CN107601888A - A kind of an ancient unit of weight fancy glaze and preparation method thereof - Google Patents
A kind of an ancient unit of weight fancy glaze and preparation method thereof Download PDFInfo
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- CN107601888A CN107601888A CN201710967070.8A CN201710967070A CN107601888A CN 107601888 A CN107601888 A CN 107601888A CN 201710967070 A CN201710967070 A CN 201710967070A CN 107601888 A CN107601888 A CN 107601888A
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Abstract
The invention discloses a kind of an ancient unit of weight fancy glaze, and it is prepared by the raw material of following parts by weight：16 24 parts of Bai Changshi, 12 18 parts of quartz, 12 18 parts of calcite, 24 32 parts of this medicine, 24 parts of talcum, 10 14 parts of frit, 46 parts of zinc oxide, 0.5 1.5 parts of tin oxide, 0.3 0.7 parts of cupric oxide, 24 parts of wood ash, 12 parts of black wool soil.The preparation method of described an ancient unit of weight fancy glaze, comprises the following steps：（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52 54%, and wet-milling 56 hours, the slurry by wet-milling crosses 200 300 mesh sieves and obtains glaze slip；（2）Base substrate leaching glaze 12 times；（3）Burn till, firing temperature is 1,280 1300 DEG C.
Description
Technical field
The present invention relates to pottery manufacturing technology field, and in particular to a kind of an ancient unit of weight fancy glaze and preparation method thereof.
Background technology
Pottery is originated in the Eastern Han Dynasty, is one of five big kiln porcelain of Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, is referred to as
National treasure, rarity.It is world-famous for the transmutation art of uniqueness, is known as " the valuable an ancient unit of weight of gold is priceless " and " there is ten thousand strings of cash in family, not as pottery
One " good reputation.
Pottery is the exclusive national treasure porcelain in Henan Province Xuchang City Yuzhou City god Hou towns, by its simple and unsophisticated moulding, consummate
Technique, the complicated magical transmutation, the beautiful scenery of lakes and mountains, rosy clouds fog, people's beast flower, bird, insect, and fish etc. with glaze, " it is color to enter kiln kiln discharge ten thousand of the same colour "
Varied figure color and marvellous charm, it is described as first of Chinese " five big porcelain ".
An ancient unit of weight fancy glaze in pottery is the glaze that can play magic.It can become multicolored imbibition, can become variegated, also may be used
To become the pattern for having meaning, the even traditional Chinese Painting similar to enjoyable formula.And everything, it is because of the gene of an ancient unit of weight fancy glaze polychrome entirely
With fuzzy individual character, because of kiln fire, freely folding is galloped with mysterious.In the prior art, the formula of an ancient unit of weight fancy glaze and its preparation side
Method is also seldom, and firing is not easy.The product for having 60% or so during firing can be scrapped, and yield rate is low, therefore to raw material
Waste it is huge, cost of manufacture is too high.
The content of the invention
The invention provides a kind of raw material and an ancient unit of weight fancy glaze of science and preparation method thereof is matched to solve existing an ancient unit of weight fancy glaze
Formula and preparation method are few, and yield rate is low, the problem of cost of manufacture and high manufacture difficulty.
The purpose of the present invention is realized with following technical proposals：
A kind of an ancient unit of weight fancy glaze, it is prepared by the raw material of following parts by weight：Bai Changshi 16-24 parts, quartzy 12-18 parts, Fang Xie
Stone 12-18 parts, this medicine 24-32 parts, talcum 2-4 parts, frit 10-14 parts, zinc oxide 4-6 parts, tin oxide 0.5-1.5 parts, oxidation
Copper 0.3-0.7 parts, wood ash 2-4 parts, black wool soil 1-2 parts.
Preferably, described an ancient unit of weight fancy glaze, it is prepared by the raw material of following parts by weight：20 parts of Bai Changshi, quartz 15
Part, 15 parts of calcite, 28 parts of this medicine, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, wood ash
3 parts, 1.5 parts of black wool soil.
The preparation method of described an ancient unit of weight fancy glaze, comprises the following steps：
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52-54%,
Wet-milling 5-6 hours, the slurry by wet-milling cross 200-300 mesh sieves and obtain glaze slip；
(2) base substrate leaching glaze 1-2 times；
(3) burn till, firing temperature is 1280-1300 DEG C.
