CN105601110A - Black silver drop reduced transmutation glaze, black silver drop reduced transmutation glaze ceramic product prepared using same and preparation method - Google Patents

Black silver drop reduced transmutation glaze, black silver drop reduced transmutation glaze ceramic product prepared using same and preparation method Download PDF

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Publication number
CN105601110A
CN105601110A CN201610022907.7A CN201610022907A CN105601110A CN 105601110 A CN105601110 A CN 105601110A CN 201610022907 A CN201610022907 A CN 201610022907A CN 105601110 A CN105601110 A CN 105601110A
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parts
glaze
black silver
transmutation
black
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CN105601110B (en
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曾华晔
颜旭东
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FUJIAN QUANZHOU DESHENG GROUP Co Ltd
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FUJIAN QUANZHOU DESHENG GROUP Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • C03C8/04Frit compositions, i.e. in a powdered or comminuted form containing zinc
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes

Abstract

The invention relates to black silver drop reduced transmutation glaze, a black silver drop reduced transmutation glaze ceramic product prepared using the same and a preparation method and belongs to the technical field of ceramic. The black silver drop reduced transmutation glaze comprises, by mass, 33-36 parts of nepheline syenite, 18-22 parts of light calcium carbonate, 4-6 parts of barium carbonate, 2-4 parts of zinc oxide, 1-3 parts of magnesium carbonate, 9-12 pats of kaolin, 14-18 parts of waste ceramic biscuit treating material, 8-12 parts of quartz, 2-6 parts of bone ash, 2-8 parts of manganese oxide and 2-7 parts of copper oxide. The black silver drop reduced transmutation glaze is simple and easy in implementing of glazing mode, and production efficiency can be improved effectively; the black silver drop reduced transmutation glaze ceramic product prepared has pitch-black glaze surface and is modest luxury, and silver drops are adopted for decorating, so that the product is more noble and elegant; the product is calcined according to the method, finished product rate of the ceramic product can be up to higher than 92%, and the black silver drop reduced transmutation glaze is suitable for being used to produce ceramic for daily use and decorating ceramic.

