CN107021632A - A kind of blue an ancient unit of weight fancy glaze - Google Patents
A kind of blue an ancient unit of weight fancy glaze Download PDFInfo
- Publication number
- CN107021632A CN107021632A CN201710375687.0A CN201710375687A CN107021632A CN 107021632 A CN107021632 A CN 107021632A CN 201710375687 A CN201710375687 A CN 201710375687A CN 107021632 A CN107021632 A CN 107021632A
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- parts
- glaze
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- blue
- ancient unit
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2204/00—Glasses, glazes or enamels with special properties
- C03C2204/04—Opaque glass, glaze or enamel
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2209/00—Compositions specially applicable for the manufacture of vitreous glazes
- C03C2209/02—Compositions specially applicable for the manufacture of vitreous glazes to produce non-uniformly coloured glazes
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
A kind of blue an ancient unit of weight fancy glaze, it is prepared from by the raw material of following parts by weight：37 43 parts of Bai Changshi, 15 21 parts of quartz, 9 15 parts of this medicine, 11 17 parts of calcite, 5.5 6.5 parts of Copper Ores, 7.5 8.5 parts of frit, 0.5 1.5 parts of cupric oxide, 0.5 1.5 parts of tin oxide.The present invention compared with prior art, only needs a glazing, you can burn out self-assembling formation reddish violet wire-drawing effect in blue an ancient unit of weight fancy glaze with a variety of glaze colours, its entire body sky blue, clean mark, beautiful in colour, with higher artistic value.
Description
Technical field
The present invention relates to a kind of glaze, and in particular to a kind of blue an ancient unit of weight fancy glaze.
Background technology
Pottery is one of five big kiln porcelain of China's Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, with unique transmutation
Art and be world-famous for, be the exclusive national treasure porcelain in Henan Province Xuchang Yuzhou City god Hou towns, have " the valuable an ancient unit of weight of gold is priceless " and
The good reputation of " there is ten thousand strings of cash in family, not as pottery one ".Glaze colours is that glaze is produced when passing through high-temperature fusion, with glaze formula with firing
Technique has important relationship.Blue glaze is one of traditional coloured glaze, is single colour glaze typically using natural earthy cobalt as main toner, tradition
Pottery orchid glaze can only be typically fired as blue, and can not be fired as the fancy glaze with a variety of glaze colours, and tone is relatively simple.
The content of the invention
The purpose of the present invention is that provides a kind of blue an ancient unit of weight fancy glaze to solve the deficiencies in the prior art.
The purpose of the present invention is realized with following technical proposals：
A kind of blue an ancient unit of weight fancy glaze, it is prepared from by the raw material of following parts by weight：37-43 parts of Bai Changshi, 15-21 parts of quartz, sheet
9-15 parts of medicine, 11-17 parts of calcite, 5.5-6.5 parts of Copper Ores, 7.5-8.5 parts of frit, 0.5-1.5 parts of cupric oxide, tin oxide
0.5-1.5 parts.
It is preferred that, it is prepared from by the raw material of following parts by weight：40 parts of Bai Changshi, 18 parts of quartz, 12 parts of this medicine, side
Solve 14 parts of stone, 6 parts of Copper Ores, 8 parts of frit, 1 part of cupric oxide, 1 part of tin oxide.
The preparation method of orchid an ancient unit of weight fancy glaze as described above, comprises the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1260-1300 DEG C.
Step（3）Middle firing process specifically includes following steps：1. heat of oxidation：Base substrate after glazing is put into kiln,
Fired under oxidizing atmosphere, temperature is ramped up 950-1000 DEG C in 3-4h；2. under reducing atmosphere, make temperature uniform in 4-5h
Rise to 1210-1260 DEG C；3. under reducing atmosphere, 1.5-2h is kept under the conditions of 1260-1300 DEG C；4. room temperature is cooled to, is made
.
The present invention compared with prior art, only needs a glazing, you can burn out blue an ancient unit of weight fancy glaze with a variety of glaze colours, its
Self-assembling formation reddish violet wire-drawing effect in entire body sky blue, it is clean mark, beautiful in colour, with higher artistic value.
Brief description of the drawings
Fig. 1 is blue an ancient unit of weight fancy glaze glaze schematic diagram that the embodiment of the present invention 2 is obtained.