Preferably, the preparation method of described an ancient unit of weight fancy glaze, firing process specifically comprises the following steps in step (3)：
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1000- in 4-6 hours
1050℃；2. temperature under reducing atmosphere, is set to be ramped up 1280-1300 DEG C within 5-6 hours；
3. annealing is cooled to room temperature, it is made.
Beneficial effects of the present invention are as follows：
1st, the invention discloses a kind of formula and preparation method of an ancient unit of weight fancy glaze, it can fire what is stablized by this technical scheme
An ancient unit of weight fancy glaze, the unique color mixed in aubergine and cyan.The raw material of product is using local abundant mineral, by matching somebody with somebody for science
Formed than being fired with rational process debugging, in colour-stable, yield rate 90% or so, realize the comprehensive utilization of resource, moreover it is possible to
Cost is reduced, there is positive economic benefit.
2nd, the calcium crystallization and not molten quartz particles that glaze is formed during high-temperature firing send out the light into glaze layer
Raw scattering, the suspension plus wood ash to glaze, can increase the milkiness sense of glaze layer.Black wool soil has good plasticity and bonding
Property, cause the risk of rupture so as to reduce the crackle increase in sintering.U.S.A of an ancient unit of weight fancy glaze is unique color and figure
Case, sight and reserve value are high, have sizable market prospects.The application of an ancient unit of weight fancy glaze, may advantageously facilitate ceramics
The raising of industrial generic technology, promote local economic development.
Brief description of the drawings
Fig. 1 is an ancient unit of weight fancy glaze schematic diagram that the embodiment of the present invention 2 obtains.
Embodiment
Embodiment 1
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight：Bai Changshi 16-24 parts, quartzy 12-18 parts, calcite 12-
18 parts, this medicine 24-32 parts, talcum 2-4 parts, frit 10-14 parts, zinc oxide 4-6 parts, tin oxide 0.5-1.5 parts, cupric oxide 0.3-
0.7 part, wood ash 2-4 parts, black wool soil 1-2 parts.
The preparation method of above-mentioned an ancient unit of weight fancy glaze comprises the following steps：
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52-54%,
Wet-milling 5-6 hours, the slurry by wet-milling cross 200-300 mesh sieves and obtain glaze slip；
(2) base substrate leaching glaze 1-2 times；
(3) burn till, firing temperature is 1280-1300 DEG C.
Firing process specifically comprises the following steps in step (3)：
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1000- in 4-6 hours
1050℃；2. temperature under reducing atmosphere, is set to be ramped up 1280-1300 DEG C within 5-6 hours；
3. annealing is cooled to room temperature, it is made.
The present invention is using white feldspar and this medicine as primary solvent, and white feldspar dioxide-containing silica is 67% or so, and aluminum oxide contains
Measure as 17% or so, iron oxide 0.3% or so, include the calcium oxide and magnesia of certain content.This medicine is Yuzhou
A kind of natural feldspar, main component are silica, and iron-holder is higher, are solubilizer.Calcite mainly reduces glaze melting temperature
Degree, the refractive index of glaze can be increased in glaze, thus improve glossiness, and the translucency of glaze can be improved.Quartz plays skeleton function,
The melting temperature of glaze is improved, increases the glossiness of glaze, the mobility of glaze can be improved.Talcum is natural hydrous magnesium silicate ore deposit
Thing, it is the cosolvent of glaze.Frit of the present invention mainly contains boron oxide, the effect of main landing low melting point.Zinc oxide and tin oxide
For assistant toner, main helps glaze slip color development to act on.Cupric oxide plays main pigmentation, makes color and luster more bright-coloured.Wood ash plays
Milkiness acts on.Black wool soil aluminium content is higher, has higher plasticity and caking property, plays suspension effect, can improve the matter of glaze
Sense.By the atmosphere and temperature in rational proportion and control sintering process, an ancient unit of weight fancy glaze prepared mixes in aubergine and cyan
Unique color, have very high art and economic value.
Embodiment 2
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight：20 parts of Bai Changshi, 15 parts of quartz, 15 parts of calcite, this medicine
28 parts, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.
The preparation method of above-mentioned an ancient unit of weight fancy glaze, comprises the following steps：
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52%, wet-milling
5 hours, the slurry by wet-milling crossed 250 mesh sieves and obtains glaze slip；
(2) base substrate leaching glaze 2 times；
(3) burn till, specifically comprise the following steps：
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature was ramped up 1020 DEG C at 5 hours；
2. temperature under reducing atmosphere, is set to be ramped up 1290 DEG C in 6 hours；
3. annealing is cooled to room temperature, it is made.
