CN107550752A - A kind of crease-resistant eye mask that compacts - Google Patents
A kind of crease-resistant eye mask that compacts Download PDFInfo
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- CN107550752A CN107550752A CN201710811614.1A CN201710811614A CN107550752A CN 107550752 A CN107550752 A CN 107550752A CN 201710811614 A CN201710811614 A CN 201710811614A CN 107550752 A CN107550752 A CN 107550752A
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Abstract
The invention discloses a kind of crease-resistant eye mask that compacts, and it contains the microballoon that parts by weight are 0.3 0.5 parts.The microballoon is (3 7) by mass ratio:(4‑5):(1‑3):Butanediol, water, peony root extractive, the coreopsis tinctoria extract composition of (1 3).Eye mask of the present invention is by improving superoxide dismutase activity, remove free radical, suppress the generation of lipid peroxide, and then the effect of anti-aging, so as to recover the elasticity of skin, compact skin, moreover it is possible to keeps eye emollient, phenomena such as avoiding eye accelerated ageing, causing crow's feet, microgroove occurs.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of crease-resistant eye mask that compacts.
Background technology
As the improvement of people's living standards, requirement of the people to quality of life also more and more higher, maintenance to skin into
The problem of for people's growing interest, due to the quickening of rhythm of life, the aging of eye skin has been universal phenomenon, therefore, tool
There are moist, improvement wrinkle, the eye mask of microgroove effect to have more wide market.
Snow chrysanthemum scientific name Coreopsis tinctoria, dichromatism golden wave, it is called and does high mountain cold chrysanthemum, blood chrysanthemum, gram force sun chrysanthemum etc., dimension language is referred to as Gu
Beautiful just that, it is the meaning of jasmine tea, is the dry capitulum of Tickseed dichromatism golden wave.Modern pharmacology research shows to avenge
Chrysanthemum has a variety of medicinal efficacies, such as reduces blood pressure, improves blood fat, anti-aging, anti-cancer, detects its chemical composition and finds snow chrysanthemum
In contain a variety of active components for being advantageous to human body, as flavonoids, volatile oil, amino acid, carbohydrate, chlorogenic acid and lot of trace member
Element etc..Coreopsis tinctoria extract can improve superoxide dismutase activity in people and Mice Body, suppress lipid peroxide and lipofuscin
Formed, to OH free radicals, O2 -Free radical, DPPH free radicals have preferable scavenging action, and it is aobvious to show that coreopsis tinctoria extract has
Anti-oxidant, anti-aging, promotion body metabolism the effect write.
The content of the invention
Based on this, it is an object of the invention to provide a kind of crease-resistant eye mask that compacts, there is anti-oxidant, anti-aging and other effects.
To achieve these goals, the present invention adopts the following technical scheme that:
A kind of crease-resistant eye mask that compacts contain chitosan reinforcing butanediol, water, peony root extractive, coreopsis tinctoria extract-
ALG/NOCC microballoons, and the parts by weight of described microballoon are 0.3-0.5 parts.
Further, described butanediol, water, peony root extractive, the mass ratio of coreopsis tinctoria extract are:(3-7):(4-
5):(1-3):(1-3), and described water is micromolecular water.
Further, the preparation method of described microballoon is as follows:By sodium alginate and N, O-CMC is made into
20ml mixed solutions;Butanediol, water, peony root extractive, coreopsis tinctoria extract and nano-calcium carbonate calcium powder is weighed in proportion to add to
In above-mentioned sodium alginate soln, stirring, ultrasound, insoluble calcium carbonate is set uniformly to suspend in the solution;Certain body is measured again
Long-pending atoleine is placed in three-necked flask, is added span 80 thereto, is stirred, and is controlled rotating speed, is added thereto above-mentioned
The sodium alginate soln containing peony root extractive, coreopsis tinctoria extract and nano-calcium carbonate prepared, stirring form the anti-phase breasts of W/O
Liquid;Then atoleine solution of the 20mL containing glacial acetic acid is slowly added dropwise with micro-injection pump, the calcium ion discharged in calcium carbonate enters
Row cross-linking reaction, stood after stirring;Washed with n-hexane, isolate butanediol, water, peony root extractive, coreopsis tinctoria extract-
ALG/NOCC microballoons;Add into 100mL 1% (w/v) chitosan solution, after magnetic agitation 40min, be washed with deionized water
Remove not participate in the chitosan of reaction, centrifuge, freeze-drying, obtain the butanediol of chitosan reinforcing, water, peony root extractive, snow chrysanthemum
Extract-ALG/NOCC microballoons.
