CN102000011A - Shrub althea flower lotion and preparation method thereof - Google Patents

Abstract

The invention provides shrub althea flower lotion and a preparation method thereof. The shrub althea flower lotion comprises the following components: shrub althea flower extract, vitamin C, honey, polyethylene glycol, glycerin, citric acid, triethanolamine, dodecyl sodium sulfate, essence, preservative and water. The preparation method comprises the steps of: washing and airing shrub althea flowers; irradiating the shrub althea flowers under ultraviolet light for 1 hour; and mashing, squeezing and filtering to obtain the shrub althea flower extract. The prepared lotion has the functions of lubrication, moisture retention and speckle removal and also makes up the defects of insufficient biologic active elements and trace elements of ordinary lotion.

Description

A kind of Flos Hibisci skin care liquid and preparation method thereof

Technical field

The invention belongs to cosmetic field, be specifically related to the technical scheme of the natural Flos Hibisci processing skin care liquid of a kind of usefulness.

Background technology

The cosmetics and skincare product main component is oils and fats and water, secondly is wetting agent.Most formulated with chemical reagent, its biological active matter composition and content of elements deficiency.Last century end, the skin expert finds that skin care item add various natural components skin is had the effect of moistening.And the minimizing content of oil and grease, increasing antioxidant composition and free radical resisting then is the feature of third generation cosmetics.

Flos Hibisci contains Vegetable oil lipoprotein, essential amino acids, and polysaccharide, the polyhydric alcohol phlegmatic temperament has the function of preserving moisture with antioxidation, removing free radical.Studies show that the 1g Flos Hibisci is equivalent to the 5.19mg vitamin C, the ability of removing DPPH is arranged.It also contains trace element such as a large amount of needed by human body nutritional labelings such as protein, cellulose, carotene, multivitamin and calcium, magnesium, zinc, copper, phosphorus, potassium, selenium, chromium, and contains flavone compound, has antiinflammatory, effect for reducing blood fat.Contain saponarin, isovitexin, materials such as Saponin and phlegmatic temperament ^[3], can suppress staphylococcus aureus and Bacillus typhi, can treat hemorrhoidal hamorrhage and rush down blood.And the custom that useful this flower juice among the people washes one's face and improves looks.Therefore on this basis, in Flos Hibisci juice, add an amount of glycerol and emulsifying agent, vitamin E etc., be made into oil-in-water type (O/W) skin care liquid, being suitable for the neutral skin uses, especially the person has certain effect of dispelling spots person in middle and old age to be had the senile plaque on hand, plays lubricated effect of preserving moisture simultaneously again, has remedied the defect of insufficient of common skin care liquid biological active matter composition and trace element.

Summary of the invention

The object of the present invention is to provide and a kind ofly contain the Flos Hibisci natural nutrient component, and the facial treatment milk manufacture method of Carboxymethyl Chitin.

The invention provides a kind of Flos Hibisci skin care liquid, it contains following component: Flos Hibisci extracting solution, vitamin E, Mel, Polyethylene Glycol, glycerol, citric acid, triethanolamine, sodium lauryl sulphate, essence, antiseptic, water, wherein the mass percent of each component is: Flos Hibisci extracting solution 10～30%, vitamin E 0.2%, Mel 0～0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate (SDS) 0.05%, essence 0.3%, antiseptic 0.02%, surplus are water; Wherein, the Flos Hibisci extracting solution is 15～20% o'clock, best results.

Above-mentioned Flos Hibisci extracting solution is that fresh petal is cleaned, dried, and sterilization adds water and squeezes the juice and filter and get, and Flos Hibisci is good with fresh Flos Carthami lobe, and the mass ratio of Flos Hibisci and water is 10～20: 100 when squeezing the juice; Used essence is rose essence.

Concrete manufacture method of the present invention comprises the steps:

The first step, all container autoclavings, 121 ℃, 20min.60 ℃ of drying baker dryings then;

The reagent of second step, preparation desired concn, autoclaving, 121 ℃, 20min;

The 3rd step, between the sterile working in, take by weighing Flos Hibisci and smash to pieces, add water and squeeze the juice, filter;

The 4th step, vitamin E and Polyethylene Glycol mixed form oil phase, and be heated to 75 ℃;

The 5th goes on foot, glycerol, citric acid, triethanolamine, sodium lauryl sulphate, water is mixed form water, and is heated to 75 ℃;

The 6th goes on foot, water is added in the oil phase stirs, and continues 20 minutes, and sterilization adds Flos Hibisci extract, Mel, antiseptic, essence when being chilled to 45 ℃, be chilled to room temperature behind the mixing promptly.

Analytical method according to national cosmetic hygienic standard detects the present invention, quality testing the results are shown in Table 1 with table 2.

