CN107412079A - A kind of eye mask with crease-resistant effect of compacting - Google Patents
A kind of eye mask with crease-resistant effect of compacting Download PDFInfo
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- CN107412079A CN107412079A CN201710815364.9A CN201710815364A CN107412079A CN 107412079 A CN107412079 A CN 107412079A CN 201710815364 A CN201710815364 A CN 201710815364A CN 107412079 A CN107412079 A CN 107412079A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The invention discloses a kind of eye mask with crease-resistant effect of compacting, and it contains the complex microsphere that parts by weight are 0.3 0.5 parts, and complex microsphere includes butanediol, water, peony root extractive, the component of Gentrin Knotweed P.E.Eye mask of the present invention is mainly butanediol, water, peony root extractive, Gentrin Knotweed P.E complex microsphere performance active function, by suppressing elastase activity, suppress the generation of wrinkle of skin, and then play a part of crease-resistant anti-aging, so as to recover the elasticity of skin, compact skin；Also there is phenomena such as water lock moisturizing, keep eye emollient, avoid eye accelerated ageing, cause obscure, microgroove to occur.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of eye mask with crease-resistant effect of compacting.
Background technology
Elastoser has the ability of the multiple proteins such as degraded collagen, elastin laminin.It is elastic during skin aging
The change of protein structure is one of major reason for causing wrinkle and cutis laxa, and suppresses elastoser and decompose elastin laminin
The crease-resistant effect of anti-aging can be played.
Giant knotweed, Chinese medicine name.For polygonaceae plant giant knotweed Polygonum cuspidatum Sieb.et Zucc. dry root
Stem and root.It is distributed in the ground such as northwest, East China, Central China, south China and southwest.Giant knotweed contains 2,3,5,4'-tetrahydroxyl diphenylethylene-2-O-BETA-D-glucoside, anthraquinone, boots matter, flavonoids etc.
Compound.Polygonin is a kind of main component of giant knotweed, belongs to three 2,3,5,4'-tetrahydroxyl diphenylethylene-2-O-BETA-D-glucosides, existing lot of documents report it have it is antitumor,
The bioactivity such as reducing blood lipid, liver protection profit liver, anti-inflammation, but Gentrin Knotweed P.E rarely has to the inhibitory action of elastase activity
Report.Gentrin Knotweed P.E be probably to Elastase Inhibitory mechanism containing polygonin the catalysis of elastoser is lived
Property division center change or be blanked, cause elastoser activity reduction.
The content of the invention
Based on this, it is an object of the invention to provide a kind of eye mask with crease-resistant effect of compacting, and it contains giant knotweed extraction
Thing isoreactivity composition, there is crease-resistant anti-aging and other effects.
To achieve these goals, the present invention adopts the following technical scheme that：
A kind of eye mask with crease-resistant effect of compacting contains the complex microsphere that parts by weight are 0.3-0.5 parts, wherein, it is compound micro-
Ball includes butanediol, water, peony root extractive, the component of Gentrin Knotweed P.E.
Further, described butanediol, water, peony root extractive, the mass ratio of Gentrin Knotweed P.E are：(4-6)：(4-
8)：(1-3)：(2-4), and described water is micromolecular water.
Further, the preparation method of described complex microsphere is：Sodium alginate is configured to solution, weighs one in proportion
Quantitative butanediol, water, peony root extractive, Gentrin Knotweed P.E and nano-calcium carbonate calcium powder adds to above-mentioned sodium alginate soln
In, stirring, ultrasound, insoluble calcium carbonate is uniformly suspended in the solution；The atoleine for measuring certain volume again is placed in
In three-necked flask, span 80 is added thereto, stirs, controls certain rotating speed, add above-mentioned preparation thereto contains tree peony
The sodium alginate soln of root extract, Gentrin Knotweed P.E and nano-calcium carbonate, certain time is stirred, form W/O reversed-phase emulsions；So
Atoleine solution of the 20mL containing glacial acetic acid is slowly added dropwise with micro-injection pump afterwards, the calcium ion discharged in calcium carbonate is crosslinked
Reaction, stood after stirring a period of time；Washed with n-hexane, isolate butanediol, water, peony root extractive, Gentrin Knotweed P.E
Complex microsphere.
