CN105218165A - Dazzling iron rust glaze and by its dazzling iron rust glaze ceramic prepared and preparation method - Google Patents
Dazzling iron rust glaze and by its dazzling iron rust glaze ceramic prepared and preparation method Download PDFInfo
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Abstract
The present invention relates to a kind of dazzling iron rust glaze and by its dazzling iron rust glaze ceramic prepared and preparation method, belong to ceramic technology field.This dazzling iron rust glaze, comprises the following component according to mass fraction meter: nepheline syenite 40-50 part, quartzy 10-20 part, calcium carbonate 2-8 part, low temperature frit 18-22 part, zinc oxide 2-6 part, lime borate 8-13 part, manganese oxide 18-23 part, cupric oxide 1-4 part; Wherein, described low temperature frit comprises the following component according to mass fraction meter: borax 44-47 part, quartzy 28-32 part, potassium felspar sand 18-22 part, kaolin 2-7 part.This glaze can imitate iron rust outward appearance, makes ceramic surface not only can present iron rust outward appearance, also has glittering dazzling and be rich in relief silver bright spot; In addition, method sintering process provided by the invention is convenient to control, and be conducive to energy-conservation, and the yield rate of burning till product is higher.
Description
Technical field
The invention belongs to ceramic technology field, be specifically related to a kind of dazzling iron rust glaze and by its dazzling iron rust glaze ceramic prepared and preparation method.
Background technology
Glaze is the glassiness thin layer covering the billet surface such as pottery, enamel, and general glaze raw material used is that raw mineral materials such as quartz, feldspar, kaolin etc. mix according to a certain ratio with chemical additive, through grinding, glazing, the step such as to burn till and obtains.Glaze surface smoothing is glossy, and has waterproof performance of not easily staiing, and not only can improve the physicals of ceramic body, can also strengthen the outward appearance of beautifying ceramic.
Although ceramic technology development is in recent years also very rapid, the ceramic glaze of many excellent property profile graces batching and firing process is had to be known by the public, but at present about the glaze of iron rust glaze and the report of technique less, and about iron rust glaze glaze composition and firing condition to the quality of glaze and outward appearance also very important, glaze finally forms iron rust glaze through oxidization-reduction in sintering process, and a kind of ground-coat enamel is black, the dazzling iron rust glaze that glaze surface has the stereoscopic sensation of silver bright spot stronger effectively can make up dazzling iron rust glaze vacancy commercially.
Summary of the invention
The object of the invention is to solve the deficiencies in the prior art, and provide a kind of dazzling iron rust glaze and by its dazzling iron rust glaze ceramic prepared and preparation method, this dazzling iron rust glaze has good stereoscopic sensation and graceful outward appearance.
The present invention adopts following technical scheme:
A kind of dazzling iron rust glaze, comprises the following component according to mass fraction meter: nepheline syenite 40-50 part, quartzy 10-20 part, calcium carbonate 2-8 part, low temperature frit 18-22 part, zinc oxide 2-6 part, lime borate 8-13 part, manganese oxide 18-23 part, cupric oxide 1-4 part; Wherein, described low temperature frit comprises the following component according to mass fraction meter: borax 44-47 part, quartzy 28-32 part, potassium felspar sand 18-22 part, kaolin 2-7 part.
Further, described dazzling iron rust glaze, wherein said low temperature frit comprises the following component according to mass fraction meter: borax 45 parts, 30 parts, quartz, potassium felspar sand 20 parts, kaolin 5 parts.
Further, described dazzling iron rust glaze, comprises the following component according to mass fraction meter: nepheline syenite 45 parts, 15 parts, quartz, 5 parts, calcium carbonate, low temperature frit 20 parts, 5 parts, zinc oxide, lime borate 10 parts, manganese oxide 20 parts, cupric oxide 3 parts.
Prepare the method for dazzling iron rust glaze ceramic with described dazzling iron rust glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 60-65% carries out ball milling, Ball-milling Time 30-35h, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 41 °-44 ° of degree Beaume, obtains glaze slurry;
Step 3, glazing: obtain ceramic first product by carrying out glazing in the biscuit of ceramics baked immersion step 2 gained glaze slurry;
Step 4, fire: step 3 gained ceramic first product is fired, be warming up to 580-600 DEG C, constant temperature fires 55-65min, continues to be warming up to 1260-1280 DEG C, and constant temperature fires 170-185min, continue to be warming up to 1300-1315 DEG C, constant temperature fires 20-30min, rear standing, obtains described dazzling iron rust glaze ceramic.
