CN109896869A - A kind of golden yellow ceramic glaze and preparation method thereof - Google Patents
A kind of golden yellow ceramic glaze and preparation method thereof Download PDFInfo
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Abstract
The present invention relates to ceramic glaze preparation technical fields, a kind of specifically golden yellow ceramic glaze and preparation method thereof, detailed process is that micro-nano silver powder, albite, quartz, talcum and calcite are formulated as glaze according to a certain percentage, glaze slip is made in glaze by planetary ball mill, glaze is applied in biscuit of ceramics surface using glaze method, dry be placed in program controllable high temperature furnace of glazing biscuit is fired under the conditions of air atmosphere, obtains the ceramic glaze product with golden yellow colouring effect.Phenomena such as present invention is using concerted reaction during high-temperature glaze is fired of other ingredients in micro-nano silver and glaze formula and the oxygen in air, diffusion effect, cohesion, under the conditions of air atmosphere, it is prepared using program controllable high temperature furnace and good golden yellow colour generation, glaze layer glossiness, the lustrous and transparent profit of enamel, the ceramic glaze with certain beautiful texture is uniformly presented with glaze, there is no the ceramic glaze product of the defects of pin hole and tangerine glaze, preparation method is simple to operation, is with a wide range of applications.
Description
Technical field
The present invention relates to ceramic glaze preparation technical fields, and in particular to a kind of golden yellow ceramic glaze and preparation method thereof.
Background technique
Ceramics originate from Ancient Times in China, have thousands of years history away from the present, are Ancient Times in China ceramics in periods in Tang, Song and the Qing Dynasty
Fast-developing period, and great representative porcelain type, such as the tri-coloured glazed pottery of the Tang Dynasty occur, the Song Dynasty " an ancient unit of weight, you,
Brother, determines official " five big porcelain, " Doucai contrasting colors " of the Qing Dynasty, " enamel porcelain " etc..A Zhang Wenhua business card of the ceramics as China, is developed to
The present has had typical typical regional characters, such as the blue and white porcelain in Jing Dezhen, the pottery in Xuchang, your porcelain in Ruzhou etc..Currently, these
Attention is all compared to the development of ceramics in great representative ceramic region, but is concentrated mainly on Ceramics Culture, research of ancient ceramic, imitates
Ancient pottery and porcelain research and development etc.；Most important component part of the ceramic glaze as ceramics, is mainly covered on ceramic surface, has and causes
The features such as close, gloss, beauty, however it is less for the research and development of novel ceramic enamel both at home and abroad at present, have been unable to meet China's conduct
The developing steps of ceramic big country and power.
Summary of the invention
In order to overcome the disadvantages of the above prior art, the present invention provides a kind of golden yellow ceramic glaze and preparation method thereof, this
Invention utilizes cooperateing with during grand feu between micro-nano silver and the oxygen in ingredients other in glaze formula and air
It phenomena such as reaction, diffusion effect, cohesion, under the conditions of air atmosphere, is prepared using program controllable high temperature furnace with glaze
Good golden yellow colour generation, glaze layer glossiness, the lustrous and transparent profit of enamel, the ceramic glaze with certain beautiful texture is uniformly presented, without pin hole and tangerine
The ceramic glaze product of the defects of glaze, this ceramic glaze can be applied to display art's porcelain field.
In order to achieve the above object, the technical scheme adopted by the invention is as follows:
A kind of preparation method of golden yellow ceramic glaze, comprising the following steps:
Step 1, ball milling is carried out after glaze, water, agate abrading-ball being mixed according to the mass ratio of 1.0:1.2:1.5-1.7, is obtained
To slurry, then filtering and filtrate is modulated into density is 1.66-1.69g/cm3Solution, obtain glaze slip；
Wherein, the glaze consists of the following mass percentage components: micro-nano silver powder 0.8%-3.5%, albite
38.5%-45.5%, quartz 20%-23.5%, calcite 19.5%-21.5%, talcum 10.5%-13%；
Step 2, biscuit of ceramics is fired in 850 DEG C -900 DEG C in air atmosphere, obtains biscuit ware green body；
By glaze slip even application obtained in step 1 in biscuit ware billet surface, and it is sufficiently dry, obtain glazing ceramics
Biscuit；
Step 3, glazing biscuit of ceramics obtained in step 2 is fired in 1180-1280 DEG C in air atmosphere, is obtained
To the uniform golden yellow ceramic glaze of glaze layer surface.