By the atmosphere and temperature in rational proportion and control sintering process, an ancient unit of weight fancy glaze prepared is in aubergine and cyan
The unique color of mixing, it so makes widely known unlike simple " red ", unlike simple " green grass or young crops " is so simple and elegant, but causes vast and uses up
It is precise and tiny, the high Ming Er roads golden mean of the Confucian school, complexity is both obscured, and it is careful clear.Individual character and calm apperance without distinctness, but have bold and unrestrained
Passion and gentle affinity.
Comparative example 1
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight：20 parts of melilite, 15 parts of quartz, 15 parts of calcite, this medicine
28 parts, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.System
Preparation Method is the same as embodiment 2.This example using melilite compared with Example 2 compared with instead of white feldspar.Melilite compares white feldspar,
Silicon and iron content are high, and aluminium content is low.It is not high using glaze mobility after melilite, easily precipitate, product is more yielding, yield rate
Only 82% or so.
Comparative example 2
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight：20 parts of Bai Changshi, 15 parts of quartz, 15 parts of calcite, this medicine
28 parts, 3 parts of talcum, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.Preparation method is the same as real
Apply example 2.This example is compared with Example 2 compared with unused frit in raw material.Because lacking the wire drawing effect of frit, the product being fired into
Color is more uniform, and the unique color for aubergine and the cyan mixing not gone out in current embodiment 2, yield rate only has 77% or so.
Comparative example 3
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight：40 parts of Bai Changshi, 15 parts of quartz, 15 parts of calcite, this medicine
8 parts, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.Prepare
Method is the same as embodiment 2.This example is compared with Example 2 compared with the usage amount of white feldspar increases to 40 parts, and the usage amount of this medicine is reduced to
8 parts.Pinprick is more readily formed in this example compared with embodiment 2 in sintering procedure, yield rate only has 78%.
The formula for an ancient unit of weight fancy glaze that 3-26 of the embodiment of the present invention is provided is shown in Table 1-4, and its preparation method is the same as embodiment 2.
Table 1
| Raw material | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | Embodiment 7 | Embodiment 8 |
| Bai Changshi | 20 | 16 | 24 | 17 | 24 | 20 |
| Quartz | 12 | 15 | 18 | 13 | 12 | 18 |
| Calcite | 18 | 15 | 14 | 15 | 12 | 12 |
| This medicine | 32 | 28 | 24 | 25 | 32 | 24 |
| Talcum | 2 | 3 | 4 | 2 | 4 | 3 |
| Frit | 10 | 11 | 12 | 13 | 14 | 14 |
| Zinc oxide | 6 | 5 | 4 | 6 | 4 | 5 |
| Tin oxide | 1 | 0.5 | 1.5 | 0.7 | 1 | 1.5 |
| Cupric oxide | 0.5 | 0.3 | 0.7 | 0.3 | 0.4 | 0.5 |
| Wood ash | 3 | 2 | 4 | 3 | 4 | 2 |
| Black wool soil | 1 | 2 | 1.5 | 2 | 1.5 | 1 |
Table 2
Table 3
| Raw material | Embodiment 15 | Embodiment 16 | Embodiment 17 | Embodiment 18 | Embodiment 19 | Embodiment 20 |
| Bai Changshi | 24 | 16 | 20 | 21 | 20 | 24 |
| Quartz | 15 | 18 | 12 | 16 | 18 | 12 |
| Calcite | 15 | 12 | 17 | 18 | 17 | 15 |
| This medicine | 28 | 32 | 24 | 29 | 32 | 24 |
| Talcum | 4 | 2 | 3 | 4 | 3 | 2 |
| Frit | 12 | 11 | 12 | 14 | 10 | 13 |
| Zinc oxide | 4 | 5 | 6 | 4 | 6 | 5 |
| Tin oxide | 1.5 | 0.5 | 1 | 1.1 | 1.5 | 1 |
| Cupric oxide | 0.3 | 0.7 | 0.5 | 0.3 | 0.5 | 0.3 |
| Wood ash | 4 | 3 | 2 | 4 | 2 | 3 |
| Black wool soil | 1.5 | 1 | 2 | 1.5 | 2 | 1 |
Table 4
Claims (4)
- A kind of 1. an ancient unit of weight fancy glaze, it is characterised in that：It is prepared by the raw material of following parts by weight：Bai Changshi 16-24 parts, quartz 12-18 parts, calcite 12-18 parts, this medicine 24-32 parts, talcum 2-4 parts, frit 10-14 parts, zinc oxide 4-6 parts, tin oxide 0.5-1.5 parts, cupric oxide 0.3-0.7 parts, wood ash 2-4 parts, black wool soil 1-2 parts.
