CN101711726A - Ginseng skin-whitening liquid soap and preparation method thereof - Google Patents

Ginseng skin-whitening liquid soap and preparation method thereof Download PDF

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Publication number
CN101711726A
CN101711726A CN200910199044A CN200910199044A CN101711726A CN 101711726 A CN101711726 A CN 101711726A CN 200910199044 A CN200910199044 A CN 200910199044A CN 200910199044 A CN200910199044 A CN 200910199044A CN 101711726 A CN101711726 A CN 101711726A
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China
Prior art keywords
skin
liquid soap
ginseng
preparation
whitening
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Pending
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CN200910199044A
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Chinese (zh)
Inventor
何木火
吴庆生
蒋良宇
陈云
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Tongji University
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Tongji University
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Priority to CN200910199044A priority Critical patent/CN101711726A/en
Publication of CN101711726A publication Critical patent/CN101711726A/en
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Abstract

The invention belongs to the technical field of detergents, and in particular relates to a ginseng skin-whitening liquid soap and a preparation method thereof. The ginseng skin-whitening liquid soap is added with a natural ginseng saponin component, thereby enhancing the anti-aging effect of skin, improving skin microcirculation, having the function of resisting roughness, wrinkles and chaps and then playing a role in facial and health care. The liquid soap is prepared from fatty alcohol polyoxyethylene ether sodium sulfate, alkyl polyglucoside, cocamidopropyl betaine, glycerine, EDTA-2Na, 2-methyl-4-isothiazoline-3-ketone, 2,2,4-trichloro-2-hydroxy-diphenyl ether, perfume, pigment, citric acid, ginseng saponin, distilled water and other raw materials. The preparation method comprises the steps of extracting ginseng saponin and other effective components from stems, leaves and roots of ginseng plants, adding various raw materials and preparing the ginseng skin-whitening liquid soap through dissolving, heating, emulsifying, stirring, standing and other processes. The liquid soap not only can play a role in resisting and inhibiting bacteria, but also can achieve the efficacy in whitening and moisturizing skin.

