CN105218167A - A kind of preparation method of blue and white material decoration Nixing pottery - Google Patents
A kind of preparation method of blue and white material decoration Nixing pottery Download PDFInfo
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Abstract
The invention discloses a kind of preparation method of blue and white material decoration Nixing pottery, it comprises the steps: 1) prepare blank: blank is made up of the raw material of following weight parts proportioning: 50 ~ 60 parts, eastern mud, 30 ~ 40 parts, western mud, kaolin 5 ~ 8 parts, wilkinite 1 ~ 3 part, feldspar 4 ~ 6 parts, 2 ~ 4 parts, quartz; 2) blank forming; 3) base substrate finishing; 4) body drying; 5) base substrate is decorated: with blue and white material depicting pattern and writing words on base substrate; 6) fire.The present invention is that the formula by adjusting blue and white material makes the colour temp scope of blue and white material consistent with the baking temperature range of Nixing pottery base substrate, and fire in conjunction with stepped continuous heating and cooling method, not only achieve blue and white material decoration Nixing pottery, increase the practical value of Nixing pottery, and formula rationally, production cost is low, and rate of burning till is high.
Description
Technical field
The present invention relates to a kind of preparation method of blue and white material decoration Nixing pottery, belong to potting technique field.
Background technology
Pottery is the utensil fired after kneading is shaped with clay or potter's clay.The invention of pottery, is that the mankind utilize chemical transformation to change the beginning of natural character the earliest, is again the important symbol of Development of Human Civilization, has great epoch-making significance in human development history.Pottery is in ancient times as one way of life articles for use, then general as artwork in the modern times.Though the kind of pottery is many, as gray pottery, red pottery, white pottery, ancient painted pottery and black pottery etc., the pottery that pottery market popularity is higher at home mainly contains: Jiangsu's purple sand ceramics, Yunnan Jian Shui pottery, Guangxi Qinzhou Nixing pottery, Chongqing Rongchang County pottery.Wherein, " transmutation " art of Guangxi Qinzhou Nixing pottery especially at home ceramic industry enjoy the good reputation of " China one exhausted ".
Guangxi Qinzhou Nixing pottery, the purple mud pottery of formal name used at school, its raw material comprises eastern mud, western mud.Mud status east, west, be distributed in the Qin Jiang two sides of crossing urban district, Qiezhou respectively because of these two kinds of mud.East mud is mainly distributed in region to the east of river of admiring, and be mostly stored in low lying areas, compact substance is soft, is soft clay, and color is show slightly yellow-white in redness, and iron-holder is high, and containing micro-quartz sand.East mud plays adjustment plasticity-and associativity in the production technique of Nixing pottery.Western mud is mainly distributed in by the emperor himself region to the west of river, and storage ground is based on hillside, and compact mass is flint clay, and be the purple mudstone that a kind of iron-holder is higher, color is red-purple, and upper layer has a small amount of irony to contaminate, and is flint clay, plasticity-and associativity poor.Neusoft is meat, and west is bone firmly, and in soft six hard four ratio mixing, kindred is mutually supported and is top grade.Concrete preparation technology mainly comprises following step: 1) prepare blank: to the east of mud 40 ~ 60%, western mud 40 ~ 60% weight percent mixing; 2) blank forming; 3) base substrate finishing; 4) body drying; 5) base substrate is decorated: Nixing pottery neither adds any pigment, not glazing in making processes, also not on base substrate with any coloured material drawing colour and pattern, only rely on the transmutation occurred once in a while to make Nixing pottery present color that is unpredictable and that control, and use artistic carving to decorate base substrate.6) fire: by the base substrate loading of kiln of having decorated, and be 1100 ~ 1200 DEG C by firing temperature, the firing time is fire for 10 hours, can obtain Nixing pottery device.Nixing pottery make use of the transmutation occurred once in a while when firing, thus makes it occur different color, and then increases its practical value.