Embodiment
Embodiment 1
A kind of blue an ancient unit of weight fancy glaze, is prepared from by the raw material of following parts by weight：37-43 parts of Bai Changshi, 15-21 parts of quartz, this medicine 9-
15 parts, 11-17 parts of calcite, 5.5-6.5 parts of Copper Ores, 7.5-8.5 parts of frit, 0.5-1.5 parts of cupric oxide, tin oxide 0.5-
1.5 part.
The preparation method of above-mentioned blue an ancient unit of weight fancy glaze, comprises the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1260-1280 DEG C；
Step（3）The middle firing process specific 1. heat of oxidation：Base substrate after glazing is put into kiln, is fired, is made under oxidizing atmosphere
Temperature is ramped up 950-1000 DEG C in 3-4h；2. under reducing atmosphere, temperature is made to be ramped up 1210-1260 DEG C in 4-5h；
3. under reducing atmosphere, 1.5-2h is kept under the conditions of 1260-1300 DEG C；4. room temperature is cooled to, is made.Highest is found in experiment
When firing temperature is less than 1250 DEG C, easily there is the uneven phenomenon of wire drawing, when firing temperature is more than 1320 DEG C, glaze mobility
By force, wire drawing texture is unintelligible, and yields is low.
White Silicon Dioxide In The Feldspar is 67% or so, and alumina content is 17% or so, and iron oxide content is 0.3% left
The right side, includes the calcium oxide and magnesia of certain content, is primary solvent, and calcite is cosolvent, and quartzy main component is two
Silica, improves the melting temperature of glaze and improves the mobility of glaze, the main hydrotropy of Copper Ores and pigmentation, frit are stable
Property it is strong, mainly for generation of wire-drawing effect in inventive formulation, preferably zinc frit in the present invention；Cupric oxide is used to increase
Color, tin oxide plays certain toning, and the glaze that above-mentioned raw materials are prepared from only needs a glazing, then molten in high-temperature firing
Melt under effect, produce unique transmutation glaze colours, be very attractive in appearance.White feldspar, calcite, quartz, Copper Ores are originated from the present embodiment
Yuzhou.
Embodiment 2
A kind of an ancient unit of weight fancy glaze, is prepared from by the raw material of following parts by weight：40 parts of Bai Changshi, 18 parts of quartz, 12 parts of this medicine, calcite
14 parts, 6 parts of Copper Ores, 8 parts of frit, 1 part of cupric oxide, 1 part of tin oxide.
The preparation method of above-mentioned blue an ancient unit of weight fancy glaze, comprises the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；Can be using mode glazings such as leaching glaze, pouring glaze, glaze sprayings；
（3）Burn till, specifically include the 1. heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is existed
3.5h is ramped up 980 DEG C；2. under reducing atmosphere, temperature is made to be ramped up 1240 DEG C in 4.5h；3. under reducing atmosphere, in
2h is kept under the conditions of 1280-1300 DEG C；4. room temperature is cooled to, is made.
Blue an ancient unit of weight fancy glaze glaze that the present embodiment is prepared is as shown in figure 1, glaze is smooth glossy, its entire body sky blue
In, alternate to have reddish violet or blue wire drawing striped, clean mark is beautiful in colour, with high artistic value.
Embodiment 3
A kind of an ancient unit of weight fancy glaze, is prepared from by the raw material of following parts by weight：43 parts of Bai Changshi, 18 parts of quartz, 14 parts of this medicine, calcite
14 parts, 6 parts of Copper Ores, 8 parts of frit, 1.2 parts of cupric oxide, 0.8 part of tin oxide.
The preparation method of above-mentioned blue an ancient unit of weight fancy glaze, comprises the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；Can be using mode glazings such as leaching glaze, pouring glaze, glaze sprayings；
（3）Burn till, specifically include the 1. heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is existed
4h is ramped up 1000 DEG C；2. under reducing atmosphere, temperature is made to be ramped up 1260 DEG C in 4h；3. under reducing atmosphere, in
2h is kept under the conditions of 1280 DEG C；4. room temperature is cooled to, is made.
