CN109456035A - A kind of Ceramic Tiles and preparation method thereof with bright mute effect - Google Patents
A kind of Ceramic Tiles and preparation method thereof with bright mute effect Download PDFInfo
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- CN109456035A CN109456035A CN201811514663.XA CN201811514663A CN109456035A CN 109456035 A CN109456035 A CN 109456035A CN 201811514663 A CN201811514663 A CN 201811514663A CN 109456035 A CN109456035 A CN 109456035A
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- bright
- bright mute
- ceramic tiles
- mute
- pattern texture
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- 239000000919 ceramic Substances 0.000 title claims abstract description 88
- 230000000694 effects Effects 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000003292 glue Substances 0.000 claims abstract description 33
- 238000007641 inkjet printing Methods 0.000 claims abstract description 15
- 238000010304 firing Methods 0.000 claims abstract description 8
- 239000008187 granular material Substances 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000005507 spraying Methods 0.000 claims abstract description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 12
- 238000002844 melting Methods 0.000 claims description 9
- 230000008018 melting Effects 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 6
- 229920001651 Cyanoacrylate Polymers 0.000 claims description 5
- FUJCRWPEOMXPAD-UHFFFAOYSA-N Li2O Inorganic materials [Li+].[Li+].[O-2] FUJCRWPEOMXPAD-UHFFFAOYSA-N 0.000 claims description 5
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 5
- 239000000853 adhesive Substances 0.000 claims description 5
- 230000001070 adhesive effect Effects 0.000 claims description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 5
- 229910052593 corundum Inorganic materials 0.000 claims description 5
- XUCJHNOBJLKZNU-UHFFFAOYSA-M dilithium;hydroxide Chemical compound [Li+].[Li+].[OH-] XUCJHNOBJLKZNU-UHFFFAOYSA-M 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 229910001845 yogo sapphire Inorganic materials 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 5
- 239000011449 brick Substances 0.000 abstract description 4
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 5
- 230000001795 light effect Effects 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000004568 cement Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000005034 decoration Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052573 porcelain Inorganic materials 0.000 description 2
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 2
- 229910052720 vanadium Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 1
- 208000003464 asthenopia Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007665 sagging Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Finishing Walls (AREA)
Abstract
The invention discloses a kind of preparation methods of Ceramic Tiles with bright mute effect comprising following processing step: 1) in charity overglaze on Ceramic Tiles green compact, obtaining cover coat；2) the inkjet printing decorative pattern texture on cover coat, drying, obtains decorative pattern texture layer；3) low-temp ceramics glue of the inkjet printing with pattern texture on decorative pattern texture layer, obtains low-temp ceramics glue layer；4) it in spraying bright mute dry granular glaze on low-temp ceramics glue layer, dries, obtains bright mute dry granule layer；5) through high temperature firing, finished product is obtained.The present invention passes through low-temp ceramics glue and bright mute dry granular glaze synergistic effect, keep the serious forgiveness of decorative pattern texture and glue pattern texture high, it realizes the effect of bright mute combination on decorative pattern texture layer while also achieving the effect of bright mute combination in the bright mute dry granule layer of ceramic brick surface, so that the bright mute effect controllability of entire Ceramic Tiles is strong and decorative pattern clarity is good.The invention also discloses the Ceramic Tiles with bright mute effect for having the above method to be prepared into.
Description
Technical field
The present invention relates to architectural pottery field, in particular to a kind of Ceramic Tiles with bright mute effect.
Background technique
Building ceramic tiles are a not retrievable ceramic-like ornament materials in home decoration instantly, and category is numerous,
It is all in polished bricks, glazed tile, Antique Imitation Tiles and tile etc..The introduction of inkjet printing technology greatly enriches Ceramic Tiles table
The heat of the pattern in face, the market for allowing one time of glazed tile to receive is held in both hands, still, also just because of the introduction of inkjet printing technology,
So that homogeneity more serious of the decorative effect on the surface of Ceramic Tiles, is easy to produce visual fatigue, also appearance gradually
Flower prod is seeped in some individual decoration products, such as ink-jet, and sink glaze, all-body tile etc..On the other hand, there is light, dumb light
Or the Ceramic Tiles of bright mute decorative effect are also come into being.
