CN105315015A - Preparation method for architectural decoration flambe art ceramic tile - Google Patents
Preparation method for architectural decoration flambe art ceramic tile Download PDFInfo
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- CN105315015A CN105315015A CN201410726519.8A CN201410726519A CN105315015A CN 105315015 A CN105315015 A CN 105315015A CN 201410726519 A CN201410726519 A CN 201410726519A CN 105315015 A CN105315015 A CN 105315015A
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Abstract
The invention discloses a preparation method for an architectural decoration flambe art ceramic tile. Ground coat is prepared from, by weight, 14%-19% of potassium feldspar+albite, 10%-15% of porcelain sand, 5%-10% of kaolin, 5%-12% of zinc oxide, 5%-10% of calcined talc, 15%-20% of barium carbonate, 3%-8% of dolomite, 11%-16% of calcium carbonate, 3%-10% of calcium phosphate and 2%-7% of aluminum oxide. Cover glaze is prepared from, by weight, 16%-23% of feldspar+albite, 5%-10% of porcelain sand, 5%-10% of kaolin, 17%-23% of zinc oxide, 5%-10% of calcined talc, 10%-16% of zirconium silicate, 14%-18% of titanium oxide, 5%-10% of glass dust and 1%-2% of colorant. The architectural decoration flambe art ceramic tile is formed through the steps of burdening, pulping, powder making, press forming, drying, ground coat sprinkling, cover glaze sprinkling, firing, fine trimming packaging and the like. The apparent size of snowflake-shaped crystal patterns ranges from 3 mm to 6 mm, and the maximum apparent size of cotton-shaped crystal patterns can reach about 20 mm. Low-temperature rapid sintering of flambe art ceramic is achieved, firing cost is reduced, and energy saving, consumption reduction and emission reduction are achieved.
Description
Technical field
The present invention relates to ceramic technology field, particularly relate to a kind of preparation method of apparatus for building transmutation art pottery ceramic tile.
Background technology
Furnace transmutation glaze is the art of Yi Menshui, soil, fire, and it is very popular as the rarity in ancient Chinese ceramics art, the outstanding person of crystallization furnace transmutation glaze product especially in transmutation.But traditional crystallization furnace transmutation glaze product is high temperature product, and its production cost is very high, survives difficulty very large, be difficult to realize industrialized production.Though so crystallization furnace transmutation glaze has initial development in modern crafts product and household china, be almost space state in the development of architectural pottery Wall or floor tile direction furnace transmutation glaze.Tradition crystallization furnace transmutation glaze artistic product firing time at least 70 minutes, temperature more than 1230 DEG C.Adopt traditional crystallization furnace transmutation glaze technique, energy consumption is high, is also unfavorable for the development of building decoration transmutation art pottery ceramic tile.
Summary of the invention
The object of the present invention is to provide a kind of sintering temperature low, firing time is short, the preparation method of the building decoration transmutation art pottery that energy consumption is low:
The technical solution used in the present invention is:
A preparation method for the building decoration transmutation art pottery, comprises following steps:
A. prepare burden: take blank raw material according to weight percent;
B. slurrying: weigh up raw material according to the ratio in A, and according to material: ball: the ratio of water=1:2:0.35 puts into ball mill ball milling mixing raw material; The slip of 250 mesh sieve screen over-sizes 1.2 ~ 1.7% was formed after ball mill ball milling;
C. powder process: by the slurry that obtains in step B by the finish mix powder of spray-dryer, then ageing 2 ~ 3 days;
D. compression moulding: be pressed into adobe by obtaining the material powder after ageing in step C;
E. dry: the powder pressing obtained by step C becomes adobe, then gradient increased temperature to 200 DEG C, after dry, adobe water ratio is 0.5 ~ 1%, base substrate temperature 65 ~ 70 DEG C;
F. ground-coat enamel is drenched: ground-coat enamel is made up of following components in weight percent:
Potassium felspar sand+albite 14 ~ 19%
Porcelain sand 10 ~ 15%
Kaolin 5 ~ 10%
Zinc oxide 5 ~ 12%
Forge talcum 5 ~ 10%
Barium carbonate 15 ~ 20%
Rhombspar 3 ~ 8%
Calcium carbonate 11 ~ 16%
Calcium phosphate 3 ~ 10%
Aluminum oxide 2 ~ 7%;
G. cover-coat enamel is drenched: cover-coat enamel is made up of following components in weight percent:
Potassium felspar sand+albite 16 ~ 23%
Porcelain sand 5 ~ 10%
Kaolin 5 ~ 10%
Zinc oxide 17 ~ 23%
Forge talcum 5 ~ 10%
Zirconium silicate 10 ~ 16%
Titanium oxide 14 ~ 18%
Glass powder 5 ~ 10%
Tinting material 1 ~ 2%;
H. burn till: the base substrate in step G after glazing is placed in kiln and burns till, gradient increased temperature to 1198 ~ 1210 DEG C, firing time 40 ~ 45min, oxic gas atmosphere;
