CN107601888A - A kind of an ancient unit of weight fancy glaze and preparation method thereof - Google Patents

A kind of an ancient unit of weight fancy glaze and preparation method thereof Download PDF

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Publication number
CN107601888A
CN107601888A CN201710967070.8A CN201710967070A CN107601888A CN 107601888 A CN107601888 A CN 107601888A CN 201710967070 A CN201710967070 A CN 201710967070A CN 107601888 A CN107601888 A CN 107601888A
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China
Prior art keywords
parts
glaze
weight
ancient unit
fancy glaze
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Withdrawn
Application number
CN201710967070.8A
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Chinese (zh)
Inventor
崔松伟
温红超
崔世豪
崔鹏豪
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Yuzhou Jinfeng Ceramic Industry Co Ltd
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Yuzhou Jinfeng Ceramic Industry Co Ltd
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Priority to CN201710967070.8A priority Critical patent/CN107601888A/en
Publication of CN107601888A publication Critical patent/CN107601888A/en
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Abstract

The invention discloses a kind of an ancient unit of weight fancy glaze, and it is prepared by the raw material of following parts by weight:16 24 parts of Bai Changshi, 12 18 parts of quartz, 12 18 parts of calcite, 24 32 parts of this medicine, 24 parts of talcum, 10 14 parts of frit, 46 parts of zinc oxide, 0.5 1.5 parts of tin oxide, 0.3 0.7 parts of cupric oxide, 24 parts of wood ash, 12 parts of black wool soil.The preparation method of described an ancient unit of weight fancy glaze, comprises the following steps:(1)Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52 54%, and wet-milling 56 hours, the slurry by wet-milling crosses 200 300 mesh sieves and obtains glaze slip;(2)Base substrate leaching glaze 12 times;(3)Burn till, firing temperature is 1,280 1300 DEG C.

