CN103735455A - Agar boiled algae mud facial mask and preparation method thereof - Google Patents
Agar boiled algae mud facial mask and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the field of cosmetics, and in particular relates to an agar boiled algae mud facial mask and a preparation method thereof. The method comprises the following steps: removing impurities from agar, washing, and baking until the agar body is crispy; mashing the dried agar into particles, immersing in alcohol for 8-20 hours, filtering, and boiling for 15-120 minutes, centrifuging the filtered algae mud to dehydrate, lyophilizing and grinding to obtain powder; weighing each raw material according to the prescription; adding the weighed algae powder into deionized water, stirring and swelling; dissolving a wetting agent, an antioxidant, a metal ion chelant, preservative, a brightening agent, deodorant, sebum secretion inhibitor, keratolytic agent, bacteriostatic agent, antisensitive agent and nutrition additive in the deionized water; adding the stirring swelled agar mud, and keeping on stirring; adding tackifier and deionized water while stirring, and uniformly stirring to obtain the facial mask. The facial mask is good in wetting performance, can be used for remarkably improving skin tone, nourishing skin and preventing skin aging, and is low in cost and price.
Description
Technical field
The invention belongs to cosmetic field, particularly main laver decocting in water algae mud facial film and preparation method thereof.
Background technology
Thallus Porphyrae is mainly one of edible economical alga kind of China, belongs to Rhodophyta, former Rhodophyceae, Bangiales, Bangia fuscopurpurea section, Porphyra.The kind of Porphyra is distributed in the Northern Hemisphere and the Southern Hemisphere widely, and the whole world approximately has over one hundred kind, and China Thallus Porphyrae has more than ten to be planted, wherein artificial cultivation mainly contain two kinds: Porphyra yezoensis Ueda and porphyra haitanensis.Porphyra yezoensis Ueda is cold warm nature Sargassum, mainly be distributed in the coastal zone along the Huanghai Sea and the Bohai Sea of North of Yangtze River, it is the main object of northern China (Jiangsu, Shandong and Liaoning and other places) cultivation, porphyra haitanensis is the distinctive warm temperate zone property Sargassum of China, mainly being distributed in the eastern Coastline of South China Sea on the south the Changjiang river, is the main object of south China (Zhejiang, Fujian and other places) cultivation.
Thallus Porphyrae is a kind of delicious flavour, and nutritious large edible Sargassum, and it not only contains rich in protein, carbohydrate, and the content of various vitamin and mineral is also abundant especially.In Thallus Porphyrae, unsaturated fatty acid ratio is also higher, and unsaturated fatty acid can make cholesterol esterification, thereby reduces the cholesterol levels of serum and liver.In recent years, people conduct extensive research the extraction composition of Thallus Porphyrae and health care value thereof, and the main component of finding it is polysaccharide and protein.
Facial film is a kind of facial cosmetics and skincare product that spreads on, utilization covers the blink of face, extraneous air and the pollution of temporary transient isolation, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to skin and get rid of the oil substances of the metabolic product of epidermis cell and accumulation, improve elasticity, pliability and the brightness of skin.The kind of facial film is a lot, and wherein seaweed mask, with the mineral composition of Sargassum extract, can be controlled oily Peppermint Extract, and moisture is provided, and calm tired, rough skin makes skin remain fine and smooth, glossy.But the moistening effect of plant seaweed mask of the prior art is not the most desirable, and use inconvenience, the shelf-life is short, expensive.
Utilize the biomass of Thallus Porphyrae to prepare facial film for raw material, in existing document and report, record not yet to some extent.
Summary of the invention
The object of this invention is to provide a main laver decocting in water algae mud facial film, the moistening effect of this facial film is excellent, also has the effect of whitening, antiinflammatory, reduce wrinkle, and uses simple, low price.
Another object of the present invention is to provide a kind of preparation method of above-mentioned Thallus Porphyrae decocting in water algae mud facial film.
Object of the present invention can be achieved through the following technical solutions:
One main laver decocting in water algae mud facial film, is characterized in that, comprises the raw material that following percentage by weight is counted meter:
Thallus Porphyrae powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
The preparation method of described Thallus Porphyrae powder is, by Thallus Porphyrae remove impurity, washing, dry and become fragile to frond till, then dry Thallus Porphyrae is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter; By the Thallus Porphyrae grain decocting in water 15-120 minute obtaining, filter and obtain algae mud again, after centrifuge dehydration, lyophilization, be ground to the Powdered Thallus Porphyrae powder that obtains.Preferably, described Thallus Porphyrae is Porphyra yezoensis Ueda or porphyra haitanensis.