I. refine packaging.
Further, after in described step F, ground-coat enamel raw material weighs by mass percentage, according to material: ball: the ratio ball milling mixing raw material of water=1:2:0.35, was formed as the slurry of 250 mesh sieve screen over-sizes 0.5 ~ 0.8% after ball mill ball milling.
Further, the proportion 1.65 ~ 1.70g/cm of ground-coat enamel in described step F
3, glaze volume 90 ~ 98g.
Further, after in described step G, cover-coat enamel raw material weighs by mass percentage, according to material: ball: the ratio ball milling mixing raw material of water=1:2:0.35, was formed as the slurry of 250 mesh sieve screen over-sizes 0.5 ~ 0.8% after ball mill ball milling.
Further, cover-coat enamel cover-coat enamel proportion 1.65 ~ 1.70g/cm3, glaze volume 53 ~ 58g in described step G.
Further, in described step G, tinting material is one or more in cobalt oxide, cupric oxide, oxidation chrome yellow, red iron oxide.
Further, in described steps A, blank raw material is made up of following components in weight percent:
Kaolin 10 ~ 15%
Weathered Sand 7 ~ 12%
Potassium felspar sand 28 ~ 35%
Low chamotte 22 ~ 32%
Pure white sand 7 ~ 12%
Useless base powder 3 ~ 8%
Black talc 2 ~ 7%.
Further, in described step F, when ground-coat enamel raw material ball grinds slurry, zinc oxide finally adds ball mill, then continues ball ball milling mixing 1 ~ 2min.
Further, in described step G, when cover-coat enamel raw material ball grinds slurry, zinc oxide finally adds ball mill, then continues ball ball milling mixing 1 ~ 2min.
Further, ground-coat enamel is made up of the raw material of following weight percent: albite 16%, porcelain sand 15%, kaolin 7.5%, and zinc oxide 6.5% forges talcum 7.5%, barium carbonate 16%, rhombspar 7%, calcium carbonate 16%, calcium phosphate 5%, aluminum oxide 3.5%;
Cover-coat enamel is made up of the raw material of following weight percent: albite 22%, porcelain sand 8%, kaolin 8%; Zinc oxide 22%; Forge talcum 5%; Titanium oxide 15%, zirconium silicate 12%, glass powder 8%, tinting material 1.2%.
The invention has the beneficial effects as follows:
1) the building decoration transmutation art pottery brick glaze face basic property adopting technology of the present invention to produce all reaches national GB/T4100-2006: " ceramic tile " product national standard.
2) in the present invention, firing temperature is about 1198-1210 DEG C, firing period is about 40-45 minute, current furnace transmutation glaze artistic product firing time at least 70 minutes, temperature more than 1230 DEG C, both compare, firing temperature reduces by more than 20 DEG C, shorten firing time at least 30 minutes, reduce and fire cost, realize saving energy, lowering energy consumption and reducing pollutants discharge.
3) the building decoration transmutation art pottery ceramic tile adopting technology of the present invention to fire, flakes crystalline substance flower apparent size reaches 3-6mm, and apparent size is maximum reaches about 20mm for cotton-shaped crystalline substance flower, solves the technical barrier that current Low Temperature and Fast Firing Crystalline Glaze is difficult to realize.
4) adopt technology of the present invention to produce 300mmX300mm specification product, every square metre than former same specification common ornamental brick raising added value of product 30 yuan meter, annual by conservative yield production 5,000,000 square metres calculating, amount to and can directly increase added value of product 15 whole year, 0000000 yuan, its economic benefit is obvious, ancient pottery and porcelain art advanced ceramics technological perfectionism is reproduced simultaneously, realize ancient times luxurious artistic popular, this technology is tradition and the fusion of fashion, embodies decorative value and the artistic value of architectural pottery fully.
Accompanying drawing explanation
Fig. 1 embodiment one scan Electron Microscopy Results.
Fig. 2 embodiment two scanning electronic microscope detected result.