Preferably, ball milling, rotational speed of ball-mill 300-400r/min, ball milling are carried out using planetary ball mill in the step 1
Time is 10-16h.
Preferably, micro-nano silver powder diameter is 30-9000 nanometers in the step 1.
Preferably, biscuit of ceramics described in the step 2 consists of the following mass percentage components: kaolin 58%,
Quartzy 28.5%, feldspar 13.5%.
Preferably, in the step 2 biscuit of ceramics sintering procedure are as follows: be warming up to according to the heating rate of 3-5 DEG C/min
850-900 DEG C, keep the temperature 20-30min.
Preferably, the glazed thickness of glazing biscuit of ceramics is 1.0-1.5mm in the step 2.
Preferably, temperature sufficiently dry in the step 2 is 90-120 DEG C, drying time 6-12h.
Preferably, in the step 3 ceramic glaze product sintering procedure are as follows: according to 3-5 DEG C/min heating rate heat up
To 1180-1280 DEG C, 20-90min is kept the temperature.
The present invention also protects the golden yellow ceramic glaze being prepared by above-mentioned preparation method.
Compared with prior art, the beneficial effects of the present invention are:
1, golden yellow ceramic glaze glaze prepared by the present invention is smooth and colour generation uniformly, glaze layer glossiness is good, the lustrous and transparent profit of enamel and
With certain beautiful texture, the defects of without pin hole, tangerine glaze, while glaze layer is stable and fires high yield rate；
2, the present invention is based on possessed by micro-nano silver itself significantly sterilization and photocatalytic pollutant degradation advantage, wound
New property micro-nano silver is introduced into ceramic glaze, and utilizes other ingredients in micro-nano silver and glaze formula and the oxygen in air
Phenomena such as concerted reaction, diffusion effect between gas during grand feu, cohesion, using program controllable high temperature furnace larger
It is uniformly golden yellow ceramic glaze that (1180-1280 DEG C), which burns out glaze, in temperature range, and glaze formula is simple and fires finished product
Rate is high, and finished product rate is up to 95% or more；
3, golden yellow ceramic glaze prepared by the present invention is burnt with existing using excess copper element compound under reducing atmosphere
The ceramic glaze that there is golden yellow spot or part glaze golden yellow is presented of system is compared, and glaze of the invention has substantially uniformity
It is golden yellow；And compared with traditional ceramics glaze prepares needs more than ten or even tens processes, present invention only requires ingredient-ball millings-
It sizes mixing-glazing-glaze firing process, preparation flow is simple；Simultaneously sintering procedure of the present invention be entirely air atmosphere, to environment without
Pollution avoids the problems such as conventional method is using the existing pollution environment of reducing atmosphere and explosive.
Detailed description of the invention
Fig. 1 is the effect picture for the golden yellow ceramic glaze that the embodiment of the present invention 1 is prepared, and Fig. 1-(a) is the examination of embodiment 1
Piece macroscopic view colouring effect, Fig. 1-(b) are the glaze layer enlarged drawing of embodiment 1；
Fig. 2 is the effect picture for the golden yellow ceramic glaze that the embodiment of the present invention 2 is prepared；
Fig. 3 is the effect picture for the golden yellow ceramic glaze that the embodiment of the present invention 3 is prepared；
Fig. 4 is the effect picture for the golden yellow ceramic glaze that the embodiment of the present invention 4 is prepared；
Fig. 5 is the effect picture for the golden yellow ceramic glaze that the embodiment of the present invention 5 is prepared.
Fig. 6 is the effect picture for the golden yellow ceramic glaze that the embodiment of the present invention 6 is prepared.
