CN108635273A - A kind of sun-proof sun screen of wrinkle resistance, whitening and preparation method thereof - Google Patents
A kind of sun-proof sun screen of wrinkle resistance, whitening and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Abstract
The sun-proof sun screen of wrinkle resistance, whitening of the present invention, is prepared from the following raw materials in parts by weight：150~180 parts of water,1.2~1.5 parts of N HOSu NHSs,1.2~1.5 parts of Magnesium ascorbate,3.2~3.6 parts of hexylene glycol,2.2~2.5 parts of valine,2.7~3 parts of alginic acid sodium sulfovinate,Two 2.5~2.8 parts of laruyl alcohol citrates,2.6~3 parts of eucommia ulmoides seed oil,2.6~3 parts of papaya seed oil,3~3.6 parts of rice bran oil,2.3~2.6 parts of beta glucan,2.2~2.5 parts of lauroyl methylaminopropionic sodium,2.5~2.8 parts of the smooth palmitate of sorb,2~2.4 parts from pleat umbrella extract of beautiful gill fungus,1~1.2 part of L lactic acid,6~7.2 parts of hydroxypropyl beta cyclodextrin,3~3.6 parts of Chinese pear-leaved crabapple bark extract,5~6 parts of beta-cyclodextrin,3.2~3.8 parts of methyl sesquistearate.The sun-proof sun screen of wrinkle resistance, whitening of the present invention has whitening and moistening effect, and prominent crease-resistant and sun-proof function.
Description
Technical field
The invention belongs to technical field of cosmetic preparation, and in particular to a kind of sun-proof sun screen of wrinkle resistance, whitening and its preparation side
Method.
Background technology
Sun-proof wrinkle resistance, whitening ingredient has very much, and phenyl benzimidazole sulfonic acid is a kind of ultraviolet (UV) B sun-screening agents, can also be absorbed
The UVA wave bands of very little part, belong to water-soluble chemical sun-screening agent, the disadvantage is that free radical is will produce under being exposed to sunlight, to damage
Hinder skin DNA, there is carcinogenic possibility when serious.4- Methylbenzylidene subunit camphors are the sun-screening agents of significant defense ultraviolet (UV) B, are belonged to
In chemical sun.Dimethicodiethylbenzalmalonate is a kind of chemical sun, colourless or light yellow liquid.Octyl salicylate be it is a kind of compared with
Weak ultraviolet (UV) B sun-screening agents, belong to chemical sun, can absorb 280~320 wave bands of UVB.Ethylaminobenzoate
It is a kind of chemical sun, European Union allows to use, but research shows that reaches being irritating to the skin property when intermediate concentration.Low molecular weight
Sodium hyaluronate, human skin cell can be penetrated into, skin deep layer and constantly repair, promote the regeneration of collagen, allow flesh
Skin elastic force is promoted, and compact face contour.Plant carnitine is extracted from fennel, is a kind of peace similar to creotoxin in effect
Complete effective product can effectively be made in three target areas (glabella line, crow's foot, muffle pomegranate wrinkle wrinkle) of wrinkle of expressing one's feelings
With to substantially reduce wrinkleization surface.Centella can substantially reduce the generation of metalloproteinases, inhibit free radical activity, together
When be effectively synthesized support fiber, rebuild collagenous fiber bundle structure, enable skin profile keep perfection compact.
Invention content
The object of the present invention is to provide one kind having whitening and moistening effect, and prominent crease-resistant and sun-proof function crease-resistant
UV shield protective day cream and preparation method thereof.
The sun-proof sun screen of wrinkle resistance, whitening of the present invention, is prepared from the following raw materials in parts by weight：150~180 parts of water, N- hydroxyls
1.2~1.5 parts of succinimide, 1.2~1.5 parts of Magnesium ascorbate, 3.2~3.6 parts of hexylene glycol, 2.2~2.5 parts of valine,
2.7~3 parts of alginic acid sodium sulfovinate, 2.5~2.8 parts of two laruyl alcohol citrate, 2.6~3 parts of eucommia ulmoides seed oil, papaya seed oil
2.6~3 parts, 3~3.6 parts of rice bran oil, 2.3~2.6 parts of beta glucan, 2.2~2.5 parts of lauroyl methylaminopropionic sodium,
2.5~2.8 parts of the smooth palmitate of sorb, beautiful 2~2.4 parts from pleat umbrella extract of gill fungus, 1~1.2 part of Pfansteihl, hydroxy propyl-Beta-ring
6~7.2 parts of dextrin, 3~3.6 parts of Chinese pear-leaved crabapple bark extract, 5~6 parts of cycloheptaamylose, methyl sesquistearate 3.2~
3.8 part.
