S2 is 0.3 ~ 1.6mm.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106396385A (en) * | 2016-08-31 | 2017-02-15 | 福建省德化佳诚陶瓷有限公司 | Golden stripe tiger skin enameled container and manufacturing technology thereof |
| CN106630934A (en) * | 2016-08-30 | 2017-05-10 | 郏县神前传奇陶瓷钧瓷厂 | Process for firing jun porcelain by aid of temmoku brown golden glaze |
| CN107651848A (en) * | 2017-11-06 | 2018-02-02 | 张韶璞 | A kind of porcelain red glaze and preparation method thereof |
| CN110066190A (en) * | 2019-06-12 | 2019-07-30 | 景德镇陶瓷大学 | A kind of preparation method, black glazed ware product and its method for cooking of high temperature ice blue lima-wood leaf black glazed ware |
| CN113956075A (en) * | 2020-12-28 | 2022-01-21 | 海南丹之海文化传播有限公司 | High-temperature raw ore blue glaze and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103864464A (en) * | 2014-03-08 | 2014-06-18 | 朱仙炳 | Ceramic basic glaze with health maintenance function and environment-friendly function and use method thereof |
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2014
- 2014-09-25 CN CN201410493797.3A patent/CN105439640B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103864464A (en) * | 2014-03-08 | 2014-06-18 | 朱仙炳 | Ceramic basic glaze with health maintenance function and environment-friendly function and use method thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106630934A (en) * | 2016-08-30 | 2017-05-10 | 郏县神前传奇陶瓷钧瓷厂 | Process for firing jun porcelain by aid of temmoku brown golden glaze |
| CN106396385A (en) * | 2016-08-31 | 2017-02-15 | 福建省德化佳诚陶瓷有限公司 | Golden stripe tiger skin enameled container and manufacturing technology thereof |
| CN106396385B (en) * | 2016-08-31 | 2019-10-22 | 福建省德化佳诚陶瓷有限公司 | Golden spot tiger fur glaze porcelain and its manufacture craft |
| CN107651848A (en) * | 2017-11-06 | 2018-02-02 | 张韶璞 | A kind of porcelain red glaze and preparation method thereof |
| CN110066190A (en) * | 2019-06-12 | 2019-07-30 | 景德镇陶瓷大学 | A kind of preparation method, black glazed ware product and its method for cooking of high temperature ice blue lima-wood leaf black glazed ware |
| CN110066190B (en) * | 2019-06-12 | 2021-10-08 | 景德镇陶瓷大学 | Preparation method of high-temperature ice blue linden leaf black glazed porcelain, black glazed porcelain product and firing method thereof |
| CN113956075A (en) * | 2020-12-28 | 2022-01-21 | 海南丹之海文化传播有限公司 | High-temperature raw ore blue glaze and preparation method thereof |
| CN113956075B (en) * | 2020-12-28 | 2023-03-10 | 海南丹之海文化传播有限公司 | High-temperature raw ore blue glaze and preparation method thereof |
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Denomination of invention: The invention relates to a kiln change glaze and a preparation method thereof Effective date of registration: 20211115 Granted publication date: 20171017 Pledgee: China Co. truction Bank Corp Chaozhou branch Pledgor: GUANGDONG SHUNXIANG PORCELAIN Co.,Ltd. Registration number: Y2021980012466 |