CN104739749B - Multiple-effect nurses one's health mask - Google Patents

Multiple-effect nurses one's health mask Download PDF

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CN104739749B
CN104739749B CN201510166344.4A CN201510166344A CN104739749B CN 104739749 B CN104739749 B CN 104739749B CN 201510166344 A CN201510166344 A CN 201510166344A CN 104739749 B CN104739749 B CN 104739749B
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mask
effect
extract
mass percent
nurses
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CN104739749A (en
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丁祥华
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Xian Shi Bio Tech Ltd Guangzhou
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Xian Shi Bio Tech Ltd Guangzhou
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Abstract

The present invention provides a kind of multiple-effect conditioning mask, the facial mask without artificial preservative, can be prevented effectively from it is allergic.Contain the active ingredients such as purslane extract, Chondrus crispus extract, elastin hydrolysis, 3 O ethylascorbyls, gadol extract, aloe extract, bright string coccus/radish root tunning filtrate, Gotu Kola P.E, acetyl group octapeptide 3 in the mask; on the basis of moisturizing and whitening, at the same concertedness play anti-oxidant, maintenance, health care and wait for a long time multiple efficacies;The mask is good to the compatibility of skin, is conducive to absorption of the skin to active ingredient.

Description

Multiple-effect nurses one's health mask
Technical field
The present invention relates to daily chemicals technical field, and in particular to a kind of multiple-effect nurses one's health mask.
Background technology
The principle of facial mask, is air and the pollution that the external world is temporarily isolating using the of short duration time for being covered in face, keeps flesh Skin humidity, the pore expansion of skin, promotes sweat gland secretion and metabolism, the oxygen content of skin is increased, be conducive to skin to arrange Except the product and the oil substances of accumulation of epidermal cell metabolism, the moisture in mask penetrates into the cuticula of epidermis, skin Skin becomes soft, and light is flexible naturally for skin.
Existing traditional facial mask effect is single, it is impossible to while multiple skin are solved the problems, such as, and most of facial mask all contains different thiophene Oxazoline ketone has the preservative of stimulation to skin.It is a kind of as disclosed in patent CN104000754A to contain the Kunlun daisy_petal part Facial mask and preparation method thereof, preservative and essence are contained in the facial mask, preservative and essence easily cause thorn to skin eyes Swash.Part active ingredient is difficult to be absorbed by the skin in facial mask, and such as flavones equimolecular quantity is big and is insoluble in the active ingredient of water, easily Cause the water oil cloth of skin uneven, meanwhile, part active ingredient easily causes the discomfort of sensitive skin type, cause allergy or More serious phenomenon.In order to be rapidly achieved visually whitening effect, the fluorescent material content overproof of some facial masks more has Facial mask with the addition of the toxic heavy metals such as mercury to reach effect of despeckle, and these mask products are used for a long time, and can not only reach To the basic function of maintenance skin, will also irreversible damage be caused to skin and body.
The content of the invention
To overcome the defect of prior art, be free of artificial preservative it is an object of the invention to provide one kind, avoid Allergic multiple-effect conditioning mask.
The technical solution adopted in the present invention is as follows to achieve the above object:
A kind of multiple-effect nurses one's health mask, contains following components by percentage to the quality:Purslane extract 1-3%, wrinkle Ripple chondrus extract 2-4%, elastin hydrolysis 1-3%, 3-O- ethylascorbyl 1-3%, gadol extract 1- 3%, aloe extract 1-3%, bright string coccus/radish root tunning filtrate 1-2%, Gotu Kola P.E 1-2%, acetyl group Octapeptide -30.3-0.8%, Sodium Hyaluronate 0.1-0.2%, hydroxyethyl cellulose 0.1-0.2%, triethanolamine 0.1-0.5%, Carbomer 0.1-0.3%, PEG/PPG/ polytetramethylene glycol -8/5/3 glycerine 0.8-1.2%, glycerine 4-6%, butanediol 4-6% are remaining Measure as water.
Preferably, in the multiple-effect conditioning mask, the mass percent of purslane extract is 2%.
Preferably, in the multiple-effect conditioning mask, the mass percent of Chondrus crispus extract is 3%.