As an optimization, the sun-proof sun screen of the wrinkle resistance, whitening, is prepared from the following raw materials in parts by weight：165 parts of water, N- hydroxyls
1.4 parts of succinimide, 1.3 parts of Magnesium ascorbate, 3.5 parts of hexylene glycol, 2.3 parts of valine, 2.8 parts of alginic acid sodium sulfovinate, two
2.6 parts of laruyl alcohol citrate, 2.7 parts of eucommia ulmoides seed oil, 2.9 parts of papaya seed oil, 3.5 parts of rice bran oil, 2.5 parts of beta glucan,
2.7 parts of the smooth palmitate of 2.4 parts of lauroyl methylaminopropionic sodium, sorb, beautiful 2.2 parts from pleat umbrella extract of gill fungus, Pfansteihl 1
Part, 6.6 parts of hydroxypropyl-β-cyclodextrin, 3.5 parts of Chinese pear-leaved crabapple bark extract, 5.6 parts of cycloheptaamylose, methyl sesquialter stearic acid
3.6 parts of ester.
The method for preparing the sun-proof sun screen of wrinkle resistance, whitening of the present invention, includes the following steps：
A, by the water of the parts by weight 2/3rds, n-hydroxysuccinimide, Magnesium ascorbate, hexylene glycol, valine, algae
Sour sodium sulfovinate, two laruyl alcohol citrates, are added in blender, under the conditions of 52 DEG C~58 DEG C, with 1500 revs/min
Rotating speed stirs 20~30 minutes；
B, by water, eucommia ulmoides seed oil, papaya seed oil, rice bran oil, beta glucan, the lauroyl of the parts by weight one third
The smooth palmitate of methylaminopropionic sodium, sorb, is added in blender, under the conditions of 85 DEG C~90 DEG C, with 900 revs/min
Rotating speed stir 20~30 minutes；
C, the hydroxypropyl-β-cyclodextrin of the parts by weight is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor
A；By the beautiful gill fungus of the parts by weight from pleat umbrella extract, it is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquor
B；Then mixed liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；It cools to
25 DEG C~30 DEG C, the Pfansteihl of the parts by weight is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, the cycloheptaamylose of the parts by weight is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；It will
The Chinese pear-leaved crabapple bark extract of the parts by weight is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then will
Mixed liquor D is slowly added into mixed liquor C, under the conditions of 65 DEG C~70 DEG C, is stirred 120~150 minutes；Cooling, filtering, freezing
It is dry；
E, the mixture in the mixture and step d in step c is slowly added into the mixture in step b, with 800 turns/
The rotating speed of minute stirs 20~30 minutes；Then the methyl sesquistearate of the parts by weight is added, with 1000 turns/
The rotating speed of minute stirs 10~15 minutes；
F, it by the mixture in step e, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
The sun-proof sun screen of wrinkle resistance, whitening of the present invention contains n-hydroxysuccinimide, the whitening spot-removings group such as Magnesium ascorbate
Divide and beta glucan, the moisturizing component of valine composition have good skin whitening, moisturizing effect；It is coated using cycloheptaamylose
Chinese pear-leaved crabapple bark extract has effects that anti-aging outstanding is crease-resistant；Eucommia ulmoides seed oil, papaya seed oil, rice bran oil mixing can mildly be gone
Except body old useless cutin, the soft and moist degree of skin is helped to improve, has the function of conditioning.Especially by Pfansteihl, hydroxy propyl-Beta-
Cyclodextrin and beautiful gill fungus form sun-proof reparation component after being included from pleat umbrella extract, have unexpected prominent sun-proof result.Through
72 h of placement at 40 DEG C are crossed, product appearance is observed：No precipitation, separation, discoloration, infiltration or particle send out phenomenon thick, and appearance is fine and smooth, light
Damp degree is good.