Specific embodiment
In order to enable those skilled in the art to more fully understand, technical solution of the present invention is practiced, with reference to the accompanying drawing
And the invention will be further described for specific embodiment, but illustrated embodiment is not as a limitation of the invention.
The test method of actual conditions is not specified in following embodiments, according to conventional methods in the art with condition into
Row, if material used is commercially available without specified otherwise.
Embodiment 1
A kind of preparation method of golden yellow ceramic glaze, includes the following steps:
Step 1, weigh following component by mass percentage: partial size is nano-silver powder 0.8%, the albite of 30nm
41.7%, quartzy 23.5%, calcite 21.5%, talcum 12.5%, mix the above components evenly, obtain glaze；
Glaze, water, agate abrading-ball are mixed according to the mass ratio of 1.0:1.2:1.5, ball is then carried out using planetary ball mill
Mill, rotation revolving speed is 300r/min when ball milling, Ball-milling Time 16h, and ball milling finishes to obtain slurry, and slurry is crossed 250 mesh mesh
Then sieve will cross the density modulation of mesh sieve slurry to 1.67g/cm with water3, modulation, which finishes, obtains glaze slip；
It is controllably high that by material composition be kaolin 58%, the biscuit of ceramics of quartz 28.5%, feldspar 13.5% is put into program
In warm furnace, after being warming up to 890 DEG C under the conditions of air atmosphere with the heating rate of 3 DEG C/min, furnace cooling after 20min is kept the temperature,
Obtain biscuit ware green body；
Step 2, the glaze slip even application prepared in step 1 is controlled into glazed thickness on the surface of biscuit ware green body
To be put into air dry oven after 1.0mm, at 100 DEG C after dry 9h, glazing biscuit of ceramics is obtained；
Step 3, glazing biscuit of ceramics obtained in step 2 is put into program controllable high temperature furnace, in air atmosphere condition
Lower firing, burning process are as follows: rise to 1200 DEG C by room temperature for 3 DEG C/min according to heating rate, cooled to the furnace after keeping the temperature 60min
Room temperature is to get to the golden yellow ceramic glaze product.
Fig. 1 provides the golden yellow ceramic glaze Product Rendering prepared using the method for embodiment 1, which presents golden yellow
Color, wherein Fig. 1-(a) the embodiment test piece macroscopic view colouring effect, Fig. 1-(b) the embodiment glaze layer enlarged drawing；We use color
Coordinate tester measures the colour space of glaze layer color, is averaged in the chromaticity coordinates that glaze randomly selects three different zones
The as chromaticity coordinates of this glaze layer；As shown in Figure 1, glaze layer chromaticity coordinates is respectively L*=80.67, a*=-1.47, b*=23.55,
Wherein L* represents brightness, and a* represents (+red ,-green), and b* represents (+yellow ,-blue), in addition, glaze layer glossiness is good, the lustrous and transparent profit of enamel and tool
There is certain beautiful texture, the defects of without pin hole, tangerine glaze.It further proves to be prepared using the method for embodiment 1 from chromaticity coordinates
Ceramic glaze golden yellow, finished product rate 98.8% is presented.
Embodiment 2
A kind of preparation method of golden yellow ceramic glaze, includes the following steps:
Step 1, weigh following component by mass percentage: partial size is nano-silver powder 1.5%, the albite of 9000nm
45.5%, quartzy 20%, calcite 21.5%, talcum 11.5%, mix the above components evenly, obtain glaze；
Glaze, water, agate abrading-ball are mixed according to the mass ratio of 1.0:1.2:1.7, ball is then carried out using planetary ball mill
Mill, ball milling rotation revolving speed are 350r/min, Ball-milling Time 10h, and ball milling finishes to obtain slurry, and slurry is crossed 250 mesh mesh sieves,
Then the density modulation of mesh sieve slurry will be crossed to 1.66g/cm with water3, modulation, which finishes, obtains glaze slip；
It is controllably high that by material composition be kaolin 58%, the biscuit of ceramics of quartz 28.5%, feldspar 13.5% is put into program
In warm furnace, after air atmosphere is warming up to 890 DEG C with the heating rate of 3 DEG C/min, furnace cooling after 20min is kept the temperature, element is obtained
Burn ceramic body；
Step 2, by the glaze slip even application prepared in step 1 in biscuit ware billet surface, controlling glazed thickness is
It is put into air dry oven after 1.0mm, at 120 DEG C after dry 6h, obtains glazing biscuit of ceramics；
Step 3, glazing biscuit of ceramics obtained in step 2 is put into program controllable high temperature furnace, in air atmosphere condition
Lower firing, burning process are as follows: rise to 1180 DEG C by room temperature for 5 DEG C/min according to heating rate, cooled to the furnace after keeping the temperature 90min
Room temperature is to get to the golden yellow ceramic glaze product.