Further, the preparation method of described CMC (NOCC) is as follows:Weigh the addition of 10g chitosans
Into 500mL three-necked flask, 120mL isopropanols, stirring are then added, heating makes its swelling;Treat that temperature reaches 50 DEG C or so,
40mL40% sodium hydroxide solution is added, stirs 30min;Then chloroacetic aqueous isopropanol, isothermal reaction 3h are added;Again
Disposable 40% sodium hydroxide solution for adding 60mL, stop stirring after reacting 1h;Products therefrom is filtered, filter residue deionization
Water dissolves;With the pH of hydrochloric acid conditioning solution, a large amount of floccules can be constantly separated out, are filtered;With washes of absolute alcohol, it is dried in vacuo
Product.
Further, the preparation method of described peony root extractive is as follows:Tree peony root is weighed, cleaning, drying, is ground into
40 mesh, according to solid-liquid ratio 1:10 (g/ml) add 85% ethanol, extract 5h, filtering, and filter residue repeats extraction 2 times, each 2h, merges
Filtrate, ethanol is recovered under reduced pressure, obtains peony root extractive.
Further, the preparation method of described coreopsis tinctoria extract is as follows:Snow chrysanthemum is weighed, cleaning, drying, is ground into 15
Mesh;According to solid-liquid ratio 1:15 (g/ml) add the ethanol of volume fraction 60%, and in ultrasonic power 350W, 60 DEG C of condition ultrasound carries
2h is taken, is filtered, filter residue repeats extraction 2 times, each 1h, merging filtrate, dries, obtains coreopsis tinctoria extract.
Further, described eye mask also includes the component of following parts by weight:Sodium Hyaluronate 0.03-0.05 parts, glycerine
3.0-5.0 parts, butanediol 5.0-8.0 parts, polyethylene glycol -14M0.01-0.03 parts, allantoin 0.1-0.3 parts, hydroxy ethyl fiber
Plain 0.2-0.3 parts, carbomer 0.05-0.1 parts, parahydroxyacet-ophenone 0.5-1.0 parts, 1,2- hexylene glycol 0.5-1.0 parts, three ethanol
Amine 0.05-1.0 parts, asiaticosid 0.2-0.3 parts, carnosine 0.03-0.05 parts, biological carbohydrate gum -13.0-5.0 parts, the poly- methyl of glycerine
Acrylate/propane diols/Gantrez AN-119 3.0-4.0 parts, deionized water are to 103 parts.
Compared with prior art, it is the device have the advantages that as follows:(1) present invention is using compounding wall material and chitosan
The method of reinforcing, using sodium alginate and CMC as wall material, prepare the butanediol of chitosan reinforcing, water, male
Red root extract, coreopsis tinctoria extract-ALG/NOCC microballoons.(2) sodium alginate and N are used, O-CMC is as compound
During wall material, half interpenetrating network structure (semi-IPN) can be formed, being interspersed in the intrapore CMC of microballoon can be with
Reduce the leakage of butanediol, water, peony root extractive, coreopsis tinctoria extract;Sodium alginate and N, O- carboxylic first are further reinforced simultaneously
The butanediol of base enclosure glycan preparation, water, peony root extractive, coreopsis tinctoria extract, further improve butanediol, water, tree peony root and carry
Thing, the envelop rate of coreopsis tinctoria extract are taken, while makes its more resistance to external environment.(3) eye mask of the present invention be mainly butanediol, water,
Peony root extractive, coreopsis tinctoria extract microballoon play active function.By improving superoxide dismutase activity, remove freely
Base, suppress the generation of lipid peroxide, and then the effect of anti-aging, so as to recover the elasticity of skin, compact skin, also
Phenomena such as eye emollient can be kept, eye accelerated ageing is avoided, cause crow's feet, microgroove, occurs.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated:
The eye mask embodiment 1~5 of the present invention is formulated, and is shown in Table 1.
Table 1
Above-mentioned liposome include butanediol, water, peony root extractive, the component of coreopsis tinctoria extract, and butanediol, water,
Peony root extractive, the mass ratio of coreopsis tinctoria extract are (3-7):(4-5):(1-3):(1-3).