There is tradition the technique of the Ceramic Tiles of bright mute effect only to combine light and dumb light dry granular, and only in ceramics
The surface of brick realizes that light and dumb light combine, i.e., can only realize the effect that light and dumb light combine in glaze.Sagging glaze
It is able to achieve light and effect that dumb light combines, basic technique is that inkjet printing sink functional ink in Ceramic Tiles, under
The compound for containing a kind of vanadium is fallen into functional ink, on the one hand it can reduce the surface tension and viscosity of glaze, on the other hand,
In the environment of high temperature, the compound of vanadium, which can decompose, to be generated gas and constantly breaks through glaze and formed local recessed to realize
The light effect of bogging down area.It is owed however, the above-mentioned obtained bright mute decorative effect of these modes has decorative pattern clarity
The drawbacks of good and bright mute effect poor controllability.
Summary of the invention
It is an object of the invention in view of the above shortcomings of the prior art, provide a kind of Ceramic Tiles with bright mute effect
Preparation method.
The technical solution used in the present invention is: a kind of preparation method of the Ceramic Tiles with bright mute effect comprising such as
Lower processing step:
1) in charity overglaze on Ceramic Tiles green compact, cover coat is obtained；
2) the inkjet printing decorative pattern texture on cover coat, drying, obtains decorative pattern texture layer；
3) low-temp ceramics glue of the inkjet printing with pattern texture on decorative pattern texture layer, obtains low-temp ceramics glue
Layer；
4) it in spraying bright mute dry granular glaze on low-temp ceramics glue layer, dries, obtains bright mute dry granule layer；
5) through high temperature firing, finished product is obtained.
Specifically, the pattern texture of the low-temp ceramics glue layer both can be with the pattern line of the decorative pattern texture layer
It manages overlapped, can also be used as the supplement of the pattern texture of decorative pattern texture layer, so that the width of its light effect
Controllably, width with low-temp ceramics glue change width, can width can be narrow, it is wide arrive decorative pattern, carefully may be implemented to line portion.
As a further improvement of the foregoing solution, low-temp ceramics glue described in step 3) are by a-cyanoacrylate second
Ester adhesive and inorganic ceramic fluxing agent composition, solid content are 5~15%.
In the present invention, due to there is the presence of the low-temp ceramics glue, when the bright mute dry granular in bright mute dry granular glaze is sticked to this
When above layer low-temp ceramics glue, because the melting temperature of dry granular is higher, the interface of the two can be in inorganic ceramic fluxing agent
Effect is lower to be occurred melting but will not melt flat dry granular completely, so just will appear the light effect of dry granular partial melting in interface
Fruit, the decorative pattern texture covered without low-temp ceramics glue layer is exactly matte effect, is filled on glazed layer to realize
Adorn the bright mute artistic effect combined of pattern texture.
As a further improvement of the foregoing solution, the SiO that the chemical composition of the inorganic ceramic fluxing agent is 50%2, 4%
Al2O3, 32% B2O3, 3% Li2O, 13% Na2O, 6% K2The CaO of O and 3%.Specifically, inorganic ceramic is fluxing
Agent chemical constituent defines the melting effect for being conducive to further improve low-temp ceramics glue and bright mute dry granular glaze interface.
As a further improvement of the foregoing solution, the melting temperature of low-temp ceramics glue described in step 3) be 900~
1100℃。
As a further improvement of the foregoing solution, bright mute dry granular glaze described in step 4) is pressed by bright mute dry granular and ceramic stamp-pad ink
Mass ratio is 1:(1~1.2) composition.
As a further improvement of the foregoing solution, the partial size of the bright mute dry granular is advantageous within the scope of 100~200 mesh
In the pattern texture clarity for improving decorative pattern texture layer under bright mute effect.
As a further improvement of the foregoing solution, the bright mute dry granular is by light dry granular and dumb light dry granular example in mass ratio
1:(1~1.5) composition.
As a further improvement of the foregoing solution, the temperature of high temperature firing described in step 5) is 1200~1250 DEG C.
The object of the invention is also to provide a kind of Ceramic Tiles with bright mute effect, by preparation method as described above
It is prepared.
The beneficial effects of the present invention are: the present invention makes to decorate by low-temp ceramics glue and bright mute dry granular glaze synergistic effect
The serious forgiveness of pattern texture and glue pattern texture is high, realizes on decorative pattern texture layer the effect of bright mute combination also reality simultaneously
The effect of bright mute combination in the bright mute dry granule layer of ceramic brick surface is showed, so that the bright mute effect controllability of entire Ceramic Tiles is strong and fills
It is good to adorn pattern definition.