Embodiment 4
A kind of an ancient unit of weight fancy glaze, is prepared from by the raw material of following parts by weight：40 parts of Bai Changshi, 15 parts of quartz, 15 parts of this medicine, calcite
14 parts, 6 parts of Copper Ores, 8 parts of frit, 1.2 parts of cupric oxide, 0.8 part of tin oxide.
The preparation method of above-mentioned blue an ancient unit of weight fancy glaze, comprises the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；Can be using mode glazings such as leaching glaze, pouring glaze, glaze sprayings；
（3）Burn till, specifically include the 1. heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is existed
3h is ramped up 950 DEG C；2. under reducing atmosphere, temperature is made to be ramped up 1210 DEG C in 5h；3. under reducing atmosphere, in
2h is kept under the conditions of 1260-1300 DEG C；4. room temperature is cooled to, is made.
Comparative example 1
A kind of an ancient unit of weight fancy glaze, is prepared from by the raw material of following parts by weight：40 parts of Bai Changshi, 15 parts of quartz, 12 parts of this medicine, calcite
14 parts, 6 parts of Copper Ores, 8 parts of frit, 1.5 parts of cupric oxide, 0.8 part of tin oxide；Preparation method be the same as Example 2.This example and embodiment
2 compare, and cupric oxide is different with the consumption of tin oxide, as a result find that the glaze glaze colour cast fired is dark.
Comparative example 2
A kind of an ancient unit of weight fancy glaze, is prepared from by the raw material of following parts by weight：40 parts of Bai Changshi, 15 parts of quartz, 12 parts of this medicine, calcite
14 parts, 6 parts of Copper Ores, 3 parts of frit, 1 part of cupric oxide, 1 part of tin oxide；Preparation method be the same as Example 2.This example and the phase of embodiment 2
Than the consumption of quartz and frit is changed, and glaze is more liquid, and wire drawing texture is unintelligible.
An ancient unit of weight fancy glaze formula that 5-20 of the embodiment of the present invention is provided is shown in Table 1-3.
Claims (4)
1. a kind of blue an ancient unit of weight fancy glaze, it is characterised in that：It is prepared from by the raw material of following parts by weight：37-43 parts of Bai Changshi, stone
15-21 parts of English, 9-15 parts of this medicine, 11-17 parts of calcite, 5.5-6.5 parts of Copper Ores, 7.5-8.5 parts of frit, cupric oxide 0.5-
1.5 parts, 0.5-1.5 parts of tin oxide.
2. orchid an ancient unit of weight fancy glaze as claimed in claim 1, it is characterised in that：It is prepared from by the raw material of following parts by weight：In vain
40 parts of feldspar, 18 parts of quartz, 12 parts of this medicine, 14 parts of calcite, 6 parts of Copper Ores, 8 parts of frit, 1 part of cupric oxide, 1 part of tin oxide.
3. the preparation method of blue an ancient unit of weight fancy glaze as described in claim any one of 1-2, it is characterised in that comprise the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1260-1300 DEG C.
4. the preparation method of orchid an ancient unit of weight fancy glaze as claimed in claim 3, it is characterised in that step（3）Middle firing process is specifically included
Following steps：1. heat of oxidation：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is uniformly risen in 3-4h
To 950-1000 DEG C；2. under reducing atmosphere, temperature is made to be ramped up 1210-1260 DEG C in 4-5h；3. under reducing atmosphere, in
1.5-2h is kept under the conditions of 1260-1300 DEG C；4. room temperature is cooled to, is made.