Description

A kind of ginseng skin-whitening liquid soap and preparation method thereof
Technical field
The invention belongs to the detergent technical field, be specifically related to a kind of ginseng skin-whitening liquid soap and preparation method thereof.
Background technology
Along with improving constantly of living standard, people are to the hygiene and health growing interest, and this makes handwashing liquid become a kind of articles for daily use.But existing handwashing liquid, major function still rests on the decontamination aspect, though portioned product has sterilizing function, skin-protecting function is poor, can damage the hand skin after long-time the use, brings coarse, crowfoot cracks, easy problem such as aging to skin.
And added natural ginsenoside's composition in the ginseng skin-whitening liquid soap among the present invention, and strengthened the skin anti-aging effect, improved skin microcirculation, have the coarse and crease-resistant effect of splitting that resists.Except keeping decontamination, the antibacterial and bacteriostasis of handwashing liquid, also play the dual function of beauty treatment and health care, life-time service can also reach the effect of whitening and moistening skin.
The ginsenoside claims Saponin again, is extensively to be present in the special glycoside of a botanic class, can produce persistent saponiform foam after its aqueous solution jolting.The ginsenoside can significantly reduce and suppress the generation of lipid peroxide, and protection Skin Cell film is avoided damage, and then prevents cell ageing; Microcirculation improvement effect to skin is remarkable, makes that cutaneous circulation is plentiful, moistens and support moist and rich gloss; Can improve the resistance of skin, prevent the Skin Cell canceration.In addition, the ginsenoside also has the degraded of the skin keratin of promotion, stratum germinativum epidermidis hyperplasia metabolism, and collagen fibers of skin upgrades, arranges effects such as parallel, and skin is tenderized and high resilience.The ginsenoside is the cosmetics of active ingredient, can resist the effect to skin such as ultraviolet and daylight, prevents skin tanning, dark brown speckle is alleviated even disappears.
Summary of the invention
The object of the present invention is to provide a kind of ginseng skin-whitening liquid soap and preparation method thereof; its objective is to solving the problem that existing handwashing liquid exists; provide a kind of can high-effective cleansing and sterilization, whitening and moistening skin well again, the handwashing liquid of hand skin can be effectively protected in long-time use.
The ginseng skin-whitening liquid soap that the present invention proposes, its mass percent consists of: 1~20% mass fraction is 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, 0.5~20% alkyl polyglucoside, 0.1~5% glycerol, 0.1~2% EDTA-2Na (disodium EDTA), 0.1~5% 2-methyl-4-isothiazoline-3-ketone, 0.1~5% 2,2,4-three chloro-2-hydroxyl-diphenyl ether, 1~40% mass fraction is the aqueous solution of 30% cocamido propyl betaine, 0.1~20% ginsenoside, 0.1~5% spice, 0.1~5% pigment, 0.01~2% citric acid, 0.1~5% NaCl, all the other are distilled water, its gross mass satisfies 100%, and described raw material is technical grade.
The preparation method of the Radix Ginseng handwashing liquid that the present invention proposes, concrete steps are as follows:
(1), and is heated to 60~80 ℃ at the distilled water of changing material still adding 20~30%;
(2) keep system temperature at 60~80 ℃, stirring adds 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, alkyl polyglucoside, glycerol, disodium EDTA, 2-methyl-4-isothiazoline-3-ketone, 2 down successively, 2,4-three chloro-2-hydroxyl-diphenyl ether stir dissolving;
(3) be cooled to 20 ℃~30 ℃, stir and to add ginsenoside, spice, pigment, 30% cocamido propyl betaine aqueous solution, NaCl down successively, add remaining distilled water, stir;
(4) regulate stock solution pH value to 5.5~6.5 with citric acid and sodium citrate;
(5) leave standstill, make the foam complete obiteration in the system, solution is transparent, uniform state;
(6) above-mentioned handwashing liquid is detected, the vanning of fill, packing.
Among the present invention, mixing time is 1~8h described in the step (2).
Among the present invention, mixing time is 1~6h described in the step (3).
Among the present invention, time of repose is 4~10h described in the step (5).
Beneficial effect of the present invention: not only contain 2,2 in this handwashing liquid, sterilizing materials such as 4-three chloro-2-hydroxyl-diphenyl ether, but also contain glycerol, betanin and alkyl polyglucoside have preserve moisture, the material of skin moistening effect.The Saponin that adding is extracted from panax ginseng plant, ginsenoside and the combination of other optimizing components, the composite generation good synergistic of each component, bactericidal is played potentiation, the hand skin is played tangible improvement, this handwashing liquid, effect such as have sterilization, decontamination simultaneously, moisten, preserve moisture, whiten.
The specific embodiment
Further specify the present invention below by embodiment.
Embodiment 1: prepare described ginseng skin-whitening liquid soap 100g, process is as follows:
1, take by weighing respectively by mass percentage: 5% mass fraction be 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, 2% alkyl polyglucoside, 2% glycerol, 0.1% EDTA-2Na, 2-methyl-4-isothiazoline-3-ketone of 0.3%, 0.15% 2,2,4-three chloro-2-hydroxyl-diphenyl ether, 8% mass fraction are aqueous solution, 3% ginsenoside, 0.06% spice, 0.25% lactic acid, 0.2% commercially pure NaCl and 81.89% the distilled water of 30% cocamido propyl betaine;