Bule and white porcelain, also known as bule and white porcelain in vain, is often called for short blue and white, is one of main flow kind of Chinese porcelain, belongs under glazed porcelain.Bule and white porcelain uses the cobalt ore containing cobalt oxide to be the blue and white material that raw material is made, and bule and white porcelain base substrate describes decorative pattern, then cover last layer transparent, through about 1300 DEG C high temperature reduction flame once-firings.Through high-temperature physics chemical transformation, be blue and whitely consolidated between base glaze, have good effect in acid caustic corrosion, not easy to wear, will never fade, never peel off.For decorative pattern can be described with blue and white material on Nixing pottery, people have carried out many-sided research, and obtain certain achievement in research, as patent of invention CN102417346B discloses one " preparation technology of blue-and-white Nixing ceramics ", it is that firing temperature by being can bear by base substrate is brought up to the temperature range (1210 ~ 1240 DEG C) consistent with blue and white material colour temp and realized.Although blue and white material can be described decorative pattern on Nixing pottery by the method well, increase its practical value, it improves firing temperature, not only improves production cost, also increases the risk of pottery distortion.Therefore, develop a kind of production cost low, and the high blue-and-white Nixing ceramics of rate of burning till is very important.
Summary of the invention
High and hold yielding technical problem for blue-and-white Nixing ceramics production cost in above-mentioned prior art, technical problem to be solved by this invention is that to propose a kind of production cost low, and the preparation method of the high blue and white material decoration Nixing pottery of rate of burning till.
The present invention for the taked technical scheme that solves the problem is:
A preparation method for blue and white material decoration Nixing pottery, its step is as follows:
1) blank is prepared: blank is made up of the raw material of following weight parts proportioning: 50 ~ 60 parts, eastern mud, 30 ~ 40 parts, western mud, kaolin 5 ~ 8 parts, wilkinite 1 ~ 3 part, feldspar 4 ~ 6 parts, 2 ~ 4 parts, quartz;
Preferably, blank is made up of the raw material of following weight parts proportioning: 55 parts, eastern mud, 35 parts, western mud, kaolin 6.5 parts, wilkinite 2 parts, feldspar 5 parts, 3 parts, quartz.
Be more suitable for shaping to make blank particle and fire, ball mill can be used to carry out ball milling mixing to raw material: first by raw material: zirconia ball: the proportioning of water=1:1.5:3 adds, the size proportioning of simultaneous oxidation zirconium ball is large: in: little=1:2:3, ball milling 8 ~ 10h; Then twice sieve is crossed: first order number is 40 ~ 60 orders, and second order number is 100 ~ 120 orders; Finally by precipitation, press filtration, vacuum pugging, after old, obtain blank;
2) blank forming: blank is made various type base substrate;
3) base substrate finishing: by base substrate finishing to reach design requirements;
4) body drying: carry out drying to base substrate, makes base substrate moisture discharge;
5) base substrate is decorated: with blue and white material depicting pattern and writing words on base substrate;
Firing temperature due to Nixing pottery is 1100 ~ 1200 DEG C, and the colour temp of blue and white material is about 1300 DEG C, far away higher than the firing temperature of Nixing pottery, in order to make the colour temp scope of blue and white material consistent with the baking temperature range of Nixing pottery, blue and white material used in the present invention is made up of the raw material of following weight: silica 18 ~ 28 parts, 20 ~ 30 parts, aluminum oxide, ferric oxide 2 ~ 6 parts, titanium dioxide 0.1 ~ 0.3 part, 0.2 ~ 0.6 part, calcium oxide, 0.2 ~ 0.4 part, magnesium oxide, cobalt oxide 2 ~ 6 parts, manganese oxide 20 ~ 30 parts, nickel oxide 0.04 ~ 0.06 part, 1 ~ 2 part, barium oxide, potassium oxide 0.1 ~ 0.7 part, sodium oxide 0.1 ~ 0.3 part, boron oxide 0.05 ~ 0.07 part, strontium oxide 0.01 ~ 0.03 part, nano zine oxide 0.2 ~ 0.8 part, nano zircite 1 ~ 3 part,
Preferably, described blue and white material is made up of the raw material of following weight: silicon-dioxide 23 parts, 25 parts, aluminum oxide, ferric oxide 4 parts, titanium dioxide 0.2 part, 0.4 part, calcium oxide, 0.3 part, magnesium oxide, cobalt oxide 4 parts, manganese oxide 25 parts, nickel oxide 0.05 part, 1.5 parts, barium oxide, potassium oxide 0.4 part, sodium oxide 0.2 part, boron oxide 0.06 part, strontium oxide 0.02 part, nano zine oxide 0.5 part, nano zircite 2 parts.