Described wetting agent is one or more the mixture in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.Preferably, described wetting agent is the mixture of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium; The weight ratio of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium is 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08.
Described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO.Preferably, described tackifier is the mixture of high molecular cellulose and HANSHENGJIAO, and the weight ratio of high molecular cellulose and HANSHENGJIAO is 3-4:1.
Described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid, and preferred described metal ion chelation agent is the mixture of L-vitamin C and citric acid, and wherein the weight ratio of L-vitamin C and citric acid is 1-3:1.
Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15.Preferably, described antiseptic is the mixture of phenoxyethanol and Sang Pu K15, and wherein, the volume ratio of phenoxyethanol and Sang Pu K15 is 1-2:1.
Described brightening agent is one or more the mixture in arbutin, nicotiamide or Trenaxmine.Preferably, described brightening agent is the mixture of arbutin, nicotiamide and Trenaxmine, and wherein, the weight ratio of arbutin, nicotiamide and Trenaxmine is 1:1-3:1.
Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.Preferably, described anti-allergic agent is the mixture of water solublity a-bisabolol and glycyrrhizic acid dipotassium, and wherein, the weight ratio of water solublity a-bisabolol and glycyrrhizic acid dipotassium is 2-6:1.
Described nourishing additive agent is one or more the mixture in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
Described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
The preparation method of above-mentioned Thallus Porphyrae decocting in water algae mud facial film, its step comprises:
(1), by Thallus Porphyrae remove impurity, washing, dry and become fragile to frond till, then dry Thallus Porphyrae is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter; Preferably, described Thallus Porphyrae is Porphyra yezoensis Ueda or porphyra haitanensis.
(2), by the Thallus Porphyrae grain decocting in water 15-120 minute obtaining in step (1), filter and to obtain algae mud, after centrifuge dehydration, lyophilization, be ground to the Powdered Thallus Porphyrae powder that obtains; Thallus Porphyrae is through after alcohol-pickled and decocting in water, can more extract can be absorbed by the skin effective ingredient in Thallus Porphyrae, improves the performance of keeping humidity of facial film.
(3), according to formula, weigh good various raw materials;
(4) deionized water and stirring swelling will be added in load weighted Thallus Porphyrae powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir the Thallus Porphyrae mud continuation stirring that swelling is good, add while stirring tackifier and deionized water, after stirring, obtain Thallus Porphyrae decocting in water algae mud facial film.
In described step (1), by Thallus Porphyrae oven dry to the baking temperature becoming fragile, be 55-65 ℃.
In described step (2), by the decocting in water temperature of Thallus Porphyrae grain decocting in water, be 40-70 ℃; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
Compared with prior art, beneficial effect of the present invention is:
1, the moisture retention of described Thallus Porphyrae decocting in water algae mud facial film is good, and the skin moisture content rate of increase applying after 20 minutes through facial film face of the present invention is more than 60%, and can obviously improve the colour of skin, Glycerin, effectively prevents skin aging, reduces wrinkle.
2, the preparation method of described Thallus Porphyrae decocting in water algae mud facial film is simple, easy to operate, and raw material is easy to get, cost is low, low price, and the medicine adding in preparation process is not only to not injury of skin, and environmentally safe, green, environmental protection.
Accompanying drawing explanation
Fig. 1 is the skin lines comparison diagram that has applied the Thallus Porphyrae decocting in water algae mud facial film front and back that make in embodiment 1.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1) preparation of Thallus Porphyrae powder
The Porphyra yezoensis Ueda gathering is removed to assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water is washed till electrical conductivity and drops to below 0.02MS; Till drying in the baking oven of 60 ℃ and becoming fragile to frond; With medicine bruisher, fully smash to pieces to algae grain length and be shorter than 5mm, adding mass concentration is 75% alcohol-pickled spending the night (12 hours), with 100 order silk cover filterings, obtain algae grain, algae grain is decocting in water 1h at 70 ℃, with 200 mesh sieve thin,tough silk filtering supernatants, obtain algae mud, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 300 seconds, finally, by fully grinding after the algae mud vacuum lyophilization of centrifuge dehydration, obtain Thallus Porphyrae powder.
