CN103720621B - A kind of Entermorpha decocting in water algae mud facial film and preparation method thereof - Google Patents
A kind of Entermorpha decocting in water algae mud facial film and preparation method thereof Download PDFInfo
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- CN103720621B CN103720621B CN201310724662.9A CN201310724662A CN103720621B CN 103720621 B CN103720621 B CN 103720621B CN 201310724662 A CN201310724662 A CN 201310724662A CN 103720621 B CN103720621 B CN 103720621B
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Abstract
The invention belongs to cosmetic field, in particular to a kind of Entermorpha decocting in water algae mud facial film and preparation method thereof, Entermorpha remove impurity, washing, oven dry are become fragile to frond, the Entermorpha of drying is smashed to pieces to graininess, to be dipped in ethanol 8-20 hour, to filter, decocting in water 15-120 minute, filtration obtains algae mud, is ground to Powdered after centrifuge dehydration, lyophilization; Various raw material has been weighed according to formula; Swelling by adding deionized water and stirring in load weighted Entermorpha powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Entermorpha mud continuation stirring, add tackifier and deionized water while stirring, stir.The moisture retention of this facial film is good, obviously improves the colour of skin, Glycerin, prevents skin aging, and cost is low, low price.
Description
Technical field
The invention belongs to cosmetic field, particularly a kind of Entermorpha decocting in water algae mud facial film and preparation method thereof.
Background technology
Facial film is a kind of cosmetics and skincare product spreading on face, utilize the blink covering face, the air that temporary transient isolation is extraneous and pollution, promote sweat gland secretion and metabolism, the oxygen content of skin is made to increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, improve the elasticity of skin, pliability and brightness.The kind of facial film is a lot, and wherein seaweed mask is with the mineral composition of Sargassum extract, can control oily Peppermint Extract, provide moisture, calm tired, rough skin, makes skin remain fine and smooth, glossy.But the moistening effect of plant seaweed mask of the prior art is not the most desirable, and use inconvenient, the shelf-life is short, expensive.
Entermorpha is a kind of common large ocean chlorella, and it belongs to Chlorophyta in Sargassum, Chlorophyceae, Ulvales, Ulvaceae.The polysaccharide of Entermorpha and protein have and reduce the pharmacological action such as cholesterol, antibacterial and antiviral, antioxidation, enhancing immunologic function, antitumor, antiinflammatory.And Entermorpha also has multiple biological activity, in cosmetic applications, main manifestations is antioxidation, radioprotective, antiviral, the aspects such as moisture retention.In recent years, along with progressively going deep into of studying its chemical composition, its medical mechanism is also illustrated gradually, and the step of drug development is constantly accelerated.
The biomass of Entermorpha are utilized to prepare facial film for raw material, described in not yet having in existing document and report.If people constantly can research and develop effect of Entermorpha, utilize the characteristic of its antioxidation, antiviral, moisture retention etc., be developed to the facial film with effects such as whitening, antiinflammatory, moisturizings, turn waste into wealth, it is made fully to be utilized, while environmental improvement, too increase economic benefit, kill two birds with one stone.
Summary of the invention
The object of this invention is to provide a kind of Entermorpha decocting in water algae mud facial film, this facial film can increase skin surface moisture, and moistening effect is excellent, also has effect of whitening, antiinflammatory, reduce wrinkle, and uses simple, low price.
Another object of the present invention is to provide a kind of preparation method of above-mentioned Entermorpha decocting in water algae mud facial film.
Object of the present invention can be achieved through the following technical solutions:
A kind of Entermorpha decocting in water algae mud facial film, is characterized in that, comprise the raw material of following percentage by weight number meter:
Entermorpha powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
The preparation method of described Entermorpha powder is, by Entermorpha remove impurity, washing, oven dry to frond becomes fragile, then smashs to pieces to graininess by the Entermorpha of drying, is dipped to 8-20 hour, filtration in ethanol; The Entermorpha grain decocting in water 15-120 minute will obtained again, filters and obtains algae mud, is ground to and Powderedly obtains Entermorpha powder after centrifuge dehydration, lyophilization.
Described wetting agent is the mixture of one or more in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.Preferably, described wetting agent is the mixture of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium; The weight ratio of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium is 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08.
Described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO.Preferably, described tackifier is the mixture of high molecular cellulose and HANSHENGJIAO, and the weight ratio of high molecular cellulose and HANSHENGJIAO is 3-4:1.
Described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid, and preferred described metal ion chelation agent is the mixture of L-vitamin C and citric acid, and wherein the weight ratio of L-vitamin C and citric acid is 1-3:1.
Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15.Preferably, described antiseptic is the mixture of phenoxyethanol and Sang Pu K15, and wherein, the volume ratio of phenoxyethanol and Sang Pu K15 is 1-2:1.
Described brightening agent is the mixture of one or more in arbutin, nicotiamide or Trenaxmine.Preferably, described brightening agent is the mixture of arbutin, nicotiamide and Trenaxmine, and wherein, the weight ratio of arbutin, nicotiamide and Trenaxmine is 1:1-3:1.
Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.Preferably, described anti-allergic agent is the mixture of water solublity a-bisabolol and glycyrrhizic acid dipotassium, and wherein, the weight ratio of water solublity a-bisabolol and glycyrrhizic acid dipotassium is 2-6:1.
Described nourishing additive agent is the mixture of one or more in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
Described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
The preparation method of above-mentioned Entermorpha decocting in water algae mud facial film, its step comprises:
(1), by Entermorpha remove impurity, washing, oven dry to frond becomes fragile, then the Entermorpha of drying is smashed to pieces to graininess, be dipped to 8-20 hour, filtration in ethanol;
(2), the Entermorpha grain decocting in water 15-120 minute that will obtain in step (1), filter and obtain algae mud, be ground to after centrifuge dehydration, lyophilization and Powderedly obtain Entermorpha powder; Entermorpha, after alcohol-pickled and decocting in water, can extract the effective biomass that can be less readily available for absorption by the skin in Entermorpha more fully, improves the moisture retention of facial film.
(3), various raw material has been weighed according to formula;
(4), swelling by adding deionized water and stirring in load weighted Entermorpha powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Entermorpha mud continuation stirring, add tackifier and deionized water while stirring, after stirring, obtain Entermorpha decocting in water algae mud facial film.
In described step (1), described Entermorpha is the one in Enteromorpha clathrata (Roth) Greville, Enteromorpha linza or bent Entermorpha; By Entermorpha dry to the baking temperature become fragile be 55-65 DEG C.
In described step (2), be 40-70 DEG C by the decocting in water temperature of Entermorpha grain decocting in water; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
Compared with prior art, beneficial effect of the present invention is:
1, the moisture retention of described Entermorpha decocting in water algae mud facial film is good, and the skin moisture content rate of increase after facial film face of the present invention applies 20 minutes is more than 33%, and can obviously improve the colour of skin, Glycerin, effectively prevent skin aging, reduce wrinkle.
2, the preparation method of described Entermorpha decocting in water algae mud facial film is simple, easy to operate, and raw material is easy to get, cost is low, low price, and the medicine added in preparation process does not only injure skin, and environmentally safe, green, environmental protection.
Accompanying drawing explanation
Fig. 1 has applied the skin lines comparison diagram before and after Entermorpha decocting in water algae mud facial film obtained in embodiment 1.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1) preparation of Entermorpha powder
The Enteromorpha clathrata (Roth) Greville gathered is removed assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water wash is until electrical conductivity of water drops to below 0.02MS; Dry in the baking oven of 60 DEG C to frond becomes fragile; Fully smash to pieces to algae grain length with medicine bruisher and be shorter than 5mm, add alcohol-pickled spend the night (12 hours) that mass concentration is 75%, algae grain is obtained with 100 order silk cover filterings, algae grain is decocting in water 1h at 70 DEG C, obtain algae mud with 200 mesh sieve thin,tough silk filtering supernatants, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 300 seconds, fully grind after the algae mud vacuum lyophilization of centrifuge dehydration recently, obtain Entermorpha powder.
(2) preparation process of facial film
Get the Entermorpha powder 10g in step (1), add the swelling stirring of 30mL deionized water, for subsequent use.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 5g, amino acid humectant 3g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, the each 0.1g of 120-160 ten thousand), red wine polyphenols 1g, L-vitamin C1g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 2g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Entermorpha mud after swelling stirring is mixed homogeneously with above-mentioned adjuvant, adds the 1.4g high molecular cellulose after Homogeneous phase mixing and 0.4g HANSHENGJIAO while stirring, add to 100g total amount with deionized water, obtain Entermorpha decocting in water algae mud facial film.
(3) testing result
For the moistening effect of Entermorpha decocting in water algae mud facial film prepared in testing example 1, respectively by green tea powder facial film, Lavender mask in contrast.Wherein the preparation method of green tea powder facial film and Lavender mask is according to the formula preparation in the present embodiment 1, and only the green tea powder of equivalent and lavandula angustifolia powder (all purchased from Chhnang daily use chemicals, Guangdong) are replaced Entermorpha powder, other raw materials and addition thereof are all constant.
Before test: inside experimenter's arm of cleaning, and with wet gauze (with deionized water) scrub, water temperature is room temperature, carries out measurement markers, within before recipient site 2-3 days, can not use any cosmetic product after cleaning at experimenter's both hands inner forearm; In test: use latex finger cot by test products and reference product uniform application in arm trial zone, smearing thickness is measurement and the observation of carrying out tested region and control zone after 2mm, 20min, each region parallel assay five times according to the order of sequence, draw meansigma methods, shown in table 1 specific as follows:
Table 1 skin moisture content rate of increase
The skin of the Entermorpha decocting in water algae mud facial film in the present embodiment 1 has been applied with 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U) observation, as shown in Figure 1, wherein Fig. 1 a does not apply the skin observation figure of Entermorpha decocting in water algae mud facial film, Fig. 1 b is the skin observation figure having applied Entermorpha decocting in water algae mud facial film, show from comparative observation figure, the facial film prepared in the present embodiment all can improve the colour of skin, Glycerin, improves the moisture content of epiderm skin.