Further, the described method preparing dazzling iron rust glaze ceramic with dazzling iron rust glaze, wherein the rotating speed of ball milling described in step one is 300-350r/min.
The dazzling iron rust glaze ceramic that a kind of method that the present invention also provides dazzling iron rust glaze to prepare dazzling iron rust glaze ceramic is obtained.
Compared with prior art, its beneficial effect is in the present invention:
The present invention is by meticulously allocating glaze proportioning, the glaze that ceramic ground-coat enamel is reddish black, glaze surface has the silver bright spot of dimpling can be made after obtaining a kind of burning till, and this glaze can imitate iron rust outward appearance, make ceramic surface not only can present iron rust outward appearance, also have glittering dazzling and be rich in relief silver bright spot; In addition, method sintering process provided by the invention is convenient to control, and adopt oxidation to burn till or reductive firing, be conducive to energy-conservation, and the yield rate of burning till product is higher, therefore, the present invention has a good application prospect and market outlook.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention, in the present invention, first prepare material according to the formula of low temperature frit, and then prepare burden according to glaze formula.
embodiment 1
A kind of dazzling iron rust glaze, comprises the following component according to mass fraction meter: nepheline syenite 45 parts, 15 parts, quartz, 5 parts, calcium carbonate, low temperature frit 20 parts, 5 parts, zinc oxide, lime borate 10 parts, manganese oxide 20 parts, cupric oxide 3 parts; Wherein, described low temperature frit comprises the following component according to mass fraction meter: borax 45 parts, 30 parts, quartz, potassium felspar sand 20 parts, kaolin 5 parts.
Prepare the method for dazzling iron rust glaze ceramic with described dazzling iron rust glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 65% carries out ball milling, Ball-milling Time 30h, and the rotating speed of ball milling is 350r/min, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 43 ° degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glazing gauge control is 1mm, obtains ceramic first product;
Step 4, fires: fired by step 3 gained ceramic first product, be warming up to 590 DEG C, constant temperature fires 60min, continue to be warming up to 1270 DEG C, constant temperature fires 180min, continues to be warming up to 1310 DEG C, constant temperature fires 25min, rear standing, obtains described dazzling iron rust glaze ceramic.
embodiment 2
A kind of dazzling iron rust glaze, comprises the following component according to mass fraction meter: nepheline syenite 40 parts, 10 parts, quartz, 2 parts, calcium carbonate, low temperature frit 18 parts, 2 parts, zinc oxide, lime borate 8 parts, manganese oxide 18 parts, cupric oxide 1 part; Wherein, described low temperature frit comprises the following component according to mass fraction meter: borax 44 parts, 28 parts, quartz, potassium felspar sand 18 parts, kaolin 2 parts.
Prepare the method for dazzling iron rust glaze ceramic with described dazzling iron rust glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 60% carries out ball milling, Ball-milling Time 30h, and the rotating speed of ball milling is 350r/min, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 41 ° degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glazing gauge control is 1.2mm, obtains ceramic first product;
Step 4, fires: fired by step 3 gained ceramic first product, be warming up to 580 DEG C, constant temperature fires 65min, continue to be warming up to 1260 DEG C, constant temperature fires 185min, continues to be warming up to 1300 DEG C, constant temperature fires 30min, rear standing, obtains described dazzling iron rust glaze ceramic.
embodiment 3
A kind of dazzling iron rust glaze, comprises the following component according to mass fraction meter: nepheline syenite 50 parts, 20 parts, quartz, 8 parts, calcium carbonate, low temperature frit 22 parts, 6 parts, zinc oxide, lime borate 13 parts, manganese oxide 23 parts, cupric oxide 4 parts; Wherein, described low temperature frit comprises the following component according to mass fraction meter: borax 47 parts, 32 parts, quartz, potassium felspar sand 22 parts, kaolin 7 parts.