Description

A kind of an ancient unit of weight fancy glaze and preparation method thereof
Technical field
The present invention relates to pottery manufacturing technology field, and in particular to a kind of an ancient unit of weight fancy glaze and preparation method thereof.
Background technology
Pottery is originated in the Eastern Han Dynasty, is one of five big kiln porcelain of Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, is referred to as National treasure, rarity.It is world-famous for the transmutation art of uniqueness, is known as " the valuable an ancient unit of weight of gold is priceless " and " there is ten thousand strings of cash in family, not as pottery One " good reputation.
Pottery is the exclusive national treasure porcelain in Henan Province Xuchang City Yuzhou City god Hou towns, by its simple and unsophisticated moulding, consummate Technique, the complicated magical transmutation, the beautiful scenery of lakes and mountains, rosy clouds fog, people's beast flower, bird, insect, and fish etc. with glaze, " it is color to enter kiln kiln discharge ten thousand of the same colour " Varied figure color and marvellous charm, it is described as first of Chinese " five big porcelain ".
An ancient unit of weight fancy glaze in pottery is the glaze that can play magic.It can become multicolored imbibition, can become variegated, also may be used To become the pattern for having meaning, the even traditional Chinese Painting similar to enjoyable formula.And everything, it is because of the gene of an ancient unit of weight fancy glaze polychrome entirely With fuzzy individual character, because of kiln fire, freely folding is galloped with mysterious.In the prior art, the formula of an ancient unit of weight fancy glaze and its preparation side Method is also seldom, and firing is not easy.The product for having 60% or so during firing can be scrapped, and yield rate is low, therefore to raw material Waste it is huge, cost of manufacture is too high.
The content of the invention
The invention provides a kind of raw material and an ancient unit of weight fancy glaze of science and preparation method thereof is matched to solve existing an ancient unit of weight fancy glaze Formula and preparation method are few, and yield rate is low, the problem of cost of manufacture and high manufacture difficulty.
The purpose of the present invention is realized with following technical proposals:
A kind of an ancient unit of weight fancy glaze, it is prepared by the raw material of following parts by weight:Bai Changshi 16-24 parts, quartzy 12-18 parts, Fang Xie Stone 12-18 parts, this medicine 24-32 parts, talcum 2-4 parts, frit 10-14 parts, zinc oxide 4-6 parts, tin oxide 0.5-1.5 parts, oxidation Copper 0.3-0.7 parts, wood ash 2-4 parts, black wool soil 1-2 parts.
Preferably, described an ancient unit of weight fancy glaze, it is prepared by the raw material of following parts by weight:20 parts of Bai Changshi, quartz 15 Part, 15 parts of calcite, 28 parts of this medicine, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, wood ash 3 parts, 1.5 parts of black wool soil.
The preparation method of described an ancient unit of weight fancy glaze, comprises the following steps:
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52-54%, Wet-milling 5-6 hours, the slurry by wet-milling cross 200-300 mesh sieves and obtain glaze slip;
(2) base substrate leaching glaze 1-2 times;
(3) burn till, firing temperature is 1280-1300 DEG C.
Preferably, the preparation method of described an ancient unit of weight fancy glaze, firing process specifically comprises the following steps in step (3):
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1000- in 4-6 hours 1050℃;2. temperature under reducing atmosphere, is set to be ramped up 1280-1300 DEG C within 5-6 hours;
3. annealing is cooled to room temperature, it is made.
Beneficial effects of the present invention are as follows:
1st, the invention discloses a kind of formula and preparation method of an ancient unit of weight fancy glaze, it can fire what is stablized by this technical scheme An ancient unit of weight fancy glaze, the unique color mixed in aubergine and cyan.The raw material of product is using local abundant mineral, by matching somebody with somebody for science Formed than being fired with rational process debugging, in colour-stable, yield rate 90% or so, realize the comprehensive utilization of resource, moreover it is possible to Cost is reduced, there is positive economic benefit.
2nd, the calcium crystallization and not molten quartz particles that glaze is formed during high-temperature firing send out the light into glaze layer Raw scattering, the suspension plus wood ash to glaze, can increase the milkiness sense of glaze layer.Black wool soil has good plasticity and bonding Property, cause the risk of rupture so as to reduce the crackle increase in sintering.U.S.A of an ancient unit of weight fancy glaze is unique color and figure Case, sight and reserve value are high, have sizable market prospects.The application of an ancient unit of weight fancy glaze, may advantageously facilitate ceramics The raising of industrial generic technology, promote local economic development.
Brief description of the drawings
Fig. 1 is an ancient unit of weight fancy glaze schematic diagram that the embodiment of the present invention 2 obtains.
Embodiment
Embodiment 1
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight:Bai Changshi 16-24 parts, quartzy 12-18 parts, calcite 12- 18 parts, this medicine 24-32 parts, talcum 2-4 parts, frit 10-14 parts, zinc oxide 4-6 parts, tin oxide 0.5-1.5 parts, cupric oxide 0.3- 0.7 part, wood ash 2-4 parts, black wool soil 1-2 parts.
The preparation method of above-mentioned an ancient unit of weight fancy glaze comprises the following steps:
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52-54%, Wet-milling 5-6 hours, the slurry by wet-milling cross 200-300 mesh sieves and obtain glaze slip;
(2) base substrate leaching glaze 1-2 times;
(3) burn till, firing temperature is 1280-1300 DEG C.
