CN105218164B - Copper red furnace transmutation glaze and the copper red furnace transmutation glaze ceramic prepared with which and preparation method - Google Patents
Copper red furnace transmutation glaze and the copper red furnace transmutation glaze ceramic prepared with which and preparation method Download PDFInfo
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Abstract
The present invention relates to a kind of copper red furnace transmutation glaze and the copper red furnace transmutation glaze ceramic prepared with which and preparation method, belong to ceramic technology field.The copper red furnace transmutation glaze includes following component in parts by weight：Glaze formula basestocks：34 35 parts of nepheline syenite, 20 22 parts of calcium carbonate, 34 parts of brium carbonate, 23 parts of zinc oxide, 12 parts of magnesium carbonate, 26 27 parts of kaolin, 9.5 10.5 parts of nano silicon oxide, colour former：1.8 2.5 parts of lithium carbonate, 24 parts of bone ash, 24 parts of copper carbonate.There is more bright-coloured redness using the ceramic that the copper red furnace transmutation glaze is fired, and glaze distribution of color is uniform, and high yield rate.
Description
Technical field
The invention belongs to ceramic technology field, and in particular to a kind of copper red furnace transmutation glaze and the copper red transmutation glazed pottery prepared with which
Ceramic products and preparation method.
Background technology
Rough flambe is loved by the people since ancient times, is a kind of famousr and precious glaze, once once lost in Ming Dynasty's mid-term, and is changed
Burn alum red.The most bright-coloured ox-blood glaze to be counted of color in rough flambe, general rough flambe are burnt through reduction i.e. with copper-containing substance as colour former
The red glaze of system, its materials and firing condition are key to the quality of glaze, as long as materials are slightly different or deviation, will
Cause reduction not exclusively, or even cause the phenomenons such as glaze nigrescence, greening.Bright-coloured copper red always than sparser, is pursued by people.
And can typically burn out the composition of raw materials of the preferable rough flambe of quality and technique is not disclosed, according to existing rough flambe
Not only color effects are not good for the rough flambe that glaze burns out, and can even produce the glaze distribution of color inequality, glaze surface having is produced
The defects such as pin hole, even if add the auxiliary agents such as stabilizer in glaze being again fired, above deficiency is also difficult to avoid that, studies carefully which main
Condition setting when reason or the unreasonable and reduction of filling a prescription of glaze are fired is unreasonable.Therefore, grinding to the glaze of rough flambe
Study carefully and exploration has great importance.
Content of the invention
The invention aims to solve the deficiencies in the prior art, and a kind of copper red furnace transmutation glaze is provided and is prepared with which
Copper red furnace transmutation glaze ceramic and preparation method, have more bright-coloured redness using the ceramic that the copper red furnace transmutation glaze is fired,
And glaze distribution of color is uniform, and high yield rate.
The present invention is adopted the following technical scheme that：
Copper red furnace transmutation glaze, is obtained by following component in parts by weight：Glaze formula basestocks：Nepheline syenite 34-35
Part, calcium carbonate 20-22 parts, brium carbonate 3-4 parts, zinc oxide 2-3 parts, magnesium carbonate 1-2 parts, kaolin 26-27 parts, nano silicon oxide
9.5-10.5 part, colour former：Lithium carbonate 1.8-2.5 parts, bone ash 2-4 parts, copper carbonate 2-4 parts.
Described copper red furnace transmutation glaze, is obtained by following component in parts by weight：Glaze formula basestocks：Nepheline syenite
34.67 parts, 21.26 parts of calcium carbonate, 3.56 parts of brium carbonate, 2.93 parts of zinc oxide, 1.45 parts of magnesium carbonate, 26.06 parts of kaolin, receive
10.07 parts of silica of rice, colour former：2 parts of lithium carbonate, 3 parts of bone ash, 3 parts of copper carbonate.
The method that copper red furnace transmutation glaze ceramic is prepared with the copper red furnace transmutation glaze, comprises the steps：
Step one, grinding：According to the weight proportion, after each raw material components are mixed, raw material gross weight 50%- is added
55% water carries out ball milling, is milled to mixture particle and crosses 200-250 mesh sieves, after to go out slurry standby；
Step 2, glaze concentration are adjusted：Water is added toward step one gained slurry, concentration is adjusted to 39-40 ° of B é, is obtained glaze slip
Material；
Step 3, glazing：The biscuit of ceramics for baking is immersed in step 2 gained glaze slurry carries out glazing, and glaze thickness is
1.2-1.5mm, dries, obtains ceramic first product；
Step 4, reduction are fired：Step 3 gained ceramic first product is fired, 865-875 DEG C is warming up to, is kept
In kiln, carbon monoxide volumetric concentration is 3%-3.5%, and constant temperature fires 35-45min, after being continuously heating to 1260-1270 DEG C, keeps
In kiln, carbon monoxide volumetric concentration is 1%-1.5%, and constant temperature firing 20-30min, rear cooling down obtain final product the copper red transmutation
Glaze ceramic.