Fig. 2 provides the golden yellow ceramic glaze effect picture prepared using the method for embodiment 2, which presents golden yellow；
We measure the colour space of glaze layer color using chromaticity coordinates tester, sit in the color that glaze randomly selects three different zones
Mark is averaged the chromaticity coordinates as this glaze layer；As shown in Figure 2, glaze layer chromaticity coordinates is respectively L*=81.56, a*=-0.23,
B*=30.79, wherein L* represents brightness, and a* represents (+red ,-green), and b* represents (+yellow ,-blue), in addition, glaze layer glossiness is good, glaze
Matter jade-like stone profit and there is certain beautiful texture, the defects of without pin hole, tangerine glaze.The side using embodiment 2 is further proved from chromaticity coordinates
Golden yellow, finished product rate 97.2% is presented in the ceramic glaze that method is prepared.
Embodiment 3
A kind of preparation method of golden yellow ceramic glaze, includes the following steps:
Step 1, weigh following component by mass percentage: nano-silver powder 3.5% that partial size is 100nm, albite 41%,
Quartzy 23.5%, calcite 21.5%, talcum 10.5%, mix the above components evenly, obtain glaze；
Glaze, water, agate abrading-ball are mixed according to the mass ratio of 1.0:1.2:1.6, ball is then carried out using planetary ball mill
Mill, ball milling rotation revolving speed are 400r/min, Ball-milling Time 12h, and ball milling finishes to obtain slurry, and slurry is crossed 250 mesh mesh sieves,
Then the density modulation of mesh sieve slurry will be crossed to 1.69g/cm with water3, modulation, which finishes, obtains glaze slip；
It is controllably high that by material composition be kaolin 58%, the biscuit of ceramics of quartz 28.5%, feldspar 13.5% is put into program
In warm furnace, after being warming up to 890 DEG C under the conditions of air atmosphere with the heating rate of 3 DEG C/min, furnace cooling after 20min is kept the temperature,
Obtain biscuit ware green body；
Step 2, by the glaze slip even application prepared in step 1 in biscuit ware billet surface, controlling glazed thickness is
It is put into air dry oven after 1.5mm, at 90 DEG C after dry 12h, obtains glazing biscuit of ceramics；
Step 3, glazing biscuit of ceramics obtained in step 2 is put into program controllable high temperature furnace, in air atmosphere condition
Lower firing, burning process are as follows: rise to 1280 DEG C by room temperature for 3 DEG C/min according to heating rate, cooled to the furnace after keeping the temperature 20min
Room temperature is to get to the golden yellow ceramic glaze product.
Fig. 3 provides the golden yellow ceramic glaze effect picture prepared using the method for embodiment 3, which is presented golden yellow,
We measure the colour space of glaze layer color using chromaticity coordinates tester, sit in the color that glaze randomly selects three different zones
Mark is averaged the chromaticity coordinates as this glaze layer；As shown in Figure 3, glaze layer chromaticity coordinates is respectively L*=72.42, a*=-2.31,
B*=28.19, wherein L* represents brightness, and a* represents (+red ,-green), and b* represents (+yellow ,-blue), in addition, glaze layer glossiness is good, glaze
Matter jade-like stone profit and there is certain beautiful texture, the defects of without pin hole, tangerine glaze.The side using embodiment 3 is further proved from chromaticity coordinates
Golden yellow, finished product rate 97.9% is presented in the ceramic glaze that method is prepared.