Firing process specifically comprises the following steps in step (3):
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1000- in 4-6 hours 1050℃;2. temperature under reducing atmosphere, is set to be ramped up 1280-1300 DEG C within 5-6 hours;
3. annealing is cooled to room temperature, it is made.
The present invention is using white feldspar and this medicine as primary solvent, and white feldspar dioxide-containing silica is 67% or so, and aluminum oxide contains Measure as 17% or so, iron oxide 0.3% or so, include the calcium oxide and magnesia of certain content.This medicine is Yuzhou A kind of natural feldspar, main component are silica, and iron-holder is higher, are solubilizer.Calcite mainly reduces glaze melting temperature Degree, the refractive index of glaze can be increased in glaze, thus improve glossiness, and the translucency of glaze can be improved.Quartz plays skeleton function, The melting temperature of glaze is improved, increases the glossiness of glaze, the mobility of glaze can be improved.Talcum is natural hydrous magnesium silicate ore deposit Thing, it is the cosolvent of glaze.Frit of the present invention mainly contains boron oxide, the effect of main landing low melting point.Zinc oxide and tin oxide For assistant toner, main helps glaze slip color development to act on.Cupric oxide plays main pigmentation, makes color and luster more bright-coloured.Wood ash plays Milkiness acts on.Black wool soil aluminium content is higher, has higher plasticity and caking property, plays suspension effect, can improve the matter of glaze Sense.By the atmosphere and temperature in rational proportion and control sintering process, an ancient unit of weight fancy glaze prepared mixes in aubergine and cyan Unique color, have very high art and economic value.
Embodiment 2
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight:20 parts of Bai Changshi, 15 parts of quartz, 15 parts of calcite, this medicine 28 parts, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.
The preparation method of above-mentioned an ancient unit of weight fancy glaze, comprises the following steps:
(1) mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52%, wet-milling 5 hours, the slurry by wet-milling crossed 250 mesh sieves and obtains glaze slip;
(2) base substrate leaching glaze 2 times;
(3) burn till, specifically comprise the following steps:
1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature was ramped up 1020 DEG C at 5 hours;
2. temperature under reducing atmosphere, is set to be ramped up 1290 DEG C in 6 hours;
3. annealing is cooled to room temperature, it is made.
By the atmosphere and temperature in rational proportion and control sintering process, an ancient unit of weight fancy glaze prepared is in aubergine and cyan The unique color of mixing, it so makes widely known unlike simple " red ", unlike simple " green grass or young crops " is so simple and elegant, but causes vast and uses up It is precise and tiny, the high Ming Er roads golden mean of the Confucian school, complexity is both obscured, and it is careful clear.Individual character and calm apperance without distinctness, but have bold and unrestrained Passion and gentle affinity.
Comparative example 1
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight:20 parts of melilite, 15 parts of quartz, 15 parts of calcite, this medicine 28 parts, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.System Preparation Method is the same as embodiment 2.This example using melilite compared with Example 2 compared with instead of white feldspar.Melilite compares white feldspar, Silicon and iron content are high, and aluminium content is low.It is not high using glaze mobility after melilite, easily precipitate, product is more yielding, yield rate Only 82% or so.
Comparative example 2
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight:20 parts of Bai Changshi, 15 parts of quartz, 15 parts of calcite, this medicine 28 parts, 3 parts of talcum, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.Preparation method is the same as real Apply example 2.This example is compared with Example 2 compared with unused frit in raw material.Because lacking the wire drawing effect of frit, the product being fired into Color is more uniform, and the unique color for aubergine and the cyan mixing not gone out in current embodiment 2, yield rate only has 77% or so.
Comparative example 3
A kind of an ancient unit of weight fancy glaze, is prepared by the raw material of following parts by weight:40 parts of Bai Changshi, 15 parts of quartz, 15 parts of calcite, this medicine 8 parts, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, 0.5 part of cupric oxide, 3 parts of wood ash, black wool soil 1.5 parts.Prepare Method is the same as embodiment 2.This example is compared with Example 2 compared with the usage amount of white feldspar increases to 40 parts, and the usage amount of this medicine is reduced to 8 parts.Pinprick is more readily formed in this example compared with embodiment 2 in sintering procedure, yield rate only has 78%.
The formula for an ancient unit of weight fancy glaze that 3-26 of the embodiment of the present invention is provided is shown in Table 1-4, and its preparation method is the same as embodiment 2.
Table 1
Raw material Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6 Embodiment 7 Embodiment 8
Bai Changshi 20 16 24 17 24 20
Quartz 12 15 18 13 12 18
Calcite 18 15 14 15 12 12
This medicine 32 28 24 25 32 24
Talcum 2 3 4 2 4 3
Frit 10 11 12 13 14 14
Zinc oxide 6 5 4 6 4 5
Tin oxide 1 0.5 1.5 0.7 1 1.5
Cupric oxide 0.5 0.3 0.7 0.3 0.4 0.5
Wood ash 3 2 4 3 4 2
Black wool soil 1 2 1.5 2 1.5 1
Table 2
Table 3
Raw material Embodiment 15 Embodiment 16 Embodiment 17 Embodiment 18 Embodiment 19 Embodiment 20
Bai Changshi 24 16 20 21 20 24
Quartz 15 18 12 16 18 12
Calcite 15 12 17 18 17 15
This medicine 28 32 24 29 32 24
Talcum 4 2 3 4 3 2
Frit 12 11 12 14 10 13
Zinc oxide 4 5 6 4 6 5
Tin oxide 1.5 0.5 1 1.1 1.5 1
Cupric oxide 0.3 0.7 0.5 0.3 0.5 0.3
Wood ash 4 3 2 4 2 3
Black wool soil 1.5 1 2 1.5 2 1
Table 4

