CN103720621A - Enteromorpha boiled alga clay mask and preparation method thereof - Google Patents
Enteromorpha boiled alga clay mask and preparation method thereof Download PDFInfo
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- CN103720621A CN103720621A CN201310724662.9A CN201310724662A CN103720621A CN 103720621 A CN103720621 A CN 103720621A CN 201310724662 A CN201310724662 A CN 201310724662A CN 103720621 A CN103720621 A CN 103720621A
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Abstract
The invention belonging to the field of cosmetics, and particularly relates to an Enteromorpha boiled alga clay mask and a preparation method thereof. The preparation method comprises the following steps: removing impurities from Enteromorpha, washing, drying until the algae become embrittled, stamping the dried Enteromorpha to granules, immersing in alcohol for 8-20 hours, filtering, boiling for 15-120 minutes, filtering to obtain alga clay, carrying out centrifugal dehydration and freeze-drying, and grinding into powder; weighing raw materials according to the formula; adding deionized water into the weighed Enteromorpha powder, and stirring to swell; and dissolving a moisturizer, an antioxidant, a metallic ion chelator, a preservative, a whitener, a deodorizer, a sebum inhibitor, a cutin dissolving agent, a bacteriostatic agent, an antiallergic agent and a nutrient additive in deionized water, adding the Enteromorpha clay, continuing stirring while adding a tackifying agent and deionized water, and stirring uniformly. The mask has the advantages of favorable moisturizing property, low cost and low price, obviously improves the skin color, moisturizes the skin, and prevents the skin from aging.
Description
Technical field
The invention belongs to cosmetic field, particularly a kind of Entermorpha decocting in water algae mud facial film and preparation method thereof.
Background technology
Facial film is a kind of facial cosmetics and skincare product that spreads on, utilization covers the blink of face, extraneous air and the pollution of temporary transient isolation, promote sweat gland secretion and metabolism, make the oxygen content of skin increase, be conducive to skin and get rid of the oil substances of the metabolic product of epidermis cell and accumulation, improve elasticity, pliability and the brightness of skin.The kind of facial film is a lot, and wherein seaweed mask, with the mineral composition of Sargassum extract, can be controlled oily Peppermint Extract, and moisture is provided, and calm tired, rough skin makes skin remain fine and smooth, glossy.But the moistening effect of plant seaweed mask of the prior art is not the most desirable, and use inconvenience, the shelf-life is short, expensive.
Entermorpha is a kind of common large ocean chlorella, and it belongs to Chlorophyta, Chlorophyceae, Ulvales, Ulvaceae in Sargassum.The polysaccharide of Entermorpha and protein have pharmacological actions such as reducing cholesterol, antibacterial and antiviral, antioxidation, enhancing immunologic function, antitumor, antiinflammatory.And Entermorpha also has multiple biological activity, in cosmetic applications, main manifestations is antioxidation, radioprotective, antiviral, the aspects such as moisture retention.In recent years, along with progressively going deep into that its chemical composition is studied, its medical mechanism is also illustrated gradually, and the step of drug development is constantly accelerated.
Utilize the biomass of Entermorpha to prepare facial film for raw material, in existing document and report, record not yet to some extent.If people can constantly research and develop the effect of Entermorpha, utilize the characteristic of its antioxidation, antiviral, moisture retention etc., be developed to there is whitening, the facial film of the effect such as antiinflammatory, moisturizing, turn waste into wealth, it is fully utilized, in environmental improvement, also increased economic benefit, killed two birds with one stone.
Summary of the invention
The object of this invention is to provide a kind of Entermorpha decocting in water algae mud facial film, this facial film can increase skin surface moisture, and moistening effect is excellent, also has the effect of whitening, antiinflammatory, reduce wrinkle, and uses simple, low price.
Another object of the present invention is to provide a kind of preparation method of above-mentioned Entermorpha decocting in water algae mud facial film.