Prepare the method for dazzling iron rust glaze ceramic with described dazzling iron rust glaze, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 65% carries out ball milling, Ball-milling Time 35h, and the rotating speed of ball milling is 300r/min, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 44 ° degree Beaume, obtains glaze slurry;
Step 3, glazing: immersed by the biscuit of ceramics baked in step 2 gained glaze slurry and carry out glazing, glazing gauge control is 1.3mm, obtains ceramic first product;
Step 4, fires: fired by step 3 gained ceramic first product, be warming up to 600 DEG C, constant temperature fires 55min, continue to be warming up to 1280 DEG C, constant temperature fires 170min, continues to be warming up to 1315 DEG C, constant temperature fires 20min, rear standing, obtains described dazzling iron rust glaze ceramic.
The ground-coat enamel of the dazzling iron rust glaze ceramic obtained according to glaze formula described in embodiment 1 to 3 and preparation method all can present reddish black, glaze surface all has the silver bright spot of dimpling.Therefore dazzling iron rust glaze of the present invention can make ceramic surface not only can present iron rust outward appearance, also has glittering dazzling and be rich in relief silver bright spot.
The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (6)
1. a dazzling iron rust glaze, it is characterized in that, comprise the following component according to mass fraction meter: nepheline syenite 40-50 part, quartzy 10-20 part, calcium carbonate 2-8 part, low temperature frit 18-22 part, zinc oxide 2-6 part, lime borate 8-13 part, manganese oxide 18-23 part, cupric oxide 1-4 part; Wherein, described low temperature frit comprises the following component according to mass fraction meter: borax 44-47 part, quartzy 28-32 part, potassium felspar sand 18-22 part, kaolin 2-7 part.
2. dazzling iron rust glaze according to claim 1, is characterized in that, described low temperature frit comprises the following component according to mass fraction meter: borax 45 parts, 30 parts, quartz, potassium felspar sand 20 parts, kaolin 5 parts.
3. dazzling iron rust glaze according to claim 1, it is characterized in that, comprise the following component according to mass fraction meter: nepheline syenite 45 parts, 15 parts, quartz, 5 parts, calcium carbonate, low temperature frit 20 parts, 5 parts, zinc oxide, lime borate 10 parts, manganese oxide 20 parts, cupric oxide 3 parts.
4. prepare the method for dazzling iron rust glaze ceramic with iron rust glaze dazzling described in claim 1, it is characterized in that, comprise the steps:
Step one, grinding: according to described weight proportion, after the mixing of each feed composition, then the water adding raw material gross weight 60-65% carries out ball milling, Ball-milling Time 30-35h, after to go out slurry for subsequent use;
Step 2, glaze concentration adjustment: add water in step one gained slurry, regulates concentration to 41 °-44 ° of degree Beaume, obtains glaze slurry;
Step 3, glazing: the biscuit of ceramics baked is immersed in step 2 gained glaze slurry and carry out glazing, obtain ceramic first product;
Step 4, fire: step 3 gained ceramic first product is fired, be warming up to 580-600 DEG C, constant temperature fires 55-65min, continues to be warming up to 1260-1280 DEG C, and constant temperature fires 170-185min, continue to be warming up to 1300-1315 DEG C, constant temperature fires 20-30min, rear standing, obtains described dazzling iron rust glaze ceramic.
5. the method preparing dazzling iron rust glaze ceramic with dazzling iron rust glaze according to claim 4, is characterized in that, the rotating speed of ball milling described in step one is 300-350r/min.