Preferably, in the multiple-effect conditioning mask, the mass percent of gadol extract is 2%.
Preferably, in the multiple-effect conditioning mask, the mass percent of aloe extract is 2%.
Preferably, in the multiple-effect conditioning mask, the mass percent of bright string coccus/radish root tunning filtrate For 1.5%.
Preferably, in the multiple-effect conditioning mask, the mass percent of Gotu Kola P.E is 1.5%.
Preferably, in the multiple-effect conditioning mask, the mass percent of elastin hydrolysis is 2%, 3-O- ethyls The mass percent of ascorbic acid is 2%, the mass percent of acetyl group octapeptide -3 is 0.5%.
Preferably, in the multiple-effect conditioning mask, the mass percent of Sodium Hyaluronate is 0.1%, and ethoxy is fine The mass percent of dimension element is 0.15%, and the mass percent of triethanolamine is 0.1-0.5%, and the mass percent of carbomer is The mass percent of the glycerine of 0.2%, PEG/PPG/ polytetramethylene glycol -8/5/3 is 1.0%, and the mass percent of glycerine is 5%, fourth The mass percent of glycol is 5%.
The method that above-mentioned multiple-effect nurses one's health mask is prepared, is comprised the following steps:
1) sterilization of instruments:First the instruments Appliances including reactor are cleaned with 80 DEG C of -100 DEG C of aqua sterilisas, Ran Houyong 75% ethanol for disinfection is rinsed, cold wind drying;
2) feed:The water of formula ratio is added into reactor, is begun to warm up, stirring is opened, by butanediol and and ethoxy Add, then successively add glycerine, the glycerine of PEG/PPG/ polytetramethylene glycols -8/5/3, carbomer, Sodium Hyaluronate after cellulose mixing Enter in reactor, be heated to 80-90 DEG C, be allowed to fully dissolving, be incubated half an hour, open cooling, horse is added when being down to 45-50 DEG C Sativa extract, Chondrus crispus extract, elastin hydrolysis, continue to be down to 40-45 DEG C add 3-O- ethylascorbyls, Gadol extract, aloe extract, bright string coccus/radish root tunning filtrate, Gotu Kola P.E, acetyl group octapeptide -3;
3) pH is adjusted:Add triethanolamine stirring and adjusting pH to 5.5-7.5;
4) quality inspection dress bag:It is down to after room temperature after passed examination and dispenses.
Relative to prior art, there is following beneficial effect in the present invention:
1) mask is nursed one's health without preservative multiple-effect the invention provides one kind, effectively reduces mask to skin Stimulate and influence, the discomfort of face skin is not easily caused;
2) the multiple-effect conditioning mask that the present invention is provided, except containing the basic moisturizing of glycerine, butanediol, Sodium Hyaluronate Beyond composition, also containing natural moisturizing ingredient Chondrus crispus extract, while promoting moisture absorption and the moisture generation of skin Thank, and promote absorption of the skin to other active ingredients;
3) the multiple-effect conditioning mask that the present invention is provided, its whitening composition includes 3-O- ethylascorbyls and rhodiola root Extract and aloe extract, act synergistically in terms of formation that is anti-oxidant, suppressing melanin, the deposition of reduction free radical, To reach effect of skin-whitening;
4) the multiple-effect conditioning mask that the present invention is provided, in addition to containing elastin hydrolysis, also containing promotion collagen egg The aloe extract synthesized in vain and acetyl group octapeptide -3, resist the loss of collagen, the elasticity of skin are kept, while centella Extract has the function of shrinking firm skin, and the senile-resistant efficacy of skin is reached with concertedness;
5) present invention provide multiple-effect conditioning mask, be not added with it is artificial synthesized preservative, bright string coccus/radish root Tunning filtrate has synergetic antibacterial effect with aloe extract;
Neurological susceptibility of the sensitive skin to active ingredient can be effectively reduced, absorption of the skin to active ingredient is more added Entirely.
The present invention is described in further detail with reference to specific embodiment.
