CN103720619B - A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof - Google Patents

A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof Download PDF

Info

Publication number
CN103720619B
CN103720619B CN201310724514.7A CN201310724514A CN103720619B CN 103720619 B CN103720619 B CN 103720619B CN 201310724514 A CN201310724514 A CN 201310724514A CN 103720619 B CN103720619 B CN 103720619B
Authority
CN
China
Prior art keywords
horneri
turn
sargassum
spongocarpus
kutz
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201310724514.7A
Other languages
Chinese (zh)
Other versions
CN103720619A (en
Inventor
蔡春尔
杨亚云
郑钰琦
胡燕
何培民
贾睿
吴维宁
吴海龙
周玲洁
张正阳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanghai Maritime University
Original Assignee
Shanghai Maritime University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shanghai Maritime University filed Critical Shanghai Maritime University
Priority to CN201310724514.7A priority Critical patent/CN103720619B/en
Publication of CN103720619A publication Critical patent/CN103720619A/en
Application granted granted Critical
Publication of CN103720619B publication Critical patent/CN103720619B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

The invention belongs to cosmetic field, in particular to a kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof, Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, oven dry are become fragile to frond, the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of drying is smashed to pieces to graininess, to be dipped in ethanol 8-20 hour, to filter, decocting in water 15-120 minute, filtration obtains algae mud, is ground to Powdered after centrifuge dehydration, lyophilization; Various raw material has been weighed according to formula; Swelling by adding deionized water and stirring in load weighted Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud continuation stirring, add tackifier and deionized water while stirring, stir.The moisture retention of this facial film is good, obviously improves the colour of skin, Glycerin, prevents skin aging, and cost is low, low price.