(2) preparation process of facial film
Get the Thallus Porphyrae powder 10g in step (1), add 30mL deionized water swelling stirring, standby.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 5g, amino acid humectant 3g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, 120-160 ten thousand each 0.1g), red wine polyphenols 1g, L-vitamin C1g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K15 is 0.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 2g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Thallus Porphyrae mud after swelling is stirred is mixed homogeneously with above-mentioned adjuvant, adds while stirring even mixed 1.4g high molecular cellulose and 0.4g HANSHENGJIAO, with deionized water, adds to 100g total amount, obtains Thallus Porphyrae decocting in water algae mud facial film.
(3) testing result
For the moistening effect of the Thallus Porphyrae decocting in water algae mud facial film for preparing in test implementation example 1, respectively by green tea powder facial film, lavandula angustifolia facial film in contrast.Wherein the preparation method of green tea powder facial film and lavandula angustifolia facial film, according to the formula preparation in the present embodiment 1, only replaces Thallus Porphyrae powder by the green tea powder of equivalent and lavandula angustifolia powder (all purchased from Chhnang daily use chemicals, Guangdong), and other raw materials and addition thereof are all constant.
Before test: experimenter's arm of cleaning inner side, and with wet gauze (with deionized water) scrub, water temperature is room temperature, after cleaning, inside experimenter's both hands forearm, carries out measurement markers, within before tested position 2-3 days, can not use any cosmetic product; In test: use latex finger cot that test products and reference product are evenly applied in arm trial zone, smearing thickness is 2mm, carries out measurement and the observation of tested region and control zone after 20min, and each region is parallel assay five times according to the order of sequence, draw meansigma methods, shown in table 1 specific as follows:
Table 1 skin moisture content rate of increase
With 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U) observation, applied the skin of the Thallus Porphyrae decocting in water algae mud facial film in the present embodiment 1, as shown in Figure 1, wherein Fig. 1 a does not apply the skin observation figure of Thallus Porphyrae decocting in water algae mud facial film, Fig. 1 b is the skin observation figure that has applied Thallus Porphyrae decocting in water algae mud facial film, from comparative observation, figure shows, the facial film of preparing in the present embodiment all can improve the colour of skin, Glycerin, the moisture content of raising epiderm skin.
Embodiment 2
(1) preparation of Thallus Porphyrae powder
The porphyra haitanensis gathering is removed to assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water is washed till electrical conductivity and drops to below 0.02MS; Till drying in the baking oven of 60 ℃ and becoming fragile to frond; With medicine bruisher, fully smash to pieces to algae grain length and be shorter than 5mm, adding mass concentration is 75% alcohol-pickled spending the night (18 hours), with 100 order silk cover filterings, obtain algae grain, algae grain decocting in water 45 minutes at 70 ℃, with 200 mesh sieve thin,tough silk filtering supernatants, obtain algae mud, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 350 seconds, by fully grinding after the algae mud vacuum lyophilization of centrifuge dehydration, obtain Thallus Porphyrae powder recently.
(2) preparation process of facial film
Get the Thallus Porphyrae powder 15g in step (1), add 30mL deionized water swelling stirring, standby.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 4g, amino acid humectant 4g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, 120-160 ten thousand each 0.1g), red wine polyphenols 2g, L-vitamin C2g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 1.5g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Thallus Porphyrae mud after swelling is stirred is mixed homogeneously with above-mentioned adjuvant, adds while stirring even mixed 1.5g high molecular cellulose and 0.5g HANSHENGJIAO, with deionized water, adds to 100g total amount, obtains Thallus Porphyrae decocting in water algae mud facial film.
(3) testing result
Method of testing is with embodiment 1, and concrete test result is as shown in table 2 below:
Table 2 skin moisture content rate of increase
In sum, use the moisture content that can obviously improve skin epidermis after Thallus Porphyrae decocting in water algae mud facial film, reached more than 60%, far away higher than green tea powder facial film and lavandula angustifolia facial film, and can improve the colour of skin, Glycerin.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the disclosed content of this embodiment.So every, do not depart from the equivalence completing under spirit disclosed in this invention or revise, all falling into the scope of protection of the invention.