Embodiment
The following is the specific embodiment of the present invention, the present invention provides a kind of multiple-effect conditioning mask, containing with quality percentage Than the following components of meter:Purslane extract 1-3%, Chondrus crispus extract 2-4%, elastin hydrolysis 1-3%, 3-O- Ethylascorbyl 1-3%, gadol extract 1-3%, aloe extract 1-3%, bright string coccus/radish root tunning filter Liquid 1-2%, Gotu Kola P.E 1-2%, acetyl group octapeptide -30.3-0.8%, Sodium Hyaluronate 0.1-0.2%, ethoxy are fine Tie up the glycerine of element 0.1-0.2%, triethanolamine 0.1-0.5%, carbomer 0.1-0.3%, PEG/PPG/ polytetramethylene glycol -8/5/3 0.8-1.2%, glycerine 4-6%, butanediol 4-6%, surplus is water.
The method that above-mentioned multiple-effect nurses one's health mask is prepared, is comprised the following steps:
1) sterilization of instruments:First the instruments Appliances including reactor are cleaned with 80 DEG C of -100 DEG C of aqua sterilisas, Ran Houyong 75% ethanol for disinfection is rinsed, cold wind drying;
2) feed:The water of formula ratio is added into reactor, is begun to warm up, stirring is opened, by butanediol and and ethoxy Add, then successively add glycerine, the glycerine of PEG/PPG/ polytetramethylene glycols -8/5/3, carbomer, Sodium Hyaluronate after cellulose mixing Enter in reactor, be heated to 80-90 DEG C, be allowed to fully dissolving, be incubated half an hour, open cooling, horse is added when being down to 45-50 DEG C Sativa extract, Chondrus crispus extract, elastin hydrolysis, continue to be down to 40-45 DEG C add 3-O- ethylascorbyls, Gadol extract, aloe extract, bright string coccus/radish root tunning filtrate, Gotu Kola P.E, acetyl group octapeptide -3;
3) pH is adjusted:Add triethanolamine stirring and adjusting pH to 5.5-7.5;
4) quality inspection dress bag:It is down to after room temperature after passed examination and dispenses.
In the examples below, gadol extract, aloe extract, bright string coccus/radish root tunning filtrate, product The careless extract of snow, acetyl group octapeptide -3 are commercially available;The main component of gadol extract kind be rhodioside, gallic acid, Jujubogenin tyrosol and network match dimension, with stronger anti-oxidant and whitening function;The main component that aloe carries extract is rheum emodin, reed Luxuriant growth polysaccharide, aloe agglutinin, on the basis of water conservation moisturizing, with antiviral, antibacterial, antitumor, anti-oxidant, immunological regulation etc. Multi-efficiency;Bright string coccus/radish root tunning filtrate is a kind of natural antibiotic bactericide;Gotu Kola P.E it is main Active ingredient is asiaticosid, madecassoside, with anti-oxidant and immunoregulation effect;Acetyl group octapeptide -3 can effectively promote Enter the synthesis of collagen.
Embodiment 1
A kind of multiple-effect nurses one's health mask, is made up of by weight percentage following components:
Sodium Hyaluronate 0.1%, hydroxyethyl cellulose 0.15%, triethanolamine 0.1-0.5%, carbomer 0.2%, PEG/ The glycerine 1.0% of PPG/ polytetramethylene glycols -8/5/3, glycerine 5%, butanediol 5%, purslane extract 2%, Chondrus crispus is extracted Thing 3%, elastin hydrolysis 2%, 3-O- ethylascorbyls 2%, gadol extract 2%, aloe extract 2%, bright string Coccus/radish root tunning filtrate 1.5%, Gotu Kola P.E 1.5%, acetyl group octapeptide -30.5%, surplus is water.