1st, the preparation method of microballoon is as follows:
By sodium alginate and N, O-CMC is made into 20ml mixed solutions;Butanediol, water, tree peony are weighed in proportion
Root extract, coreopsis tinctoria extract and nano-calcium carbonate calcium powder are added in above-mentioned sodium alginate soln, stirring, ultrasound, are made insoluble
Calcium carbonate uniformly suspend in the solution;The atoleine for measuring certain volume again is placed in three-necked flask, is added thereto
Span80, stir, control rotating speed, add above-mentioned preparation thereto contains peony root extractive, coreopsis tinctoria extract and nanometer
The sodium alginate soln of calcium carbonate, stirring form W/O reversed-phase emulsions;Then 20mL is slowly added dropwise with micro-injection pump and contains glacial acetic acid
Atoleine solution, discharge calcium carbonate in calcium ion carry out cross-linking reaction, stood after stirring;Washed, separated with n-hexane
Go out butanediol, water, peony root extractive, coreopsis tinctoria extract-ALG/NOCC microballoons;Add to 100mL 1% (w/v) chitosan
In solution, after magnetic agitation 40min, the chitosan for not participating in reaction is washed with deionized water, centrifuges, freeze-drying, obtains shell and gathers
Butanediol, water, peony root extractive, the coreopsis tinctoria extract-ALG/NOCC microballoons of sugar reinforcing.
2nd, N, the preparation method of O-CMC (NOCC) are as follows:
Weigh 10g chitosans to be added in 500mL three-necked flask, then add 120mL isopropanols, stirring, heating makes
It is swelled;Treat that temperature reaches 50 DEG C or so, add 40mL40% sodium hydroxide solution, stir 30min;Then monoxone is added
Aqueous isopropanol, isothermal reaction 3h;Property adds 60mL 40% sodium hydroxide solution again, stops stirring after reacting 1h;
Products therefrom is filtered, filter residue deionized water dissolving;With the pH of hydrochloric acid conditioning solution, a large amount of floccules can be constantly separated out, are taken out
Filter;With washes of absolute alcohol, product is dried in vacuo to obtain.
3rd, the preparation method of peony root extractive is as follows:
Tree peony root is weighed, cleaning, drying, is ground into 40 mesh, according to solid-liquid ratio 1:10 (g/ml) add 85% ethanol, extraction
5h, filtering, filter residue repeat extraction 2 times, each 2h, merging filtrate, ethanol are recovered under reduced pressure, obtain peony root extractive.
4th, the preparation method of coreopsis tinctoria extract is as follows:
Snow chrysanthemum is weighed, cleaning, drying, is ground into 15 mesh;According to solid-liquid ratio 1:15 (g/ml) add the second of volume fraction 60%
Alcohol, in ultrasonic power 350W, 60 DEG C of condition ultrasonic extraction 2h, filtering, filter residue repeats extraction 2 times, each 1h, merges filter
Liquid, dry, obtain coreopsis tinctoria extract.
Comparative example 1:
Difference with embodiment 3 is only the microballoon without butanediol and water, the addition of remaining each group material, is prepared with technique not
Change.
Comparative example 2:
Difference with embodiment 3 is only the microballoon without peony root extractive, the addition of remaining each group material, preparation and technique
Do not change.
Comparative example 3:
Difference with embodiment 3 is only the microballoon without coreopsis tinctoria extract, the addition of remaining each group material, is prepared with technique not
Change.
Comparative example 4:
Microballoon is not added in difference with embodiment 3 only, and remaining each material addition, conditions and technology of preparation does not change
Become.
Flexibility test
Tested crowd:The voluntary tester of selection 120 20-35 year, man 60, female 60, are divided into 10 groups.
Instrument:German CK companies skin elasticity tester MPA580
Method:Constant negative pressure pattern is selected, everyone tests one group of data, removes two maximums and two in each group
After minimum value, residue 10 is taken to be worth for each person.30min is tested after periocualr skin cleaning, and subject adheres to making daily sooner or later
It is skip test when test is not used respectively, elastic using periocualr skin after 2 weeks, 4 weeks, in test process with above-mentioned trial target
Constant negative pressure is 450mbar.Flexibility test explanation:Skin springback capacity when Ua- is without negative pressure;Skin maximum tension when Uf- has negative pressure
Amount;After Ue- constant negative pressures are added on skin, positioning elastic amount of tension;Uv:Uf-Ue is the visco-elastic portions of skin, or is modeling
Property part amount of tension;Ur:After cancelling negative pressure, skin will restore to the original state rapidly state, the elastic part tension values of recovery process;R2
Definition:R2=Ua/Uf, ratio illustrate that skin elasticity is better closer to 1;R5 definition:R5=Ur/Ue, skin recovery process
Middle elastic part with plus negative pressure process and the ratio between elastic part, ratio illustrates that skin elasticity is better closer to 1;R6 definition:
The ratio between R6=Uv/Ue, the plastic and elastic part of skin, ratio is smaller, illustrates that skin elasticity is better;R7 definition:R7
=Ur/Uf, the ratio between elastic part and maximum tension amount in skin recovery process, ratio illustrate that skin elasticity is better closer to 1;
Index explanation:Wherein R2, R5, R7 are closer to 1, R6 closer to 0, and the elasticity of skin is better, as a result such as table 2 below.