Description

Black silver droplet reduction transmutation glazed pottery ceramic products and preparation method that black silver drips reduction furnace transmutation glaze and prepares with it
Technical field
The invention belongs to ceramic technology field, be specifically related to black silver droplet reduction transmutation glazed pottery ceramic products and preparation method that a kind of black silver drips reduction furnace transmutation glaze and prepares with it.
Background technology
Glaze is the nature of glass thin layer that covers billet surface, and its surface smoothing is glossy, and has the performance of waterproof difficult contamination, not only can improve the physical property of ceramic body, can also strengthen the outward appearance of beautifying ceramic. Black glaze has the glaze of black glossy, and general black glaze all need burn till at high temperature, and black glaze is favored by common people extensively because its glaze colours is unique.
Furnace transmutation glaze is that porcelain when burn till in kiln, owing to containing multiple pigmentation element in glaze, through oxidation or reduction, after kiln discharge, present beyond thought glaze chromatic effect, because its glaze colours is unexpected, form is special, people do not know again its principle, only know that roasting process changes and obtains in kiln, therefore be referred to as " transmutation ", common saying has " transmutation is unparalleled " to call it to change unpredictably, unique. Due to the uniqueness of furnace transmutation glaze and market prospects widely, people have also dropped into increasing concern to furnace transmutation glaze. And to fire the special and unique furnace transmutation glaze of a kind of glaze colours, need to spend a large amount of manpower and materials, and the yield rate of furnace transmutation glaze is generally on the low side. Although at present more about the report of black glaze, yet there are no the silver-colored relevant report of dripping furnace transmutation glaze of black.
The Chinese patent that is 200710193874.3 as application number discloses the preparation method of a kind of black glaze gold drip glaze and products thereof, although it discloses the preparation method of a kind of black glaze gold glaze of firing under higher temperature and products thereof, this glaze is done the end with black, decorate with golden yellow, wide adaptability, Heat stability is good, but the glazing techniques of this glaze is more loaded down with trivial details, need to go up respectively inside and outside glaze, caused certain inconvenience to production, the yield rate of the product making according to its preparation method is in addition also barely satisfactory.
Summary of the invention
The object of the invention is in order to solve the deficiencies in the prior art, and the black silver droplet reduction transmutation glazed pottery ceramic products and the preparation method that provide a kind of black silver to drip reduction furnace transmutation glaze and prepare with it, this black silver drips reduction furnace transmutation glaze and has pitch-black glaze, low-key, silver drips to be decorated, more aobvious noble atmosphere, and fire according to the inventive method, the yield rate of ceramic product is higher, is applicable to domestic ceramics and decorative porcelain.
The present invention adopts following technical scheme:
Black silver drips reduction furnace transmutation glaze, comprises the following component according to mass fraction meter: nepheline orthoclase 33-36 part, precipitated calcium carbonate 18-22 part, brium carbonate 4-6 part, zinc oxide 2-4 part, magnesium carbonate 1-3 part, kaolin 9-12 part, waste old ceramics biscuit are processed material 14-18 part, quartzy 8-12 part, bone ash 2-6 part, manganese oxide 2-8 part, cupric oxide 2-7 part.
Further, described black silver drips reduction furnace transmutation glaze, wherein said waste old ceramics biscuit is processed material and is obtained through following methods: waste old ceramics biscuit is crushed to 200-300 order, after add polyvinyl alcohol, stir, briquet under 0.5-0.8MPa, after be crushed to graininess, obtain waste old ceramics biscuit and process material, the mass ratio of the polyvinyl alcohol wherein adding and waste old ceramics biscuit is 1:5 ~ 1:9.
Further, described black silver drips reduction furnace transmutation glaze, comprises the following component according to mass fraction meter: 35 parts, nepheline orthoclase, 20.26 parts of precipitated calcium carbonates, 4.56 parts of brium carbonates, 2.93 parts, zinc oxide, 1.45 parts, magnesium carbonate, 10.06 parts of kaolin, waste old ceramics biscuit are processed 16 parts, material, 10.07 parts, quartz, 3 parts, bone ash, 5 parts of manganese oxide, 5 parts of cupric oxide.
Drip reduction furnace transmutation glaze with described black silver and prepare the silver-colored method of dripping reduction transmutation glazed pottery ceramic products of black, comprise the steps:
Step 1, the ball milling of getting the raw materials ready: according to described weight proportion, get nepheline orthoclase, precipitated calcium carbonate, brium carbonate, zinc oxide, magnesium carbonate, kaolin, waste old ceramics biscuit processing material, quartz, bone ash, manganese oxide, cupric oxide ready, above-mentioned each raw material is mixed, obtain compound, water is added in compound, after ball milling, sieve, obtain ball milling material;
Step 2, glaze slip is made: step 1 gained ball milling material is adjusted to 37-38 Baume degrees, stirs, obtain glaze slurry;