Further, the preparation method of described peony root extractive is as follows：Tree peony root is weighed, cleaning, drying, is ground into
40 mesh, according to solid-liquid ratio 1:10 (g/ml) add 85% ethanol, extract 5h, filtering, and filter residue repeats extraction 2 times, each 2h, merges
Filtrate, ethanol is recovered under reduced pressure, obtains peony root extractive.
Further, the preparation method of described Gentrin Knotweed P.E is as follows：Giant knotweed is weighed, cleaning, drying, is ground into 15
Mesh；15 times of amount (g/ml) 65% EtOH Sonicate extraction 5h, filtering, filter residue are added under conditions of ultrasonic power 350W, 60 DEG C
Extraction 2 times, each 2h is repeated, merging filtrate, dries, obtains Gentrin Knotweed P.E.
Further, described eye mask also includes the component of following parts by weight：Sodium Hyaluronate 0.03-0.05 parts, glycerine
3.0-5.0 parts, butanediol 5.0-8.0 parts, polyethylene glycol -14M0.01-0.03 parts, allantoin 0.1-0.3 parts, hydroxy ethyl fiber
Plain 0.2-0.3 parts, carbomer 0.05-0.1 parts, parahydroxyacet-ophenone 0.5-1.0 parts, 1,2- hexylene glycol 0.5-1.0 parts, three ethanol
Amine 0.05-1.0 parts, asiaticosid 0.2-0.3 parts, carnosine 0.03-0.05 parts, biological carbohydrate gum -13.0-5.0 parts, the poly- methyl of glycerine
Acrylate/propane diols/Gantrez AN-119 3.0-4.0 parts, deionized water are to 103 parts.
Compared with prior art, it is the device have the advantages that as follows：Eye mask of the present invention is mainly butanediol, water, male
Red root extract, Gentrin Knotweed P.E complex microsphere play active function.Prepared using the natural wall material sodium alginate (ALG) of safety micro-
Ball encapsulating butanediol, water, peony root extractive, Gentrin Knotweed P.E, microballoon has to these active components to be transmitted, protects, stably
And slow releasing function；Slow releasing function can be such that active component is progressively released from microballoon with certain speed by infiltration or diffusion
Put, reduce stimulation of some active components to skin and extend the action time of active component.Eye mask of the present invention passes through suppression
Elastase activity processed, suppresses the generation of wrinkle of skin, and then plays a part of crease-resistant anti-aging, so as to recover skin
Elasticity, compact skin；Also there is water lock moisturizing, keep eye emollient, avoid eye accelerated ageing, cause obscure, microgroove etc. existing
As occurring.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated：
The eye mask embodiment 1~5 of the present invention is formulated, and is shown in Table 1.
Table 1
Liposome in above-described embodiment includes butanediol, water, peony root extractive, the component of Gentrin Knotweed P.E, and fourth
Glycol, water, peony root extractive, the mass ratio of Gentrin Knotweed P.E are (4-6)：(4-8)：(1-3)：(2-4).
1st, the preparation method of complex microsphere is as follows：
Sodium alginate is configured to solution, a certain amount of butanediol, water, peony root extractive, giant knotweed is weighed in proportion and carries
Take thing and nano-calcium carbonate calcium powder to add in above-mentioned sodium alginate soln, stir, ultrasound, insoluble calcium carbonate is uniformly hanged
Float in the solution；The atoleine for measuring certain volume again is placed in three-necked flask, is added span 80 thereto, is stirred,
Certain rotating speed is controlled, adds the marine alga containing peony root extractive, Gentrin Knotweed P.E and nano-calcium carbonate of above-mentioned preparation thereto
Acid sodium solution, certain time is stirred, form W/O reversed-phase emulsions；Then 20mL is slowly added dropwise containing glacial acetic acid with micro-injection pump
Atoleine solution, the calcium ion discharged in calcium carbonate carry out cross-linking reaction, stood after stirring a period of time；Washed with n-hexane
Wash, isolate the complex microsphere of butanediol, water, peony root extractive, Gentrin Knotweed P.E.