Table 2
As shown in Table 2:Using eye part skin R2, R5, R7 numerical value after embodiment 1-5 eye mask the 2nd week and the 4th week significantly
Increase, its index levels off to 1, R6 reductions after the 4th week, and its exponential approach is in 0 after the 4th week, and uses comparative example 1-4 and control
Eye part skin R2, R5, R7 ascensional range is significantly less than embodiment 1-5 with R6 reductions amplitude after the eye mask of group, and its using effect is equal
Not as embodiment, the elasticity of skin can be increased by illustrating the eye mask of the present invention, mitigate periocualr skin wrinkle problem.
Anti-oxidation efficacy is verified:
Compound concentration is 1 × 10-4Mol/L DPPH ethanol solutions.It will be made in embodiment 1-5 and comparative example 1-4
Eye mask, with 80% ethanol be configured to concentration be respectively 0.02,0.06,0.10,0.14,0.18,0.20 testing sample it is molten
Liquid.5mL sample solutions and DPPH solution are taken respectively, and is well mixed, and avoid light place 30min, are returned to zero with 80% ethanol,
Absorbance A i is determined at 517BITI;Same method, take 5mL80% alcohol solvents to be mutually mixed uniformly with sample solution respectively, keep away
Light determines absorbance A j after placing 30min;5mL80% alcohol solvents add 5mLDPPH solution to mix, avoid light place 30min, survey
Determine absorbance A c.Finally free radical scavenging activity is calculated according to below equation:IP%=[1 one (Ai-Aj)/Ac] × 100, in formula
Ai is sample and the absorption values after DPPH effects;Aj is contribution of the sample itself to absorbance;Ac is DPPH itself
Absorption.
The ability measurement result that DPPH is removed in spraying to embodiment 1-5 and comparative example 1-4 see the table below 3.
Table 3
As shown in Table 3, it is removed DPPH ability and increased with the increase of each extraction moiety concentrations.Data above shows
Eye mask antioxidation activity made from embodiment 1-5 is apparently higher than comparative example 1-4, it is seen that in eye mask of the present invention, forms each of microballoon
Composition acts synergistically, and can effectively remove free radical, serve significant antioxidation.
Above example is merely to illustrate embodiment of the present invention, does not have any formal limit to the present invention
System;It is any to be engaged in professional and technical personnel, all have the ability using the technology contents having revealed that, some are made to it and changes or repaiies
Decorations, turn into the equivalent embodiment of equivalent variations.According to the technology of the present invention essence, simply modification, equivalent variations are carried out to the present invention
With modification, belong in the range of technical solution of the present invention.
Claims (9)
1. a kind of crease-resistant eye mask that compacts, it is characterised in that described eye mask contains the butanediol, water, tree peony root of chitosan reinforcing
Extract, coreopsis tinctoria extract-ALG/NOCC microballoons.
2. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that the parts by weight of described microballoon are 0.3-
0.5 part.
3. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that described butanediol, water, tree peony root carry
The mass ratio for taking thing, coreopsis tinctoria extract is:(3-7):(4-5):(1-3):(1-3).
4. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that described water is micromolecular water.
5. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that the preparation method of described microballoon is such as
Under:By sodium alginate and N, O-CMC is made into 20ml mixed solutions;Butanediol, water, tree peony root is weighed in proportion to carry
Take thing, coreopsis tinctoria extract and nano-calcium carbonate calcium powder to add in above-mentioned sodium alginate soln, stir, ultrasound, make insoluble carbon
Sour calcium uniformly suspends in the solution;The atoleine for measuring certain volume again is placed in three-necked flask, adds span thereto
80, stir, control rotating speed, add above-mentioned preparation thereto contains peony root extractive, coreopsis tinctoria extract and nano-calcium carbonate
The sodium alginate soln of calcium, stirring form W/O reversed-phase emulsions;Then liquid of the 20mL containing glacial acetic acid is slowly added dropwise with micro-injection pump
Body paraffin solution, the calcium ion discharged in calcium carbonate carry out cross-linking reaction, stood after stirring;Washed with n-hexane, isolate fourth
Glycol, water, peony root extractive, coreopsis tinctoria extract-ALG/NOCC microballoons;Add to 100mL 1% (w/v) chitosan solution
In, after magnetic agitation 40min, the chitosan for not participating in reaction is washed with deionized water, centrifuges, freeze-drying, obtains chitosan and adds
Solid butanediol, water, peony root extractive, coreopsis tinctoria extract-ALG/NOCC microballoons.
6. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that described CMC
(NOCC) preparation method is as follows:Weigh 10g chitosans to be added in 500mL three-necked flask, then add 120mL isopropyls
Alcohol, stirring, heating make its swelling;Treat that temperature reaches 50 DEG C or so, add 40mL40% sodium hydroxide solution, stir 30min;
Then chloroacetic aqueous isopropanol, isothermal reaction 3h are added;Property adds 60mL 40% sodium hydroxide solution, reaction again
Stop stirring after 1h;Products therefrom is filtered, filter residue deionized water dissolving;With the pH of hydrochloric acid conditioning solution, can constantly separate out
A large amount of floccules, filter;With washes of absolute alcohol, product is dried in vacuo to obtain.
7. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that the preparation of described peony root extractive
Method is as follows:Tree peony root is weighed, cleaning, drying, is ground into 40 mesh, according to solid-liquid ratio 1:10 (g/ml) add 85% ethanol, carry
5h is taken, is filtered, filter residue repeats extraction 2 times, each 2h, merging filtrate, ethanol is recovered under reduced pressure, obtains peony root extractive.
8. the crease-resistant eye mask that compacts of one kind according to claim 1, it is characterised in that the preparation side of described coreopsis tinctoria extract
Method is as follows:Snow chrysanthemum is weighed, cleaning, drying, is ground into 15 mesh;According to solid-liquid ratio 1:15 (g/ml) add the second of volume fraction 60%
Alcohol, in ultrasonic power 350W, 60 DEG C of condition ultrasonic extraction 2h, filtering, filter residue repeats extraction 2 times, each 1h, merges filter
Liquid, dry, obtain coreopsis tinctoria extract.
9. a kind of crease-resistant eye mask that compacts according to claim any one of 1-8, it is characterised in that described eye mask also includes
The component of following parts by weight:Sodium Hyaluronate 0.03-0.05 parts, glycerine 3.0-5.0 parts, butanediol 5.0-8.0 parts, poly- second two
It is alcohol -14M 0.01-0.03 parts, allantoin 0.1-0.3 parts, hydroxyethyl cellulose 0.2-0.3 parts, carbomer 0.05-0.1 parts, right
Hydroxy acetophenone 0.5-1.0 parts, 1,2- hexylene glycol 0.5-1.0 parts, triethanolamine 0.05-1.0 parts, asiaticosid 0.2-0.3 parts,
Carnosine 0.03-0.05 parts, biological carbohydrate gum -13.0-5.0 parts, glycerine polymethacrylates/propane diols/Gantrez AN-119
3.0-4.0 parts, deionized water are to 103 parts.
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CN108379163A (en) * | 2018-04-26 | 2018-08-10 | 王玉玉 | A kind of ocular region massaging cream and its application method |
WO2022105301A1 (en) * | 2020-11-19 | 2022-05-27 | 广东海洋大学 | Asiaticoside-chitosan-sodium-alginate microsphere, and preparation method therefor and use thereof |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108338950A (en) * | 2018-03-27 | 2018-07-31 | 上海清轩生物科技有限公司 | With stablizing the anti-apolexis composition and application thereof for being adhered effect between epidermis and corium |
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CN108379163A (en) * | 2018-04-26 | 2018-08-10 | 王玉玉 | A kind of ocular region massaging cream and its application method |
WO2022105301A1 (en) * | 2020-11-19 | 2022-05-27 | 广东海洋大学 | Asiaticoside-chitosan-sodium-alginate microsphere, and preparation method therefor and use thereof |
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