Step 3, soaks glaze: the biscuit of ceramics baking is in advance immersed in step 2 gained glaze slurry and carries out glazing, obtain ceramic first product;
Step 4, fire: step 3 gained ceramic first product is fired in reducing atmosphere, specifically burn till as follows: in 2h, be warming up to 405-415 DEG C, continue to heat up, in 2h, be warming up to 650-660 DEG C, continue to heat up, in 2h, be warming up to 960-970 DEG C, continue to heat up, be warming up to 1150-1155 DEG C with the heating rate of 1-1.3 DEG C/min again, then be warming up to 1265-1275 DEG C with the heating rate of 0.5-1 DEG C/min, insulation 1h, treat that nature is cooling, obtain described black silver and drip reduction transmutation glazed pottery ceramic products.
Further, describedly drip the method that reduction furnace transmutation glaze is prepared black silver and drip reduction transmutation glazed pottery ceramic products with black silver, wherein in step 1, after ball milling, cross 200-250 mesh sieve.
Further, the described method of preparing a black silver reduction transmutation glazed pottery ceramic products with a black silver reduction furnace transmutation glaze, wherein said biscuit of ceramics is Red Stone Ware or cosmetic soil biscuit.
The present invention also provides the black silver described in a kind of use to drip the black silver reduction transmutation glazed pottery ceramic products that reduction furnace transmutation glaze makes.
Compared with prior art, its beneficial effect is in the present invention:
The present invention utilizes waste old ceramics biscuit material, by waste old ceramics biscuit material is processed again, coordinate with other glaze afterwards and mix rear enamel frit makeing slurry, undertaken after glazing by soaking glaze mode, can drip reduction furnace transmutation glaze by get Hei Seyin through reductive firing, its glazing techniques is simple, can effectively enhance productivity, in addition, the black silver making according to the present invention drips reduction transmutation glazed pottery ceramic products and has pitch-black glaze, low-key, and adopt silver to drip decoration, more aobvious noble atmosphere, in sintering procedure, first adopt and be rapidly heated at short notice, reducing heating rate slowly heats up again, rear continuation increases heating rate and heats up, after reduce again heating rate and be slowly warming up to 1150-1155 DEG C, be warming up to 1265-1275 DEG C with the heating rate of 0.5-1 DEG C/min again, insulation 1h, make glaze between intensification cooling, form pitch-black glaze and make silver drip crystallization, thereby uniqueness and the aesthetic property of glaze are ensured, and fire according to the inventive method, the yield rate of ceramic product is higher, can be up to more than 92%, be applicable to producing domestic ceramics and decorative porcelain.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example is only for the present invention is described, and should not be considered as limiting scope of the present invention.
Embodiment 1
Black silver drips reduction furnace transmutation glaze, comprises the following component according to mass fraction meter: 35 parts, nepheline orthoclase, 20.26 parts of precipitated calcium carbonates, 4.56 parts of brium carbonates, 2.93 parts, zinc oxide, 1.45 parts, magnesium carbonate, 10.06 parts of kaolin, waste old ceramics biscuit are processed 16 parts, material, 10.07 parts, quartz, 3 parts, bone ash, 5 parts of manganese oxide, 5 parts of cupric oxide. Wherein said waste old ceramics biscuit is processed material and is obtained through following methods: waste old ceramics biscuit is crushed to 300 orders, after add polyvinyl alcohol, stir, briquet under 0.6MPa, after be crushed to graininess, obtain waste old ceramics biscuit and process material, the mass ratio of the polyvinyl alcohol wherein adding and waste old ceramics biscuit is 1:8.
Drip reduction furnace transmutation glaze with described black silver and prepare the silver-colored method of dripping reduction transmutation glazed pottery ceramic products of black, comprise the steps:
Step 1, the ball milling of getting the raw materials ready: according to described weight proportion, get nepheline orthoclase, precipitated calcium carbonate, brium carbonate, zinc oxide, magnesium carbonate, kaolin, waste old ceramics biscuit processing material, quartz, bone ash, manganese oxide, cupric oxide ready, above-mentioned each raw material is mixed, obtain compound, water is added in compound, after ball milling, cross 250 mesh sieves, obtain ball milling material;
Step 2, glaze slip is made: step 1 gained ball milling material is adjusted to 38 Baume degrees, stirs, obtain glaze slurry;
Step 3, soaks glaze: the biscuit of ceramics baking is in advance immersed in step 2 gained glaze slurry and carries out glazing, obtain ceramic first product, wherein said biscuit of ceramics is Red Stone Ware biscuit;
Step 4, fires: step 3 gained ceramic first product is fired in reducing atmosphere, specifically burnt till as follows: in 2h, be warming up to 410 DEG C, continue to heat up, in 2h, be warming up to 655 DEG C, continue to heat up, in 2h, be warming up to 965 DEG C, continue to heat up, be warming up to 1152 DEG C with the heating rate of 1.1 DEG C/min again, then be warming up to 1270 DEG C with the heating rate of 0.8 DEG C/min, insulation 1h, treat that nature is cooling, obtain described black silver and drip reduction transmutation glazed pottery ceramic products.