Object of the present invention can be achieved through the following technical solutions:
An Entermorpha decocting in water algae mud facial film, is characterized in that, comprises the raw material that following percentage by weight is counted meter:
Entermorpha powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
The preparation method of described Entermorpha powder is, by Entermorpha remove impurity, washing, dry and become fragile to frond till, then dry Entermorpha is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter; By the Entermorpha grain decocting in water 15-120 minute obtaining, filter and obtain algae mud again, after centrifuge dehydration, lyophilization, be ground to the Powdered Entermorpha powder that obtains.
Described wetting agent is one or more the mixture in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.Preferably, described wetting agent is the mixture of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium; The weight ratio of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium is 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08.
Described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO.Preferably, described tackifier is the mixture of high molecular cellulose and HANSHENGJIAO, and the weight ratio of high molecular cellulose and HANSHENGJIAO is 3-4:1.
Described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid, and preferred described metal ion chelation agent is the mixture of L-vitamin C and citric acid, and wherein the weight ratio of L-vitamin C and citric acid is 1-3:1.
Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15.Preferably, described antiseptic is the mixture of phenoxyethanol and Sang Pu K15, and wherein, the volume ratio of phenoxyethanol and Sang Pu K15 is 1-2:1.
Described brightening agent is one or more the mixture in arbutin, nicotiamide or Trenaxmine.Preferably, described brightening agent is the mixture of arbutin, nicotiamide and Trenaxmine, and wherein, the weight ratio of arbutin, nicotiamide and Trenaxmine is 1:1-3:1.
Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.Preferably, described anti-allergic agent is the mixture of water solublity a-bisabolol and glycyrrhizic acid dipotassium, and wherein, the weight ratio of water solublity a-bisabolol and glycyrrhizic acid dipotassium is 2-6:1.
Described nourishing additive agent is one or more the mixture in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
Described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
The preparation method of above-mentioned Entermorpha decocting in water algae mud facial film, its step comprises:
(1), by Entermorpha remove impurity, washing, dry and become fragile to frond till, then dry Entermorpha is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter;
(2), by the Entermorpha grain decocting in water 15-120 minute obtaining in step (1), filter and to obtain algae mud, after centrifuge dehydration, lyophilization, be ground to the Powdered Entermorpha powder that obtains; Entermorpha is through after alcohol-pickled and decocting in water, can extract more fully can, by effective biomass that skin absorbed, improve the moisture retention of facial film in Entermorpha.
(3), according to formula, weigh good various raw materials;
(4), deionized water and stirring swelling will be added in load weighted Entermorpha powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir the Entermorpha mud continuation stirring that swelling is good, add while stirring tackifier and deionized water, after stirring, obtain Entermorpha decocting in water algae mud facial film.
In described step (1), described Entermorpha is a kind of in bar Entermorpha, edge pipe Entermorpha or bent Entermorpha; By Entermorpha oven dry to the baking temperature becoming fragile, be 55-65 ℃.
In described step (2), by the decocting in water temperature of Entermorpha grain decocting in water, be 40-70 ℃; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
Compared with prior art, beneficial effect of the present invention is:
1, the moisture retention of described Entermorpha decocting in water algae mud facial film is good, and the skin moisture content rate of increase applying after 20 minutes through facial film face of the present invention is more than 33%, and can obviously improve the colour of skin, Glycerin, effectively prevents skin aging, reduces wrinkle.
2, the preparation method of described Entermorpha decocting in water algae mud facial film is simple, easy to operate, and raw material is easy to get, cost is low, low price, and the medicine adding in preparation process is not only to not injury of skin, and environmentally safe, green, environmental protection.
Accompanying drawing explanation
Fig. 1 is the skin lines comparison diagram that has applied the Entermorpha decocting in water algae mud facial film front and back that make in embodiment 1.
The specific embodiment
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1) preparation of Entermorpha powder
The bar Entermorpha gathering is removed to assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, distilled water wash until electrical conductivity of water drop to below 0.02MS; Till drying in the baking oven of 60 ℃ and becoming fragile to frond; With medicine bruisher, fully smash to pieces to algae grain length and be shorter than 5mm, adding mass concentration is 75% alcohol-pickled spending the night (12 hours), with 100 order silk cover filterings, obtain algae grain, algae grain is decocting in water 1h at 70 ℃, with 200 mesh sieve thin,tough silk filtering supernatants, obtain algae mud, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 300 seconds, by fully grinding after the algae mud vacuum lyophilization of centrifuge dehydration, obtain Entermorpha powder recently.