Table 1, organoleptic examination result:

Table 2, physical and chemical inspection result:

To the present invention carry out animal acute with the chronic skin toxicity test, choose two groups of mices, each 5 of every group of male and female are smeared the Flos Hibisci skin care liquid in the ear epithelium, do skin acute experiment, observe 24h white mice ear skin and change no abnormality seen.Smeared continuously 5 days, and did the chronic skin toxicity test, observe white mice ear skin and change no abnormality seen.Put to death, do leukocyte, lymphocyte is checked no abnormal change, the results are shown in Table 3.

Table 3, mouse skin are smeared toxic measurement result (5 days):

With mice smear skin care liquid after 5 days ear weigh, and experimental group and matched group ear weight differential are carried out t check, t＜t _0.05/2,10,P＞0.05, not statistically significant according to available sample information, can not think that still experimental group and matched group are variant.Show that the Flos Hibisci skin care liquid is to reactions such as the non-stimulated swelling of mouse ear skin.

The present invention is carried out skin irritation test, 6 adult females that choose skin health do skin irritation test, the regiones brachii medialis territory was for being tried the position in the past, and a side is the test block, and opposite side is the check plot, get three of cotton pads, coat Flos Hibisci skin care liquid 0.05g, the U.S. rose water 0.05g in lining, Gherkin water 0.05g respectively, be attached to the inboard test block of forearm, fix with medical proof fabric, duration of test is suitable for the not edible maror of person, irritable food, and the experiment position does not get wet.24h opens observation. and see the fruit that comes to an end and see Table 4.

Table 4, Flos Hibisci skin care liquid tuerculoderma testing result:

Sample	The Flos Hibisci skin care liquid	In U.S. rose water	Gherkin water
				4h result	No erythema, pimple, edema	No erythema, pimple, edema	No erythema, pimple, edema
24h result	No erythema, pimple, edema	No erythema, pimple, edema	No erythema, pimple, edema

Test result: experimental group Flos Hibisci skin care liquid and matched group gone on the market in also zero difference of the no significant difference as a result of U.S. rose water and Gherkin water and check plot.

The present invention is carried out stability experiment, the present invention has been carried out 5 ± 0.1 ℃, 15 ± 0.1 ℃, 25 ± 0.1 ℃, 37 ± 0.1 ℃ constant temperature study on the stability, no layering and turbid phenomenon.

Spend in vain with Hibiscus syriacus L. pale reddish brownly because of plant fat and Vitamin C content in the Hibiscus syriacus L. Flos Carthami are higher than Hibiscus syriacus L., easily gather simultaneously, select the Flos Hibisci nutritional labeling analysis in table 5 of different colours for use so the Hibiscus syriacus L. Flos Carthami is the best of Flos Hibisci skin care liquid raw material.

Table 5, Flos Hibisci nutritional labeling (unit: g/g, %)

The invention has the beneficial effects as follows: the Flos Hibisci skin care liquid that special formula and manufacture method are produced, 1. nonalcoholic skin care liquid contains abundant vegetative grease, performance skin smoothing opsonic action.2. contain saponarin in the Flos Hibisci; materials such as isovitexin; can suppress staphylococcus aureus and Bacillus typhi; improving skin 3. gives up chemical addition agent and adopts natural Hibiscus syriacus L. petal to squeeze the juice the individual effect of pathogenic bacteria resistance; under safe and harmless prerequisite the effect of performance skin care 4. the phlegmatic temperament of Flos Hibisci self and fat effectively chap, exsiccant Leatherwear surface forms one deck natural water fat protecting film, give the skin enough moisture and produce emollescence.5. green skin protection has been satisfied people and has been wished that natural active substance participates in the hope of skin metabolism process directly.

Description of drawings

Fig. 1, Flos Hibisci skin care liquid preparation manipulation process chart.

The specific embodiment

Embodiment 1,

Raw materials used mass percent is in the present embodiment: Flos Hibisci extracting solution 10%, vitamin E 0.2%, Mel 0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate 0.05%, essence 0.3%, antiseptic 0.02%, surplus is a water.

Described Flos Hibisci extracting solution is the fresh Flos Carthami lobe of 10% a Flos Hibisci filtrate.

The manufacture method of described a kind of Flos Hibisci skin care liquid is characterized in that described Hibiscus syriacus L. Flos Carthami is to clean, dry under the fresh petal room temperature, in uviol lamp irradiation sterilization in 1 hour down, seals standby

Concrete preparation technology is as follows:

The first step, all container autoclavings, 121 ℃, 20min.60 ℃ of drying baker dryings then;

The reagent of second step, preparation desired concn, autoclaving, 121 ℃, 20min;

The 3rd step, between the sterile working in, take by weighing Flos Hibisci and smash to pieces, add water and squeeze the juice, filter;

The 4th step, vitamin E and Polyethylene Glycol mixed form oil phase, and be heated to 75 ℃;

The 5th goes on foot, glycerol, citric acid, triethanolamine, sodium lauryl sulphate, water is mixed form water, and is heated to 75 ℃;

The 6th goes on foot, water is added in the oil phase stirs, and continues 20 minutes, and sterilization adds Flos Hibisci extract, Mel, antiseptic, essence when being chilled to 45 ℃, be chilled to room temperature behind the mixing promptly.