The preparation method of described blue and white material is prepared by the method for the blue and white material of existing preparation; Described nano zine oxide, the particle size range of nano zircite are 10 ~ 80nm.
6) fire: in order to the color developing effect of the rate of burning till and blue and white material that effectively can improve base substrate, the present invention adopts stepped continuous heating and cooling method.
A) pre-heating stage: the base substrate kiln-firing first will decorated, is then raised to 70 ~ 90 DEG C by the heat-up rate of 40 ~ 60 DEG C/h by kiln temperature, and is incubated 10 ~ 16h, makes preheating and the drying of kiln, base substrate;
B) liter, holding stage: first kiln temperature is warmed up to 110 ~ 120 DEG C with the speed of 60 ~ 80 DEG C/h, and is incubated 0.1 ~ 0.3h, this stage is mainly further dry to base substrate; Secondly be warmed up to 250 ~ 350 DEG C with the speed of 70 ~ 90 DEG C/h, and be incubated 0.1 ~ 0.3h, this stage mainly arranges moisture remaining in base substrate, makes the particle of base substrate progressively draw close contraction; Then be warmed up to 650 ~ 800 DEG C with the speed of 90 ~ 100 DEG C/h, and be incubated 0.3 ~ 0.5h, this stage is base substrate compound generation chemical transformation mainly, as oxidizing reaction, decomposition reaction; Finally be warmed up to 1150 ~ 1180 DEG C with the speed of 110 ~ 120 DEG C/h, and be incubated 0.6 ~ 0.9h, this stage is mainly oxidized Sum decomposition reaction more fully, evenly, and insulation for some time, kiln temperature is even, and base substrate is well-done;
C) temperature-fall period: first kiln temperature is cooled to 850 ~ 900 DEG C with the speed of 150 ~ 200 DEG C/h, and be incubated 0.1 ~ 0.3h, this stage mainly prevents the oxidation once again of liquid phase crystallization and low-valent metal in base substrate, thus improves physical strength and the glaze paint glossiness of base substrate; Secondly cool to 400 ~ 850 DEG C with the speed of 40 ~ 60 DEG C/h, and be incubated 0.1 ~ 0.2h, this stage mainly base substrate liquid phase solidify, make the color developing effect of blue and white material more obvious; Then cool to 100 ~ 400 DEG C with the speed of 80 ~ 100 DEG C/h, and be incubated 0.1 ~ 0.2h, this stage mainly increases the hardness of base substrate; Finally, Temperature fall, to room temperature, takes out pottery.
Unlike the prior art, the present invention adds wilkinite, feldspar and quartz in base substrate composition, this adds due to kaolinic, although the content of aluminum oxide in base substrate can be increased, improve base substrate firing temperature, reduce distortion when burning till, improve intensity and the quality of pottery, but its receptivity is little, plasticity-and associativity poor, be unfavorable for that blank is shaping.But wilkinite plasticity-is strong, can improve blank plasticity-and dry body strength; Feldspar can be filled between each particle, promotes blank Densification; Quartz not only can regulate the plasticity-of blank, reduces and shrinks, and reduces blank deformation, and can strengthen base substrate physical strength.These composition add, not only solve kaolinic defect, and improve pottery burn till rate.In addition, kaolin, quartz improve firing temperature, and wilkinite, feldspar reduce firing temperature, combined, base substrate firing temperature is controlled better at 1150 ~ 1180 DEG C by high/low temperature.