Specific implementation mode
The embodiments given below are intended to further illustrate the invention, but is not to be construed as to the scope of the present invention
Limitation, some the nonessential modifications and adaptations of those skilled in the art according to the content of present invention to the present invention still fall within this
The protection domain of invention.
In instant component, eucommia ulmoides seed oil, papaya seed oil, rice bran oil mixing can mildly remove body old useless cutin, have
The soft and moist degree for helping improve skin, has the function of conditioning.N-hydroxysuccinimide CAS:6066-82-6 is as whitening spot-removing
Agent, can be to activate chloasma.Magnesium ascorbate CAS:15431-40-0 is a kind of ascorbic derivative, and there is whitening to make
With.Beta glucan CAS:160872-27-5 is natural plant glycan, is used as skin conditioning agent and moisturizer.Hexylene glycol
CAS:107-41-5 is a kind of dihydric alcohol, belongs to the solvent quickly to volatilize, completely soluble.Antiseptic is can simultaneously serve as, is had
There is the effect of antibacterial.Valine CAS:72-18-4 has effects that moisturizing.There is promoting blood circulation simultaneously and accelerate wound healing.Beautiful gill fungus
From pleat umbrella（Lyophyllum shimeji (Kawam.) Hongo）Extract is ethanol extract, can be, but not limited to use
Following methods obtain：By beautiful gill fungus from pleat umbrella crushed after being dried, absolute ethyl alcohol is added, by solid-liquid ratio 1:35, it is extracted at 80-85 DEG C
It after 50min, filters, concentration；Again through low temperature drying to get.By Pfansteihl, hydroxypropyl-β-cyclodextrin and beautiful gill fungus are extracted from pleat umbrella
Sun-proof reparation component is formed after object inclusion.Chinese pear-leaved crabapple（Malus asiatica）Bark extract, be ethanol extract, can with but it is unlimited
It is obtained in using following steps：It is crushed after taking Chinese pear-leaved crabapple skin to dry, according to 1：95% ethyl alcohol, heating stirring, 80- is added in 20 solid-liquid ratios
85 DEG C of extraction 2h, centrifugal filtration obtain extracting solution, concentrate, be freeze-dried to obtain the final product.Cycloheptaamylose coats Chinese pear-leaved crabapple bark extract,
As the crease-resistant component of anti-aging.Methyl sesquistearate CAS:68936-95-8 makees emollients, emulsifier, skin condition
Agent and moisturizer use.Two laruyl alcohol citrate CAS:25637-88-1 is emollients, skin conditioning agent.Alginic acid sulfuric ester
Sodium CAS:9010-06-4 is as thickener, emulsifier, sustained release agent, dispersant.Lauroyl methylaminopropionic sodium CAS:
21539-58-2 is a kind of surfactant of amino acids, has the function of good cleaning, foaming.The smooth palmitate of sorb
CAS:5050-91-9 makees emulsifier, surfactant, adhesive and uses.