Further, the described method for preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze, wherein described pottery
Porcelain biscuit is fired using potter's clay and is obtained.
Further, the described method for preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze, wherein step one
Described in ball milling rotating speed be 400-450r/min.
The present invention also provides copper red kiln obtained in a kind of method that copper red furnace transmutation glaze prepares copper red furnace transmutation glaze ceramic
Become glaze ceramic.
Compared with prior art, its advantage is the present invention：
The present invention by studying intensively to copper red furnace transmutation glaze glaze, can make after obtaining a kind of firing ceramic journey compared with
The glaze of hunting pink, the glaze are not only bright-colored, and distribution of color is uniform, and glaze surface is moist, smooth uniform, additionally,
Up to more than 90%, therefore, the present invention has good the yield rate of the copper red furnace transmutation glaze ceramic that fires according to the inventive method
Good market prospects, are suitable to popularization and application on a large scale.
Specific embodiment
With reference to embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example is merely to illustrate the present invention, and should not be regarded as limiting this
Bright scope.
Embodiment 1
Copper red furnace transmutation glaze, is obtained by following component in parts by weight：Glaze formula basestocks：Nepheline syenite 34.67
Part, 21.26 parts of calcium carbonate, 3.56 parts of brium carbonate, 2.93 parts of zinc oxide, 1.45 parts of magnesium carbonate, 26.06 parts of kaolin, nano oxygen
10.07 parts of SiClx, colour former：2 parts of lithium carbonate, 3 parts of bone ash, 3 parts of copper carbonate.
The method that copper red furnace transmutation glaze ceramic is prepared with the copper red furnace transmutation glaze, comprises the steps：
Step one, grinding：According to the weight proportion, after each raw material components are mixed, raw material gross weight 50% is added
Water carry out ball milling, be milled to mixture particle and cross 250 mesh sieves, after to go out slurry standby；
Step 2, glaze concentration are adjusted：Water is added toward step one gained slurry, concentration is adjusted to 40 ° of B é, is obtained glaze slurry；
Step 3, glazing：The biscuit of ceramics for baking is immersed in step 2 gained glaze slurry carries out glazing, and glaze thickness is
1.4mm, dries, obtains ceramic first product；
Step 4, reduction are fired：Step 3 gained ceramic first product is fired, 870 DEG C are warming up to, is kept in kiln
Carbon monoxide volumetric concentration is 3.2%, and constant temperature fires 40min, after being continuously heating to 1270 DEG C, keeps carbon monoxide volume in kiln
Concentration is 1.3%, and constant temperature fires 25min, and rear cooling down obtains final product the copper red furnace transmutation glaze ceramic.
Embodiment 2
Copper red furnace transmutation glaze, is obtained by following component in parts by weight：Glaze formula basestocks：34 parts of nepheline syenite,
20 parts of calcium carbonate, 3 parts of brium carbonate, 2 parts of zinc oxide, 1 part of magnesium carbonate, 26 parts of kaolin, 9.5 parts of nano silicon oxide, colour former：Carbon
1.8 parts of sour lithium, 2 parts of bone ash, 2 parts of copper carbonate.
The method that copper red furnace transmutation glaze ceramic is prepared with the copper red furnace transmutation glaze, comprises the steps：
Step one, grinding：According to the weight proportion, after each raw material components are mixed, raw material gross weight 50% is added
Water carry out ball milling, be milled to mixture particle and cross 200 mesh sieves, after to go out slurry standby；
Step 2, glaze concentration are adjusted：Water is added toward step one gained slurry, concentration is adjusted to 39 ° of B é, is obtained glaze slurry；
Step 3, glazing：The biscuit of ceramics for baking is immersed in step 2 gained glaze slurry carries out glazing, and glaze thickness is
1.2mm, dries, obtains ceramic first product；
Step 4, reduction are fired：Step 3 gained ceramic first product is fired, 865 DEG C are warming up to, is kept in kiln
Carbon monoxide volumetric concentration is 3%, and constant temperature fires 35min, after being continuously heating to 1260 DEG C, keeps carbon monoxide volume in kiln dense
Spend for 1%, constant temperature fires 30min, rear cooling down obtains final product the copper red furnace transmutation glaze ceramic.
Embodiment 3
Copper red furnace transmutation glaze, is obtained by following component in parts by weight：Glaze formula basestocks：35 parts of nepheline syenite,
22 parts of calcium carbonate, 4 parts of brium carbonate, 3 parts of zinc oxide, 2 parts of magnesium carbonate, 27 parts of kaolin, 10.5 parts of nano silicon oxide, colour former：
2.5 parts of lithium carbonate, 4 parts of bone ash, 4 parts of copper carbonate.