Embodiment 2,

Raw materials used mass percent is in the present embodiment: the pale reddish brown extracting solution 15% of Hibiscus syriacus L., vitamin E 0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate 0.05%, essence 0.3%, antiseptic 0.02%, surplus is a water.

Described Flos Hibisci extracting solution is the fresh Flos Carthami lobe of 15% a Flos Hibisci filtrate.

Concrete preparation technology is with embodiment 1.

Embodiment 3,

Raw materials used quality proportioning is in the present embodiment: Flos Hibisci extracting solution 20%, vitamin E 0.2%, Mel 0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate 0.05%, essence 0.3%, antiseptic 0.02%, surplus is a water.

Described Flos Hibisci extracting solution is that 20% Hibiscus syriacus L. is spent filtrate in vain.

Concrete preparation technology is with embodiment 1.

Raw materials used quality percentage Flos Hibisci extracting solution 30% in embodiment 4, the present embodiment, vitamin E 0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate 0.05%, essence 0.3%, antiseptic 0.02%, surplus is a water.

Described Flos Hibisci extracting solution is the fresh pale reddish brown lobe filtrate of 30% Flos Hibisci.

Concrete preparation technology is with embodiment 1.

Above-mentioned four embodiment have been carried out analysis-by-synthesis, the result is as follows: transparency: embodiment 1＞embodiment 2＞embodiment 3＞embodiment 4, spreadability: embodiment 2＞embodiment 3＞embodiment 1＞embodiment 4, viscid sense: embodiment 4＞embodiment 3＞embodiment 2＞embodiment 1.General effect embodiment 2 and embodiment 3 are better, so Flos Hibisci extracting solution mass percent is ideal at 15～20% o'clock.

Claims (5)

1. Flos Hibisci skin care liquid, it is characterized in that containing following component: Flos Hibisci extracting solution, vitamin E, Mel, Polyethylene Glycol, glycerol, citric acid, triethanolamine, sodium lauryl sulphate, essence, antiseptic, water, the mass percent of described each component is: Flos Hibisci extracting solution 10～30%, vitamin E 0.2%, Mel 0～0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate 0.05%, essence 0.03%, antiseptic 0.02%, surplus are water.

2. a kind of Flos Hibisci skin care liquid according to claim 1 is characterized in that the mass percent of Flos Hibisci extracting solution is preferably 15～20%.

3. a kind of Flos Hibisci skin care liquid according to claim 1, it is characterized in that described Flos Hibisci extracting solution is to clean under the fresh petal room temperature, dry Burdick lamp irradiation 1 hour, smash, add the water after-filtration of squeezing the juice to pieces, the mass ratio of Flos Hibisci and water is 10～30: 100.

4. a kind of Flos Hibisci skin care liquid according to claim 1 is characterized in that described essence is rose essence.

5. the preparation method of a Flos Hibisci skin care liquid, it is characterized in that by following component formulated: the Flos Hibisci extracting solution, vitamin E, Mel, Polyethylene Glycol, glycerol, citric acid, triethanolamine, sodium lauryl sulphate, essence, antiseptic, water, the mass percent of described each component is: Flos Hibisci extracting solution 10～30%, vitamin E 0.2%, Mel 0～0.2%, Polyethylene Glycol 0.5%, glycerol 5.0%, citric acid 1.0%, triethanolamine 0.4%, sodium lauryl sulphate 0.05%, essence 0.03%, antiseptic 0.02%, surplus are water, and concrete manufacture method comprises the steps:

The first step, all container autoclavings, 121 ℃, 20min.60 ℃ of drying baker dryings then;

The reagent of second step, preparation desired concn, autoclaving, 121 ℃, 20min;

The 3rd step, between the sterile working in, take by weighing Flos Hibisci and smash to pieces, squeeze the juice, filter;

The 4th step, vitamin E and Polyethylene Glycol mixed form oil phase, and be heated to 75 ℃;

The 5th goes on foot, glycerol, citric acid, triethanolamine, sodium lauryl sulphate, water is mixed form water, and is heated to 75 ℃;

The 6th goes on foot, water is added in the oil phase stirs, and continues 20 minutes, and sterilization adds Flos Hibisci extract, Mel, antiseptic, essence when being chilled to 45 ℃, be chilled to room temperature behind the mixing and promptly get this product.

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