In order to make the colour temp of blue and white material also at 1150 ~ 1180 DEG C, the present invention is realized by the formula adjusting blue and white material on existing basis.Adding of magnesium oxide, boron oxide, strontium oxide, nano zine oxide and nano zircite, impart different blue and white material: magnesium oxide, the fusion range of blue and white material can be increased, also improve elasticity and the thermostability of blue and white material simultaneously; Boron oxide, then can promote blue and white material melting, reduces colour temp, and improve its physical and chemical performance; Strontium oxide, then can reduce blue and white material bubble effectively; Nano zine oxide, then can impel blue and white material melting, reduces colour temp, improves thermostability and snappiness; Nano zircite, then can improve the thermostability of blue and white material, chemical stability and wear resisting property.
The present invention additionally uses stepped continuous heating and cooling method and fires, and makes that body drying is even, shrinking percentage is little, sufficient reacting, liquid phase solidifiability are good, improves and burns till rate.In addition, the method can also to prevent in sintering procedure the defects such as output cracking, distortion effectively, can also eliminate the stress that base substrate inside is formed simultaneously, thus obtain the pottery of more good quality.
Beneficial effect of the present invention is embodied in following several respects:
1, the present invention is that formula by adjusting blue and white material makes the colour temp scope of blue and white material consistent with the baking temperature range (1150 ~ 1180 DEG C) of Nixing pottery base substrate, and prior art is consistent with the colour temp scope (1210 ~ 1240 DEG C) of blue and white material by the baking temperature range of raising Nixing pottery base substrate, by comparing, can find: firing temperature of the present invention is lower than present technology, greatly reduces production cost.
2, present invention employs stepped continuous heating and cooling method to fire, effectively can to prevent in sintering procedure the defects such as output cracking, distortion, the stress that base substrate inside is formed can also be eliminated simultaneously, thus improve base substrate burn till rate.
Embodiment
Embodiment 1
A preparation method for blue and white material decoration Nixing pottery, its step is as follows:
1) blank is prepared: blank is made up of the raw material of following weight parts proportioning: 55 parts, eastern mud, 35 parts, western mud, kaolin 6.5 parts, wilkinite 2 parts, feldspar 5 parts, 3 parts, quartz, and use ball milling to mix: first by raw material: zirconia ball: the proportioning of water=1:1.5:3 adds, the size proportioning of simultaneous oxidation zirconium ball is large: in: little=1:2:3, ball milling 9h; Then 50 orders, 110 mesh sieves are crossed successively; Finally by precipitation, press filtration, vacuum pugging, after old, obtain blank;
2) blank forming: blank is made vase base substrate;
3) base substrate finishing: by the finishing of vase base substrate to reach design requirements;
4) body drying: after carrying out drying to vase base substrate, obtains 150 vase base substrates;
5) base substrate is decorated: with blue and white material depicting pattern and writing words on vase base substrate; Wherein, described blue and white material is made up of the raw material of following weight: silicon-dioxide 23 parts, 25 parts, aluminum oxide, ferric oxide 4 parts, titanium dioxide 0.2 part, 0.4 part, calcium oxide, 0.3 part, magnesium oxide, cobalt oxide 4 parts, manganese oxide 25 parts, nickel oxide 0.05 part, 1.5 parts, barium oxide, potassium oxide 0.4 part, sodium oxide 0.2 part, boron oxide 0.06 part, strontium oxide 0.02 part, nano zine oxide 0.5 part, nano zircite 2 parts;
6) fire:
A) pre-heating stage: the vase base substrate kiln-firing first will decorated, is then raised to 80 DEG C by the heat-up rate of 50 DEG C/h by kiln temperature, and is incubated 13h;
B) liter, holding stage: first kiln temperature is warmed up to 115 DEG C with the speed of 70 DEG C/h, and is incubated 0.2h; Secondly be warmed up to 300 DEG C with the speed of 80 DEG C/h, and be incubated 0.2h; Then be warmed up to 725 DEG C with the speed of 95 DEG C/h, and be incubated 0.4h; Finally be warmed up to 1170 DEG C with the speed of 115 DEG C/h, and be incubated 0.8h;
C) temperature-fall period: first kiln temperature is cooled to 875 DEG C with the speed of 175 DEG C/h, and be incubated 0.2h; Secondly cool to 625 DEG C with the speed of 50 DEG C/h, and be incubated 0.2h; Then cool to 250 DEG C with the speed of 90 DEG C/h, and be incubated 0.2h; Finally, Temperature fall is to room temperature, and obtain 145 qualified Nixing pottery vase base substrates, 5 defective.
