CN107098586A - A kind of red glaze of wire drawing and preparation method thereof - Google Patents

A kind of red glaze of wire drawing and preparation method thereof Download PDF

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Publication number
CN107098586A
CN107098586A CN201710375270.4A CN201710375270A CN107098586A CN 107098586 A CN107098586 A CN 107098586A CN 201710375270 A CN201710375270 A CN 201710375270A CN 107098586 A CN107098586 A CN 107098586A
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CN
China
Prior art keywords
parts
wire
glaze
talcum
red glaze
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Application number
CN201710375270.4A
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Chinese (zh)
Inventor
张占领
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Yuzhou City Jun Artifact Co Ltd
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Yuzhou City Jun Artifact Co Ltd
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Priority to CN201710375270.4A priority Critical patent/CN107098586A/en
Publication of CN107098586A publication Critical patent/CN107098586A/en
Withdrawn legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2209/00Compositions specially applicable for the manufacture of vitreous glazes
    • C03C2209/02Compositions specially applicable for the manufacture of vitreous glazes to produce non-uniformly coloured glazes

Abstract

The invention discloses red glaze of a kind of wire drawing and preparation method thereof, the red glaze of wire drawing is prepared from by the raw material of following parts by weight:45 55 parts of melilite, 46 parts of white feldspar, 10 14 parts of calcite, 24 parts of Copper Ores, 8 12 parts of quartz, 8 12 parts of this medicine, 1.5 2.5 parts of tin oxide, 3.5 5.5 parts of zinc oxide, 24 parts of talcum, 0.3 0.7 parts of cupric oxide, 46 parts of talcum of burning, blue or green 24 parts of alkali.Compared with prior art, the red glaze glaze colours jade-like stone profit of wire drawing, crackle are few, resistance to mechanical ability is strong, the characteristic trickled downwards in high-temperature calcination process using red glaze by the present invention, glazing just may occur in which a variety of wire-drawing effects, it is easy to make, the diversity of the red glaze of wire drawing is improved, its ornamental value is added.