(2) preparation process of facial film
Get the Entermorpha powder 10g in step (1), add 30mL deionized water swelling stirring, standby.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 5g, amino acid humectant 3g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, 120-160 ten thousand each 0.1g), red wine polyphenols 1g, L-vitamin C1g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 2g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Entermorpha mud after swelling is stirred is mixed homogeneously with above-mentioned adjuvant, adds while stirring even mixed 1.4g high molecular cellulose and 0.4g HANSHENGJIAO, with deionized water, adds to 100g total amount, obtains Entermorpha decocting in water algae mud facial film.
(3) testing result
For the moistening effect of the Entermorpha decocting in water algae mud facial film for preparing in test implementation example 1, respectively by green tea powder facial film, lavandula angustifolia facial film in contrast.Wherein the preparation method of green tea powder facial film and lavandula angustifolia facial film, according to the formula preparation in the present embodiment 1, only replaces Entermorpha powder by the green tea powder of equivalent and lavandula angustifolia powder (all purchased from Chhnang daily use chemicals, Guangdong), and other raw materials and addition thereof are all constant.
Before test: experimenter's arm of cleaning inner side, and with wet gauze (with deionized water) scrub, water temperature is room temperature, after cleaning, inside experimenter's both hands forearm, carries out measurement markers, within before tested position 2-3 days, can not use any cosmetic product; In test: use latex finger cot that test products and reference product are evenly applied in arm trial zone, smearing thickness is 2mm, carries out measurement and the observation of tested region and control zone after 20min, and each region is parallel assay five times according to the order of sequence, draw meansigma methods, shown in table 1 specific as follows:
Table 1 skin moisture content rate of increase
With 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U) observation, applied the skin of the Entermorpha decocting in water algae mud facial film in the present embodiment 1, as shown in Figure 1, wherein Fig. 1 a does not apply the skin observation figure of Entermorpha decocting in water algae mud facial film, Fig. 1 b is the skin observation figure that has applied Entermorpha decocting in water algae mud facial film, from comparative observation, figure shows, the facial film of preparing in the present embodiment all can improve the colour of skin, Glycerin, the moisture content of raising epiderm skin.
Embodiment 2
(1) preparation of Entermorpha powder
The edge pipe Entermorpha gathering is removed to assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, distilled water wash until electrical conductivity of water drop to below 0.02MS; Till drying in the baking oven of 60 ℃ and becoming fragile to frond; With medicine bruisher, fully smash to pieces to algae grain length and be shorter than 5mm, adding mass concentration is 75% alcohol-pickled spending the night (18 hours), with 100 order silk cover filterings, obtain algae grain, algae grain decocting in water 45 minutes at 70 ℃, with 200 mesh sieve thin,tough silk filtering supernatants, obtain algae mud, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 300 seconds, by fully grinding after the algae mud vacuum lyophilization of centrifuge dehydration, obtain Entermorpha powder recently.
(2) preparation process of facial film
Get the Entermorpha powder 15g in step (1), add 30mL deionized water swelling stirring, standby.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 4g, amino acid humectant 4g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, 120-160 ten thousand each 0.1g), red wine polyphenols 2g, L-vitamin C2g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 1.5g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Entermorpha mud after swelling is stirred is mixed homogeneously with above-mentioned adjuvant, adds while stirring even mixed 1.5g high molecular cellulose and 0.5g HANSHENGJIAO, with deionized water, adds to 100g total amount, obtains Entermorpha decocting in water algae mud facial film.
