CA2888298C - Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde - Google Patents

Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde Download PDF

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Publication number
CA2888298C
CA2888298C CA2888298A CA2888298A CA2888298C CA 2888298 C CA2888298 C CA 2888298C CA 2888298 A CA2888298 A CA 2888298A CA 2888298 A CA2888298 A CA 2888298A CA 2888298 C CA2888298 C CA 2888298C
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Canada
Prior art keywords
liquid
phase
cmf
organic phase
biphasic
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CA2888298A
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English (en)
French (fr)
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CA2888298A1 (en
Inventor
Aviad Cahana
Edward NIKITIN
Jeremy STANDIFORD
Kyle ELLIS
Zhang LUZHENG
Timothy George
Peter Mikochik
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XF TECHNOLOGIES Inc
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XF TECHNOLOGIES Inc
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Publication of CA2888298A1 publication Critical patent/CA2888298A1/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C07D307/50—Preparation from natural products

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
CA2888298A 2012-10-16 2013-09-03 Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde Active CA2888298C (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261714225P 2012-10-16 2012-10-16
US61/714,225 2012-10-16
US201361818418P 2013-05-01 2013-05-01
US61/818,418 2013-05-01
PCT/US2013/057795 WO2014062303A2 (en) 2012-10-16 2013-09-03 Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde

Publications (2)

Publication Number Publication Date
CA2888298A1 CA2888298A1 (en) 2014-04-24
CA2888298C true CA2888298C (en) 2022-05-31

Family

ID=50488863

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2888298A Active CA2888298C (en) 2012-10-16 2013-09-03 Efficient, high-yield conversion of monosaccharides to 5-(chloromethyl)-2-furaldehyde

Country Status (10)

Country Link
US (1) US9102644B2 (enExample)
EP (1) EP2909187A4 (enExample)
CN (1) CN105102440A (enExample)
BR (1) BR112015008477B1 (enExample)
CA (1) CA2888298C (enExample)
IN (1) IN2015DN03835A (enExample)
MX (1) MX363821B (enExample)
PH (1) PH12015500818A1 (enExample)
SG (1) SG11201502939WA (enExample)
WO (1) WO2014062303A2 (enExample)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9126964B2 (en) 2011-06-09 2015-09-08 Micromidas, Inc. Utilizing a multiphase reactor for the conversion of biomass to produce substituted furans
KR20150072453A (ko) 2012-10-26 2015-06-29 마이크로마이다스, 인코포레이티드 5-(할로메틸) 푸르푸랄 생산 방법
MY193787A (en) 2013-03-14 2022-10-27 Micromidas Inc Solid forms of 5-(halomethyl) furfural and methods for preparing thereof
CN109020930A (zh) 2013-03-14 2018-12-18 微麦德斯公司 5-(卤代甲基)糠醛的提纯方法
PL3046914T3 (pl) 2013-09-20 2023-02-13 Origin Materials Operating, Inc. Sposoby wytwarzania 5-(halogenometylo)furfuralu
EP3498699A1 (en) 2017-12-13 2019-06-19 Basf Se Chromatography method for the purification of furfural derivatives
JP2021511412A (ja) 2018-01-19 2021-05-06 キューマックス プロダクツ グループ， インク．Ｑｍａｘｘ Ｐｒｏｄｕｃｔｓ Ｇｒｏｕｐ， Ｉｎｃ． フロ酸エステルを含む金属洗浄組成物及びその使用
FI3746427T3 (fi) 2018-01-31 2023-09-04 Furanix Technologies Bv Prosessi kiinteän lignoselluloosa-aineksen jalostamiseen
US11578046B2 (en) 2018-01-31 2023-02-14 Furanix Technologies B.V. Process for the conversion of a solid lignocellulosic material
KR20210032437A (ko) 2018-08-23 2021-03-24 노파르티스 아게 심부전의 치료를 위한 신규한 약제학적 용도
WO2020039394A1 (en) 2018-08-24 2020-02-27 Novartis Ag New drug combinations
WO2023166122A1 (en) * 2022-03-04 2023-09-07 Avantium Knowledge Centre B.V. Method of extracting 5-chloromethylfurfural with an organic solvent from cellulosic fibers and man-made non-cellulosic fibers hydrolysed together with hydrochloric acid

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4154744A (en) * 1976-10-12 1979-05-15 Sumitomo Chemical Company, Limited Process for producing a furan derivative
US4335049A (en) * 1980-07-16 1982-06-15 Sumitomo Chemical Company, Limited Process for producing 5-methylfurfural
DE3842825A1 (de) * 1988-01-08 1989-07-20 Krupp Gmbh Verfahren und vorrichtung zur herstellung von furfural
US7829732B2 (en) * 2008-03-17 2010-11-09 Regents Of The University Of California High-yield conversion of cellulosic biomass into furanic biofuels and value-added products
BR112013022047B1 (pt) * 2011-02-28 2020-11-17 Cadena Bio, Inc catalisadores de ácidos poliméricos e seus usos

Also Published As

Publication number Publication date
US20140187802A1 (en) 2014-07-03
SG11201502939WA (en) 2015-05-28
WO2014062303A2 (en) 2014-04-24
CN105102440A (zh) 2015-11-25
US9102644B2 (en) 2015-08-11
WO2014062303A3 (en) 2015-07-16
BR112015008477B1 (pt) 2020-12-08
MX363821B (es) 2019-04-04
PH12015500818A1 (en) 2015-06-08
MX2015004716A (es) 2016-08-17
CA2888298A1 (en) 2014-04-24
EP2909187A2 (en) 2015-08-26
BR112015008477A2 (pt) 2017-07-04
EP2909187A4 (en) 2016-05-11
IN2015DN03835A (enExample) 2015-10-02

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