The preparation method of the mask, comprises the following steps:
1) sterilization of instruments:First the instruments Appliances including reactor are cleaned with 80 DEG C of aqua sterilisas, then disappeared with 75% Malicious alcohol rinse, cold wind drying;
2) feed:The water of formula ratio is added into reactor, is begun to warm up, stirring is opened, by butanediol and and ethoxy Add, then successively add glycerine, the glycerine of PEG/PPG/ polytetramethylene glycols -8/5/3, carbomer, Sodium Hyaluronate after cellulose mixing Enter in reactor, be heated to 80 DEG C, be allowed to fully dissolving, be incubated half an hour, open cooling, purslane is added when being down to 50 DEG C (PORTULACA OLERACEA) extract, Chondrus crispus (CHONDRUS CRISPUS) extract, elastin hydrolysis, after It is continuous to be down to 45 DEG C of addition 3-O- ethylascorbyls, rhodiola root (RHODIOLA ROSEA) extract, aloe extract, bright string balls Bacterium/radish (RAPHANUS SATIVUS) root tunning filtrate, centella (CENTELLA ASIATICA) extract, acetyl group Octapeptide -3;
3) pH is adjusted:Add triethanolamine stirring and adjusting pH to 6.0;
4) quality inspection dress bag:It is down to after room temperature after passed examination and dispenses.
Embodiment 2:
A kind of multiple-effect nurses one's health mask, is made up of by weight percentage following components:
Sodium Hyaluronate 0.15%, hydroxyethyl cellulose 0.20%, triethanolamine 0.1-0.5%, carbomer 0.3%, The glycerine 0.8% of PEG/PPG/ polytetramethylene glycols -8/5/3, glycerine 8%, butanediol 4%, purslane extract 1%, Chondrus crispus Extract 3%, elastin hydrolysis 3%, 3-O- ethylascorbyls 1%, gadol extract 1%, aloe extract 3%, Bright string coccus/radish root tunning filtrate 2.0%, Gotu Kola P.E 1.2%, acetyl group octapeptide -30.8%, surplus is water.
The preparation method of the mask, comprises the following steps:
1) sterilization of instruments:First the instruments Appliances including reactor are cleaned with 100 DEG C of aqua sterilisas, then disappeared with 75% Malicious alcohol rinse, cold wind drying;
2) feed:The water of formula ratio is added into reactor, is begun to warm up, stirring is opened, by butanediol and and ethoxy Add, then successively add glycerine, the glycerine of PEG/PPG/ polytetramethylene glycols -8/5/3, carbomer, Sodium Hyaluronate after cellulose mixing Enter in reactor, be heated to 80 DEG C, be allowed to fully dissolving, be incubated half an hour, open cooling, purslane is added when being down to 45 DEG C (PORTULACA OLERACEA) extract, Chondrus crispus (CHONDRUS CRISPUS) extract, elastin hydrolysis, after It is continuous to be down to 40 DEG C of addition 3-O- ethylascorbyls, rhodiola root (RHODIOLA ROSEA) extract, aloe extract, bright string balls Bacterium/radish (RAPHANUS SATIVUS) root tunning filtrate, centella (CENTELLA ASIATICA) extract, acetyl Base octapeptide -3;
3) pH is adjusted:Add triethanolamine stirring and adjusting pH to 6.5;
4) quality inspection dress bag:It is down to after room temperature after passed examination and dispenses.
Embodiment 3:
A kind of multiple-effect nurses one's health mask, is made up of by weight percentage following components:
Sodium Hyaluronate 0.2%, hydroxyethyl cellulose 0.1%, triethanolamine 0.1-0.5%, carbomer 0.1%, PEG/ The glycerine 1.2% of PPG/ polytetramethylene glycols -8/5/3, glycerine 8%, butanediol 4%, purslane extract 1%, Chondrus crispus is extracted Thing 3%, elastin hydrolysis 1%, 3-O- ethylascorbyls 3%, gadol extract 3%, aloe extract 1%, bright string Coccus/radish root tunning filtrate 1.0%, Gotu Kola P.E 2.0%, acetyl group octapeptide -30.3%, surplus is water.