(3) testing result
Method of testing is with embodiment 1, and concrete test result is as shown in table 2 below:
Table 2 skin moisture content rate of increase
In sum, use the moisture content that can obviously improve skin epidermis after Entermorpha decocting in water algae mud facial film, improved the colour of skin, Glycerin.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the disclosed content of this embodiment.So every, do not depart from the equivalence completing under spirit disclosed in this invention or revise, all falling into the scope of protection of the invention.
Claims (10)
1. an Entermorpha decocting in water algae mud facial film, is characterized in that, comprises the raw material that following percentage by weight is counted meter:
Entermorpha powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
2. Entermorpha decocting in water algae mud facial film according to claim 1, it is characterized in that: the preparation method of described Entermorpha powder is, by Entermorpha remove impurity, washing, dry and become fragile to frond till, then dry Entermorpha is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter; By the Entermorpha grain decocting in water 15-120 minute obtaining, filter and obtain algae mud again, after centrifuge dehydration, lyophilization, be ground to the Powdered Entermorpha powder that obtains.
3. Entermorpha decocting in water algae mud facial film according to claim 1, is characterized in that: described wetting agent is one or more the mixture in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.
4. Entermorpha decocting in water algae mud facial film according to claim 1, is characterized in that: described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO; Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.
5. the Entermorpha decocting in water algae mud facial film described in 1 as requested, is characterized in that: described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid; Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15; Described brightening agent is one or more the mixture in arbutin, nicotiamide or Trenaxmine.
6. Entermorpha decocting in water algae mud facial film according to claim 1, is characterized in that: described nourishing additive agent is one or more the mixture in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
7. Entermorpha decocting in water algae mud facial film according to claim 1, is characterized in that: described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
8. a preparation method for Entermorpha decocting in water algae mud facial film claimed in claim 1, its step comprises:
(1), by Entermorpha remove impurity, washing, dry and become fragile to frond till, then dry Entermorpha is smashed to pieces to graininess, be dipped in ethanol 8-20 hour, filter;
(2), by the Entermorpha grain decocting in water 15-120 minute obtaining in step (1), filter and to obtain algae mud, after centrifuge dehydration, lyophilization, be ground to the Powdered Entermorpha powder that obtains;
(3), according to formula, weigh good various raw materials;
(4) deionized water and stirring swelling will be added in load weighted Entermorpha powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir the Entermorpha mud continuation stirring that swelling is good, add while stirring tackifier and deionized water, after stirring, obtain Entermorpha decocting in water algae mud facial film.
9. the preparation method of Entermorpha decocting in water algae mud facial film according to claim 8, is characterized in that: in described step (1), described Entermorpha is a kind of in bar Entermorpha, edge pipe Entermorpha or bent Entermorpha; By Entermorpha oven dry to the baking temperature becoming fragile, be 55-65 ℃.
10. the preparation method of Entermorpha decocting in water algae mud facial film according to claim 8, is characterized in that: in described step (2), by the decocting in water temperature of Entermorpha grain decocting in water, be 40-70 ℃; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
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Cited By (5)
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| CN104434630A (en) * | 2014-11-13 | 2015-03-25 | 龙骏 | Product for enhancing skin activity and preparation method thereof |
| CN104473812A (en) * | 2014-11-28 | 2015-04-01 | 海南海之润生物工程有限公司 | Biological fiber facial mask |
| CN104958241A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Moisturizing traditional Chinese medicine mask product and preparation method thereof |
| CN104958240A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Freckle expelling facial mask and preparation method thereof |
| CN104958242A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Anti-ultraviolet mask liquid and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434630A (en) * | 2014-11-13 | 2015-03-25 | 龙骏 | Product for enhancing skin activity and preparation method thereof |
| CN104473812A (en) * | 2014-11-28 | 2015-04-01 | 海南海之润生物工程有限公司 | Biological fiber facial mask |
| CN104958241A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Moisturizing traditional Chinese medicine mask product and preparation method thereof |
| CN104958240A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Freckle expelling facial mask and preparation method thereof |
| CN104958242A (en) * | 2015-07-31 | 2015-10-07 | 桂林市宏旭生物科技有限公司 | Anti-ultraviolet mask liquid and preparation method thereof |
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