Fig. 3 embodiment three scanning electronic microscope detected result.
Embodiment
In order to make the advantage of object of the present invention and technical scheme clearly understand, below in conjunction with example, the present invention is further elaborated.
Embodiment one
A preparation method for the building decoration transmutation art pottery, comprises following steps:
A. prepare burden: take blank raw material according to weight percent, blank raw material is made up of following components in weight percent:
Kaolin 10%
Weathered Sand 7%
Potassium felspar sand 28%
Low chamotte 32%
Pure white sand 12%
Useless base powder 4%
Black talc 7%.
B. slurrying: weigh up raw material according to the ratio in A, and according to material: ball: the ratio of water=1:2:0.35 puts into ball mill ball milling mixing raw material; The slip of 250 mesh sieve screen over-sizes 1.2 ~ 1.7% was formed after ball mill ball milling.
C. powder process: by the slurry that obtains in step B by the finish mix powder of spray-dryer, then ageing 2 ~ 3 days.
D. compression moulding: be pressed into adobe by obtaining the material powder after ageing in step C.
E. dry: the powder pressing obtained by step C becomes adobe, then gradient increased temperature to 200 DEG C, after dry, adobe water ratio is 0.5 ~ 1%, base substrate temperature 65 ~ 70 DEG C.
F. ground-coat enamel is drenched: ground-coat enamel is made up of following components in weight percent:
Potassium felspar sand+albite 14%
Porcelain sand 15%
Kaolin 5%
Zinc oxide 12%
Forge talcum 5%
Barium carbonate 20%
Rhombspar 3%
Calcium carbonate 16%
Calcium phosphate 3%
Aluminum oxide 7%;
After being weighed by mass percentage by ground-coat enamel raw material, according to material: ball: the ratio ball milling mixing raw material of water=1:2:0.35, zinc oxide finally adds ball mill, then continues ball milling mixing 1 ~ 2min.The slurry of 250 mesh sieve screen over-sizes 0.5 ~ 0.8% was formed as after ball mill ball milling; Proportion 1.65 ~ the 1.70g/cm of ground-coat enamel
3, glaze volume 90 ~ 98g.
G. cover-coat enamel is drenched: cover-coat enamel is made up of following components in weight percent:
Potassium felspar sand+albite 16%
Porcelain sand 10%
Kaolin 5%
Zinc oxide 23%
Forge talcum 5%
Zirconium silicate 16%
Titanium oxide 14%
Glass powder 10%
Tinting material 1%;
After being weighed by mass percentage by cover-coat enamel raw material, according to material: ball: the ratio ball milling mixing raw material of water=1:2:0.35, zinc oxide finally adds ball mill, then continues ball milling mixing 1 ~ 2min.The slurry of 250 mesh sieve screen over-sizes 0.5 ~ 0.8% was formed as after ball mill ball milling; Proportion 1.65 ~ the 1.70g/cm of ground-coat enamel
3, glaze volume 53 ~ 58g.
H. burn till: the base substrate in step G after glazing is placed in kiln and burns till, gradient increased temperature to 1198 ~ 1210 DEG C, firing time 40 ~ 45min, oxic gas atmosphere;
I. refine packaging.
Embodiment two
Blank is made up of the component of following weight percent: kaolin 15%, Weathered Sand 12%, potassium felspar sand 35%, low chamotte 22%, pure white sand 7%.Useless base powder 7%, black talc 2%;
Ground-coat enamel is made up of the component of following weight percent: potassium felspar sand 19%, porcelain sand 10%, kaolin 10%, and zinc oxide 5% forges talcum 10%, barium carbonate 15%, rhombspar 8%, calcium carbonate 11%, calcium phosphate 10%, aluminum oxide 2%
Cover-coat enamel is made up of the component of following weight percent: potassium felspar sand 23%, porcelain sand 5%, kaolin 10%, and zinc oxide 17% forges talcum 10%, zirconium silicate 10%, titanium oxide 18%, glass powder 5%, cobalt oxide 2%.
Other steps are with embodiment one.