Description

A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof
Technical field
The invention belongs to cosmetic field, particularly a kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof.
Background technology
Facial film is a kind of cosmetics and skincare product spreading on face, utilize the blink covering face, the air that temporary transient isolation is extraneous and pollution, promote sweat gland secretion and metabolism, the oxygen content of skin is made to increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, improve the elasticity of skin, pliability and brightness.The kind of facial film is a lot, and wherein seaweed mask is with the mineral composition of Sargassum extract, can control oily Peppermint Extract, provide moisture, calm tired, rough skin, makes skin remain fine and smooth, glossy.But the moistening effect of plant seaweed mask of the prior art is not the most desirable, and use inconvenient, the shelf-life is short, expensive.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.), also known as post capsule Alga Sgrgassi Enerves, grass madder, the alizarin dish of bamboo, that one is distributed in Japan, Korea S and north of China marine site, the common temperate zone Alga Sgrgassi Enerves of normal formation seaweed woods, can at the beginning of annual winter Mo, spring amount reproduction, algae plant height can reach 7 meters, single-strain fresh weight more than 3 kilograms, flourishing, swim in the water surface in flakes.Due to Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) fast growth, Biomass is large, has caused the concern of Marine Biologist and Sargassum worker.Spring, north Taiwan seashore often has Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) to come from the drift of marine site, temperate zone, be deposited in bank and bay, 2013 because of ocean temperature lower, more Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) is had successfully to float to Taiwan, comparatively each scenic spot was all initiated movable being picked up by a large amount of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) in clean beach and was destroyed by fire, takes a large amount of energy and material resources for many former years to make Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) amount.In recent years, along with progressively going deep into of studying Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) chemical composition, its medical mechanism is also illustrated gradually, and the step of drug development is constantly accelerated.
Utilize Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) to prepare facial film as raw material, existing document and report in not yet have described in.If people constantly can research and develop effect of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.), utilize its characteristic, be developed to the facial film with the effect such as whitening, moisturizing, turn waste into wealth, make it fully be utilized, while environmental improvement, too increase economic benefit, kill two birds with one stone.
Summary of the invention
The object of this invention is to provide a kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, this facial film can increase skin surface moisture, and moistening effect is excellent, also has effect of whitening, antiinflammatory, reduce wrinkle, and uses simple, low price.
Another object of the present invention is to provide a kind of preparation method of above-mentioned Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film.
Object of the present invention can be achieved through the following technical solutions:
A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, is characterized in that, comprise the raw material of following percentage by weight number meter:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water.
The preparation method of described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder is, by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, oven dry to frond becomes fragile, then smashs to pieces to graininess by the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of drying, is dipped to 8-20 hour, filtration in ethanol; The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain decocting in water 15-120 minute will obtained again, filters and obtains algae mud, is ground to and Powderedly obtains Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder after centrifuge dehydration, lyophilization.
Described wetting agent is the mixture of one or more in glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium.Preferably, described wetting agent is the mixture of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium; The weight ratio of glycerol, amino acid humectant, propylene glycol, butanediol, hyaluronate sodium is 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08.
Described tackifier is one or both the mixture in high molecular cellulose or HANSHENGJIAO.Preferably, described tackifier is the mixture of high molecular cellulose and HANSHENGJIAO, and the weight ratio of high molecular cellulose and HANSHENGJIAO is 3-4:1.
Described metal ion chelation agent is one or both the mixture in L-vitamin C or citric acid, and preferred described metal ion chelation agent is the mixture of L-vitamin C and citric acid, and wherein the weight ratio of L-vitamin C and citric acid is 1-3:1.
Described antiseptic is one or both the mixture in phenoxyethanol or Sang Pu K15.Preferably, described antiseptic is the mixture of phenoxyethanol and Sang Pu K15, and wherein, the volume ratio of phenoxyethanol and Sang Pu K15 is 1-2:1.
Described brightening agent is the mixture of one or more in arbutin, nicotiamide or Trenaxmine.Preferably, described brightening agent is the mixture of arbutin, nicotiamide and Trenaxmine, and wherein, the weight ratio of arbutin, nicotiamide and Trenaxmine is 1:1-3:1.
Described anti-allergic agent is one or both the mixture in water solublity a-bisabolol or glycyrrhizic acid dipotassium.Preferably, described anti-allergic agent is the mixture of water solublity a-bisabolol and glycyrrhizic acid dipotassium, and wherein, the weight ratio of water solublity a-bisabolol and glycyrrhizic acid dipotassium is 2-6:1.
Described nourishing additive agent is the mixture of one or more in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
Described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
The preparation method of above-mentioned Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, its step comprises:
(1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, oven dry to frond becomes fragile, then the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of drying is smashed to pieces to graininess, be dipped to 8-20 hour, filtration in ethanol;
(2), the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain decocting in water 15-120 minute that will obtain in step (1), filter and obtain algae mud, be ground to after centrifuge dehydration, lyophilization and Powderedly obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder; Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.), after alcohol-pickled and decocting in water, more can extract the effective ingredient that can be absorbed by the skin in Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.), improves the moistening effect of facial film.
(3), various raw material has been weighed according to formula;
(4), swelling by adding deionized water and stirring in load weighted Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder; Moisturizing, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud continuation stirring, add tackifier and deionized water while stirring, after stirring, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film.
In described step (1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) dry to the baking temperature become fragile be 55-65 DEG C.