Embodiment 2
(1) preparation of Entermorpha powder
The Enteromorpha linza gathered is removed assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water wash is until electrical conductivity of water drops to below 0.02MS; Dry in the baking oven of 60 DEG C to frond becomes fragile; Fully smash to pieces to algae grain length with medicine bruisher and be shorter than 5mm, add alcohol-pickled spend the night (18 hours) that mass concentration is 75%, algae grain is obtained with 100 order silk cover filterings, algae grain decocting in water 45 minutes at 70 DEG C, obtain algae mud with 200 mesh sieve thin,tough silk filtering supernatants, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 300 seconds, fully grind after the algae mud vacuum lyophilization of centrifuge dehydration recently, obtain Entermorpha powder.
(2) preparation process of facial film
Get the Entermorpha powder 15g in step (1), add the swelling stirring of 30mL deionized water, for subsequent use.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 4g, amino acid humectant 4g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, the each 0.1g of 120-160 ten thousand), red wine polyphenols 2g, L-vitamin C2g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 1.5g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Entermorpha mud after swelling stirring is mixed homogeneously with above-mentioned adjuvant, adds the 1.5g high molecular cellulose after Homogeneous phase mixing and 0.5g HANSHENGJIAO while stirring, add to 100g total amount with deionized water, obtain Entermorpha decocting in water algae mud facial film.
(3) testing result
Method of testing is with embodiment 1, and concrete test result is as shown in table 2 below:
Table 2 skin moisture content rate of increase
In sum, the moisture content of skin epidermis can be significantly improved after employing Entermorpha decocting in water algae mud facial film, improve the colour of skin, Glycerin.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the content disclosed in this embodiment.The equivalence completed under not departing from spirit disclosed in this invention so every or amendment, all fall into the scope of protection of the invention.
Claims (6)
1. an Entermorpha decocting in water algae mud facial film, is characterized in that, comprises the raw material of following percentage by weight number meter:
Entermorpha powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water;
Described wetting agent is the mixture that glycerol, amino acid humectant, propylene glycol, butanediol and hyaluronate sodium mix according to weight ratio 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08;
Described tackifier is high molecular cellulose and HANSHENGJIAO is the mixture of 3-4:1 mixing according to weight ratio;
Described anti-allergic agent is the mixture that water solublity a-bisabolol and glycyrrhizic acid dipotassium mix according to 2-6:1;
Described metal ion chelation agent is L-vitamin C and citric acid is the mixture of 1-3:1 mixing according to weight ratio;
Described antiseptic is phenoxyethanol and Sang Pu K15 is the mixture of 1-2:1 mixing according to weight ratio;
Described brightening agent is arbutin, nicotiamide and Trenaxmine is the mixture of 1:1-3:1 mixing according to weight ratio;
Described nourishing additive agent is the mixture of one or more in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
2. Entermorpha decocting in water algae mud facial film according to claim 1, it is characterized in that: the preparation method of described Entermorpha powder is, by Entermorpha remove impurity, washing, oven dry to frond becomes fragile, then the Entermorpha of drying is smashed to pieces to graininess, be dipped to 8-20 hour, filtration in ethanol; The Entermorpha grain decocting in water 15-120 minute will obtained again, filters and obtains algae mud, is ground to and Powderedly obtains Entermorpha powder after centrifuge dehydration, lyophilization.
3. Entermorpha decocting in water algae mud facial film according to claim 1, is characterized in that: described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
4. a preparation method for Entermorpha decocting in water algae mud facial film according to claim 1, its step comprises:
(1), by Entermorpha remove impurity, washing, oven dry to frond becomes fragile, then the Entermorpha of drying is smashed to pieces to graininess, be dipped to 8-20 hour, filtration in ethanol;
(2), the Entermorpha grain decocting in water 15-120 minute that will obtain in step (1), filter and obtain algae mud, be ground to after centrifuge dehydration, lyophilization and Powderedly obtain Entermorpha powder;
(3), various raw material has been weighed according to formula;
(4) swelling by adding deionized water and stirring in load weighted Entermorpha powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Entermorpha mud continuation stirring, add tackifier and deionized water while stirring, after stirring, obtain Entermorpha decocting in water algae mud facial film.
5. the preparation method of Entermorpha decocting in water algae mud facial film according to claim 4, it is characterized in that: in described step (1), described Entermorpha is the one in Enteromorpha clathrata (Roth) Greville, Enteromorpha linza or bent Entermorpha; By Entermorpha dry to the baking temperature become fragile be 55-65 DEG C.
6. the preparation method of Entermorpha decocting in water algae mud facial film according to claim 4, it is characterized in that: in described step (2), is 40-70 DEG C by the decocting in water temperature of Entermorpha grain decocting in water; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
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| CN104473812B (en) * | 2014-11-28 | 2018-08-21 | 海南海润生物科技股份有限公司 | A kind of Biofibre facial mask |
| CN104958241A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Moisturizing traditional Chinese medicine mask product and preparation method thereof |
| CN104958242A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Anti-ultraviolet mask liquid and preparation method thereof |
| CN104958240A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Freckle expelling facial mask and preparation method thereof |
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