Embodiment three
Blank is made up of the component of following weight percent: kaolin 12%, Weathered Sand 10%, potassium felspar sand 30%, low chamotte 28%, pure white sand 9%.Useless base powder 6%, black talc 5%;
Ground-coat enamel is made up of the raw material of following weight percent: albite 16%, porcelain sand 15%, kaolin 7.5%, and zinc oxide 6.5% forges talcum 7.5%, barium carbonate 16%, rhombspar 7%, calcium carbonate 16%, calcium phosphate 5%, aluminum oxide 3.5%;
Cover-coat enamel is made up of the raw material of following weight percent: albite 22%, porcelain sand 8%, kaolin 8%; Zinc oxide 22%; Forge talcum 5%; Titanium oxide 15%, zirconium silicate 12%, glass powder 8%, tinting material 1.2%.
Other steps are with embodiment one.
The crystalline substance flower of transmutation art pottery ceramic tile detects as shown in drawings.
Claims (10)
1. a preparation method for the building decoration transmutation art pottery, its spy is to comprise following steps:
A. prepare burden: take blank raw material according to weight percent;
B. slurrying: weigh up raw material according to the ratio in A, and according to material: ball: the ratio of water=1:2:0.35 puts into ball mill ball milling mixing raw material; The slip of 250 mesh sieve screen over-sizes 1.2 ~ 1.7% was formed after ball mill ball milling;
C. powder process: by the slurry that obtains in step B by the finish mix powder of spray-dryer, then ageing 2 ~ 3 days;
D. compression moulding: be pressed into adobe by obtaining the material powder after ageing in step C;
E. dry: the powder pressing obtained by step C becomes adobe, then gradient increased temperature to 200 DEG C, after dry, adobe water ratio is 0.5 ~ 1%, base substrate temperature 65 ~ 70 DEG C;
F. ground-coat enamel is drenched: ground-coat enamel is made up of following components in weight percent:
Potassium felspar sand+albite 14 ~ 19%
Porcelain sand 10 ~ 15%
Kaolin 5 ~ 10%
Zinc oxide 5 ~ 12%
Forge talcum 5 ~ 10%
Barium carbonate 15 ~ 20%
Rhombspar 3 ~ 8%
Calcium carbonate 11 ~ 16%
Calcium phosphate 3 ~ 10%
Aluminum oxide 2 ~ 7%;
G. cover-coat enamel is drenched: cover-coat enamel is made up of following components in weight percent:
Potassium felspar sand+albite 16 ~ 23%
Porcelain sand 5 ~ 10%
Kaolin 5 ~ 10%
Zinc oxide 17 ~ 23%
Forge talcum 5 ~ 10%
Zirconium silicate 10 ~ 16%
Titanium oxide 14 ~ 18%
Glass powder 5 ~ 10%
Tinting material 1 ~ 2%;
H. burn till: the base substrate in step G after glazing is placed in kiln and burns till, gradient increased temperature to 1198 ~ 1210 DEG C, firing time 40 ~ 45min, oxic gas atmosphere;
I. refine packaging.
2. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1, it is characterized in that: after in described step F, ground-coat enamel raw material weighs by mass percentage, according to material: ball: the ratio ball milling mixing raw material of water=1:2:0.35, was formed as the slurry of 250 mesh sieve screen over-sizes 0.5 ~ 0.8% after ball mill ball milling.
3. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1 and 2, is characterized in that: the proportion 1.65 ~ 1.70g/cm of ground-coat enamel in described step F
3, glaze volume 90 ~ 98g.
4. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1, it is characterized in that: after in described step G, cover-coat enamel raw material weighs by mass percentage, according to material: ball: the ratio ball milling mixing raw material of water=1:2:0.35, was formed as the slurry of 250 mesh sieve screen over-sizes 0.5 ~ 0.8% after ball mill ball milling.
5. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1 or 4, is characterized in that: cover-coat enamel cover-coat enamel proportion 1.65 ~ 1.70g/cm in described step G
3, glaze volume 53 ~ 58g.
6. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1, is characterized in that: in described step G, tinting material is one or more in cobalt oxide, cupric oxide, oxidation chrome yellow, red iron oxide.
7. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1, is characterized in that: in described steps A, blank raw material is made up of following components in weight percent:
Kaolin 10 ~ 15%
Weathered Sand 7 ~ 12%
Potassium felspar sand 28 ~ 35%
Low chamotte 22 ~ 32%
Pure white sand 7 ~ 12%
Useless base powder 3 ~ 8%
Black talc 2 ~ 7%.
8. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 2, it is characterized in that: in described step F, when ground-coat enamel raw material ball grinds slurry, zinc oxide finally adds ball mill, ball milling mixing 1 ~ 2min.
9. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 4, it is characterized in that: in described step G, when cover-coat enamel raw material ball grinds slurry, zinc oxide finally adds ball mill, ball milling mixing 1 ~ 2min.