The method that copper red furnace transmutation glaze ceramic is prepared with the copper red furnace transmutation glaze, comprises the steps：
Step one, grinding：According to the weight proportion, after each raw material components are mixed, raw material gross weight 55% is added
Water carry out ball milling, be milled to mixture particle and cross 220 mesh sieves, after to go out slurry standby；
Step 2, glaze concentration are adjusted：Water is added toward step one gained slurry, concentration is adjusted to 39 ° of B é, is obtained glaze slurry；
Step 3, glazing：The biscuit of ceramics for baking is immersed in step 2 gained glaze slurry carries out glazing, and glaze thickness is
1.5mm, dries, obtains ceramic first product；
Step 4, reduction are fired：Step 3 gained ceramic first product is fired, 875 DEG C are warming up to, is kept in kiln
Carbon monoxide volumetric concentration is 3.5%, and constant temperature fires 35min, after being continuously heating to 1270 DEG C, keeps carbon monoxide volume in kiln
Concentration is 1.5%, and constant temperature fires 20min, and rear cooling down obtains final product the copper red furnace transmutation glaze ceramic.
It is respectively provided with according to copper red furnace transmutation glaze ceramic obtained in glaze formula described in embodiment 1 to 3 and preparation method bright-coloured
Copper red color, and distribution of color is uniform, and glaze surface is moist, smooth uniform, and yield rate is up to more than 90%, its
In, the yield rate of embodiment 1 can be considered most preferred embodiment up to 95%.
It should be understood by those skilled in the art that, the present invention is not restricted to the described embodiments, above-described embodiment and explanation
Merely illustrating the principles of the invention described in book, without departing from the spirit and scope of the present invention, the present invention also has
Various changes and modifications, these changes and improvements are both fallen within scope of the claimed invention.The claimed scope of the invention
By appending claims and its equivalent thereof.
Claims (6)
1. copper red furnace transmutation glaze, it is characterised in that be obtained by following component in parts by weight：Glaze formula basestocks：Nepheline is just
Feldspar 34-35 parts, calcium carbonate 20-22 parts, brium carbonate 3-4 parts, zinc oxide 2-3 parts, magnesium carbonate 1-2 parts, kaolin 26-27 parts,
Nano silicon oxide 9.5-10.5 parts, colour former：Lithium carbonate 1.8-2.5 parts, bone ash 2-4 parts, copper carbonate 2-4 parts.
2. copper red furnace transmutation glaze according to claim 1, it is characterised in that by following component system in parts by weight
?：Glaze formula basestocks：34.67 parts of nepheline syenite, 21.26 parts of calcium carbonate, 3.56 parts of brium carbonate, 2.93 parts of zinc oxide, carbonic acid
1.45 parts of magnesium, 26.06 parts of kaolin, 10.07 parts of nano silicon oxide, colour former：2 parts of lithium carbonate, 3 parts of bone ash, 3 parts of copper carbonate.
3. the method for preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze described in claim 1, it is characterised in that include as
Lower step：
Step one, grinding：According to the weight proportion, after each raw material components are mixed, raw material gross weight 50%-55% is added
Water carries out ball milling, is milled to mixture particle and crosses 200-250 mesh sieves, after to go out slurry standby；
Step 2, glaze concentration are adjusted：Water is added toward step one gained slurry, concentration is adjusted to 39-40 ° of B é, is obtained glaze slurry；
Step 3, glazing：The biscuit of ceramics for baking is immersed carries out glazing in step 2 gained glaze slurry, glaze thickness is 1.2-
1.5mm, dries, obtains ceramic first product；
Step 4, reduction are fired：Step 3 gained ceramic first product is fired, 865-875 DEG C is warming up to, is kept in kiln
Carbon monoxide volumetric concentration is 3%-3.5%, and constant temperature fires 35-45min, after being continuously heating to 1260-1270 DEG C, keeps one in kiln
Carbonoxide volumetric concentration is 1%-1.5%, and constant temperature firing 20-30min, rear cooling down obtain final product the copper red furnace transmutation glaze pottery system
Product.
4. the method for preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze according to claim 3, it is characterised in that
The biscuit of ceramics is fired using potter's clay and is obtained.
5. the method for preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze according to claim 3, it is characterised in that
The rotating speed of ball milling described in step one is 400-450r/min.
6. copper red furnace transmutation glaze obtained in the method for preparing copper red furnace transmutation glaze ceramic with copper red furnace transmutation glaze described in claim 3
Ceramic.
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| CN105731799A (en) * | 2016-01-14 | 2016-07-06 | 福建省泉州得盛集团有限公司 | Copper red reduction transmutation glaze, copper red reduction transmutation glaze ceramic product and preparation method thereof |
| CN105601110B (en) * | 2016-01-14 | 2019-04-09 | 福建省泉州得盛集团有限公司 | Black silver drop reduction furnace transmutation glaze and the black silver drop prepared with it restore transmutation glazed pottery ceramic products and preparation method |
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| CN112679197B (en) * | 2021-02-05 | 2022-07-19 | 景德镇卓铭陶瓷有限责任公司 | Method for firing ceramic |
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