In described step (2), be 40-70 DEG C by the decocting in water temperature of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain decocting in water; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
Compared with prior art, beneficial effect of the present invention is:
1, the moisture retention of described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film is good, and the skin moisture content rate of increase after facial film face of the present invention applies 20 minutes is more than 27%, and can obviously improve the colour of skin, Glycerin, effectively prevent skin aging, reduce wrinkle.
2, the preparation method of described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film is simple, easy to operate, and raw material is easy to get, cost is low, low price, and the medicine added in preparation process does not only injure skin, and environmentally safe, green, environmental protection.
Accompanying drawing explanation
Fig. 1 has applied the skin lines comparison diagram before and after Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film obtained in embodiment 1.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described:
Embodiment 1
(1) preparation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder
The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) gathered is removed assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water is washed till electrical conductivity and drops to below 0.02MS; Dry in the baking oven of 60 DEG C to frond becomes fragile; Fully smash to pieces to algae grain length with medicine bruisher and be shorter than 5mm, add alcohol-pickled spend the night (12 hours) that mass concentration is 75%, algae grain is obtained with 100 order silk cover filterings, algae grain is decocting in water 1h at 70 DEG C, obtain algae mud with 200 mesh sieve thin,tough silk filtering supernatants, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 300 seconds, fully grind after the algae mud vacuum lyophilization of centrifuge dehydration recently, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder.
(2) preparation process of facial film
Get the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 10g in step (1), add the swelling stirring of 30mL deionized water, for subsequent use.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 5g, amino acid humectant 3g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, the each 0.1g of 120-160 ten thousand), red wine polyphenols 1g, L-vitamin C1g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K15 is 0.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 2g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud after swelling stirring is mixed homogeneously with above-mentioned adjuvant, adds the 1.4g high molecular cellulose after Homogeneous phase mixing and 0.4g HANSHENGJIAO while stirring, add to 100g total amount with deionized water, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film.
(3) testing result
For the moistening effect of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film prepared in testing example 1, respectively by green tea powder facial film, Lavender mask in contrast.Wherein the preparation method of green tea powder facial film and Lavender mask is according to the formula preparation in the present embodiment 1, and only the green tea powder of equivalent and lavandula angustifolia powder (all purchased from Chhnang daily use chemicals, Guangdong) are replaced Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder, other raw materials and addition thereof are all constant.
Before test: inside experimenter's arm of cleaning, and with wet gauze (with deionized water) scrub, water temperature is room temperature, carries out measurement markers, within before recipient site 2-3 days, can not use any cosmetic product after cleaning at experimenter's both hands inner forearm; In test: use latex finger cot by test products and reference product uniform application in arm trial zone, smearing thickness is measurement and the observation of carrying out tested region and control zone after 2mm, 20min, each region parallel assay five times according to the order of sequence, draw meansigma methods, shown in table 1 specific as follows:
Table 1 skin moisture content rate of increase
The skin of the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film in the present embodiment 1 has been applied with 2,000,000 pixel CCD50X portable high-definition intelligent skin detection instrument (EH-800U) observation, as shown in Figure 1, wherein Fig. 1 a does not apply the skin observation figure of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, Fig. 1 b is the skin observation figure having applied Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, show from comparative observation figure, the facial film prepared in the present embodiment all can improve the colour of skin, Glycerin, improves the moisture content of epiderm skin.
Embodiment 2
(1) preparation of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder
The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) gathered is removed assorted algae and other non-algae substances, and fresh water washes away salinity and sea mud, and distilled water is washed till electrical conductivity and drops to below 0.02MS; Dry in the baking oven of 60 DEG C to frond becomes fragile; Fully smash to pieces to algae grain length with medicine bruisher and be shorter than 5mm, add alcohol-pickled spend the night (18 hours) that mass concentration is 75%, algae grain is obtained with 100 order silk cover filterings, algae grain decocting in water 45 minutes at 70 DEG C, obtain algae mud with 200 mesh sieve thin,tough silk filtering supernatants, adopt 1000g centrifugal force to remove moisture in algae mud, centrifugation time is 350 seconds, finally fully grind after the algae mud vacuum lyophilization of centrifuge dehydration, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder.
(2) preparation process of facial film
Get the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 15g in step (1), add the swelling stirring of 30mL deionized water, for subsequent use.
Following adjuvant is dissolved in the deionized water of 20mL:
Glycerol 4g, amino acid humectant 4g, propylene glycol 0.5g, butanediol 0.5g, hyaluronate sodium 0.3g(wherein, molecular weight 20-40 ten thousand, 90-120 ten thousand, the each 0.1g of 120-160 ten thousand), red wine polyphenols 2g, L-vitamin C2g, citric acid 2g, phenoxyethanol 0.025g, Sang Pu K150.025g, arbutin 0.5g, nicotiamide 1g, Trenaxmine 0.5g, trehalose 1.5g, vitamin B6 0.5g, glycolic acid 1g, azelaic acid 1g, water solublity a-bisabolol 0.5g, glycyrrhizic acid dipotassium 0.1g, ceramide 0.2g, silk fibroin powder 0.2g, collagen protein powder 0.2g, avenabeta glucosan 0.2g, polymerization almond protein 0.2g, Argireline 0.1g, Margarita hydrolyzed solution 0.2g.
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud after swelling stirring is mixed homogeneously with above-mentioned adjuvant, adds the 1.5g high molecular cellulose after Homogeneous phase mixing and 0.5g HANSHENGJIAO while stirring, add to 100g total amount with deionized water, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film.
(3) testing result
Method of testing is with embodiment 1, and concrete test result is as shown in table 2 below:
Table 2 skin moisture content rate of increase
In sum, the moisture content of skin epidermis can be significantly improved after employing Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, improve the colour of skin, Glycerin.
The above is preferred embodiment of the present invention, but the present invention should not be confined to the content disclosed in this embodiment.The equivalence completed under not departing from spirit disclosed in this invention so every or amendment, all fall into the scope of protection of the invention.