2, with aqueous solution, alkyl polyglucoside, glycerol, EDTA-2Na, the 2-methyl-4-isothiazoline-3-ketone, 2 of the polyoxyethylenated alcohol sodium sulfate described in the step 1,2,4-three chloro-2-hydroxyl-diphenyl ether and distilled water join in the beaker of 200ml, and adding magnetic force rotor, place on the magnetic stirring apparatus, open to stir, heat temperature raising to 60 ℃ also keeps 1h; 3, being cooled to 30 ℃, is that 30% cocamido propyl betaine aqueous solution joins in the beaker with the mass fraction described in the step 1, stirs also to keep 0.5h under 30 ℃ of conditions; 4, ginsenoside and the spice in the adding step 1 continues to stir 10min; Add NaCl at last, stirring promptly gets ginseng skin-whitening liquid soap.
More than each raw material be technical grade.
Embodiment 2: the ginseng skin-whitening liquid soap of present embodiment, preparation ginseng skin-whitening liquid soap 100g, by mass percentage by: 10% mass fraction is 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, 0.5% alkyl polyglucoside, 1% glycerol, 0.15% EDTA-2Na, 0.15% 2-methyl-4-isothiazoline-3-ketone, 0.25% 2,2,4-three chloro-2-hydroxyl-diphenyl ether, 6% mass fraction is the aqueous solution of 30% cocamido propyl betaine, 8% ginsenoside, 0.08% spice, 0.3% lactic acid, 2.8% NaCl and 72% distilled water are made.
More than each raw material be technical grade.
Embodiment 3: the ginseng skin-whitening liquid soap of present embodiment, preparation ginseng skin-whitening liquid soap 100kg, be the aqueous solution of 70% polyoxyethylenated alcohol sodium sulfate by mass percentage by: 5.0% mass fraction, 9.5% alkyl polyglucoside, 2.0% glycerol, 0.20% EDTA-2Na, 0.20% 2-methyl-4-isothiazoline-3-ketone, 0.20% 2,2,4-three chloro-2-hydroxyl-diphenyl ether, 12% mass fraction is 30% cocamido propyl betaine aqueous solution, 1.5% ginsenoside, 0.05% spice, 0.5% NaCl and 76.85% distilled water are made.
More than each raw material be technical grade.
The ginseng skin-whitening liquid soap of present embodiment is according to the regulation of " handwashing liquid industry standard ", and every index test result is as follows:
1, outward appearance: not stratified, no suspended substance or precipitation do not have the water white transparency product of obvious impurity.
2, abnormal smells from the patient: free from extraneous odour.
3, gross activity thing assay: gross activity thing content (percentage by weight) is 9.3, meets index gross activity thing content greater than 9 requirement.
4, pH value is measured: adopting acidometer to measure pH is 6.36, in index p H is 4.0~10.0 scopes.
5, methanol content measuring: methanol content is 453mg/kg after measured, meets the requirement that the index methanol content is lower than 2000mg/kg.
6, content of formaldehyde is measured: content of formaldehyde is 78mg/kg after measured, meets the requirement that the index content of formaldehyde is lower than 500mg/kg.
7, arsenic content (in As): arsenic content is 0.6mg/kg after measured, meets the requirement that index arsenic content is lower than 10mg/kg.
8, content of beary metal is measured (in Pb): content of beary metal is 7.8mg/kg after measured, meets the requirement that the index content of beary metal is lower than 40mg/kg.
9, mercury content is measured: mercury content is 0.07mg/kg after measured, meets the requirement that the index mercury content is lower than 1mg/kg.
10, microbiological indicator detects: total plate count is 213 after measured, meets the index total plate count and is lower than 1000 requirement.Excrement colibacillus group does not detect.
The ginseng skin-whitening liquid soap abnormal smells from the patient of the ginseng skin-whitening liquid soap present embodiment gained of present embodiment pure and fresh pleasant, the pathogenicity Gram-positive that causes infection and negative bacterium, fungus, yeast and virus etc. are all had kill widely and inhibitory action, pathogenicity skin bacteria effect to stubbornness is especially outstanding, all effectively same to antibiotic resistant bacteria and non-antibiotic fastbacteria, use after three days, cutaneous circulation is plentiful, moisten and support moist and rich gloss, the skin delicacy, dark brown speckle is alleviated even disappears.
Embodiment 4: present embodiment is identical with the mass ratio of each component of raw material in the specific embodiment three, and the ginseng skin-whitening liquid soap gross weight is 500kg.Concrete production technology is as follows: in the reactor (volume 1000L) that has stirring and temperature-controlling system, add the 1500kg distilled water by centrifugal pump, and be heated to 80 ℃.Keep system temperature at 78~80 ℃, under the stirring, add 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, alkyl polyglucoside, glycerol, EDTA-2Na, 2-methyl-4-isothiazoline-3-ketone, 2 on request successively, 2,4-three chloro-2-hydroxyl-diphenyl ether, fully stir 5h, uniform dissolution.Be cooled to 22 ℃, stir and to add ginsenoside, spice, pigment, 30% cocamido propyl betaine aqueous solution, NaCl down successively, add remaining distilled water, continue to stir 6h.Substance dissolves is complete in the sample analysis, still, and system is even.Regulate stock solution pH value to 5.8 with the 1.5kg citric acid.Stop to stir, leave standstill 8h, observe the foam complete obiteration of liquid-covered, solution is transparent, uniform state by visor.
More than each raw material be technical grade.