The preparation method of the mask, comprises the following steps:
1) sterilization of instruments:First the instruments Appliances including reactor are cleaned with 100 DEG C of aqua sterilisas, then disappeared with 75% Malicious alcohol rinse, cold wind drying;
2) feed:The water of formula ratio is added into reactor, is begun to warm up, stirring is opened, by butanediol and and ethoxy Add, then successively add glycerine, the glycerine of PEG/PPG/ polytetramethylene glycols -8/5/3, carbomer, Sodium Hyaluronate after cellulose mixing Enter in reactor, be heated to 80 DEG C, be allowed to fully dissolving, be incubated half an hour, open cooling, dent is added when being down to 50-45 DEG C Amaranth (PORTULACA OLERACEA) extract, Chondrus crispus (CHONDRUS CRISPUS) extract, elastin hydrolysis, Continue to be down to 45-40 DEG C add 3-O- ethylascorbyls, rhodiola root (RHODIOLA ROSEA) extract, aloe extract, Bright string coccus/radish (RAPHANUS SATIVUS) root tunning filtrate, centella (CENTELLA ASIATICA) extract, Acetyl group octapeptide -3;
3) pH is adjusted:Add triethanolamine stirring and adjusting pH to 5.5;
4) quality inspection dress bag:It is down to after room temperature after passed examination and dispenses.
Quality index and measured result
Multiple-effect conditioning mask made the present embodiment 1-3, quality is carried out by light industry standard QB/T 2872-2007 Detection, the quality index and measured result for the multiple-effect conditioning mask that the present invention is provided is as shown in table 1.
The quality index and measured result of the multiple-effect of the present invention of table 1 conditioning mask
Multiple-effect conditioning mask prepared by the method that embodiment 1-3 is provided meets QB/T 2872-2007 standards.
Performance detection:
1. Microbial Challenge is tested
Multiple-effect conditioning mask made embodiment 1-3, with reference to world CTFA (international cosmetic, essence and detergent association Meeting) recommend Microbial Challenge tested.
Weigh the made multiple-effect conditioning masks of above-described embodiment 1-3 respectively, respectively in experiment the 1st week, the 3rd week and the Inoculation plus bacterium operation are carried out within 5 weeks, each refinement bacterium amount is 1 × 106-1×107, mould amount is 1 × 105-1×106, after bacterium is added The 0th day, the 7th day and the 14th day sampling analysis sample in bacteria containing amount.
Result of the test is as shown in table 2:
The Microbial Challenge of table 2 is tested
The multiple-effect conditioning mask of embodiment 2, the 7th day and the 14th day after being inoculated with three times, clump count was equal<10cfu/g, The bacterium amount of survival is respectively less than the 0.01% of initial concentration, and test data shows, the mask has good fungistatic effect.
The multiple-effect conditioning mask of embodiment 1, the 7th day and the 14th day after being inoculated with three times, clump count was respectively less than the super beginning The 0.01% of concentration, shows, the mask has good fungistatic effect;
The multiple-effect conditioning mask of embodiment 3, at the 14th day of third time inoculation, clump count was more than initial concentration 0.01%, and less than the 0.1% of initial concentration, Microbial Challenge experiment carries out pass the test.
2. animal experiment
Multiple-effect conditioning mask made embodiment 1-3, takes 2000mg/kg b.w. dosage, mouse eye is carried out respectively Irritant test, rat skin irritant test and allergic reaction on guinea pigs, result of the test are as shown in table 3,
The animal experiment of table 3
Eye irritation Skin irritatin It is allergic
Embodiment 1 Subexcite Without erythema without oedema Non- sensitizer
Embodiment 2 Subexcite Without erythema without oedema Non- sensitizer
Embodiment 3 Subexcite Without erythema without oedema Non- sensitizer
It was found from the data of table 2, the multiple-effect conditioning mask that the present invention is provided, to the excitant of the eyes skin of animal It is small, it is difficult to cause allergic.
3. skin clinical test
Choose 45 come the ages 35-45 one full year of life volunteer temperature be 25-28 DEG C, relative humidity be 60-65% permanent Steady temperature damp test room is tested:
Take 5g 5% and 5g butanediols to add water and complement to 1L reagents as a comparison;
Volunteer uses distilled water arm of cleaning, in after laboratory's inner equilibrium 1 hour, in volunteer's right hand arm mark One piece of 2cm × 2cm of mark region to be tested, it is one piece same big with mark hair mark in the opposite position of volunteer's left hand Small region region as a comparison;
Take 1mL embodiments 1-3 made multiple-effect adjustment mask, be labelled to region to be tested, take 1mL contain 20min after wash Go, take 1mL contrast agent to be applied to contrast district, be placed under infrared lamp and irradiate 1min, then to pilot region and contrast district Moisture, colourity test are carried out, and is compared with the data before experiment, as a result as shown in table 4,
The irradiation influence experiment of table 4
Product Moisture increases number Colourity reduces number
Embodiment 1 40 42
Embodiment 2 39 42
Embodiment 3 37 43
As shown in table 4, mask is nursed one's health using the embodiment 1-3 multiple-effect provided, under conditions of acceleration, had in volunteer No less than the tested moisture of skin increase of 37 volunteers, no less than the people of the skin colourity reduction of 42 volunteers, it is seen that this The multiple-effect conditioning mask that invention is provided can rapidly moisturizing and the whitening in short period.