Embodiment 2
A preparation method for blue and white material decoration Nixing pottery, its step is as follows:
1) blank is prepared: blank is made up of the raw material of following weight parts proportioning: 50 parts, eastern mud, 30 parts, western mud, kaolin 5 parts, wilkinite 1 part, feldspar 4 parts, 2 parts, quartz, and use ball milling to mix: first by raw material: zirconia ball: the proportioning of water=1:1.5:3 adds, the size proportioning of simultaneous oxidation zirconium ball is large: in: little=1:2:3, ball milling 8h; Then 40 orders, 100 mesh sieves are crossed successively; Finally by precipitation, press filtration, vacuum pugging, after old, obtain blank;
2) blank forming: blank is made vase base substrate;
3) base substrate finishing: by the finishing of vase base substrate to reach design requirements;
4) body drying: after carrying out drying to vase base substrate, obtains 100 vase base substrates;
5) base substrate is decorated: with blue and white material depicting pattern and writing words on vase base substrate; Wherein, described blue and white material is made up of the raw material of following weight: silica 18 parts, 20 parts, aluminum oxide, ferric oxide 2 parts, titanium dioxide 0.1 part, 0.2 part, calcium oxide, 0.2 part, magnesium oxide, cobalt oxide 2 parts, manganese oxide 20 parts, nickel oxide 0.04 part, 1 part, barium oxide, potassium oxide 0.1 part, sodium oxide 0.1 part, boron oxide 0.05 part, strontium oxide 0.01 part, nano zine oxide 0.2 part, nano zircite 1 part.
6) fire:
A) pre-heating stage: the vase base substrate kiln-firing first will decorated, is then raised to 70 DEG C by the heat-up rate of 40 DEG C/h by kiln temperature, and is incubated 10h;
B) liter, holding stage: first kiln temperature is warmed up to 110 DEG C with the speed of 60 DEG C/h, and is incubated 0.1h; Secondly be warmed up to 250 DEG C with the speed of 70 DEG C/h, and be incubated 0.1h; Then be warmed up to 650 DEG C with the speed of 90 DEG C/h, and be incubated 0.3h; Finally be warmed up to 1150 DEG C with the speed of 110 DEG C/h, and be incubated 0.6h;
C) temperature-fall period: first kiln temperature is cooled to 850 DEG C with the speed of 150 DEG C/h, and be incubated 0.1h; Secondly cool to 400 DEG C with the speed of 40 DEG C/h, and be incubated 0.1h; Then cool to 100 DEG C with the speed of 80 DEG C/h, and be incubated 0.1h; Finally, Temperature fall is to room temperature, and obtain 97 qualified Nixing pottery vase base substrates, 3 defective.