Embodiment 1：The sun-proof sun screen of wrinkle resistance, whitening, is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 6.6 kilograms of hydroxypropyl-β-cyclodextrin is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor A；It will be beautiful
2.2 kilograms from pleat umbrella extract of gill fungus, is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquid B；It then will mixing
Liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；25 DEG C~30 DEG C are cooled to,
1 kilogram of Pfansteihl is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, 5.6 kilograms of cycloheptaamylose is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；Chinese pear-leaved crabapple skin is carried
3.5 kilograms of object is taken, is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then mixed liquor D is slowly added to
Into mixed liquor C, under the conditions of 65 DEG C~70 DEG C, stir 120~150 minutes；Cooling, filtering, freeze-drying；
E, the mixture in the mixture and step d in step c is slowly added into the mixture in step b, with 800 turns/
The rotating speed of minute stirs 20~30 minutes；Then 3.6 kilograms of methyl sesquistearate is added, with 1000 revs/min
Rotating speed stirs 10~15 minutes；
F, it by the mixture in step e, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Embodiment 2：The sun-proof sun screen of wrinkle resistance, whitening, is made up of following steps：
A, by water double centner, 1.2 kilograms of n-hydroxysuccinimide, 1.2 kilograms of Magnesium ascorbate, 3.2 kilograms of hexylene glycol, figured silk fabrics
2.2 kilograms of propylhomoserin, 2.7 kilograms of alginic acid sodium sulfovinate, 2.5 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 50 kilograms of water, 2.6 kilograms of eucommia ulmoides seed oil, 2.6 kilograms of papaya seed oil, 3 kilograms of rice bran oil, beta glucan 2.3 thousand
Gram, 2.2 kilograms of lauroyl methylaminopropionic sodium, 2.5 kilograms of the smooth palmitate of sorb, be added in blender, at 85 DEG C
Under the conditions of~90 DEG C, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 6 kilograms of hydroxypropyl-β-cyclodextrin is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor A；By beautiful gill fungus
It 2 kilograms from pleat umbrella extract, is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquid B；Then mixed liquid B is delayed
Slowly it is added in mixed liquor A, under the conditions of 73 DEG C~78 DEG C, stirs 120~150 minutes；25 DEG C~30 DEG C are cooled to, L- is added
1 kilogram of lactic acid stirs 20~30 minutes；Filtering, freeze-drying；
D, 5 kilograms of cycloheptaamylose is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；Chinese pear-leaved crabapple skin is extracted
3 kilograms of object is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then mixed liquor D is slowly added into mixed
It closes in liquid C, under the conditions of 65 DEG C~70 DEG C, stirs 120~150 minutes；Cooling, filtering, freeze-drying；
E, the mixture in the mixture and step d in step c is slowly added into the mixture in step b, with 800 turns/
The rotating speed of minute stirs 20~30 minutes；Then 3.2 kilograms of methyl sesquistearate is added, with 1000 revs/min
Rotating speed stirs 10~15 minutes；
F, it by the mixture in step e, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Embodiment 3：The sun-proof sun screen of wrinkle resistance, whitening, is made up of following steps：
A, by 120 kilograms of water, 1.5 kilograms of n-hydroxysuccinimide, 1.5 kilograms of Magnesium ascorbate, 3.6 kilograms of hexylene glycol, figured silk fabrics
2.5 kilograms of propylhomoserin, 3 kilograms of alginic acid sodium sulfovinate, 2.8 kilograms of two laruyl alcohol citrate, are added in blender, 52 DEG C~
Under the conditions of 58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 60 kilograms of water, 3 kilograms of eucommia ulmoides seed oil, 3 kilograms of papaya seed oil, 3.6 kilograms of rice bran oil, 2.6 kilograms of beta glucan,
2.8 kilograms of the smooth palmitate of 2.5 kilograms of lauroyl methylaminopropionic sodium, sorb, is added in blender, 85 DEG C~90
Under the conditions of DEG C, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 7.2 kilograms of hydroxypropyl-β-cyclodextrin is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor A；It will be beautiful
2.4 kilograms from pleat umbrella extract of gill fungus, is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquid B；It then will mixing
Liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；25 DEG C~30 DEG C are cooled to,
1.2 kilograms of Pfansteihl is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, 6 kilograms of cycloheptaamylose is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；Chinese pear-leaved crabapple skin is extracted
3.6 kilograms of object is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then mixed liquor D is slowly added into