Embodiment 4
A kind of preparation method of golden yellow ceramic glaze, includes the following steps:
Step 1, weigh following component by mass percentage: partial size is nano-silver powder 3.5%, the albite of 40nm
38.5%, quartzy 23.5%, calcite 21.5%, talcum 13%, mix the above components evenly, obtain glaze；
Glaze, water, agate abrading-ball are mixed according to the mass ratio of 1.0:1.2:1.5, ball is then carried out using planetary ball mill
Mill, ball milling rotation revolving speed are 350r/min, Ball-milling Time 16h, and ball milling finishes to obtain slurry, and slurry is crossed 250 mesh mesh sieves,
Then the density modulation of mesh sieve slurry will be crossed to 1.66g/cm with water3, modulation, which finishes, obtains glaze slip；
It is controllably high that by material composition be kaolin 58%, the biscuit of ceramics of quartz 28.5%, feldspar 13.5% is put into program
In warm furnace, after being warming up to 890 DEG C under the conditions of air atmosphere with the heating rate of 3 DEG C/min, furnace cooling after 20min is kept the temperature,
Obtain biscuit ware green body；
Step 2, by the glaze slip even application prepared in step 1 in biscuit ware billet surface, controlling glazed thickness is
It is put into air dry oven after 1.2mm, obtains glazing biscuit of ceramics after dry 6h at 120 DEG C；
Step 3, glazing biscuit of ceramics obtained in step 2 is put into program controllable high temperature furnace, in air atmosphere condition
Lower firing, burning process are as follows: rise to 1230 DEG C by room temperature for 3 DEG C/min according to heating rate, cooled to the furnace after keeping the temperature 30min
Room temperature is to get to the golden yellow ceramic glaze product.
Fig. 4 provides the golden yellow ceramic glaze effect picture prepared using the method for embodiment 4, which presents golden yellow；
We measure the colour space of glaze layer color using chromaticity coordinates tester, sit in the color that glaze randomly selects three different zones
Mark is averaged chromaticity coordinates as this glaze layer, and as shown in Figure 4, glaze layer chromaticity coordinates is respectively L*=74.93, a*=-1.8,
B*=25.93, wherein L* represents brightness, and a* represents (+red ,-green), and b* represents (+yellow ,-blue), in addition, glaze layer glossiness is good, glaze
Matter jade-like stone profit and there is certain beautiful texture, the defects of without pin hole, tangerine glaze.The side using embodiment 4 is further proved from chromaticity coordinates
Golden yellow, finished product rate 98.9% is presented in the ceramic glaze that method is prepared.
Embodiment 5
A kind of preparation method of golden yellow ceramic glaze, includes the following steps:
Step 1, weigh following component by mass percentage: partial size is nano-silver powder 1.0%, the albite of 40nm
45.5%, quartzy 20.5%, calcite 21.5%, talcum 11.5%, mix the above components evenly, obtain glaze；
Glaze, water, agate abrading-ball are mixed according to the mass ratio of 1.0:1.2:1.5, ball is then carried out using planetary ball mill
Mill, ball milling rotation revolving speed are 300r/min, Ball-milling Time 10h, and ball milling finishes to obtain slurry, and slurry is crossed 250 mesh mesh sieves,
Then the density modulation of mesh sieve slurry will be crossed to 1.66g/cm with water3, modulation, which finishes, obtains glaze slip；
It is controllably high that by material composition be kaolin 58%, the biscuit of ceramics of quartz 28.5%, feldspar 13.5% is put into program
In warm furnace, after being warming up to 890 DEG C under the conditions of air atmosphere with the heating rate of 3 DEG C/min, furnace cooling after 20min is kept the temperature,
Obtain biscuit ware green body；
Step 2, by the glaze slip even application prepared in step 1 in biscuit ware billet surface, controlling glazed thickness is
It is put into air dry oven after 1.0mm, obtains glazing biscuit of ceramics after dry 6h at 120 DEG C；
Step 3, glazing biscuit of ceramics obtained in step 2 is put into program controllable high temperature furnace, in air atmosphere condition
Lower firing, burning process are as follows: rise to 1250 DEG C by room temperature for 5 DEG C/min according to heating rate, cooled to the furnace after keeping the temperature 30min
Room temperature is to get to the golden yellow ceramic glaze product.
