CN106746655A - A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere - Google Patents
A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere Download PDFInfo
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- CN106746655A CN106746655A CN201611108150.XA CN201611108150A CN106746655A CN 106746655 A CN106746655 A CN 106746655A CN 201611108150 A CN201611108150 A CN 201611108150A CN 106746655 A CN106746655 A CN 106746655A
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- glaze
- pottery
- rough flambe
- glaze slip
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
A kind of method the invention discloses imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere, belongs to traditional ceramics technical field of material.A kind of method the invention discloses imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere, glaze based on potassium feldspar, quartz, calcite, talcum and nano cupric oxide are well mixed by a certain percentage, the micro-nano carbon compound of different proportion is added in base glaze and modified glaze is made, modified glaze is evenly coated at biscuit ware billet surface, imitative pottery rough flambe is obtained after dry, glaze firing.The present invention solves the problems, such as that traditional copper red vitreous enamel needs reducing atmosphere to prepare, and improves the stability of rough flambe, reduces the production cost of rough flambe, reaches environment-friendly and reducing energy consumption purpose.
Description
Technical field
The present invention relates to traditional ceramics technical field of material, and in particular to one kind is fired imitative under the conditions of oxidizing atmosphere
The method of pottery rough flambe.
Background technology
Pottery rough flambe has a long history, and is still considered as rarity by ceramic fan so far.Its glaze layer is mainly presented
Different degrees of is red or red inner purplish blue, and glossiness is excellent, and enamel is good, with not being the beautiful texture for surpassing jade.However, current city
Pottery rough flambe is produced on field and is required to reducing atmosphere, technique is difficult to control to, and existed certain dangerous.In addition, can also give ring
Bring pollution in border.In the last few years, some ceramists be also carried out a series of research to pottery rough flambe, were concentrated mainly on it
Colouration mechanism and feed change formula aspect, but the reducing atmosphere for using prepares pottery rough flambe, could not reach reduction
Production cost and the purpose of reduction environmental pollution.
Therefore, imitative pottery rough flambe is fired in research and development under the conditions of oxidizing atmosphere can energetically promote the development of pottery industry.
The content of the invention
The present invention fires the method for imitating pottery rough flambe under the conditions of providing a kind of oxidizing atmosphere, can solve in the prior art
Above mentioned problem.
Method the invention provides imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere, comprises the following steps：
(1) basic glaze slip is prepared：Potassium feldspar, quartz, calcite, talcum and nano cupric oxide are mixed in proportion simultaneously
Base glaze is prepared into, the water of the base glaze quality 55~65% is added, 200 mesh are finely ground to, basic glaze slip is obtained；
(2) biscuit ware base substrate is prepared：Ceramic body is put into Muffle furnace, under the conditions of oxidizing atmosphere, 890 DEG C of insulations
Furnace cooling obtains biscuit ware base substrate after 20min；
(3) modified glaze slip is prepared：Micro-nano carbon compound is added in the basic glaze slip and is well mixed and obtain modified glaze
Slurry；
(4) apply：The modified glaze slip is evenly coated at the surface of the biscuit ware base substrate；
(5) dry：The biscuit ware base substrate of coated modified glaze slip is put into air dry oven, in 50~70 DEG C of conditions
It is lower fully to dry；
(6) imitative pottery rough flambe is fired：Abundant dried biscuit ware base substrate is placed in Muffle furnace, 1250 are warming up to
~1300 DEG C, 10~45min is incubated, the glaze firing under the conditions of oxidizing atmosphere cools to room temperature taking-up with the furnace, obtains imitative pottery copper red
Glaze.
It is preferred that the preparation process of the base glaze is：By mass fraction be respectively 52.5~54.5% potassium feldspar,
18~20% quartz, 16~19% calcite, 8~11% talcum and 0.5~0.8% nano cupric oxide carry out ball milling
It is well mixed, 200 mesh sieves are crossed, obtained final product after fully drying.
It is preferred that the mass fraction is respectively：Potassium feldspar 53.7%, quartz 18.9%, calcite 16.8%, talcum
10%th, nano cupric oxide 0.6%.
It is preferred that the nano cupric oxide average grain diameter is 40nm.
It is preferred that the micro-nano carbon compound is carborundum and boron carbide, the average grain diameter of the carborundum is 30nm, institute
The average grain diameter for stating boron carbide is 1 μm.