In mixed liquor C, under the conditions of 65 DEG C~70 DEG C, stir 120~150 minutes；Cooling, filtering, freeze-drying；
E, the mixture in the mixture and step d in step c is slowly added into the mixture in step b, with 800 turns/
The rotating speed of minute stirs 20~30 minutes；Then 3.8 kilograms of methyl sesquistearate is added, with 1000 revs/min
Rotating speed stirs 10~15 minutes；
F, it by the mixture in step e, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Comparative example 1：Skin whitener is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 6.6 kilograms of hydroxypropyl-β-cyclodextrin is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor A；It will be beautiful
2.2 kilograms from pleat umbrella extract of gill fungus, is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquid B；It then will mixing
Liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；25 DEG C~30 DEG C are cooled to,
1 kilogram of Pfansteihl is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, the mixture in step c is slowly added into the mixture in step b, with 800 revs/min of rotating speed stirring 20~
30 minutes；Then 3.6 kilograms of methyl sesquistearate, 5.6 kilograms of cycloheptaamylose, Chinese pear-leaved crabapple bark extract 3.5 is added
Kilogram, it is stirred 10~15 minutes with 1000 revs/min of rotating speed；
E, it by the mixture in step d, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Comparative example 2：Skin whitener is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 6.6 kilograms of hydroxypropyl-β-cyclodextrin is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor A；It will be beautiful
2.2 kilograms from pleat umbrella extract of gill fungus, is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquid B；It then will mixing
Liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；25 DEG C~30 DEG C are cooled to,
1 kilogram of Pfansteihl is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, the mixture in step c is slowly added into the mixture in step b, with 800 revs/min of rotating speed stirring 20~
30 minutes；Then 3.6 kilograms of methyl sesquistearate, 5.6 kilograms of cycloheptaamylose is added, with 1000 revs/min
Rotating speed stirs 10~15 minutes；
E, it by the mixture in step d, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Comparative example 3：Skin whitener is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 6.6 kilograms of hydroxypropyl-β-cyclodextrin is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor A；It will be beautiful
2.2 kilograms from pleat umbrella extract of gill fungus, is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquid B；It then will mixing
Liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；25 DEG C~30 DEG C are cooled to,
1 kilogram of Pfansteihl is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, the mixture in step c is slowly added into the mixture in step b, with 800 revs/min of rotating speed stirring 20~
30 minutes；Then 3.6 kilograms of methyl sesquistearate, 3.5 kilograms of Chinese pear-leaved crabapple bark extract is added, with 1000 revs/min
Rotating speed stir 10~15 minutes；
E, it by the mixture in step d, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Crease-resistant test：Use human skin fast optical imaging system Primospico(GFM companies, Germany) is to eye
Microgroove is analyzed, and includes mainly three parameters：Ra is (in the arithmetic average of whole testing length range inner outline upward peaks
Value)；Rq (in the square root of the average value of whole testing length range inner outline upward peaks square)；Rz is (in all test length
Spend the peak-peak on range inner outline).The smaller skin that represents of three parameters is better, and wrinkle is fewer.168 aspirations are chosen altogether
Person is divided into 4 groups in the identical environment of humidity, every group of 42 people, is respectively adopted embodiment 1, product in comparative example 1,2,3.Daily
Twice with 1.75 μ l/cm2 coating even densities coatings, using preceding test initial value, test result after one month is shown in Table 1, passes through
The 1 visible embodiment of the present invention of table, 1 anti-wrinkle effect, hence it is evident that be better than comparative example 1,2,3.
Comparative example 4：Skin whitener is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 5.6 kilograms of cycloheptaamylose is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；Chinese pear-leaved crabapple skin is carried
3.5 kilograms of object is taken, is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then mixed liquor D is slowly added to
Into mixed liquor C, under the conditions of 65 DEG C~70 DEG C, stir 120~150 minutes；Cooling, filtering, freeze-drying；