2nd, the preparation method of peony root extractive is as follows：
Tree peony root is weighed, cleaning, drying, is ground into 40 mesh, according to solid-liquid ratio 1:10 (g/ml) add 85% ethanol, extraction
5h, filtering, filter residue repeat extraction 2 times, each 2h, merging filtrate, ethanol are recovered under reduced pressure, obtain peony root extractive.
3rd, the preparation method of Gentrin Knotweed P.E is as follows：
Giant knotweed is weighed, cleaning, drying, is ground into 15 mesh；15 times of amounts are added under conditions of ultrasonic power 350W, 60 DEG C
(g/ml) 65% EtOH Sonicate extraction 5h, filtering, filter residue repeat extraction 2 times, each 2h, merging filtrate, dried, and obtain giant knotweed extraction
Thing.
Comparative example 1：
Difference with embodiment 3 is only the complex microsphere without butanediol and water, the addition of remaining each group material, preparation and work
Skill does not change.
Comparative example 2：
With embodiment 3 difference be only without peony root extractive complex microsphere, remaining each group material addition, prepare with
Technique does not change.
Comparative example 3：
Difference with embodiment 3 is only the complex microsphere without Gentrin Knotweed P.E, the addition of remaining each group material, preparation and work
Skill does not change.
Comparative example 4：
Complex microsphere is not added in difference with embodiment 3 only, and remaining each material addition, conditions and technology of preparation is not sent out
It is raw to change.
Crease-resistant efficacy validation：
Tested crowd：The voluntary tester of selection 120 25-45 year, man 60, female 60, are divided into 10 groups.
Instrument：German CK companies skin elasticity tester MPA580
Method：Constant negative pressure pattern is selected, everyone tests one group of data, removes two maximums and two in each group
After minimum value, residue 10 is taken to be worth for each person.30min is tested after periocualr skin cleaning, and subject adheres to making daily sooner or later
With above-mentioned trial target, it is skip test when test is not used respectively, using periocualr skin elasticity and moisture-holding capacity after 2 weeks, 4 weeks, surveys
It is 450mbar that negative pressure is constant during examination.Flexibility test explanation:Skin springback capacity when Ua- is without negative pressure；Skin when Uf- has negative pressure
Maximum tension amount；After Ue- constant negative pressures are added on skin, positioning elastic amount of tension；Uv:Uf-Ue is the visco-elastic portions of skin,
Or it is plastic amount of tension；Ur:After cancelling negative pressure, skin will restore to the original state rapidly state, the elastic part of recovery process
Tension values；R2 definition:R2=Ua/Uf, ratio illustrate that skin elasticity is better closer to 1；R5 definition:R5=Ur/Ue, skin
In skin recovery process elastic part with plus negative pressure process and the ratio between elastic part, ratio illustrates that skin elasticity is got over closer to 1
It is good；R6 definition:The ratio between R6=Uv/Ue, the plastic and elastic part of skin, ratio is smaller, illustrates that skin elasticity is better；
R7 definition:R7=Ur/Uf, the ratio between elastic part and maximum tension amount in skin recovery process, ratio illustrates skin closer to 1
Skin elasticity is better；Index explanation:Closer to 1, R6 closer to 0, the elasticity of skin is better by wherein R2, R5, R7.Water content test is said
It is bright:Skin moisture content scope is classified:0-33 is water deficient, and 33-66 is normal, and 66-99 is that moisture is full.
Test result such as table 2 below and table 3：
Table 2
As shown in Table 2:Using eye part skin R2, R5, R7 numerical value after embodiment 1-5 eye mask the 2nd week and the 4th week significantly
Increase, its index levels off to 1, R6 reductions after the 4th week, and its exponential approach is in 0 after the 4th week, and uses comparative example 1-4 and control
Eye part skin R2, R5, R7 ascensional range is significantly less than embodiment 1-5 with R6 reductions amplitude after the eye mask of group, and its using effect is equal
Not as embodiment, the elasticity of skin can be increased by illustrating the eye mask of the present invention, mitigate periocualr skin wrinkle problem.