- 2. an ancient unit of weight fancy glaze according to claim 1, it is characterised in that：It is prepared by the raw material of following parts by weight：In vain 20 parts of feldspar, 15 parts of quartz, 15 parts of calcite, 28 parts of this medicine, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, oxygen Change 0.5 part of copper, 3 parts of wood ash, 1.5 parts of black wool soil.
- 3. a kind of preparation method of an ancient unit of weight fancy glaze as claimed in claim 1 or 2, it is characterised in that comprise the following steps：（1）Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52-54%, wet 5-6 hours are ground, the slurry by wet-milling crosses 200-300 mesh sieves and obtains glaze slip；（2）Base substrate leaching glaze 1-2 times；（3）Burn till, firing temperature is 1280-1300 DEG C.
- 4. the preparation method of an ancient unit of weight fancy glaze described in claim 3, it is characterised in that step（3）Middle firing process specifically includes as follows Step：1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1000- in 4-6 hours 1050℃；2. temperature under reducing atmosphere, is set to be ramped up 1280-1300 DEG C within 5-6 hours；3. annealing is cooled to room temperature, it is made.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109095773A (en) * | 2018-10-11 | 2018-12-28 | 周彩云 | A kind of pottery white opaque glaze |
| CN109111117A (en) * | 2018-10-11 | 2019-01-01 | 周彩云 | A kind of red glaze of pottery using flyash |
| CN110255910A (en) * | 2019-07-16 | 2019-09-20 | 禹州大唐钧瓷文化有限公司 | A kind of pottery Lu Jun fancy glaze and its preparation and method for cooking |
| CN112279514A (en) * | 2020-11-24 | 2021-01-29 | 禹州大唐钧瓷文化有限公司 | Glaze for firing Tanghua glaze and method for preparing porcelain by adopting glaze for firing Tanghua glaze |
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| CN106145683A (en) * | 2016-08-18 | 2016-11-23 | 温书强 | A kind of peacock blue pottery glaze and preparation method thereof |
| CN107010834A (en) * | 2017-05-24 | 2017-08-04 | 禹州市神器钧窑有限公司 | A kind of Lu's chun glaze |
| CN107021632A (en) * | 2017-05-24 | 2017-08-08 | 禹州市神器钧窑有限公司 | A kind of blue an ancient unit of weight fancy glaze |
| CN107056053A (en) * | 2017-05-24 | 2017-08-18 | 禹州市神器钧窑有限公司 | A kind of pottery jade glaze |
| CN107098589A (en) * | 2017-05-24 | 2017-08-29 | 禹州市神器钧窑有限公司 | A kind of new blue an ancient unit of weight fancy glaze |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106145683A (en) * | 2016-08-18 | 2016-11-23 | 温书强 | A kind of peacock blue pottery glaze and preparation method thereof |
| CN107010834A (en) * | 2017-05-24 | 2017-08-04 | 禹州市神器钧窑有限公司 | A kind of Lu's chun glaze |
| CN107021632A (en) * | 2017-05-24 | 2017-08-08 | 禹州市神器钧窑有限公司 | A kind of blue an ancient unit of weight fancy glaze |
| CN107056053A (en) * | 2017-05-24 | 2017-08-18 | 禹州市神器钧窑有限公司 | A kind of pottery jade glaze |
| CN107098589A (en) * | 2017-05-24 | 2017-08-29 | 禹州市神器钧窑有限公司 | A kind of new blue an ancient unit of weight fancy glaze |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109095773A (en) * | 2018-10-11 | 2018-12-28 | 周彩云 | A kind of pottery white opaque glaze |
| CN109111117A (en) * | 2018-10-11 | 2019-01-01 | 周彩云 | A kind of red glaze of pottery using flyash |
| CN110255910A (en) * | 2019-07-16 | 2019-09-20 | 禹州大唐钧瓷文化有限公司 | A kind of pottery Lu Jun fancy glaze and its preparation and method for cooking |
| CN112279514A (en) * | 2020-11-24 | 2021-01-29 | 禹州大唐钧瓷文化有限公司 | Glaze for firing Tanghua glaze and method for preparing porcelain by adopting glaze for firing Tanghua glaze |
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Application publication date: 20180119 |