D, the mixture in step c is slowly added into the mixture in step b, with 800 revs/min of rotating speed stirring 20~
30 minutes；Then 3.6 kilograms of methyl sesquistearate, 6.6 kilograms of hydroxypropyl-β-cyclodextrin, beautiful gill fungus is added from pleat umbrella
2.2 kilograms of extract, 1 kilogram of Pfansteihl are stirred 10~15 minutes with 1000 revs/min of rotating speed；
E, it by the mixture in step d, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Comparative example 5：Skin whitener is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 5.6 kilograms of cycloheptaamylose is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；Chinese pear-leaved crabapple skin is carried
3.5 kilograms of object is taken, is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then mixed liquor D is slowly added to
Into mixed liquor C, under the conditions of 65 DEG C~70 DEG C, stir 120~150 minutes；Cooling, filtering, freeze-drying；
D, the mixture in step c is slowly added into the mixture in step b, with 800 revs/min of rotating speed stirring 20~
30 minutes；Then 3.6 kilograms of methyl sesquistearate, 6.6 kilograms of hydroxypropyl-β-cyclodextrin, Pfansteihl 1,000 is added
Gram, it is stirred 10~15 minutes with 1000 revs/min of rotating speed；
E, it by the mixture in step d, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Comparative example 6：Skin whitener is made up of following steps：
A, by 110 kilograms of water, 1.4 kilograms of n-hydroxysuccinimide, 1.3 kilograms of Magnesium ascorbate, 3.5 kilograms of hexylene glycol, figured silk fabrics
2.3 kilograms of propylhomoserin, 2.8 kilograms of alginic acid sodium sulfovinate, 2.6 kilograms of two laruyl alcohol citrate, are added in blender, at 52 DEG C
Under the conditions of~58 DEG C, stirred 20~30 minutes with 1500 revs/min of rotating speed；
B, by 55 kilograms of water, 2.7 kilograms of eucommia ulmoides seed oil, 2.9 kilograms of papaya seed oil, 3.5 kilograms of rice bran oil, beta glucan 2.5
Kilogram, 2.4 kilograms of lauroyl methylaminopropionic sodium, 2.7 kilograms of the smooth palmitate of sorb, be added in blender, 85
DEG C~90 DEG C under the conditions of, stirred 20~30 minutes with 900 revs/min of rotating speed；
C, 5.6 kilograms of cycloheptaamylose is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；Chinese pear-leaved crabapple skin is carried
3.5 kilograms of object is taken, is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then mixed liquor D is slowly added to
Into mixed liquor C, under the conditions of 65 DEG C~70 DEG C, stir 120~150 minutes；Cooling, filtering, freeze-drying；
D, the mixture in step c is slowly added into the mixture in step b, with 800 revs/min of rotating speed stirring 20~
30 minutes；Then 3.6 kilograms of methyl sesquistearate, beautiful 2.2 kilograms from pleat umbrella extract of gill fungus is added, with 1000 turns/
The rotating speed of minute stirs 10~15 minutes；
E, it by the mixture in step d, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
Sun-proof result is tested:According to the evaluation method of sun care preparations sun-proof result as defined in QB/T 2410-1998 into
Row operation.Each 1 gram of samples of latex in Example 1-3 and comparative example 4-6.Even application is on 3M medical air-permeable adhesive tapes, so
After place and be attached to cuvette transparent surface side after 30 min and carry out data determination.Surveyed on ultraviolet specrophotometer its 280~
The absorbance A value of 320nm wave-length coverages judges the sun-proof result of lotion under ultraviolet light by the size of absorbance A value.It is logical
Crossing 2 visible implementation 1-3 of table has the ultraviolet light effect of high efficient protected, and ultraviolet absorptivity A values are apparently higher than comparative example 4,6, and compare
Example 5 is only the minimum ultraviolet light effect of protection.
Claims (3)
1. a kind of sun-proof sun screen of wrinkle resistance, whitening, it is characterised in that be to be prepared from the following raw materials in parts by weight：Water 150~180
Part, 1.2~1.5 parts of n-hydroxysuccinimide, 1.2~1.5 parts of Magnesium ascorbate, 3.2~3.6 parts of hexylene glycol, valine 2.2
~2.5 parts, 2.7~3 parts of alginic acid sodium sulfovinate, 2.5~2.8 parts of two laruyl alcohol citrate, 2.6~3 part, kind wood of eucommia ulmoides seed oil
2.6~3 parts of melon seeds oil, 3~3.6 parts of rice bran oil, 2.3~2.6 parts of beta glucan, lauroyl methylaminopropionic sodium 2.2~
2.5 parts, 2.5~2.8 parts of the smooth palmitate of sorb, beautiful 2~2.4 parts from pleat umbrella extract of gill fungus, 1~1.2 part of Pfansteihl, hydroxypropyl
6~7.2 parts of group-beta-cyclodextrin, 3~3.6 parts of Chinese pear-leaved crabapple bark extract, 5~6 parts of cycloheptaamylose, methyl sesquialter stearic acid
3.2~3.8 parts of ester.