Description

A kind of red glaze of wire drawing and preparation method thereof
Technical field
The present invention relates to pottery manufacturing technology field, and in particular to a kind of red glaze of wire drawing.
Background technology
Pottery is originated in the Eastern Han Dynasty, is one of five big kiln porcelain of Song Dynasty, the treasure in Chinese tradition technology in producing porcelain is referred to as National treasure, rarity.It is world-famous for unique transmutation art, is the exclusive national treasure porcelain in Henan Province Xuchang City Yuzhou City god Hou towns Device.Pottery is using glaze thickness as this, in its color or heavy glaze bottom or outstanding glaze or floating glaze table, and the thick muddy work of glaze, glaze layer opalescence jade-like stone profit, level is numerous Many work thoroughly are intended to drip, and third dimension is extremely strong.Red glaze in pottery is red and dense, moistens uniform, China and it is original, have tiny tortoise in glaze layer Crackle is managed, typically using cupric oxide as colouring agent, the rough flambe burnt till in reducing atmosphere.But red glaze is during high-temperature roasting Stream, and the red glaze dull coloring of an ancient unit of weight being made can be dropped down downwards.
The content of the invention
The invention provides red glaze of a kind of wire drawing and preparation method thereof with solve red glaze in high-temperature calcination process to flow down The problem of the problem of dropping down and an ancient unit of weight being made red glaze dull coloring.
The purpose of the present invention is realized with following technical proposals:
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:45-55 parts of melilite, white feldspar 4-6 parts, calcite 10-14 parts, it is 2-4 parts of Copper Ores, 8-12 parts of quartz, 8-12 parts of this medicine, 1.5-2.5 parts of tin oxide, 3.5-5.5 parts of zinc oxide, sliding 2-4 parts of stone, 0.3-0.7 parts of cupric oxide, 4-6 parts of talcum of burning, blue or green 2-4 parts of alkali.
It is preferred that, the red glaze of described wire drawing is prepared from by the raw material of following parts by weight:50 parts of melilite, white feldspar 5 Part, 12 parts of calcite, 3 parts of Copper Ores, 10 parts of quartz, 10 parts of this medicine, 2 parts of tin oxide, 4.5 parts of zinc oxide, 3 parts of talcum, oxidation 0.5 part of copper, 5 parts of talcum of burning, blue or green 3 parts of alkali.
The preparation method of the red glaze of described wire drawing, comprises the following steps:
(1)Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip;
(2)Glazing;
(3)Burn till, firing temperature is 1280-1300 DEG C.
It is preferred that, the preparation method step of the red glaze of described wire drawing(3)Middle firing process specifically includes following steps:1. oxygen The change phase:Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is ramped up 1000-1050 in 3.5-4h ℃;2. under reducing atmosphere, temperature is made to be ramped up 1280-1300 DEG C in 12-13h;3. under reducing atmosphere, in 1280- 3.5-4h is kept under the conditions of 1300 DEG C;4. room temperature is cooled to, is made.
Compared with prior art, the red glaze glaze colours jade-like stone profit of wire drawing, crackle are few, resistance to mechanical ability is strong, are existed using red glaze by the present invention The characteristic trickled downwards in high-temperature calcination process a, glazing just may occur in which a variety of wire-drawing effects, easy to make, improve drawing The diversity of the red glaze of silk, adds its ornamental value.
Brief description of the drawings
Fig. 1 is the red glaze glaze schematic diagram of wire drawing that the embodiment of the present invention 2 is obtained.
Embodiment
Embodiment 1
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:45-55 parts of melilite, white feldspar 4-6 parts, calcite 10-14 parts, it is 2-4 parts of Copper Ores, 8-12 parts of quartz, 8-12 parts of this medicine, 1.5-2.5 parts of tin oxide, 3.5-5.5 parts of zinc oxide, sliding 2-4 parts of stone, 0.3-0.7 parts of cupric oxide, 4-6 parts of talcum of burning, blue or green 2-4 parts of alkali.
The preparation method of the red glaze of above-mentioned wire drawing comprises the following steps:
(1)Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip;
(2)Glazing;
(3)Burn till, firing temperature is 1280-1300 DEG C.
Step(3)Middle firing process specifically includes following steps:1. heat of oxidation:Base substrate after glazing is put into kiln, Fired under oxidizing atmosphere, temperature is ramped up 1000-1050 DEG C in 3.5-4h;2. under reducing atmosphere, temperature is made in 12- 13h is ramped up 1280-1300 DEG C;3. under reducing atmosphere, 3.5-4h is kept under the conditions of 1280-1300 DEG C;4. it is cooled to Room temperature, is made.
The present invention is using melilite, white feldspar as primary solvent, and melilite dioxide-containing silica is 77% or so, aluminum oxide 13% Left and right, iron oxide 0.6%, magnesia 0.16%;White Silicon Dioxide In The Feldspar is 67% or so, and alumina content is 17% left The right side, iron oxide content is 0.3% or so, includes the calcium oxide and magnesia of certain content, calcite plays hydrotropy, quartz The mobility of glaze can be improved, tin oxide, zinc oxide are assistant toner, talcum plays hydrotropy and milkiness.Copper Ores rise main Hydrotropy and pigmentation.It is product after talcum high-temperature calcination to burn talcum, impure less, can improve tire glaze Percentage bound;Blue or green alkali is A kind of trona stone of Yuzhou, belongs to kaolinite class clay mineral, and silicon, aluminium content are higher, and outward appearance is in cyan, can improve glaze Expect mobility.
After above-mentioned raw materials are used cooperatively, first under oxidizing atmosphere, moisture in glaze, then under reducing atmosphere, glaze are excluded Face starts to melt glassing, and " transmutation " starts, reached after firing temperature, glaze reaches light, smoothly.By rational proportion and Control the atmosphere and temperature in sintering process, the red glaze of wire drawing prepared is red and dense, glaze colours jade-like stone profit, wire drawing length and it is distinct, into Product rate is higher.
Embodiment 2
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:50 parts of melilite, 5 parts of white feldspar, 12 parts of calcite, 3 parts of Copper Ores, 10 parts of quartz, 10 parts of this medicine, 2 parts of tin oxide, 4.5 parts of zinc oxide, 3 parts of talcum, 0.5 part of cupric oxide, burning talcum 5 Part, blue or green 3 parts of alkali.
The preparation method of the above-mentioned red glaze of wire drawing, comprises the following steps:
(1)Above-mentioned raw materials are added water mixing, ball milling crosses 250 mesh sieves, obtains glaze slip;
(2)Glazing;
(3)Burn till, specifically include following steps:1. heat of oxidation:Base substrate after glazing is put into kiln, is burnt under oxidizing atmosphere System, makes temperature be ramped up 1050 DEG C in 3.5h;2. under reducing atmosphere, temperature is made to be ramped up 1300 DEG C in 13h;3. also Under Primordial Qi atmosphere, 3.5h is kept under the conditions of 1300 DEG C;4. room temperature is cooled to, is made.
The red glaze of wire drawing obtained using said ratio and method is as shown in figure 1, by rational proportion and control sintering process In atmosphere, time and temperature, the red glaze glaze colours jade-like stone profit of the wire drawing prepared, bright in colour, crackle is few, wire drawing length and it is distinct, one Secondary glazing just may occur in which a variety of wire-drawing effects, improve the diversity of the red glaze of wire drawing, add its ornamental value, and finished product Rate up to 80%.
Comparative example 1
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:Red 50 parts of feldspar, 5 parts of white feldspar, 12 parts of calcite, 3 parts of Copper Ores, 10 parts of quartz, 10 parts of this medicine, 2 parts of tin oxide, 4.5 parts of zinc oxide, 3 parts of talcum, 0.5 part of cupric oxide, burning talcum 5 Part, blue or green 3 parts of alkali.Preparation method in preparation method be the same as Example 2.This example compared with Example 2, changes melilite in raw material into Red feldspar, the oil plant that red feldspar makes easily is precipitated, and firing glaze texture is poor, and yield rate only has 62% or so.
Comparative example 2
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:60 parts of melilite, 5 parts of white feldspar, 12 parts of calcite, 3 parts of Copper Ores, 2 parts of quartz, 10 parts of this medicine, 2 parts of tin oxide, 4.5 parts of zinc oxide, 3 parts of talcum, 0.5 part of cupric oxide, burning talcum 5 Part, blue or green 3 parts of alkali.Preparation method in preparation method be the same as Example 2.This example is compared with Example 2 compared with melilite in raw material Parts by weight increase 60 parts, and quartzy parts by weight have been reduced to 2 parts, and pinprick, finished product are easily formed in this formula sintering procedure Rate only has 70% or so.
Comparative example 3
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:50 parts of melilite, 5 parts of white feldspar, 12 parts of calcite, 3 parts of Copper Ores, 10 parts of quartz, 10 parts of this medicine, 4.5 parts of zinc oxide, 3 parts of talcum, 0.5 part of cupric oxide, 5 parts of talcum of burning, blue or green alkali 3 Part.Preparation method in preparation method be the same as Example 2.This example is compared with Example 2 compared with unused tin oxide, is fired in raw material Into the easy yellowing of glaze color and luster, yield rate only has 60% or so.
Comparative example 4
A kind of red glaze of wire drawing, is prepared from by the raw material of following parts by weight:50 parts of melilite, 5 parts of white feldspar, 12 parts of calcite, 3 parts of Copper Ores, 10 parts of quartz, 10 parts of this medicine, 2 parts of tin oxide, 4.5 parts of zinc oxide, 3 parts of talcum, 0.5 part of cupric oxide, burning talcum 5 Part.Preparation method in preparation method be the same as Example 2.This example is compared with Example 2 compared with unused green grass or young crops alkali, is fired into raw material Glaze easily there is drying shrinkage or go out pinprick, yield rate only has 66% or so.
The red glaze formula of wire drawing that 3-25 of the embodiment of the present invention is provided is shown in Table 1-4, and its preparation method is same as Example 2.