The black silver making according to the present embodiment drips its yield rate of reduction transmutation glazed pottery ceramic products can reach 95%, and it makes glaze have third dimension.
Embodiment 2
Black silver drips reduction furnace transmutation glaze, comprises the following component according to mass fraction meter: 33 parts, nepheline orthoclase, 18 parts of precipitated calcium carbonates, 4 parts of brium carbonates, 2 parts, zinc oxide, 1 part, magnesium carbonate, 9 parts of kaolin, waste old ceramics biscuit are processed 14 parts, material, 8 parts, quartz, 2 parts, bone ash, 2 parts of manganese oxide, 2 parts of cupric oxide. Wherein said waste old ceramics biscuit is processed material and is obtained through following methods: waste old ceramics biscuit is crushed to 200 orders, after add polyvinyl alcohol, stir, briquet under 0.5MPa, after be crushed to graininess, obtain waste old ceramics biscuit and process material, the mass ratio of the polyvinyl alcohol wherein adding and waste old ceramics biscuit is 1:5.
Drip reduction furnace transmutation glaze with described black silver and prepare the silver-colored method of dripping reduction transmutation glazed pottery ceramic products of black, comprise the steps:
Step 1, the ball milling of getting the raw materials ready: according to described weight proportion, get nepheline orthoclase, precipitated calcium carbonate, brium carbonate, zinc oxide, magnesium carbonate, kaolin, waste old ceramics biscuit processing material, quartz, bone ash, manganese oxide, cupric oxide ready, above-mentioned each raw material is mixed, obtain compound, water is added in compound, after ball milling, cross 200 mesh sieves, obtain ball milling material;
Step 2, glaze slip is made: step 1 gained ball milling material is adjusted to 37 Baume degrees, stirs, obtain glaze slurry;
Step 3, soaks glaze: the biscuit of ceramics baking is in advance immersed in step 2 gained glaze slurry and carries out glazing, obtain ceramic first product, wherein said biscuit of ceramics is cosmetic soil biscuit;
Step 4, fires: step 3 gained ceramic first product is fired in reducing atmosphere, specifically burnt till as follows: in 2h, be warming up to 405 DEG C, continue to heat up, in 2h, be warming up to 650 DEG C, continue to heat up, in 2h, be warming up to 960 DEG C, continue to heat up, be warming up to 1150 DEG C with the heating rate of 1 DEG C/min again, then be warming up to 1265 DEG C with the heating rate of 0.5 DEG C/min, insulation 1h, treat that nature is cooling, obtain described black silver and drip reduction transmutation glazed pottery ceramic products.
The black silver making according to the present embodiment drips its yield rate of reduction transmutation glazed pottery ceramic products can reach 93%, and it makes glaze have third dimension.
Embodiment 3
Black silver drips reduction furnace transmutation glaze, comprises the following component according to mass fraction meter: 36 parts, nepheline orthoclase, 22 parts of precipitated calcium carbonates, 6 parts of brium carbonates, 4 parts, zinc oxide, 3 parts, magnesium carbonate, 12 parts of kaolin, waste old ceramics biscuit are processed 18 parts, material, 12 parts, quartz, 6 parts, bone ash, 8 parts of manganese oxide, 7 parts of cupric oxide. Wherein said waste old ceramics biscuit is processed material and is obtained through following methods: waste old ceramics biscuit is crushed to 250 orders, after add polyvinyl alcohol, stir, briquet under 0.8MPa, after be crushed to graininess, obtain waste old ceramics biscuit and process material, the mass ratio of the polyvinyl alcohol wherein adding and waste old ceramics biscuit is 1:9.
Drip reduction furnace transmutation glaze with described black silver and prepare the silver-colored method of dripping reduction transmutation glazed pottery ceramic products of black, comprise the steps:
Step 1, the ball milling of getting the raw materials ready: according to described weight proportion, get nepheline orthoclase, precipitated calcium carbonate, brium carbonate, zinc oxide, magnesium carbonate, kaolin, waste old ceramics biscuit processing material, quartz, bone ash, manganese oxide, cupric oxide ready, above-mentioned each raw material is mixed, obtain compound, water is added in compound, after ball milling, cross 250 mesh sieves, obtain ball milling material;
Step 2, glaze slip is made: step 1 gained ball milling material is adjusted to 38 Baume degrees, stirs, obtain glaze slurry;
Step 3, soaks glaze: the biscuit of ceramics baking is in advance immersed in step 2 gained glaze slurry and carries out glazing, obtain ceramic first product, wherein said biscuit of ceramics is Red Stone Ware biscuit;
Step 4, fires: step 3 gained ceramic first product is fired in reducing atmosphere, specifically burnt till as follows: in 2h, be warming up to 415 DEG C, continue to heat up, in 2h, be warming up to 660 DEG C, continue to heat up, in 2h, be warming up to 970 DEG C, continue to heat up, be warming up to 1155 DEG C with the heating rate of 1.3 DEG C/min again, then be warming up to 1275 DEG C with the heating rate of 1 DEG C/min, insulation 1h, treat that nature is cooling, obtain described black silver and drip reduction transmutation glazed pottery ceramic products.
The black silver making according to the present embodiment drips its yield rate of reduction transmutation glazed pottery ceramic products can reach 92%, and it makes glaze have third dimension.
The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention. The claimed scope of the present invention is defined by appending claims and equivalent thereof.