It is preferred that the detailed process of the modified glaze slip of preparation is：Addition accounts for the parent glaze in the basic glaze slip
The carborundum and 0.005~0.01% boron carbide of quality 0.01~0.03% are expected, using magnetic stirring apparatus at 200 revs/min
Under conditions of stir 30min, be well mixed, be prepared into modified glaze slip.
It is preferred that the proportion of the modified glaze slip is 1.65~1.75g/cm3。
It is preferred that the thickness that the modified glaze slip is coated in the biscuit ware billet surface is 0.8~1.2mm.
It is preferred that the oxidizing atmosphere is air.
Compared with prior art, the beneficial effects of the invention are as follows：The invention provides a kind of new imitative pottery rough flambe side
Method, can realize firing rough flambe under the conditions of oxidizing atmosphere, can reach the mesh for reducing production cost and reducing environmental pollution
's.The present invention is realized with reduction effect pottery by simple equipment under oxidizing atmosphere and relatively low temperature conditionss
Rough flambe, largely improves the stability and controllability of rough flambe, and firing success rate is greatly improved.
Brief description of the drawings
Fig. 1 is the imitative pottery rough flambe design sketch of the embodiment of the present invention 1；
Fig. 2 is the imitative pottery rough flambe design sketch of the embodiment of the present invention 2；
Fig. 3 is the imitative pottery rough flambe design sketch of the embodiment of the present invention 3.
Specific embodiment
1-3, is described in detail to specific embodiment of the invention below in conjunction with the accompanying drawings, it is to be understood that of the invention
Protection domain is not limited by specific embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art are not having
There is the every other embodiment obtained on the premise of making creative work, belong to the scope of protection of the invention.
Embodiment 1：
A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere, comprises the following steps：
(1) basic glaze slip is prepared：Mass fraction is respectively 53.7% potassium feldspar, 18.9% quartz, 16.8%
Calcite, 10% talcum and 0.6% nano cupric oxide, carry out ball milling mixing uniformly, cross 200 mesh sieves, after fully drying i.e.
Obtain base glaze.The water of the base glaze quality 55% will be added in the base glaze, be finely ground to 200 mesh, compared
Weight is 1.65g/cm3Basic glaze slip.Wherein, nano cupric oxide average grain diameter is 40nm.
(2) biscuit ware base substrate is prepared：Ceramic body is put into Muffle furnace, under the conditions of air atmosphere, 890 DEG C of insulations
Furnace cooling obtains biscuit ware base substrate after 20min；
(3) modified glaze slip is prepared：Addition accounts for the carborundum of the base glaze quality 0.03% in the basic glaze slip
And 0.005% boron carbide, 30min is stirred under conditions of 200 revs/min using magnetic stirring apparatus, be well mixed, be prepared into
Modified glaze slip.Wherein, carborundum average grain diameter is 30nm, and boron carbide average grain diameter is 1 μm.
(4) apply：The modified glaze slip is evenly coated at the surface of the biscuit ware base substrate, glazed thickness is controlled
About 1mm.
(5) dry：The biscuit ware base substrate of coated modified glaze slip is put into air dry oven, is filled under the conditions of 60 DEG C
Divide drying；
(6) imitative pottery rough flambe is fired：Abundant dried biscuit ware base substrate is placed in Muffle furnace, 1270 are warming up to
DEG C, 20min is incubated, the glaze firing under the conditions of air atmosphere cools to room temperature taking-up with the furnace, imitative pottery rough flambe is obtained, such as Fig. 1 institutes
Show, glaze layer is mainly presented red.
Embodiment 2：
A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere, comprises the following steps：
(1) basic glaze slip is prepared：Mass fraction is respectively 54.5% potassium feldspar, 18% quartz, 19% side's solution
Stone, 8% talcum and 0.5% nano cupric oxide, carry out ball milling mixing uniformly, cross 200 mesh sieves, and base is obtained after fully drying
Plinth glaze.The water of the base glaze quality 60% will be added in the base glaze, be finely ground to 200 mesh, obtaining proportion is
1.70g/cm3Basic glaze slip.Wherein, nano cupric oxide average grain diameter is 40nm.
(2) biscuit ware base substrate is prepared：Ceramic body is put into Muffle furnace, under the conditions of air atmosphere, 890 DEG C of insulations
Furnace cooling obtains biscuit ware base substrate after 20min；
(3) modified glaze slip is prepared：Addition accounts for the carborundum of the base glaze quality 0.02% in the basic glaze slip
And 0.0075% boron carbide, 30min is stirred under conditions of 200 revs/min using magnetic stirring apparatus, be well mixed, prepare
Into modified glaze slip.Wherein, carborundum average grain diameter is 30nm, and boron carbide average grain diameter is 1 μm.