Specific embodiment
The present invention is specifically described below with reference to embodiment, in order to technical field personnel to of the invention
Understand.It is necessary to it is emphasized that embodiment is only intended to, the present invention will be further described herein, should not be understood as to this
The limitation of invention protection scope, fields person skilled in the art, the non-intrinsically safe that the present invention is made according to foregoing invention content
The modifications and adaptations of property, should still fall within protection scope of the present invention.Mentioned raw materials following simultaneously are unspecified, are
Commercial product；The processing step or preparation method not referred in detail be processing step known to a person skilled in the art or
Preparation method.
Embodiment 1
A kind of preparation method of the Ceramic Tiles with bright mute effect comprising following processing step:
1) in charity overglaze on Ceramic Tiles green compact, cover coat is obtained；
2) the inkjet printing decorative pattern texture on cover coat, drying, obtains decorative pattern texture layer；
3) low temperature that melting temperature of the inkjet printing with pattern texture is 900~1100 DEG C on decorative pattern texture layer is made pottery
Porcelain cement water obtains low-temp ceramics glue layer；
4) taking particle size range is 100~150 mesh light dry granulars and dumb light dry granular, and light dry granular and dumb light dry granular are pressed quality
Than mixing for 1:1, ceramic stamp-pad ink is then added, the mass ratio of ceramic stamp-pad ink and bright mute dry granular is 1:1, obtains bright mute dry granular glaze；
5) it in spraying bright mute dry granular glaze on low-temp ceramics glue layer, dries, obtains bright mute dry granule layer；
6) through 1200 DEG C of high temperature firings, 1 finished product of embodiment is obtained.
Wherein, the low-temp ceramics glue is made of a-cyanoacrylate ethyl ester adhesive and inorganic ceramic fluxing agent,
Its solid content is 5%, the SiO that the chemical composition of the inorganic ceramic fluxing agent is 50%2, 4% Al2O3, 32% B2O3、
3% Li2O, 13% Na2O, 6% K2The CaO of O and 3%.
Embodiment 2
A kind of preparation method of the Ceramic Tiles with bright mute effect comprising following processing step:
1) in charity overglaze on Ceramic Tiles green compact, cover coat is obtained；
2) the inkjet printing decorative pattern texture on cover coat, drying, obtains decorative pattern texture layer；
3) low temperature that melting temperature of the inkjet printing with pattern texture is 1050~1100 DEG C on decorative pattern texture layer
Ceramic glue obtains low-temp ceramics glue layer；
4) taking particle size range is 150~200 mesh light dry granulars and dumb light dry granular, and light dry granular and dumb light dry granular are pressed quality
Than mixing for 1:1.5, ceramic stamp-pad ink is then added, the mass ratio of ceramic stamp-pad ink and bright mute dry granular is 1:1.2, obtains bright mute dry granular
Glaze；
5) it in spraying bright mute dry granular glaze on low-temp ceramics glue layer, dries, obtains bright mute dry granule layer；
6) through 1250 DEG C of high temperature firings, 2 finished product of embodiment is obtained.
Wherein, the low-temp ceramics glue is made of a-cyanoacrylate ethyl ester adhesive and inorganic ceramic fluxing agent,
Its solid content is 15%, the SiO that the chemical composition of the inorganic ceramic fluxing agent is 50%2, 4% Al2O3, 32% B2O3、
3% Li2O, 13% Na2O, 6% K2The CaO of O and 3%.
Embodiment 3
A kind of preparation method of the Ceramic Tiles with bright mute effect comprising following processing step:
1) in charity overglaze on Ceramic Tiles green compact, cover coat is obtained；
2) the inkjet printing decorative pattern texture on cover coat, drying, obtains decorative pattern texture layer；
3) low temperature that melting temperature of the inkjet printing with pattern texture is 950~1100 DEG C on decorative pattern texture layer is made pottery
Porcelain cement water obtains low-temp ceramics glue layer；
4) taking particle size range is 100~200 mesh light dry granulars and dumb light dry granular, and light dry granular and dumb light dry granular are pressed quality
Than mixing for 1:1.2, ceramic stamp-pad ink is then added, the mass ratio of ceramic stamp-pad ink and bright mute dry granular is 1:1.1, obtains bright mute dry granular
Glaze；
5) it in spraying bright mute dry granular glaze on low-temp ceramics glue layer, dries, obtains bright mute dry granule layer；
6) through 1230 DEG C of high temperature firings, 3 finished product of embodiment is obtained.
Wherein, the low-temp ceramics glue is made of a-cyanoacrylate ethyl ester adhesive and inorganic ceramic fluxing agent,
Its solid content is 10%, the SiO that the chemical composition of the inorganic ceramic fluxing agent is 50%2, 4% Al2O3, 32% B2O3、
3% Li2O, 13% Na2O, 6% K2The CaO of O and 3%.