Claims (7)

1. black silver drips reduction furnace transmutation glaze, it is characterized in that, comprise the following component according to mass fraction meter: nepheline orthoclase 33-36 part, precipitated calcium carbonate 18-22 part, brium carbonate 4-6 part, zinc oxide 2-4 part, magnesium carbonate 1-3 part, kaolin 9-12 part, waste old ceramics biscuit are processed material 14-18 part, quartzy 8-12 part, bone ash 2-6 part, manganese oxide 2-8 part, cupric oxide 2-7 part.
2. black silver according to claim 1 drips reduction furnace transmutation glaze, it is characterized in that, described waste old ceramics biscuit is processed material and is obtained through following methods: waste old ceramics biscuit is crushed to 200-300 order, after add polyvinyl alcohol, stir, briquet under 0.5-0.8MPa, after be crushed to graininess, obtain waste old ceramics biscuit and process material, the mass ratio of the polyvinyl alcohol wherein adding and waste old ceramics biscuit is 1:5 ~ 1:9.
3. black silver according to claim 1 drips reduction furnace transmutation glaze, it is characterized in that, comprise the following component according to mass fraction meter: 35 parts, nepheline orthoclase, 20.26 parts of precipitated calcium carbonates, 4.56 parts of brium carbonates, 2.93 parts, zinc oxide, 1.45 parts, magnesium carbonate, 10.06 parts of kaolin, waste old ceramics biscuit are processed 16 parts, material, 10.07 parts, quartz, 3 parts, bone ash, 5 parts of manganese oxide, 5 parts of cupric oxide.
4. drip with black silver described in claim 1 method that reduction furnace transmutation glaze is prepared a black silver reduction transmutation glazed pottery ceramic products, it is characterized in that, comprise the steps:
Step 1, the ball milling of getting the raw materials ready: according to described weight proportion, get nepheline orthoclase, precipitated calcium carbonate, brium carbonate, zinc oxide, magnesium carbonate, kaolin, waste old ceramics biscuit processing material, quartz, bone ash, manganese oxide, cupric oxide ready, above-mentioned each raw material is mixed, obtain compound, water is added in compound, after ball milling, sieve, obtain ball milling material;
Step 2, glaze slip is made: step 1 gained ball milling material is adjusted to 37-38 Baume degrees, stirs, obtain glaze slurry;
Step 3, soaks glaze: the biscuit of ceramics baking is in advance immersed in step 2 gained glaze slurry and carries out glazing, obtain ceramic first product;
Step 4, fire: step 3 gained ceramic first product is fired in reducing atmosphere, specifically burn till as follows: in 2h, be warming up to 405-415 DEG C, continue to heat up, in 2h, be warming up to 650-660 DEG C, continue to heat up, in 2h, be warming up to 960-970 DEG C, continue to heat up, be warming up to 1150-1155 DEG C with the heating rate of 1-1.3 DEG C/min again, then be warming up to 1265-1275 DEG C with the heating rate of 0.5-1 DEG C/min, insulation 1h, treat that nature is cooling, obtain described black silver and drip reduction transmutation glazed pottery ceramic products.
5. drip with black silver the method that reduction furnace transmutation glaze is prepared a black silver reduction transmutation glazed pottery ceramic products according to claim 4, it is characterized in that, in step 1, after ball milling, cross 200-250 mesh sieve.
6. drip with black silver the method that reduction furnace transmutation glaze is prepared a black silver reduction transmutation glazed pottery ceramic products according to claim 4, it is characterized in that, described biscuit of ceramics is Red Stone Ware or cosmetic soil biscuit.
7. drip reduction furnace transmutation glaze with black silver and prepare the black silver that method that black silver drips reduction transmutation glazed pottery ceramic products makes and drip reduction transmutation glazed pottery ceramic products by claimed in claim 4.
CN201610022907.7A 2016-01-14 2016-01-14 Black silver drop reduction furnace transmutation glaze and the black silver drop prepared with it restore transmutation glazed pottery ceramic products and preparation method Active CN105601110B (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
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CN106082670A (en) * 2016-06-22 2016-11-09 德化县太阳鸟工艺品有限公司 Foaming glaze and the glaze foamed ceramic made of it
CN106082670B (en) * 2016-06-22 2018-12-11 德化县太阳鸟工艺品有限公司 Foam glaze and the glaze paint foamed ceramic with its production
CN107540224A (en) * 2016-06-24 2018-01-05 江西省康舒陶瓷有限公司 A kind of animal bone Application way and heat-resistant porcelain glaze material formula
CN109095884A (en) * 2018-08-29 2018-12-28 巫贵豪 Build a preparation process
CN109095884B (en) * 2018-08-29 2021-06-15 巫贵豪 Process for preparing cup
CN110818259A (en) * 2019-12-10 2020-02-21 醴陵市良盛陶瓷制造有限公司 Dark devitrification reaction black glaze and preparation method thereof
CN111875344A (en) * 2020-06-28 2020-11-03 卓瑶养 Black-bottom silver drop building cup firing process
CN111875344B (en) * 2020-06-28 2022-07-08 卓瑶养 Black-bottom silver drop building cup firing process

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