(4) apply：The modified glaze slip is evenly coated at the surface of the biscuit ware base substrate, glazed thickness is controlled
About 0.8mm.
(5) dry：The biscuit ware base substrate of coated modified glaze slip is put into air dry oven, is filled under the conditions of 70 DEG C
Divide drying；
(6) imitative pottery rough flambe is fired：Abundant dried biscuit ware base substrate is placed in Muffle furnace, 1250 are warming up to
DEG C, 45min is incubated, the glaze firing under the conditions of air atmosphere cools to room temperature taking-up with the furnace, imitative pottery rough flambe is obtained, such as Fig. 2 institutes
Show, glaze layer mainly present it is red in it is purplish blue.
Embodiment 3：
A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere, comprises the following steps：
(1) basic glaze slip is prepared：Mass fraction is respectively 52.5% potassium feldspar, 19.5% quartz, 16.2%
Calcite, 11% talcum and 0.8% nano cupric oxide, carry out ball milling mixing uniformly, cross 200 mesh sieves, after fully drying i.e.
Obtain base glaze.The water of the base glaze quality 65% will be added in the base glaze, be finely ground to 200 mesh, compared
Weight is 1.75g/cm3Basic glaze slip.Wherein, nano cupric oxide average grain diameter is 40nm.
(2) biscuit ware base substrate is prepared：Ceramic body is put into Muffle furnace, under the conditions of air atmosphere, 890 DEG C of insulations
Furnace cooling obtains biscuit ware base substrate after 20min；
(3) modified glaze slip is prepared：Addition accounts for the carborundum of the base glaze quality 0.01% in the basic glaze slip
And 0.01% boron carbide, 30min is stirred under conditions of 200 revs/min using magnetic stirring apparatus, be well mixed, be prepared into
Modified glaze slip.Wherein, carborundum average grain diameter is 30nm, and boron carbide average grain diameter is 1 μm.
(4) apply：The modified glaze slip is evenly coated at the surface of the biscuit ware base substrate, glazed thickness is controlled
About 1.2mm.
(5) dry：The biscuit ware base substrate of coated modified glaze slip is put into air dry oven, is filled under the conditions of 50 DEG C
Divide drying；
(6) imitative pottery rough flambe is fired：Abundant dried biscuit ware base substrate is placed in Muffle furnace, 1300 are warming up to
DEG C, 10min is incubated, the glaze firing under the conditions of oxidizing atmosphere cools to room temperature taking-up with the furnace, imitative pottery rough flambe is obtained, such as Fig. 3 institutes
Show, glaze layer mainly present it is red in it is purplish blue.
The invention provides a kind of new imitative pottery rough flambe method, can realize firing copper red under the conditions of oxidizing atmosphere
Glaze, can reach the purpose for reducing production cost and reducing environmental pollution.The present invention by simple equipment in oxidizing atmosphere and
Realized under relatively low temperature conditionss with reduction effect pottery rough flambe, largely improve the stability of rough flambe
And controllability, firing success rate is greatly improved.
Claims (9)
1. it is a kind of that the method for imitating pottery rough flambe is fired under the conditions of oxidizing atmosphere, it is characterised in that to comprise the following steps：
(1) basic glaze slip is prepared：Potassium feldspar, quartz, calcite, talcum and nano cupric oxide are mixed in proportion and prepared
Into base glaze, the water of the base glaze quality 55~65% is added, be finely ground to 200 mesh, obtain basic glaze slip；
(2) biscuit ware base substrate is prepared：Ceramic body is put into Muffle furnace, under the conditions of oxidizing atmosphere, 890 DEG C of insulations
Furnace cooling obtains biscuit ware base substrate after 20min；
(3) modified glaze slip is prepared：Micro-nano carbon compound is added in the basic glaze slip and is well mixed and obtain modified glaze slip；
(4) apply：The modified glaze slip is evenly coated at the surface of the biscuit ware base substrate；
(5) dry：The biscuit ware base substrate of coated modified glaze slip is put into air dry oven, is filled under the conditions of 50~70 DEG C
Divide drying；
(6) imitative pottery rough flambe is fired：Abundant dried biscuit ware base substrate is placed in Muffle furnace, it is warming up to 1250~
1300 DEG C, 10~45min is incubated, the glaze firing under the conditions of oxidizing atmosphere cools to room temperature taking-up with the furnace, obtains imitative pottery copper red
Glaze.