Embodiment 3
A preparation method for blue and white material decoration Nixing pottery, its step is as follows:
1) blank is prepared: blank is made up of the raw material of following weight parts proportioning: 60 parts, eastern mud, 40 parts, western mud, kaolin 8 parts, wilkinite 3 parts, feldspar 6 parts, 4 parts, quartz, and use ball milling to mix: first by raw material: zirconia ball: the proportioning of water=1:1.5:3 adds, the size proportioning of simultaneous oxidation zirconium ball is large: in: little=1:2:3, ball milling 10h; Then 60 orders, 120 mesh sieves are crossed successively; Finally by precipitation, press filtration, vacuum pugging, after old, obtain blank;
2) blank forming: blank is made vase base substrate;
3) base substrate finishing: by the finishing of vase base substrate to reach design requirements;
4) body drying: after carrying out drying to vase base substrate, obtains 200 vase base substrates;
5) base substrate is decorated: with blue and white material depicting pattern and writing words on vase base substrate; Wherein, described blue and white material is made up of the raw material of following weight: silicon-dioxide 28 parts, 30 parts, aluminum oxide, ferric oxide 6 parts, titanium dioxide 0.3 part, 0.6 part, calcium oxide, 0.4 part, magnesium oxide, cobalt oxide 6 parts, manganese oxide 30 parts, nickel oxide 0.06 part, 2 parts, barium oxide, potassium oxide 0.7 part, sodium oxide 0.3 part, boron oxide 0.07 part, strontium oxide 0.03 part, nano zine oxide 0.8 part, nano zircite 3 parts;
6) fire:
A) pre-heating stage: the vase base substrate kiln-firing first will decorated, is then raised to 90 DEG C by the heat-up rate of 60 DEG C/h by kiln temperature, and is incubated 16h;
B) liter, holding stage: first kiln temperature is warmed up to 120 DEG C with the speed of 80 DEG C/h, and is incubated 0.3h; Secondly be warmed up to 350 DEG C with the speed of 90 DEG C/h, and be incubated 0.3h; Then be warmed up to 800 DEG C with the speed of 100 DEG C/h, and be incubated 0.5h; Finally be warmed up to 1180 DEG C with the speed of 120 DEG C/h, and be incubated 0.9h;
C) temperature-fall period: first kiln temperature is cooled to 900 DEG C with the speed of 200 DEG C/h, and be incubated 0.3h; Secondly cool to 850 DEG C with the speed of 60 DEG C/h, and be incubated 0.2h; Then cool to 400 DEG C with the speed of 100 DEG C/h, and be incubated 0.2h; Finally, Temperature fall is to room temperature, and obtain 196 qualified Nixing pottery vase base substrates, 4 defective.
Certainly, just the preferred embodiments of the disclosure is described in detail above, not limits practical range of the present invention with this, and all equivalence changes done according to principle of the present invention, structure and structure, all should be covered by protection scope of the present invention.