Claims (5)

1. ginseng skin-whitening liquid soap, it is characterized in that its mass percent consists of: 1~20% mass fraction is 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, 0.5~20% alkyl polyglucoside, 0.1~5% glycerol, 0.1~2% disodium EDTA, 0.1~5% 2-methyl-4-isothiazoline-3-ketone, 0.1~5% 2,2,4-three chloro-2-hydroxyl-diphenyl ether, 1~40% mass fraction is the aqueous solution of 30% cocamido propyl betaine, 0.1~20% ginsenoside, 0.1~5% spice, 0.1~5% pigment, 0.01~2% citric acid, 0.1~5% NaCl, all the other are distilled water, its gross mass satisfies 100%, and described raw material is technical grade.
2. the preparation method of a ginseng skin-whitening liquid soap as claimed in claim 1 is characterized in that concrete steps are as follows:
(1) in changing the material still, adds 20~30% distilled water, and be heated to 60~80 ℃;
(2) keep system temperature at 60~80 ℃, stirring adds 70% polyoxyethylenated alcohol sodium sulfate aqueous solution, alkyl polyglucoside, glycerol, disodium EDTA, 2-methyl-4-isothiazoline-3-ketone, 2 down successively, 2,4-three chloro-2-hydroxyl-diphenyl ether stir dissolving;
(3) be cooled to 20 ℃~30 ℃, stir and to add ginsenoside, spice, pigment, 30% cocamido propyl betaine aqueous solution, NaCl down successively, add remaining distilled water, stir;
(4) regulate stock solution pH value to 5.5~6.5 with citric acid and sodium citrate;
(5) leave standstill, make the foam complete obiteration in the system, solution is transparent, uniform state;
(6) above-mentioned handwashing liquid is detected, the vanning of fill, packing.
3. the preparation method of ginseng skin-whitening liquid soap according to claim 2 is characterized in that mixing time is 1~8h described in the step (2).
4. the preparation method of ginseng skin-whitening liquid soap according to claim 2 is characterized in that mixing time is 1~6h described in the step (3).
5. the preparation method of ginseng skin-whitening liquid soap according to claim 2 is characterized in that time of repose is 4~10h described in the step (5).
CN200910199044A 2009-11-19 2009-11-19 Ginseng skin-whitening liquid soap and preparation method thereof Pending CN101711726A (en)

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CN200910199044A CN101711726A (en) 2009-11-19 2009-11-19 Ginseng skin-whitening liquid soap and preparation method thereof

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102041188A (en) * 2010-12-28 2011-05-04 中国农业大学 Sterilizing detergent and application thereof
CN103893046A (en) * 2012-12-28 2014-07-02 青岛锦涟鑫商贸有限公司 Preparation method of hand sanitizer
CN104606077A (en) * 2015-02-02 2015-05-13 同济大学 Nanometer ultraviolet-resistant ginseng whitening hand sanitizer and preparation method thereof
CN105078816A (en) * 2014-12-19 2015-11-25 赵雅珺 Skin cleaning liquid
CN105902429A (en) * 2016-05-08 2016-08-31 杭州氧泡泡生物科技有限公司 Plant type anti-bacterial foaming hand sanitizer

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102041188A (en) * 2010-12-28 2011-05-04 中国农业大学 Sterilizing detergent and application thereof
CN103893046A (en) * 2012-12-28 2014-07-02 青岛锦涟鑫商贸有限公司 Preparation method of hand sanitizer
CN105078816A (en) * 2014-12-19 2015-11-25 赵雅珺 Skin cleaning liquid
CN104606077A (en) * 2015-02-02 2015-05-13 同济大学 Nanometer ultraviolet-resistant ginseng whitening hand sanitizer and preparation method thereof
CN105902429A (en) * 2016-05-08 2016-08-31 杭州氧泡泡生物科技有限公司 Plant type anti-bacterial foaming hand sanitizer
CN105902429B (en) * 2016-05-08 2019-01-11 浙江艾卡医学科技有限公司 A kind of foam type hand cleanser of plant type degerming

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Open date: 20100526