2. it is as claimed in claim 1 to fire the method for imitating pottery rough flambe, it is characterised in that the preparation step of the base glaze
Suddenly it is：By mass fraction be respectively 52.5~54.5% potassium feldspar, 18~20% quartz, 16~19% calcite, 8~
11% talcum and 0.5~0.8% nano cupric oxide carry out ball milling mixing uniformly, cross 200 mesh sieves, are obtained final product after fully drying.
3. it is as claimed in claim 2 to fire the method for imitating pottery rough flambe, it is characterised in that the mass fraction is respectively：
Potassium feldspar 53.7%, quartz 18.9%, calcite 16.8%, talcum 10%, nano cupric oxide 0.6%.
4. the method for the imitative pottery rough flambe of firing as described in claim 1-3 is any, it is characterised in that the nano cupric oxide
Average grain diameter is 40nm.
5. it is as claimed in claim 1 to fire the method for imitating pottery rough flambe, it is characterised in that the micro-nano carbon compound is carbon
SiClx and boron carbide, the average grain diameter of the carborundum is 30nm, and the average grain diameter of the boron carbide is 1 μm.
6. it is as claimed in claim 5 to fire the method for imitating pottery rough flambe, it is characterised in that the tool of the modified glaze slip of the preparation
Body process is：In the basic glaze slip addition account for the base glaze quality 0.01~0.03% carborundum and 0.005~
0.01% boron carbide, 30min is stirred using magnetic stirring apparatus under conditions of 200 revs/min, is well mixed, and is prepared into and is changed
Property glaze slip.
7. the as claimed in claim 6 method for firing imitative pottery rough flambe, it is characterised in that the proportion of the modified glaze slip is
1.65~1.75g/cm3。
8. it is as claimed in claim 1 to fire the method for imitating pottery rough flambe, it is characterised in that the modified glaze slip is coated in institute
The thickness for stating biscuit ware billet surface is 0.8~1.2mm.
9. it is as claimed in claim 1 to fire the method for imitating pottery rough flambe, it is characterised in that the oxidizing atmosphere is air.
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| CN201611108150.XA CN106746655A (en) | 2016-12-06 | 2016-12-06 | A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere |
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| CN201611108150.XA CN106746655A (en) | 2016-12-06 | 2016-12-06 | A kind of method that imitative pottery rough flambe is fired under the conditions of oxidizing atmosphere |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108285271A (en) * | 2018-04-12 | 2018-07-17 | 许昌学院 | A kind of method that original position vapour deposition process fires the red glaze of imitative an ancient unit of weight |
| CN109133629A (en) * | 2018-09-22 | 2019-01-04 | 醴陵市良盛陶瓷制造有限公司 | Unglazed unleaded metal glaze of copper red color and preparation method thereof |
| CN109896869A (en) * | 2019-04-04 | 2019-06-18 | 许昌学院 | A kind of golden yellow ceramic glaze and preparation method thereof |
| CN110577363A (en) * | 2019-10-21 | 2019-12-17 | 陕西科技大学 | Method for self-reduction imitation of Jun porcelain copper red glaze |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108285271A (en) * | 2018-04-12 | 2018-07-17 | 许昌学院 | A kind of method that original position vapour deposition process fires the red glaze of imitative an ancient unit of weight |
| CN108285271B (en) * | 2018-04-12 | 2020-07-24 | 许昌学院 | Method for firing jun-red-imitation glaze by in-situ vapor deposition method |
| CN109133629A (en) * | 2018-09-22 | 2019-01-04 | 醴陵市良盛陶瓷制造有限公司 | Unglazed unleaded metal glaze of copper red color and preparation method thereof |
| CN109896869A (en) * | 2019-04-04 | 2019-06-18 | 许昌学院 | A kind of golden yellow ceramic glaze and preparation method thereof |
| CN109896869B (en) * | 2019-04-04 | 2021-08-17 | 许昌学院 | Golden yellow ceramic glaze and preparation method thereof |
| CN110577363A (en) * | 2019-10-21 | 2019-12-17 | 陕西科技大学 | Method for self-reduction imitation of Jun porcelain copper red glaze |
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