Fig. 5 provides the golden yellow ceramic glaze effect picture prepared using the method for embodiment 5, which presents golden yellow；
We measure the colour space of glaze layer color using chromaticity coordinates tester, sit in the color that glaze randomly selects three different zones
Mark is averaged chromaticity coordinates as this glaze layer, and as shown in Figure 5, glaze layer chromaticity coordinates is respectively L*=68.89, a*=-0.24,
B*=30.1, wherein L* represents brightness, and a* represents (+red ,-green), and b* represents (+yellow ,-blue), in addition, glaze layer glossiness is good, glaze
Matter jade-like stone profit and there is certain beautiful texture, the defects of without pin hole, tangerine glaze.The side using embodiment 5 is further proved from chromaticity coordinates
Golden yellow, finished product rate 98.5% is presented in the ceramic glaze that method is prepared.
Embodiment 6
A kind of preparation method of golden yellow ceramic glaze, includes the following steps:
Step 1, weigh following component by mass percentage: partial size is nano-silver powder 3.5%, the albite of 1000nm
45.5%, quartzy 20%, calcite 19.5%, talcum 11.5%, mix the above components evenly, obtain glaze；
Glaze, water, agate abrading-ball are mixed according to the mass ratio of 1.0:1.2:1.5, ball is then carried out using planetary ball mill
Mill, ball milling rotation revolving speed are 350r/min, Ball-milling Time 14h, and ball milling finishes to obtain slurry, and slurry is crossed 250 mesh mesh sieves,
Then the density modulation of mesh sieve slurry will be crossed to 1.66g/cm with water3, modulation, which finishes, obtains glaze slip；
Step 2, be kaolin 58% by material composition, the biscuit of ceramics of quartz 28.5%, feldspar 13.5% is put into program
In controllable high temperature furnace, after being warming up to 890 DEG C under the conditions of air atmosphere with the heating rate of 5 DEG C/min, with furnace after heat preservation 20min
It is cooling, obtain biscuit ware green body；
Step 3, by the glaze slip even application prepared in step 1 biscuit ware billet surface in step 2, glaze layer is controlled
With a thickness of air dry oven is put into after 1.0mm, glazing biscuit of ceramics is obtained after dry 6h at 120 DEG C；
Step 4, glazing biscuit of ceramics obtained in step 3 is put into program controllable high temperature furnace, in air atmosphere condition
Lower firing, burning process are as follows: rise to 1220 DEG C by room temperature for 4 DEG C/min according to heating rate, cooled to the furnace after keeping the temperature 50min
Room temperature is to get to the golden yellow ceramic glaze product.
Fig. 6 provides the golden yellow ceramic glaze effect picture prepared using the method for embodiment 6, which presents golden yellow；
We measure the colour space of glaze layer color using chromaticity coordinates tester, sit in the color that glaze randomly selects three different zones
Mark is averaged the chromaticity coordinates as this glaze layer, and as shown in Figure 6, which is respectively L*=78.64, a*
=-0.26, b*=33.34, wherein L* represents brightness, and a* represents (+red,-green), and b* represents (+yellow,-blue), in addition, glaze layer light
Damp degree is good, the lustrous and transparent profit of enamel and has certain beautiful texture, the defects of without pin hole, tangerine glaze.It proves from chromaticity coordinates using embodiment 6
Golden yellow, finished product rate 96.9% is presented in the ceramic glaze that method is prepared.
Embodiment 7
It is identical as the preparation method of embodiment 4, the difference is that the firing temperature of biscuit of ceramics is 850 DEG C in step 1.
