CN106396638B - Low temperature lightweight lime gradual change glaze ceramics and its manufacture craft - Google Patents

Low temperature lightweight lime gradual change glaze ceramics and its manufacture craft Download PDF

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CN106396638B
CN106396638B CN201610791036.5A CN201610791036A CN106396638B CN 106396638 B CN106396638 B CN 106396638B CN 201610791036 A CN201610791036 A CN 201610791036A CN 106396638 B CN106396638 B CN 106396638B
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parts
glaze
gradual change
low temperature
lime
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CN106396638A (en
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林睦清
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FUJIAN DEHUA COUNTY HUANGMING CERAMIC Co Ltd
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FUJIAN DEHUA COUNTY HUANGMING CERAMIC Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • C03C8/02Frit compositions, i.e. in a powdered or comminuted form
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/03Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on magnesium oxide, calcium oxide or oxide mixtures derived from dolomite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/52Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/89Coating or impregnation for obtaining at least two superposed coatings having different compositions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • C04B2235/3463Alumino-silicates other than clay, e.g. mullite
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/349Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite

Abstract

The invention belongs to ceramic glaze fields, and in particular to a kind of the low temperature lightweight lime gradual change glaze ceramics and its manufacture craft of energy-saving and environmental protection.Low temperature lightweight lime gradual change glaze ceramics provided by the invention, including light china green body and the low temperature light china lime gradual change glaze being set on light china green body.Above-mentioned low temperature lightweight lime gradual change glaze ceramics, glaze is formed by milky white, canescence after firing, light gray, dark-grey polychrome are alternate and gradually transition, glaze glossiness is good, there is difference with the change in shape of green body in gradual change direction, the effect of glaze can be adjusted by the formula and thickness of ground coat enamel and overglaze, have unique artistic effect;That base glaze is combined closely in addition, the blank raw material of this kind of low temperature lightweight lime gradual change glaze ceramics is selected according to glaze, can once-firing, firing temperature is low, realizes energy conservation and environmental protection, reduces energy consumption.