Claims (10)
1. a main laver decocting in water algae mud facial film, is characterized in that, comprises the raw material that following percentage by weight is counted meter:
Thallus Porphyrae powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
2. Thallus Porphyrae decocting in water algae mud facial film according to claim 1, it is characterized in that: the preparation method of described Thallus Porphyrae powder is, by Thallus Porphyrae remove impurity, washing, dry and become fragile to frond till, then dry Thallus Porphyrae is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter; By the Thallus Porphyrae grain decocting in water 15-120 minute obtaining, filter and obtain algae mud again, after centrifuge dehydration, lyophilization, be ground to the Powdered Thallus Porphyrae powder that obtains.
3. Thallus Porphyrae decocting in water algae mud facial film according to claim 1, is characterized in that: described wetting agent is one or more the mixture in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.
4. Thallus Porphyrae decocting in water algae mud facial film according to claim 1, is characterized in that: described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO; Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.
5. Thallus Porphyrae decocting in water algae mud facial film according to claim 1, is characterized in that: described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid; Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15; Described brightening agent is one or more the mixture in arbutin, nicotiamide or Trenaxmine.
6. Thallus Porphyrae decocting in water algae mud facial film according to claim 1, is characterized in that: described nourishing additive agent is one or more the mixture in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
7. Thallus Porphyrae decocting in water algae mud facial film according to claim 1, is characterized in that: described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
8. a preparation method for Thallus Porphyrae decocting in water algae mud facial film claimed in claim 1, its step comprises:
(1), by Thallus Porphyrae remove impurity, washing, dry and become fragile to frond till, then dry Thallus Porphyrae is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter;
(2), by the Thallus Porphyrae grain decocting in water 15-120 minute obtaining in step (1), filter and to obtain algae mud, after centrifuge dehydration, lyophilization, be ground to the Powdered Thallus Porphyrae powder that obtains;
(3), according to formula, weigh good various raw materials;
(4) deionized water and stirring swelling will be added in load weighted Thallus Porphyrae powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir the Thallus Porphyrae mud continuation stirring that swelling is good, add while stirring tackifier and deionized water, after stirring, obtain Thallus Porphyrae decocting in water algae mud facial film.
9. the preparation method of Thallus Porphyrae decocting in water algae mud facial film according to claim 8, is characterized in that: in described step (1), by Thallus Porphyrae oven dry to the baking temperature becoming fragile, be 55-65 ℃.
10. the preparation method of Thallus Porphyrae decocting in water algae mud facial film according to claim 8, is characterized in that: in described step (2), by the decocting in water temperature of Thallus Porphyrae grain decocting in water, be 40-70 ℃; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
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| CN104434630A (en) * | 2014-11-13 | 2015-03-25 | 龙骏 | Product for enhancing skin activity and preparation method thereof |
| CN104546560A (en) * | 2014-12-29 | 2015-04-29 | 广州维观生物科技有限公司 | Dry-type film containing antibacterial peptide and epidermal growth factor, as well as preparation method and application thereof |
| CN108524420A (en) * | 2018-06-12 | 2018-09-14 | 四川农业大学 | A kind of food-grade moisturizing skin rejuvenating facial mask and preparation method thereof |
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| CN103263361A (en) * | 2013-06-08 | 2013-08-28 | 广州暨南生物医药研究开发基地有限公司 | Application of porphyra polysaccharide to preparation of ultraviolet ray injury resistant skin care product |
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| CN103263361A (en) * | 2013-06-08 | 2013-08-28 | 广州暨南生物医药研究开发基地有限公司 | Application of porphyra polysaccharide to preparation of ultraviolet ray injury resistant skin care product |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434630A (en) * | 2014-11-13 | 2015-03-25 | 龙骏 | Product for enhancing skin activity and preparation method thereof |
| CN104546560A (en) * | 2014-12-29 | 2015-04-29 | 广州维观生物科技有限公司 | Dry-type film containing antibacterial peptide and epidermal growth factor, as well as preparation method and application thereof |
| CN108524420A (en) * | 2018-06-12 | 2018-09-14 | 四川农业大学 | A kind of food-grade moisturizing skin rejuvenating facial mask and preparation method thereof |
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