CN105102440A - 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化 - Google Patents

单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化 Download PDF

Info

Publication number
CN105102440A
CN105102440A CN201380057105.4A CN201380057105A CN105102440A CN 105102440 A CN105102440 A CN 105102440A CN 201380057105 A CN201380057105 A CN 201380057105A CN 105102440 A CN105102440 A CN 105102440A
Authority
CN
China
Prior art keywords
phase
cmf
liquid
hydrochloric acid
methods
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201380057105.4A
Other languages
English (en)
Chinese (zh)
Inventor
阿维亚德·卡哈纳
爱德华·尼基丁
杰里米·斯坦迪福德
凯尔·埃利斯
张吕正
蒂莫西·乔治
彼得·米考奇克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
XF TECHNOLOGIES Inc
Original Assignee
XF TECHNOLOGIES Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by XF TECHNOLOGIES Inc filed Critical XF TECHNOLOGIES Inc
Publication of CN105102440A publication Critical patent/CN105102440A/zh
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
CN201380057105.4A 2012-10-16 2013-09-03 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化 Pending CN105102440A (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261714225P 2012-10-16 2012-10-16
US61/714,225 2012-10-16
US201361818418P 2013-05-01 2013-05-01
US61/818,418 2013-05-01
PCT/US2013/057795 WO2014062303A2 (en) 2012-10-16 2013-09-03 Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde

Publications (1)

Publication Number Publication Date
CN105102440A true CN105102440A (zh) 2015-11-25

Family

ID=50488863

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380057105.4A Pending CN105102440A (zh) 2012-10-16 2013-09-03 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化

Country Status (10)

Country Link
US (1) US9102644B2 (enExample)
EP (1) EP2909187A4 (enExample)
CN (1) CN105102440A (enExample)
BR (1) BR112015008477B1 (enExample)
CA (1) CA2888298C (enExample)
IN (1) IN2015DN03835A (enExample)
MX (1) MX363821B (enExample)
PH (1) PH12015500818A1 (enExample)
SG (1) SG11201502939WA (enExample)
WO (1) WO2014062303A2 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111936477A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936478A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2718275A1 (en) 2011-06-09 2014-04-16 Micromidas, Inc. Utilizing a multiphase reactor for the conversion of biomass to produce substituted furans
TW201431844A (zh) 2012-10-26 2014-08-16 Micromidas Inc 用以製造５－（鹵甲基）糠醛之方法
BR112015023313B8 (pt) 2013-03-14 2022-12-13 Micromidas Inc Métodos para purificação de 5-(halometil)furfural
EP2970167A4 (en) 2013-03-14 2016-11-16 Micromidas Inc SOLID FORMS OF 5- (HALOMETHYL) FURFURAL AND PROCESS FOR THE PREPARATION THEREOF
BR112016005974B8 (pt) 2013-09-20 2022-12-06 Micromidas Inc Métodos para produção de 5-(halometil) furfural
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
WO2019143893A1 (en) 2018-01-19 2019-07-25 Q-Maxx Products Group, Inc. Metal cleaning compositions comprising furoate esters and uses therefor
WO2020039386A1 (en) 2018-08-23 2020-02-27 Novartis Ag New pharmaceutical use for the treatment of heart failure
WO2020039394A1 (en) 2018-08-24 2020-02-27 Novartis Ag New drug combinations
WO2023166122A1 (en) * 2022-03-04 2023-09-07 Avantium Knowledge Centre B.V. Method of extracting 5-chloromethylfurfural with an organic solvent from cellulosic fibers and man-made non-cellulosic fibers hydrolysed together with hydrochloric acid

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4335049A (en) * 1980-07-16 1982-06-15 Sumitomo Chemical Company, Limited Process for producing 5-methylfurfural
US20090234142A1 (en) * 2008-03-17 2009-09-17 The Regents Of The Unversity Of California High-yield conversion of cellulosic biomass into furanic biofuels and value-added products

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4154744A (en) * 1976-10-12 1979-05-15 Sumitomo Chemical Company, Limited Process for producing a furan derivative
DE3842825A1 (de) * 1988-01-08 1989-07-20 Krupp Gmbh Verfahren und vorrichtung zur herstellung von furfural
AU2012223494B2 (en) * 2011-02-28 2017-04-06 Dsm Nutritional Products, Llc Polymeric acid catalysts and uses thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4335049A (en) * 1980-07-16 1982-06-15 Sumitomo Chemical Company, Limited Process for producing 5-methylfurfural
US20090234142A1 (en) * 2008-03-17 2009-09-17 The Regents Of The Unversity Of California High-yield conversion of cellulosic biomass into furanic biofuels and value-added products