Description

Low temperature lightweight lime gradual change glaze ceramics and its manufacture craft
Technical field
The invention belongs to ceramic glaze fields, and in particular to a kind of low temperature lightweight lime gradual change glaze ceramics of energy-saving and environmental protection And its manufacture craft.
Background technique
Dehua is the maximum art ceramics production in the whole nation and export base, and Dehua ceramics produced are mostly based on outlet. The ceramics of existing outlet are mostly the environment-friendly light porcelain of low temperature, lightweight, and low temperature light china is once-firing and firing temperature is low, Generally at 980-1050 DEG C or so, has the characteristics that plasticity is strong, ornamental value is high, environmentally friendly, safe, be in the world by favor Ceramic category.
With the development of ceramics, existing light china is able to achieve once-firing substantially, as application publication number is Lightweight porcelain low temperature transmutation covellite color glaze material formula, method of preparation and use, utilize glaze disclosed in CN201510534458.X It improves to light china into decorating.Existing, solid existing fade effect, then need on ceramic body respectively on light china Upper light color, Neutral colour, dark color glaze after, by firing be just able to achieve, this kind of method be burnt into fade effect porcelain in color Block transition portion conversion it is stiff, and want multiple glazing, apply during also to avoid the glaze between different color blocks from mix, life Production. art is complicated, therefore no matter all needs further to be improved from effect or in manufacture craft.
Summary of the invention
To solve the above-mentioned problems, black the black of the art pottery or Household ceramic is widely portable to the present invention provides a kind of Jinsha glaze porcelain.
For achieving the above object, the present invention provides low temperature lightweight lime gradual change glaze ceramics, which is characterized in that including Light china green body and the low temperature light china lime gradual change glaze being set on light china green body;Light china green body is in parts by weight such as Under: 40-50 parts of dolomite, zeolite 20-30,10-15 parts of bentonite, 15-20 parts of feldspar, 5-10 parts of talcum;Low temperature light china is white The parts by weight meter of grey gradual change glaze is as follows: 20-30 parts of feldspar, 20-30 parts of cullet, 10-15 parts of clear frit, lime stone 5-10 Part, burn talcum 5-10 parts, 1-5 parts of copper oxide, 1-5 parts of zinc oxide, 1-5 parts of tin oxide, 1-5 parts of titanium oxide, 1-5 parts of zirconium oxide, 1-5 parts of silicic acid powder.
Optimization, light china green body is as follows in parts by weight: 42 parts of dolomite, zeolite 25,11 parts of bentonite, feldspar 16 Part, 6 parts of talcum.
Optimization, the parts by weight meter of low temperature light china lime gradual change glaze is as follows: 28 parts of feldspar, 29 parts of cullet, transparent molten 13 parts of block, 6 parts of lime stone, burn 6 parts of talcum, 4 parts of copper oxide, 3 parts of zinc oxide, 1 part of tin oxide, 3 parts of titanium oxide, 5 parts of zirconium oxide, 2 parts of silicic acid powder.
Optimization, light china green body is as follows in parts by weight: 48 parts of dolomite, zeolite 21,11 parts of bentonite, feldspar 15 Part, 5 parts of talcum.
Optimization, the parts by weight meter of low temperature light china lime gradual change glaze is as follows: 23 parts of feldspar, 25 parts of cullet, transparent molten 15 parts of block, 8 parts of lime stone, burn 7 parts of talcum, 5 parts of copper oxide, 2 parts of zinc oxide, 4 parts of tin oxide, 2 parts of titanium oxide, 5 parts of zirconium oxide, 4 parts of silicic acid powder.
The manufacture craft of low temperature lightweight lime gradual change glaze ceramics, which comprises the following steps:
Raw material is mixed, is crushed, screening, wet ball mill, be made according to lightweight porcelain billet composition of raw materials weighing and proportioning by step 1 Green body slurry, when ball milling expect: ball: water=1:1.5-2:0.6-0.8 crosses 150 meshes;
Step 2, according to low temperature light china lime gradual change glaze formula weighing and proportioning, raw material mixing is crushed, screening, wet bulb Mill, overglaze glaze slip is made, when ball milling, material: ball: water=1:2:1.0-1.2 crosses 250 meshes;
Slurry made from step 1 is made ceramic body, waits ceramic body surface natural air drying by step 3;
Step 4, obtained overglaze glaze slip uniformly impose on ceramic body surface, wait body drying;
Step 5, kiln-firing after ceramic blank drying, under reducing atmosphere, firing temperature is 950-1030 DEG C to kiln, Obtain low temperature lightweight lime gradual change glaze ceramics.
Further, the glaze slip in step 4 after glazing with a thickness of 0.5-1mm.
Further, after kiln reaches firing temperature, slow cooling.
Further, when kiln is cooled to 900 DEG C, 1-2 hours are kept the temperature, the glaze for being conducive to multi-color gradual change is formed.