10. the preparation method of a kind of building decoration transmutation art pottery ceramic tile according to claim 1, is characterized in that:
Ground-coat enamel is made up of the raw material of following weight percent: albite 16%, porcelain sand 15%, kaolin 7.5%, and zinc oxide 6.5% forges talcum 7.5%, barium carbonate 16%, rhombspar 7%, calcium carbonate 16%, calcium phosphate 5%, aluminum oxide 3.5%;
Cover-coat enamel is made up of the raw material of following weight percent: albite 22%, porcelain sand 8%, kaolin 8%; Zinc oxide 22%; Forge talcum 5%; Titanium oxide 15%, zirconium silicate 12%, glass powder 8%, tinting material 1.2%.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106045577A (en) * | 2016-05-30 | 2016-10-26 | 泉州阳光创艺陶瓷股份有限公司 | Medium-temperature snowflake glaze ceramic and manufacturing method thereof |
| CN106219978A (en) * | 2016-07-18 | 2016-12-14 | 北京杭瑞商贸有限公司 | Margarita glaze, pearl glaze and preparation method thereof and pearl glaze ceramic |
| CN106365453A (en) * | 2016-08-29 | 2017-02-01 | 佛山市高明区明城镇新能源新材料产业技术创新中心 | Anti-radiation ceramic tile and preparing method thereof |
| CN109231829A (en) * | 2018-09-29 | 2019-01-18 | 广东新润成陶瓷有限公司 | A kind of soft polished metal brick and preparation method thereof |
| CN110577406A (en) * | 2019-09-29 | 2019-12-17 | 江西金泰源陶瓷有限公司 | ceramic tile and preparation method thereof |
| CN112441845A (en) * | 2020-12-16 | 2021-03-05 | 广东欧文莱陶瓷有限公司 | Preparation method of low-color-difference ceramic |
| WO2021218132A1 (en) * | 2020-04-30 | 2021-11-04 | 佛山市陶莹新型材料有限公司 | 3d dazzling ceramic tile and preparation method therefor |
| CN114163245A (en) * | 2021-12-16 | 2022-03-11 | 重庆唯美陶瓷有限公司 | Transmutation glaze ceramic tile and preparation method thereof |
| CN115700229A (en) * | 2022-11-23 | 2023-02-07 | 珠海市白兔陶瓷有限公司 | Process for manufacturing crystal glazed tile |
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| CN106045577A (en) * | 2016-05-30 | 2016-10-26 | 泉州阳光创艺陶瓷股份有限公司 | Medium-temperature snowflake glaze ceramic and manufacturing method thereof |
| CN106045577B (en) * | 2016-05-30 | 2019-05-28 | 泉州阳光创艺陶瓷股份有限公司 | Medium temperature snowflake glaze ceramic and its production method |
| CN106219978A (en) * | 2016-07-18 | 2016-12-14 | 北京杭瑞商贸有限公司 | Margarita glaze, pearl glaze and preparation method thereof and pearl glaze ceramic |
| CN106365453A (en) * | 2016-08-29 | 2017-02-01 | 佛山市高明区明城镇新能源新材料产业技术创新中心 | Anti-radiation ceramic tile and preparing method thereof |
| CN109231829A (en) * | 2018-09-29 | 2019-01-18 | 广东新润成陶瓷有限公司 | A kind of soft polished metal brick and preparation method thereof |
| CN109231829B (en) * | 2018-09-29 | 2019-09-20 | 广东新润成陶瓷有限公司 | A kind of soft polished metal brick and preparation method thereof |
| CN110577406A (en) * | 2019-09-29 | 2019-12-17 | 江西金泰源陶瓷有限公司 | ceramic tile and preparation method thereof |
| WO2021218132A1 (en) * | 2020-04-30 | 2021-11-04 | 佛山市陶莹新型材料有限公司 | 3d dazzling ceramic tile and preparation method therefor |
| CN112441845A (en) * | 2020-12-16 | 2021-03-05 | 广东欧文莱陶瓷有限公司 | Preparation method of low-color-difference ceramic |
| CN114163245A (en) * | 2021-12-16 | 2022-03-11 | 重庆唯美陶瓷有限公司 | Transmutation glaze ceramic tile and preparation method thereof |
| CN115700229A (en) * | 2022-11-23 | 2023-02-07 | 珠海市白兔陶瓷有限公司 | Process for manufacturing crystal glazed tile |
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