Claims (4)

1. a kind of red glaze of wire drawing, it is characterised in that:It is prepared from by the raw material of following parts by weight:It is 45-55 parts of melilite, white 4-6 parts of feldspar, 10-14 parts of calcite, 2-4 parts of Copper Ores, 8-12 parts of quartz, 8-12 parts of this medicine, 1.5-2.5 parts of tin oxide, oxygen Change 3.5-5.5 parts of zinc, 2-4 parts of talcum, 0.3-0.7 parts of cupric oxide, 4-6 parts of talcum of burning, blue or green 2-4 parts of alkali.
2. the red glaze of wire drawing according to claim 1, it is characterised in that:It is prepared from by the raw material of following parts by weight: 50 parts of melilite, 5 parts of white feldspar, 12 parts of calcite, 3 parts of Copper Ores, 10 parts of quartz, 10 parts of this medicine, 2 parts of tin oxide, zinc oxide 4.5 parts, 3 parts of talcum, 0.5 part of cupric oxide, burn 5 parts of talcum, blue or green 3 parts of alkali.
3. a kind of preparation method of the red glaze of wire drawing as claimed in claim 1 or 2, it is characterised in that comprise the following steps:
(1)Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip;
(2)Glazing;
(3)Burn till, firing temperature is 1280-1300 DEG C.
4. the preparation method of the red glaze of wire drawing as claimed in claim 3, it is characterised in that step(3)Middle firing process is specifically included Following steps:1. heat of oxidation:Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, is made temperature uniform in 3.5-4h Rise to 1000-1050 DEG C;2. under reducing atmosphere, temperature is made to be ramped up 1280-1300 DEG C in 12-13h;3. in reducing atmosphere Under, 3.5-4h is kept under the conditions of 1280-1300 DEG C;4. room temperature is cooled to, is made.
CN201710375270.4A 2017-05-24 2017-05-24 A kind of red glaze of wire drawing and preparation method thereof Withdrawn CN107098586A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107663022A (en) * 2017-09-28 2018-02-06 禹州市正玉钧窑有限公司 A kind of reddish black pottery glaze and preparation method thereof
CN107673615A (en) * 2017-10-12 2018-02-09 禹州市锦丰源瓷业有限公司 A kind of hacking Lu chun glaze

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106007380A (en) * 2016-05-27 2016-10-12 高根长 Red glaze and preparation method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106007380A (en) * 2016-05-27 2016-10-12 高根长 Red glaze and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
孙彦春 等: "《中国钧窑研究与探索》", 31 July 2011, 中国古籍出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107663022A (en) * 2017-09-28 2018-02-06 禹州市正玉钧窑有限公司 A kind of reddish black pottery glaze and preparation method thereof
CN107663022B (en) * 2017-09-28 2020-06-26 禹州市正玉钧窑有限公司 Celeste jun porcelain glaze and preparation method thereof
CN107673615A (en) * 2017-10-12 2018-02-09 禹州市锦丰源瓷业有限公司 A kind of hacking Lu chun glaze

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