Above-described embodiment is the preferred embodiment of the present invention, all with similar technique of the invention and made equivalence changes,
It should belong to protection category of the invention.
Claims (9)
1. a kind of preparation method of the Ceramic Tiles with bright mute effect, it is characterised in that comprise the technical steps that:
1) in charity overglaze on Ceramic Tiles green compact, cover coat is obtained；
2) the inkjet printing decorative pattern texture on cover coat, drying, obtains decorative pattern texture layer；
3) low-temp ceramics glue of the inkjet printing with pattern texture on decorative pattern texture layer, obtains low-temp ceramics glue layer；
4) it in spraying bright mute dry granular glaze on low-temp ceramics glue layer, dries, obtains bright mute dry granule layer；
5) through high temperature firing, finished product is obtained.
2. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 1, it is characterised in that: step 3)
Described in low-temp ceramics glue be made of a-cyanoacrylate ethyl ester adhesive and inorganic ceramic fluxing agent, solid content is
5~15%.
3. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 2, it is characterised in that: the nothing
The SiO that the chemical composition of machine ceramics fluxing agent is 50%2, 4% Al2O3, 32% B2O3, 3% Li2O, 13% Na2O、
6% K2The CaO of O and 3%.
4. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 1, it is characterised in that: step 3)
Described in low-temp ceramics glue melting temperature be 900~1100 DEG C.
5. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 1, it is characterised in that: step 4)
Described in bright mute dry granular glaze by bright mute dry granular and ceramic stamp-pad ink be in mass ratio 1:(1~1.2) form.
6. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 5, it is characterised in that: described bright
The partial size of mute dry granular is within the scope of 100~200 mesh.
7. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 5, it is characterised in that: described bright
Mute dry granular is 1:(1~1.5 by light dry granular and dumb light dry granular example in mass ratio) it forms.
8. a kind of preparation method of Ceramic Tiles with bright mute effect according to claim 1, it is characterised in that: step 5)
Described in high temperature firing temperature be 1200~1250 DEG C.
9. a kind of Ceramic Tiles with bright mute effect, it is characterised in that by preparation method system according to any one of claims 1 to 8
It is standby to form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811514663.XA CN109456035B (en) | 2018-12-11 | 2018-12-11 | Ceramic tile with bright and matte effect and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811514663.XA CN109456035B (en) | 2018-12-11 | 2018-12-11 | Ceramic tile with bright and matte effect and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109456035A true CN109456035A (en) | 2019-03-12 |
| CN109456035B CN109456035B (en) | 2020-06-16 |
Family
ID=65613054
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811514663.XA Active CN109456035B (en) | 2018-12-11 | 2018-12-11 | Ceramic tile with bright and matte effect and preparation method thereof |
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| Country | Link |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110128172A (en) * | 2019-04-28 | 2019-08-16 | 东莞市唯美陶瓷工业园有限公司 | A kind of method improving Ceramic Tiles green surface performance of keeping humidity and the Ceramic Tiles using this method preparation |
| CN110357428A (en) * | 2019-08-09 | 2019-10-22 | 东莞市唯美陶瓷工业园有限公司 | A kind of preparation method and Ceramic Tiles of the controllable Ceramic Tiles of glaze glossiness |
| CN110668846A (en) * | 2019-10-11 | 2020-01-10 | 山东狮王陶瓷有限公司 | Preparation process of matte wear-resistant dry particle brick |
| CN111499201A (en) * | 2020-06-17 | 2020-08-07 | 佛山东华盛昌新材料有限公司 | Low-temperature eutectic ink, preparation method thereof and preparation method of ceramic tile thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110128172A (en) * | 2019-04-28 | 2019-08-16 | 东莞市唯美陶瓷工业园有限公司 | A kind of method improving Ceramic Tiles green surface performance of keeping humidity and the Ceramic Tiles using this method preparation |
| CN110357428A (en) * | 2019-08-09 | 2019-10-22 | 东莞市唯美陶瓷工业园有限公司 | A kind of preparation method and Ceramic Tiles of the controllable Ceramic Tiles of glaze glossiness |
| CN110668846A (en) * | 2019-10-11 | 2020-01-10 | 山东狮王陶瓷有限公司 | Preparation process of matte wear-resistant dry particle brick |
| CN111499201A (en) * | 2020-06-17 | 2020-08-07 | 佛山东华盛昌新材料有限公司 | Low-temperature eutectic ink, preparation method thereof and preparation method of ceramic tile thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109456035B (en) | 2020-06-16 |
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