2. the sun-proof sun screen of wrinkle resistance, whitening according to claim 1, it is characterised in that be by the raw material of following parts by weight
It is made：165 parts of water, 1.4 parts of n-hydroxysuccinimide, 1.3 parts of Magnesium ascorbate, 3.5 parts of hexylene glycol, 2.3 parts of valine, algae
2.8 parts of sour sodium sulfovinate, 2.6 parts of two laruyl alcohol citrate, 2.7 parts of eucommia ulmoides seed oil, 2.9 parts of papaya seed oil, rice bran oil 3.5
Part, 2.5 parts of beta glucan, 2.4 parts of lauroyl methylaminopropionic sodium, 2.7 parts of the smooth palmitate of sorb, beautiful gill fungus carry from pleat umbrella
Take 2.2 parts of object, 1 part of Pfansteihl, 6.6 parts of hydroxypropyl-β-cyclodextrin, 3.5 parts of Chinese pear-leaved crabapple bark extract, 5.6 parts of cycloheptaamylose, first
3.6 parts of base glucose sesquistearate.
3. a kind of method preparing the sun-proof sun screen of wrinkle resistance, whitening described in claims 1 or 2, it is characterised in that including following step
Suddenly：
A, by the water of the parts by weight 2/3rds, n-hydroxysuccinimide, Magnesium ascorbate, hexylene glycol, valine, algae
Sour sodium sulfovinate, two laruyl alcohol citrates, are added in blender, under the conditions of 52 DEG C~58 DEG C, with 1500 revs/min
Rotating speed stirs 20~30 minutes；
B, by water, eucommia ulmoides seed oil, papaya seed oil, rice bran oil, beta glucan, the lauroyl of the parts by weight one third
The smooth palmitate of methylaminopropionic sodium, sorb, is added in blender, under the conditions of 85 DEG C~90 DEG C, with 900 revs/min
Rotating speed stir 20~30 minutes；
C, the hydroxypropyl-β-cyclodextrin of the parts by weight is added in the pure water of 20 times of weight and stirs evenly to obtain mixed liquor
A；By the beautiful gill fungus of the parts by weight from pleat umbrella extract, it is added in the absolute ethyl alcohol of 30 times of weight and stirs evenly to obtain mixed liquor
B；Then mixed liquid B is slowly added into mixed liquor A, under the conditions of 73 DEG C~78 DEG C, is stirred 120~150 minutes；It cools to
25 DEG C~30 DEG C, the Pfansteihl of the parts by weight is added, stirs 20~30 minutes；Filtering, freeze-drying；
D, the cycloheptaamylose of the parts by weight is added in the pure water of 30 times of weight and stirs evenly to obtain mixed liquor C；It will
The Chinese pear-leaved crabapple bark extract of the parts by weight is added in the absolute ethyl alcohol of 20 times of weight and stirs evenly to obtain mixed liquor D；Then will
Mixed liquor D is slowly added into mixed liquor C, under the conditions of 65 DEG C~70 DEG C, is stirred 120~150 minutes；Cooling, filtering, freezing
It is dry；
E, the mixture in the mixture and step d in step c is slowly added into the mixture in step b, with 800 turns/
The rotating speed of minute stirs 20~30 minutes；Then the methyl sesquistearate of the parts by weight is added, with 1000 turns/
The rotating speed of minute stirs 10~15 minutes；
F, it by the mixture in step e, is slowly added into the mixture in step a, 10 is stirred with 1500 revs/min of rotating speed
~15 minutes；Then ultrasonic dispersing machine is used, under the conditions of 75 DEG C~80 DEG C, is handled 120~150 minutes.
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| CN109276471A (en) * | 2018-11-07 | 2019-01-29 | 上海上水和肌化妆品有限公司 | Polypeptide anti-apolexis composition of fluid inclusion techniques and preparation method thereof |
| WO2021220124A1 (en) * | 2020-04-26 | 2021-11-04 | Shyam Sunder Singh | A pharmaceutical composition and method of treatment using l-carnosine and glutathione, its precursors or derivatives thereof |
| WO2022106536A1 (en) * | 2020-11-18 | 2022-05-27 | Lantmännen Oats AB | Anti-microbial skin-care composition comprising beta-glucan and natural oil |
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Effective date of registration: 20190108 Address after: 030000 Shanxi Taiyuan Shanxi comprehensive reform demonstration zone Taiyuan Education Park Industrial Road 38 high tech real estate 608 room Applicant after: Taiyuan Blue Technology Co., Ltd. Address before: 030000 Shanxi Shanxi Taiyuan comprehensive reform demonstration zone, Taiyuan school building, 122 9925-Y, ktong building, No. Applicant before: Taiyuan orchid technology limited liability company |
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