Seen from the above description, low temperature lightweight lime gradual change glaze ceramics provided by the invention, glaze is formed by cream after firing White, canescence, light gray, dark-grey polychrome be alternate and gradually transition, and glaze glossiness is good, gradual change direction with green body change in shape And there is difference, the effect of glaze can be adjusted by the formula and thickness of ground coat enamel and overglaze, have unique artistic effect; It is that base glaze is combined closely in addition, the blank raw material of this kind of low temperature lightweight lime gradual change glaze ceramics is selected according to glaze, it can one Secondary firing, firing temperature is low, realizes energy conservation and environmental protection, reduces energy consumption.
Specific embodiment
For a better understanding of the technical solution of the present invention, being discussed further below with reference to embodiment to the present invention.
Low temperature lightweight lime gradual change glaze ceramics, which is characterized in that including light china green body and be set on light china green body Low temperature light china lime gradual change glaze;
Light china green body is as follows in parts by weight: 40-50 parts of dolomite, zeolite 20-30,10-15 parts of bentonite, feldspar 15-20 parts, 5-10 parts of talcum;
The parts by weight meter of low temperature light china lime gradual change glaze is as follows: 20-30 parts of feldspar, 20-30 parts of cullet, clear frit 10-15 parts, 5-10 parts of lime stone, burning talcum 5-10 parts, 1-5 parts of copper oxide, 1-5 parts of zinc oxide, 1-5 parts of tin oxide, titanium oxide 1-5 parts, 1-5 parts of zirconium oxide, 1-5 parts of silicic acid powder.
The manufacture craft of above-mentioned low temperature lightweight lime gradual change glaze ceramics, which comprises the following steps:
Raw material is mixed, is crushed, screening, wet ball mill, be made according to lightweight porcelain billet composition of raw materials weighing and proportioning by step 1 Green body slurry, when ball milling expect: ball: water=1:1.5-2:0.6-0.8 crosses 150 meshes;
Step 2, according to low temperature light china lime gradual change glaze formula weighing and proportioning, raw material mixing is crushed, screening, wet bulb Mill, overglaze glaze slip is made, when ball milling, material: ball: water=1:2:1.0-1.2 crosses 250 meshes;
Slurry made from step 1 is made ceramic body, waits ceramic body surface natural air drying by step 3;
Step 4, obtained overglaze glaze slip uniformly impose on ceramic body surface, wait body drying glaze slip with a thickness of 0.5-1mm;
Step 5, kiln-firing after ceramic blank drying, under reducing atmosphere, firing temperature is 950-1030 DEG C to kiln, After kiln reaches firing temperature, slow cooling keeps the temperature 1-2 hours, is conducive to multi-color gradual change when kiln is cooled to 900 DEG C Glaze is formed, and low temperature lightweight lime gradual change glaze ceramics are obtained.
Specific embodiment one:
Light china green body is as follows in parts by weight: 42 parts of dolomite, zeolite 25,11 parts of bentonite, 16 parts of feldspar, talcum 6 parts;
The parts by weight meter of low temperature light china lime gradual change glaze is as follows: 28 parts of feldspar, 29 parts of cullet, 13 parts of clear frit, 6 parts of lime stone burns 6 parts of talcum, 4 parts of copper oxide, 3 parts of zinc oxide, 1 part of tin oxide, 3 parts of titanium oxide, 5 parts of zirconium oxide, silicic acid powder 2 Part.
Specific embodiment two:
Light china green body is as follows in parts by weight: 48 parts of dolomite, zeolite 21,11 parts of bentonite, 15 parts of feldspar, talcum 5 parts;
The parts by weight meter of low temperature light china lime gradual change glaze is as follows: 23 parts of feldspar, 25 parts of cullet, 15 parts of clear frit, 8 parts of lime stone burns 7 parts of talcum, 5 parts of copper oxide, 2 parts of zinc oxide, 4 parts of tin oxide, 2 parts of titanium oxide, 5 parts of zirconium oxide, silicic acid powder 4 Part.
Low temperature lightweight lime gradual change glaze provided by the invention ceramics, after firing glaze formed by milky white, canescence, light gray, Dark-grey polychrome is alternate and gradually transition, and glaze glossiness is good, and gradual change direction difference occurs with the change in shape of green body, glaze Effect can be adjusted by the formula and thickness of ground coat enamel and overglaze, have unique artistic effect;In addition, this kind of low temperature is light Combining closely with lightweight white clouds porcelain billet body for matter lime gradual change glaze ceramics, can be with white clouds porcelain billet body once-firing, and firing temperature is low, It realizes energy conservation and environmental protection, reduces energy consumption.
The above is only the preferred embodiment of the present invention, therefore cannot be limited the scope of implementation of the present invention with this, i.e., according to Equivalent changes and modifications made by scope of the present invention patent and description should still belong to the model that the invention patent covers In enclosing.