Claims (4)

  1. A kind of 1. an ancient unit of weight fancy glaze, it is characterised in that:It is prepared by the raw material of following parts by weight:Bai Changshi 16-24 parts, quartz 12-18 parts, calcite 12-18 parts, this medicine 24-32 parts, talcum 2-4 parts, frit 10-14 parts, zinc oxide 4-6 parts, tin oxide 0.5-1.5 parts, cupric oxide 0.3-0.7 parts, wood ash 2-4 parts, black wool soil 1-2 parts.
  2. 2. an ancient unit of weight fancy glaze according to claim 1, it is characterised in that:It is prepared by the raw material of following parts by weight:In vain 20 parts of feldspar, 15 parts of quartz, 15 parts of calcite, 28 parts of this medicine, 3 parts of talcum, 12 parts of frit, 5 parts of zinc oxide, 1 part of tin oxide, oxygen Change 0.5 part of copper, 3 parts of wood ash, 1.5 parts of black wool soil.
  3. 3. a kind of preparation method of an ancient unit of weight fancy glaze as claimed in claim 1 or 2, it is characterised in that comprise the following steps:
    (1)Mixing is put into ball mill ball milling after above-mentioned raw materials are crushed, and adding water makes the mass concentration of glaze reach 52-54%, wet 5-6 hours are ground, the slurry by wet-milling crosses 200-300 mesh sieves and obtains glaze slip;
    (2)Base substrate leaching glaze 1-2 times;
    (3)Burn till, firing temperature is 1280-1300 DEG C.
  4. 4. the preparation method of an ancient unit of weight fancy glaze described in claim 3, it is characterised in that step(3)Middle firing process specifically includes as follows Step:
    1. the base substrate after glazing is put into kiln, fired under oxidizing atmosphere, temperature is ramped up 1000- in 4-6 hours 1050℃;
    2. temperature under reducing atmosphere, is set to be ramped up 1280-1300 DEG C within 5-6 hours;
    3. annealing is cooled to room temperature, it is made.
CN201710967070.8A 2017-10-17 2017-10-17 A kind of an ancient unit of weight fancy glaze and preparation method thereof Withdrawn CN107601888A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109095773A (en) * 2018-10-11 2018-12-28 周彩云 A kind of pottery white opaque glaze
CN109111117A (en) * 2018-10-11 2019-01-01 周彩云 A kind of red glaze of pottery using flyash
CN110255910A (en) * 2019-07-16 2019-09-20 禹州大唐钧瓷文化有限公司 A kind of pottery Lu Jun fancy glaze and its preparation and method for cooking

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106145683A (en) * 2016-08-18 2016-11-23 温书强 A kind of peacock blue pottery glaze and preparation method thereof
CN107010834A (en) * 2017-05-24 2017-08-04 禹州市神器钧窑有限公司 A kind of Lu's chun glaze
CN107021632A (en) * 2017-05-24 2017-08-08 禹州市神器钧窑有限公司 A kind of blue an ancient unit of weight fancy glaze
CN107056053A (en) * 2017-05-24 2017-08-18 禹州市神器钧窑有限公司 A kind of pottery jade glaze
CN107098589A (en) * 2017-05-24 2017-08-29 禹州市神器钧窑有限公司 A kind of new blue an ancient unit of weight fancy glaze

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106145683A (en) * 2016-08-18 2016-11-23 温书强 A kind of peacock blue pottery glaze and preparation method thereof
CN107010834A (en) * 2017-05-24 2017-08-04 禹州市神器钧窑有限公司 A kind of Lu's chun glaze
CN107021632A (en) * 2017-05-24 2017-08-08 禹州市神器钧窑有限公司 A kind of blue an ancient unit of weight fancy glaze
CN107056053A (en) * 2017-05-24 2017-08-18 禹州市神器钧窑有限公司 A kind of pottery jade glaze
CN107098589A (en) * 2017-05-24 2017-08-29 禹州市神器钧窑有限公司 A kind of new blue an ancient unit of weight fancy glaze

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109095773A (en) * 2018-10-11 2018-12-28 周彩云 A kind of pottery white opaque glaze
CN109111117A (en) * 2018-10-11 2019-01-01 周彩云 A kind of red glaze of pottery using flyash
CN110255910A (en) * 2019-07-16 2019-09-20 禹州大唐钧瓷文化有限公司 A kind of pottery Lu Jun fancy glaze and its preparation and method for cooking

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Application publication date: 20180119