Embodiment 8
It is identical as the preparation method of embodiment 4, the difference is that the firing temperature of biscuit of ceramics is 900 DEG C in step 1.
It should be noted that involved in description of the invention when numberical range, it is thus understood that two of each numberical range
Any one numerical value can be selected between endpoint and two endpoints, and the step method not selected must be with embodiment 1-8 phase
Together；In addition, the colour space of glaze layer color is surveyed with chromaticity coordinates tester, and since glaze colour generation is uniform, the chromaticity coordinates provided
For the average value of three different zones of glaze random test；It repeats in order to prevent, the present invention describes preferred embodiment, but this
Technical staff in field once knows basic creative concept, then can make other change to these embodiments and repair
Change.Include preferred embodiment and fall into having altered and repairing for the scope of the invention so the following claims are intended to be interpreted as
Change.
Obviously, various changes and modifications can be made to the invention without departing from essence of the invention by those skilled in the art
Mind and range.In this way, if these modifications and changes of the present invention belongs to the range of the claims in the present invention and its equivalent technologies
Within, then the present invention is also intended to include these modifications and variations.
Claims (9)
1. a kind of preparation method of golden yellow ceramic glaze, which comprises the following steps:
Step 1, ball milling is carried out after glaze, water, agate abrading-ball being mixed according to the mass ratio of 1.0:1.2:1.5-1.7, is starched
Material, then filtering and filtrate is modulated into density is 1.66-1.69g/cm3Solution, obtain glaze slip；
Wherein, the glaze consists of the following mass percentage components: micro-nano silver powder 0.8%-3.5%, albite
38.5%-45.5%, quartz 20%-23.5%, calcite 19.5%-21.5%, talcum 10.5%-13%；
Step 2, biscuit of ceramics is fired in 850 DEG C -900 DEG C in air atmosphere, obtains biscuit ware green body；
By glaze slip even application obtained in step 1 in biscuit ware billet surface, and it is sufficiently dry, obtain glazing ceramics element
Base；
Step 3, glazing biscuit of ceramics obtained in step 2 is fired in 1180-1280 DEG C in air atmosphere, obtains glaze
The uniform golden yellow ceramic glaze of layer surface.
2. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that ball in the step 1
Mill revolving speed is 300-400r/min, Ball-milling Time 10-16h.
3. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that micro- in the step 1
Nano-silver powder partial size is 30-9000 nanometers.
4. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that institute in the step 2
It states biscuit of ceramics to consist of the following mass percentage components: kaolin 58%, quartzy 28.5%, feldspar 13.5%.
5. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that make pottery in the step 2
The sintering procedure of porcelain biscuit are as follows: be warming up to 850-900 DEG C according to the heating rate of 3-5 DEG C/min, keep the temperature 20-30min.
6. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that applied in the step 2
The glazed thickness of glaze biscuit of ceramics is 1.0-1.5mm.
7. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that filled in the step 2
Dividing dry temperature is 90-120 DEG C, drying time 6-12h.
8. a kind of preparation method of golden yellow ceramic glaze according to claim 1, which is characterized in that applied in the step 3
The sintering procedure of glaze biscuit of ceramics are as follows: be warming up to 1180-1280 DEG C according to the heating rate of 3-5 DEG C/min, keep the temperature 20-90min.
9. the golden yellow ceramic glaze that preparation method according to claim 1-8 is prepared.
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Cited By (2)
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| CN111423120A (en) * | 2020-04-27 | 2020-07-17 | 许昌学院 | Preparation method of pine and cypress green ceramic glaze |
| CN111533577A (en) * | 2020-05-20 | 2020-08-14 | 许昌学院 | Dredged sediment resource utilization method and application |
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| CN111423120A (en) * | 2020-04-27 | 2020-07-17 | 许昌学院 | Preparation method of pine and cypress green ceramic glaze |
| CN111533577A (en) * | 2020-05-20 | 2020-08-14 | 许昌学院 | Dredged sediment resource utilization method and application |
| CN111533577B (en) * | 2020-05-20 | 2022-06-07 | 许昌学院 | Dredged sediment resource utilization method and application |
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