Claims (5)

1. low temperature lightweight lime gradual change glaze ceramics, which is characterized in that including light china green body and be set on light china green body Low temperature light china lime gradual change glaze;
Light china green body is as follows in parts by weight: 40-50 parts of dolomite, zeolite 20-30,10-15 parts of bentonite, feldspar 15- 20 parts, 5-10 parts of talcum;
The parts by weight meter of low temperature light china lime gradual change glaze is as follows: 20-30 parts of feldspar, 20-30 parts of cullet, clear frit 10- 15 parts, 5-10 parts of lime stone, burning talcum 5-10 parts, 1-5 parts of copper oxide, 1-5 parts of zinc oxide, 1-5 parts of tin oxide, titanium oxide 1-5 Part, 1-5 parts of zirconium oxide, 1-5 parts of silicic acid powder;
Glaze slip after glazing with a thickness of 0.5-1mm.
2. low temperature lightweight lime gradual change glaze according to claim 1 ceramics, which is characterized in that the light china green body according to Parts by weight meter is as follows: 42 parts of dolomite, 25 parts of zeolite, 11 parts of bentonite, 16 parts of feldspar, 6 parts of talcum.
3. low temperature lightweight lime gradual change glaze ceramics according to claim 1 or 2, which is characterized in that the low temperature light china The parts by weight meter of lime gradual change glaze is as follows: 28 parts of feldspar, 13 parts of clear frit, 6 parts of lime stone, burns talcum 6 at 29 parts of cullet Part, 4 parts of copper oxide, 3 parts of zinc oxide, 1 part of tin oxide, 3 parts of titanium oxide, 5 parts of zirconium oxide, 2 parts of silicic acid powder.
4. low temperature lightweight lime gradual change glaze according to claim 1 ceramics, which is characterized in that the light china green body according to Parts by weight meter is as follows: 48 parts of dolomite, 21 parts of zeolite, 11 parts of bentonite, 15 parts of feldspar, 5 parts of talcum.
5. low temperature lightweight lime gradual change glaze ceramics according to claim 1, which is characterized in that the low temperature light china lime The parts by weight meter of gradual change glaze is as follows: 23 parts of feldspar, 15 parts of clear frit, 8 parts of lime stone, burns 7 parts of talcum, oxygen at 25 parts of cullet Change 5 parts of copper, 2 parts of zinc oxide, 4 parts of tin oxide, 2 parts of titanium oxide, 5 parts of zirconium oxide, 4 parts of silicic acid powder.
CN201610791036.5A 2016-08-31 2016-08-31 Low temperature lightweight lime gradual change glaze ceramics and its manufacture craft Active CN106396638B (en)

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CN107056234A (en) * 2017-04-28 2017-08-18 福建省德化县艺韵陶瓷有限公司 Health ceramic is formulated
CN107814488B (en) * 2017-11-16 2020-05-22 九牧厨卫股份有限公司 Preparation method of sanitary ceramic with blue gradient glaze
CN109133855A (en) * 2018-09-17 2019-01-04 泉州市陶瓷科学技术研究所 Low temperature light ceramics and its preparation process
CN112939466B (en) * 2021-03-30 2022-02-22 广东欧文莱陶瓷有限公司 Leather grain ceramic glaze
CN113105225A (en) * 2021-03-30 2021-07-13 广东欧文莱陶瓷有限公司 Dermatoglyph ceramic and preparation method thereof

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JPS60108346A (en) * 1983-11-14 1985-06-13 Matsushita Electric Ind Co Ltd Enamel frit having low softening point
CN103319207A (en) * 2013-07-04 2013-09-25 佛山市艾陶制釉有限公司 Non-radiative opal fritted glaze for ceramic tiles and preparation method of non-radiative opal fritted glaze
CN105669161A (en) * 2016-01-20 2016-06-15 景德镇市中天鑫源陶瓷有限公司 Method of reductive firing of ceramic at medium temperature (1190-1260 DEG C)

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