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| CN201710375687.0A CN107021632A (en) | 2017-05-24 | 2017-05-24 | A kind of blue an ancient unit of weight fancy glaze |
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| CN201710375687.0A CN107021632A (en) | 2017-05-24 | 2017-05-24 | A kind of blue an ancient unit of weight fancy glaze |
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ID=59529270
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107540223A (en) * | 2017-10-17 | 2018-01-05 | 禹州市锦丰源瓷业有限公司 | A kind of pottery jewel blue glaze of high rigidity and preparation method thereof |
| CN107540220A (en) * | 2017-10-12 | 2018-01-05 | 禹州市锦丰源瓷业有限公司 | A kind of Lu's chun glaze of blue tail band gold spot |
| CN107555796A (en) * | 2017-10-13 | 2018-01-09 | 禹州市锦丰源瓷业有限公司 | A kind of bluish white snowflake glaze of pottery |
| CN107572791A (en) * | 2017-10-16 | 2018-01-12 | 禹州市锦丰源瓷业有限公司 | A kind of imitation Song-Dynasty-style typeface orchid chun glaze |
| CN107572807A (en) * | 2017-10-17 | 2018-01-12 | 禹州市锦丰源瓷业有限公司 | A kind of hacking jewel blue glaze and preparation method thereof |
| CN107601888A (en) * | 2017-10-17 | 2018-01-19 | 禹州市锦丰源瓷业有限公司 | A kind of an ancient unit of weight fancy glaze and preparation method thereof |
| CN107619192A (en) * | 2017-10-17 | 2018-01-23 | 禹州市锦丰源瓷业有限公司 | A kind of new an ancient unit of weight fancy glaze and preparation method thereof |
| CN107721172A (en) * | 2017-10-17 | 2018-02-23 | 禹州市锦丰源瓷业有限公司 | A kind of high rigidity an ancient unit of weight fancy glaze and preparation method thereof |
| CN112479591A (en) * | 2020-12-24 | 2021-03-12 | 湖州海程塑业有限公司 | Sacrificial red glaze and preparation method thereof |
| CN113979636A (en) * | 2021-11-19 | 2022-01-28 | 禹州市神后镇孔家钧窑有限公司 | Copper series blue-green glaze and preparation method thereof |
| CN114524614A (en) * | 2021-12-24 | 2022-05-24 | 福建省威尔陶瓷股份有限公司 | Yunxiahua glaze and oxidation sintering method thereof |
| CN116589186A (en) * | 2023-05-12 | 2023-08-15 | 陕西科技大学 | Blue-grain Jin Banhua glaze and preparation method thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107540220A (en) * | 2017-10-12 | 2018-01-05 | 禹州市锦丰源瓷业有限公司 | A kind of Lu's chun glaze of blue tail band gold spot |
| CN107555796A (en) * | 2017-10-13 | 2018-01-09 | 禹州市锦丰源瓷业有限公司 | A kind of bluish white snowflake glaze of pottery |
| CN107572791A (en) * | 2017-10-16 | 2018-01-12 | 禹州市锦丰源瓷业有限公司 | A kind of imitation Song-Dynasty-style typeface orchid chun glaze |
| CN107619192A (en) * | 2017-10-17 | 2018-01-23 | 禹州市锦丰源瓷业有限公司 | A kind of new an ancient unit of weight fancy glaze and preparation method thereof |
| CN107572807A (en) * | 2017-10-17 | 2018-01-12 | 禹州市锦丰源瓷业有限公司 | A kind of hacking jewel blue glaze and preparation method thereof |
| CN107601888A (en) * | 2017-10-17 | 2018-01-19 | 禹州市锦丰源瓷业有限公司 | A kind of an ancient unit of weight fancy glaze and preparation method thereof |
| CN107540223A (en) * | 2017-10-17 | 2018-01-05 | 禹州市锦丰源瓷业有限公司 | A kind of pottery jewel blue glaze of high rigidity and preparation method thereof |
| CN107721172A (en) * | 2017-10-17 | 2018-02-23 | 禹州市锦丰源瓷业有限公司 | A kind of high rigidity an ancient unit of weight fancy glaze and preparation method thereof |
| CN112479591A (en) * | 2020-12-24 | 2021-03-12 | 湖州海程塑业有限公司 | Sacrificial red glaze and preparation method thereof |
| CN113979636A (en) * | 2021-11-19 | 2022-01-28 | 禹州市神后镇孔家钧窑有限公司 | Copper series blue-green glaze and preparation method thereof |
| CN113979636B (en) * | 2021-11-19 | 2023-06-20 | 禹州市神后镇孔家钧窑有限公司 | Copper blue glaze and preparation method thereof |
| CN114524614A (en) * | 2021-12-24 | 2022-05-24 | 福建省威尔陶瓷股份有限公司 | Yunxiahua glaze and oxidation sintering method thereof |
| CN116589186A (en) * | 2023-05-12 | 2023-08-15 | 陕西科技大学 | Blue-grain Jin Banhua glaze and preparation method thereof |
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