6. the dazzling iron rust glaze ceramic obtained by the method that dazzling iron rust glaze prepares dazzling iron rust glaze ceramic according to claim 4.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105601110A (en) * | 2016-01-14 | 2016-05-25 | 福建省泉州得盛集团有限公司 | Black silver drop reduced transmutation glaze, black silver drop reduced transmutation glaze ceramic product prepared using same and preparation method |
| CN106186700A (en) * | 2016-07-22 | 2016-12-07 | 福建省德化县华泰陶瓷有限公司 | Environmental protection shell pearl glaze, the environmental protection shell pearl glaze ceramic and preparation method thereof prepared with it |
| CN107777883A (en) * | 2016-08-31 | 2018-03-09 | 天津市中高科技有限公司 | The processing method of nitride ceramics glaze |
| CN108484111A (en) * | 2016-03-20 | 2018-09-04 | 德化县万盛陶瓷有限公司 | A kind of preparation method of imitative iron porcelain |
| CN108972352A (en) * | 2018-08-31 | 2018-12-11 | 张柳松 | A kind of production method that iron plate enamel decorative is drawn |
| CN109015395A (en) * | 2018-08-31 | 2018-12-18 | 张柳松 | A kind of production method of list glaze layer aluminium sheet decoration painting |
| CN109206014A (en) * | 2018-09-30 | 2019-01-15 | 湖南益嘉瓷业有限公司 | Iron oxidation glaze and preparation method thereof |
| CN109264995A (en) * | 2018-09-21 | 2019-01-25 | 醴陵市良盛陶瓷制造有限公司 | Iron rust mottled enamels and preparation method thereof |
| CN111689762A (en) * | 2020-06-15 | 2020-09-22 | 江苏省宜兴彩陶工艺厂 | Blank for crack glaze ceramic product |
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| US20080220960A1 (en) * | 2004-06-16 | 2008-09-11 | Jih-Hsin Tsai | Far infrared emitting nano glaze |
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| US20080220960A1 (en) * | 2004-06-16 | 2008-09-11 | Jih-Hsin Tsai | Far infrared emitting nano glaze |
| CN103183526A (en) * | 2011-12-28 | 2013-07-03 | 郑国明 | Rust glaze and method for making product thereof |
| CN103086747A (en) * | 2013-02-06 | 2013-05-08 | 陕西科技大学 | Preparation method of flare aventurine glaze |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105601110A (en) * | 2016-01-14 | 2016-05-25 | 福建省泉州得盛集团有限公司 | Black silver drop reduced transmutation glaze, black silver drop reduced transmutation glaze ceramic product prepared using same and preparation method |
| CN105601110B (en) * | 2016-01-14 | 2019-04-09 | 福建省泉州得盛集团有限公司 | Black silver drop reduction furnace transmutation glaze and the black silver drop prepared with it restore transmutation glazed pottery ceramic products and preparation method |
| CN108484111A (en) * | 2016-03-20 | 2018-09-04 | 德化县万盛陶瓷有限公司 | A kind of preparation method of imitative iron porcelain |
| CN108484111B (en) * | 2016-03-20 | 2021-07-20 | 德化县万盛陶瓷有限公司 | Preparation method of imitation iron porcelain |
| CN106186700B (en) * | 2016-07-22 | 2019-01-15 | 福建省德化县华泰陶瓷有限公司 | Environmentally friendly shell pearl glaze, environmental protection shell pearl glaze ceramic and preparation method thereof made from it |
| CN106186700A (en) * | 2016-07-22 | 2016-12-07 | 福建省德化县华泰陶瓷有限公司 | Environmental protection shell pearl glaze, the environmental protection shell pearl glaze ceramic and preparation method thereof prepared with it |
| CN107777883A (en) * | 2016-08-31 | 2018-03-09 | 天津市中高科技有限公司 | The processing method of nitride ceramics glaze |
| CN108972352A (en) * | 2018-08-31 | 2018-12-11 | 张柳松 | A kind of production method that iron plate enamel decorative is drawn |
| CN109015395A (en) * | 2018-08-31 | 2018-12-18 | 张柳松 | A kind of production method of list glaze layer aluminium sheet decoration painting |
| CN108972352B (en) * | 2018-08-31 | 2020-09-04 | 张柳松 | Method for making iron plate enamel decorative picture |
| CN109264995A (en) * | 2018-09-21 | 2019-01-25 | 醴陵市良盛陶瓷制造有限公司 | Iron rust mottled enamels and preparation method thereof |
| CN109206014A (en) * | 2018-09-30 | 2019-01-15 | 湖南益嘉瓷业有限公司 | Iron oxidation glaze and preparation method thereof |
| CN111689762A (en) * | 2020-06-15 | 2020-09-22 | 江苏省宜兴彩陶工艺厂 | Blank for crack glaze ceramic product |
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