Claims (3)
1. a preparation method for blue and white material decoration Nixing pottery, is characterized in that: its step is as follows:
1) blank is prepared: blank is made up of the raw material of following weight parts proportioning: 50 ~ 60 parts, eastern mud, 30 ~ 40 parts, western mud, kaolin 5 ~ 8 parts, wilkinite 1 ~ 3 part, feldspar 4 ~ 6 parts, 2 ~ 4 parts, quartz;
2) blank forming: blank is made various type base substrate;
3) base substrate finishing: by base substrate finishing to reach design requirements;
4) body drying: carry out drying to base substrate, makes base substrate moisture discharge;
5) base substrate is decorated: with blue and white material depicting pattern and writing words on base substrate;
6) fire:
A) pre-heating stage: the base substrate kiln-firing first will decorated, is then raised to 70 ~ 90 DEG C by the heat-up rate of 40 ~ 60 DEG C/h by kiln temperature, and is incubated 10 ~ 16h;
B) liter, holding stage: first kiln temperature is warmed up to 110 ~ 120 DEG C with the speed of 60 ~ 80 DEG C/h, and is incubated 0.1 ~ 0.3h; Secondly be warmed up to 250 ~ 350 DEG C with the speed of 70 ~ 90 DEG C/h, and be incubated 0.1 ~ 0.3h; Then be warmed up to 650 ~ 800 DEG C with the speed of 90 ~ 100 DEG C/h, and be incubated 0.3 ~ 0.5h; Finally be warmed up to 1150 ~ 1180 DEG C with the speed of 110 ~ 120 DEG C/h, and be incubated 0.6 ~ 0.9h;
C) temperature-fall period: first kiln temperature is cooled to 850 ~ 900 DEG C with the speed of 150 ~ 200 DEG C/h, and be incubated 0.1 ~ 0.3h; Secondly cool to 400 ~ 850 DEG C with the speed of 40 ~ 60 DEG C/h, and be incubated 0.1 ~ 0.2h; Then cool to 100 ~ 400 DEG C with the speed of 80 ~ 100 DEG C/h, and be incubated 0.1 ~ 0.2h; Finally, Temperature fall, to room temperature, takes out pottery.
2. the preparation method of blue and white material decoration Nixing pottery according to claim 1, it is characterized in that: described blue and white material is made up of the raw material of following weight: silica 18 ~ 28 parts, 20 ~ 30 parts, aluminum oxide, ferric oxide 2 ~ 6 parts, titanium dioxide 0.1 ~ 0.3 part, 0.2 ~ 0.6 part, calcium oxide, 0.2 ~ 0.4 part, magnesium oxide, cobalt oxide 2 ~ 6 parts, manganese oxide 20 ~ 30 parts, nickel oxide 0.04 ~ 0.06 part, 1 ~ 2 part, barium oxide, potassium oxide 0.1 ~ 0.7 part, sodium oxide 0.1 ~ 0.3 part, boron oxide 0.05 ~ 0.07 part, strontium oxide 0.01 ~ 0.03 part, nano zine oxide 0.2 ~ 0.8 part, nano zircite 1 ~ 3 part.
3. the preparation method of blue and white material decoration Nixing pottery according to claim 2, is characterized in that: described blue and white material is made up of the raw material of following weight: silicon-dioxide 23 parts, 25 parts, aluminum oxide, ferric oxide 4 parts, titanium dioxide 0.2 part, 0.4 part, calcium oxide, 0.3 part, magnesium oxide, cobalt oxide 4 parts, manganese oxide 25 parts, nickel oxide 0.05 part, 1.5 parts, barium oxide, potassium oxide 0.4 part, sodium oxide 0.2 part, boron oxide 0.06 part, strontium oxide 0.02 part, nano zine oxide 0.5 part, nano zircite 2 parts.
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| CN110963804A (en) * | 2019-12-24 | 2020-04-07 | 清远市简一陶瓷有限公司 | Method for solving surface unevenness in ceramic tile firing process |
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| CN108529881A (en) * | 2018-07-16 | 2018-09-14 | 界首市伟盛古窑彩陶制作发展有限公司 | A kind of high-compactness viridescent colour glaze |
| CN110627492A (en) * | 2019-10-21 | 2019-12-31 | 山东崯基新材料科技发展有限公司 | Novel environment-friendly high-temperature colored porcelain aggregate and preparation process thereof |
| CN110963804A (en) * | 2019-12-24 | 2020-04-07 | 清远市简一陶瓷有限公司 | Method for solving surface unevenness in ceramic tile firing process |
| CN110963804B (en) * | 2019-12-24 | 2022-02-08 | 清远市简一陶瓷有限公司 | Method for solving surface unevenness in ceramic tile firing process |
| CN111348907A (en) * | 2020-03-16 | 2020-06-30 | 福建省德化县鸿骏陶瓷有限公司 | Preparation method of matt bean blue glaze antique porcelain |
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Application publication date: 20160106 |