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
HÉCTOR QUIROZ-FLORENTINO ET AL.: "Total Synthesis of Naturally Occurring Furan Compounds 5-{[(4-Hydroxybenzyl)oxy]methyl}-2-furaldehyde and Pichiafuran C", 《SYNTHESIS》 *
MALTE BRASHOLZ ET AL.,: "Highly efficient dehydration of carbohydrates to 5-(chloromethyl)furfural(CMF),5-(hydroxymethyl)furfural(HMF)and levulinic acid by biphasic continuous flow processing", 《GREEN CHEM》 *
MARK MASCAL AND EDWARD B. NIKITIN: "Dramatic Advancements in the Saccharide to 5-(Chloromethyl)furfural Conversion Reaction", 《CHEMSUSCHEM》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111936477A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936478A (zh) * 2018-01-31 2020-11-13 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936478B (zh) * 2018-01-31 2023-10-10 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺
CN111936477B (zh) * 2018-01-31 2023-10-10 福兰尼克斯科技公司 用于转化固体木质纤维素材料的工艺

Also Published As

Publication number Publication date
SG11201502939WA (en) 2015-05-28
BR112015008477B1 (pt) 2020-12-08
IN2015DN03835A (enExample) 2015-10-02
BR112015008477A2 (pt) 2017-07-04
WO2014062303A3 (en) 2015-07-16
US20140187802A1 (en) 2014-07-03
US9102644B2 (en) 2015-08-11
WO2014062303A2 (en) 2014-04-24
PH12015500818A1 (en) 2015-06-08
MX363821B (es) 2019-04-04
EP2909187A2 (en) 2015-08-26
CA2888298C (en) 2022-05-31
CA2888298A1 (en) 2014-04-24
MX2015004716A (es) 2016-08-17
EP2909187A4 (en) 2016-05-11

Similar Documents

Publication Publication Date Title
CN105102440A (zh) 单醣至5-(氯甲基)-2-呋喃甲醛的有效、高产率转化
EP1827644B1 (en) Use of fiber film reactors to effect extraction between two immiscible components
US9783517B2 (en) Method for synthesis of an output including diesters of 5-methyl-2-furoic acid
AU2005249612B2 (en) Apparatus and method for osmotic membrane distillation
CN111138651A (zh) 一种全氟聚醚过氧化物的合成方法
WO2013083015A1 (zh) 五氟丙酰氟的合成方法
CN101528719A (zh) 六氟环氧丙烷的制造方法
CN111902384B (zh) 在氯化烷烃生产中回收催化剂的方法
JP2018514577A (ja) ビス（フルオロスルホニル）−イミドの製造方法
CN107253913B (zh) 一种微通道反应器制备氯烯炔的方法
CN110746265B (zh) 一种液相法管道化连续化生产氟化烷烃的方法
CN116328685B (zh) 一种硅粉直接法制备四烷氧基硅烷的系统与工艺方法
WO2016057676A1 (en) Use of carboxylic acids in the production of 2,5-furandicarboxylic acid
CN101100293A (zh) 肟水解反应与渗透汽化膜分离耦合技术一步法制备羟胺盐
CN117986081A (zh) 在244bb脱氯化氢为1234yf期间减少杂质形成的系统和方法
CN107698630A (zh) 一种三苄糖苷的制备方法
US9745241B2 (en) Production method for hexachloroacetone
KR20220050984A (ko) 4,4'-디클로로디페닐 설폰의 제조 방법
CN117772087B (zh) 一种联产1,1-氟氯乙烷和1,1-二氟乙烷的装置及方法
CN118561779B (zh) 一种连续合成1,2-环氧十二烷的方法及生产系统
CN117384064B (zh) 一种丙硫菌唑中间体的连续化制备方法及其生产系统
CN216005723U (zh) 一种聚醚分离装置
CN114728873B (zh) 工业化合成全氟甲基乙烯基醚和1,1,2,2-四氟-1-三氟甲氧基乙烷的工艺
JP5670654B2 (ja) 微小流路内のフルオラス不均一多相系反応方法
CN119855803A (zh) 氟烯烃的制造方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20151125