Table 3
As shown in Table 3:Use eye circumference skin water content after embodiment 1-5 and comparative example 1-3 eye mask the 2nd week and the 4th week
Significantly improve, and embodiment is more excellent than comparative example and control group effect, illustrates that the present invention has good replenishing water and preserving moisture effect.
Anti-oxidation efficacy is verified：
Test method：Remove the electronic paramagnetic resonance spectrometer experiment of hydroxyl radical free radical
At room temperature, in 4ml test tubes, phosphate buffer (pH 7.4) 0.5ml is sequentially added, 5 μ L 5,5- dimethyl-
1- pyrrolin-N oxides (DMP0), 250 μ L0.1M H202, eye made from 1.5ml 0.1mM embodiments 1-5 and comparative example 1-4
Film, while using a commercially available declaring to have well, anti-oxidant eye mask is control group, 250 μ L3mMFeS04 solution, in 6 minutes left sides
ESR detections are carried out in right injection quartz capillary.As a result such as table 2 below：
Table 2
It was found from upper table data, the facial mask of 1-5 of embodiment of the present invention enhancing oxidation resistances has to free radical compositions
There is very strong antioxidation activity, free radical can be removed in time
Above example is merely to illustrate embodiment of the present invention, does not have any formal limit to the present invention
System；It is any to be engaged in professional and technical personnel, all have the ability using the technology contents having revealed that, some are made to it and changes or repaiies
Decorations, turn into the equivalent embodiment of equivalent variations.According to the technology of the present invention essence, simply modification, equivalent variations are carried out to the present invention
With modification, belong in the range of technical solution of the present invention.
Claims (7)
1. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting, it is characterised in that described eye mask contains parts by weight and is
The complex microsphere of 0.3-0.5 parts, wherein, complex microsphere includes butanediol, water, peony root extractive, the component of Gentrin Knotweed P.E.
2. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting according to claim 1, it is characterised in that described
Butanediol, water, peony root extractive, the mass ratio of Gentrin Knotweed P.E are：(4-6)：(4-8)：(1-3)：(2-4).
3. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting according to claim 1, it is characterised in that described
Water is micromolecular water.
4. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting according to claim 1, it is characterised in that described
The preparation method of complex microsphere is：Sodium alginate is configured to solution, weighs a certain amount of butanediol, water, tree peony root in proportion
Extract, Gentrin Knotweed P.E and nano-calcium carbonate calcium powder are added in above-mentioned sodium alginate soln, stirring, ultrasound, are made insoluble
Calcium carbonate uniformly suspends in the solution；The atoleine for measuring certain volume again is placed in three-necked flask, is added thereto
Span 80, stirs, and controls certain rotating speed, add thereto above-mentioned preparation containing peony root extractive, Gentrin Knotweed P.E and
The sodium alginate soln of nano-calcium carbonate, certain time is stirred, form W/O reversed-phase emulsions；Then slowly dripped with micro-injection pump
Add atoleine solution of the 20mL containing glacial acetic acid, the calcium ion discharged in calcium carbonate carries out cross-linking reaction, after stirring a period of time
Stand；Washed with n-hexane, isolate the complex microsphere of butanediol, water, peony root extractive, Gentrin Knotweed P.E.
5. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting according to claim 1, it is characterised in that described
The preparation method of peony root extractive is as follows：Tree peony root is weighed, cleaning, drying, is ground into 40 mesh, according to solid-liquid ratio 1:10(g/
Ml 85% ethanol) is added, extracts 5h, filtering, filter residue repeats extraction 2 times, each 2h, merging filtrate, ethanol is recovered under reduced pressure, obtains male
Red root extract.
6. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting according to claim 1, it is characterised in that described
The preparation method of Gentrin Knotweed P.E is as follows：Giant knotweed is weighed, cleaning, drying, is ground into 15 mesh；In ultrasonic power 350W, 60 DEG C
Under conditions of add 15 times amount (g/ml) 65% EtOH Sonicates extraction 5h, filtering, filter residue repeat extraction 2 times, each 2h, merge filter
Liquid, dry, obtain Gentrin Knotweed P.E.
7. a kind of crease-resistant eye mask that compacts with crease-resistant effect of compacting according to claim any one of 1-6, its feature exist
In described eye mask also includes the component of following parts by weight：Sodium Hyaluronate 0.03-0.05 parts, glycerine 3.0-5.0 parts, fourth two
Alcohol 5.0-8.0 parts, polyethylene glycol -14M0.01-0.03 parts, allantoin 0.1-0.3 parts, hydroxyethyl cellulose 0.2-0.3 parts, card
Ripple nurse 0.05-0.1 parts, parahydroxyacet-ophenone 0.5-1.0 parts, 1,2- hexylene glycol 0.5-1.0 parts, triethanolamine 0.05-1.0 parts,
Asiaticosid 0.2-0.3 parts, carnosine 0.03-0.05 parts, biological carbohydrate gum -13.0-5.0 parts, glycerine polymethacrylates/the third two
Alcohol/Gantrez AN-119 3.0-4.0 parts, deionized water are to 103 parts.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710815364.9A CN107412079A (en) | 2017-09-11 | 2017-09-11 | A kind of eye mask with crease-resistant effect of compacting |
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| CN201710815364.9A CN107412079A (en) | 2017-09-11 | 2017-09-11 | A kind of eye mask with crease-resistant effect of compacting |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108210436A (en) * | 2018-03-14 | 2018-06-29 | 佛山市迭蓓生物科技有限公司 | A kind of microcapsules eye compacts skin base solution and preparation method |
| CN110037952A (en) * | 2019-04-09 | 2019-07-23 | 上海悦目化妆品有限公司 | A kind of crease-resistant and Vitamin K eye mask patch |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102860961A (en) * | 2012-09-24 | 2013-01-09 | 彭再辉 | Eye pad essence containing peony root extracts and preparation method for eye pad essence |
| CN104224683A (en) * | 2014-09-16 | 2014-12-24 | 上海芊墨化妆品有限公司 | Natural plant skin care product for improving skin metabolism of yellow race and delaying senescence |
| CN104856963A (en) * | 2015-05-26 | 2015-08-26 | 大连理工大学 | Astaxanthin-sodium alginate sustained release microspheres as well as preparation method and application thereof |
| CN106606447A (en) * | 2016-12-08 | 2017-05-03 | 浙江百惠生物科技有限公司 | Green plum enzyme-fibroin mask |
-
2017
- 2017-09-11 CN CN201710815364.9A patent/CN107412079A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102860961A (en) * | 2012-09-24 | 2013-01-09 | 彭再辉 | Eye pad essence containing peony root extracts and preparation method for eye pad essence |
| CN104224683A (en) * | 2014-09-16 | 2014-12-24 | 上海芊墨化妆品有限公司 | Natural plant skin care product for improving skin metabolism of yellow race and delaying senescence |
| CN104856963A (en) * | 2015-05-26 | 2015-08-26 | 大连理工大学 | Astaxanthin-sodium alginate sustained release microspheres as well as preparation method and application thereof |
| CN106606447A (en) * | 2016-12-08 | 2017-05-03 | 浙江百惠生物科技有限公司 | Green plum enzyme-fibroin mask |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108210436A (en) * | 2018-03-14 | 2018-06-29 | 佛山市迭蓓生物科技有限公司 | A kind of microcapsules eye compacts skin base solution and preparation method |
| CN110037952A (en) * | 2019-04-09 | 2019-07-23 | 上海悦目化妆品有限公司 | A kind of crease-resistant and Vitamin K eye mask patch |
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Application publication date: 20171201 |
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