Above-mentioned embodiment is only the preferred embodiment of the present invention, it is impossible to limit the scope of protection of the invention with this, The change and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention Claimed scope.

Claims (10)

1. a kind of multiple-effect nurses one's health mask, it is characterised in that contain following components by percentage to the quality:Purslane extract 1-3%, Chondrus crispus extract 2-4%, elastin hydrolysis 1-3%, 3-O- ethylascorbyl 1-3%, rhodiola root are carried Thing 1-3%, aloe extract 1-3%, bright string coccus/radish root tunning filtrate 1-2%, Gotu Kola P.E 1-2% are taken, Acetyl group octapeptide -30.3-0.8%, Sodium Hyaluronate 0.1-0.2%, hydroxyethyl cellulose 0.1-0.2%, triethanolamine 0.1- 0.5%, carbomer 0.1-0.3%, PEG/PPG/ polytetramethylene glycol -8/5/3 glycerine 0.8-1.2%, glycerine 4-6%, butanediol 4- 6%, surplus is water.
2. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, purslane The mass percent of extract is 2%.
3. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, ripple angle The mass percent for pitching dish extract is 3%.
4. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, rhodiola root The mass percent of extract is 2%.
5. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, aloe carries The mass percent for taking thing is 2%.
6. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, bright string ball The mass percent of bacterium/radish root tunning filtrate is 1.5%.
7. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, centella The mass percent of extract is 1.5%.
8. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, hydrolyze bullet The mass percent of property albumen is that the mass percent of 2%, 3-O- ethylascorbyls is 2%, the quality of acetyl group octapeptide -3 Percentage is 0.5%.
9. multiple-effect as claimed in claim 1 nurses one's health mask, it is characterised in that in the multiple-effect conditioning mask, hyalomitome The mass percent of sour sodium is 0.1%, and the mass percent of hydroxyethyl cellulose is 0.15%, the quality percentage of triethanolamine Than for 0.1-0.5%, the mass percent of carbomer is the quality percentage of the glycerine of 0.2%, PEG/PPG/ polytetramethylene glycols -8/5/3 It is 5% than the mass percent for 1.0%, glycerine, the mass percent of butanediol is 5%.
10. preparing the method that multiple-effect as claimed in claim 1 nurses one's health mask, comprise the following steps:
1) sterilization of instruments:First the instruments Appliances including reactor are cleaned with 80 DEG C of -100 DEG C of aqua sterilisas, then with 75% Ethanol for disinfection is rinsed, cold wind drying;
2) feed:The water of formula ratio is added into reactor, is begun to warm up, stirring is opened, by butanediol and hydroxyethyl cellulose Added after mixing, then successively by glycerine, the glycerine of PEG/PPG/ polytetramethylene glycols -8/5/3, carbomer, Sodium Hyaluronate addition reaction In kettle, 80-90 DEG C is heated to, fully dissolving is allowed to, is incubated half an hour, open cooling, purslane is added when being down to 45-50 DEG C and is carried Thing, Chondrus crispus extract, elastin hydrolysis are taken, continues to be down to 40-45 DEG C of addition 3-O- ethylascorbyls, rhodiola root Extract, aloe extract, bright string coccus/radish root tunning filtrate, Gotu Kola P.E and acetyl group octapeptide -3;
3) pH is adjusted:Add triethanolamine stirring and adjusting pH to 5.5-7.5;
4) quality inspection dress bag:It is down to after room temperature after passed examination and dispenses.
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