Claims (6)

1. a Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film, is characterized in that, comprises the raw material of following percentage by weight number meter:
Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder 10-20%, wetting agent 6-13%, tackifier 1.5-3%, antioxidant 1-5%, metal ion chelation agent 2-15%, antiseptic 0.05-1%, brightening agent 1.5-5%, deodorizer 1-5%, sebum inhibitor 0.1-1%, keratin-lytic agent 1-5%, antibacterial 1-5%, anti-allergic agent 0.6-2.5%, nourishing additive agent 1.2-8%, surplus are deionized water;
Described wetting agent is glycerol, amino acid humectant, propylene glycol, butanediol and hyaluronate sodium is the mixture of 1:0.5-1:0.05-0.15:0.05-0.15:0.04-0.08 mixing according to weight ratio;
Described tackifier is high molecular cellulose and HANSHENGJIAO is the mixture of 3-4:1 mixing according to weight ratio;
Described anti-allergic agent is water solublity a-bisabolol and glycyrrhizic acid dipotassium is the mixture of 2-6:1 mixing according to weight ratio;
Described metal ion chelation agent is L-vitamin C and citric acid is the mixture of 1-3:1 mixing according to weight ratio;
Described antiseptic is phenoxyethanol and Sang Pu K15 is the mixture of 1-2:1 mixing according to volume ratio;
Described brightening agent is arbutin, nicotiamide and Trenaxmine is the mixture of 1:1-3:1 mixing according to weight ratio;
Described nourishing additive agent is the mixture of one or more in ceramide, silk fibroin powder, collagen protein powder, avenabeta glucosan, polymerization almond protein, Argireline and Margarita hydrolyzed solution.
2. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film according to claim 1, it is characterized in that: the preparation method of described Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder is, by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, oven dry to frond becomes fragile, then the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of drying is smashed to pieces to graininess, be dipped to 8-20 hour, filtration in ethanol; The Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain decocting in water 15-120 minute will obtained again, filters and obtains algae mud, is ground to and Powderedly obtains Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder after centrifuge dehydration, lyophilization.
3. Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film according to claim 1, is characterized in that: described antioxidant is red wine polyphenols; Described deodorizer is trehalose; Described sebum inhibitor is vitamin B6; Described keratin-lytic agent is glycolic acid; Described antibacterial is azelaic acid.
4. a preparation method for Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film according to claim 1, its step comprises:
(1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) remove impurity, washing, oven dry to frond becomes fragile, then the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) of drying is smashed to pieces to graininess, be dipped to 8-20 hour, filtration in ethanol;
(2), the Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain decocting in water 15-120 minute that will obtain in step (1), filter and obtain algae mud, be ground to after centrifuge dehydration, lyophilization and Powderedly obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder;
(3), various raw material has been weighed according to formula;
(4), swelling by adding deionized water and stirring in load weighted Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) powder; Wetting agent, antioxidant, metal ion chelation agent, antiseptic, brightening agent, deodorizer, sebum inhibitor, keratin-lytic agent, antibacterial, anti-allergic agent, nourishing additive agent are dissolved in deionized water, then add and stir swelling good Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) mud continuation stirring, add tackifier and deionized water while stirring, after stirring, obtain Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film.
5. the preparation method of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film according to claim 4, is characterized in that: in described step (1), by Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) dry to the baking temperature become fragile be 55-65 DEG C.
6. the preparation method of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film according to claim 4, it is characterized in that: in described step (2), is 40-70 DEG C by the decocting in water temperature of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) grain decocting in water; The centrifugal force during centrifuge dehydration of algae mud is 1000g, and centrifugation time is 200-400 second.
CN201310724514.7A 2013-12-24 2013-12-24 A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof Active CN103720619B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310724514.7A CN103720619B (en) 2013-12-24 2013-12-24 A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310724514.7A CN103720619B (en) 2013-12-24 2013-12-24 A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof

Publications (2)

Publication Number Publication Date
CN103720619A CN103720619A (en) 2014-04-16
CN103720619B true CN103720619B (en) 2015-12-09

Family

ID=50445086

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310724514.7A Active CN103720619B (en) 2013-12-24 2013-12-24 A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof

Country Status (1)

Country Link
CN (1) CN103720619B (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104586740A (en) * 2015-01-30 2015-05-06 通江县东泰食品有限公司 Moisturizing beauty mask and preparation method thereof
CN105662984B (en) * 2016-04-01 2018-11-13 南京理工大学 A kind of moisturizing emulsion and preparation method thereof
CN105943441A (en) * 2016-06-01 2016-09-21 合肥丰瑞隆生物科技有限公司 Lucid ganoderma paste mask and preparation method thereof
CN105943439A (en) * 2016-06-01 2016-09-21 合肥丰瑞隆生物科技有限公司 Straw mushroom mud mask and preparation method thereof
CN108096129A (en) * 2018-03-05 2018-06-01 湖南科技大学 A kind of preparation method of novel alga clay mask

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
《铜藻在化妆品中的应用研究》;王建新;《天然化妆品的博客》;20131021;http//blog.sina.com.cn/s/blog_573513f30101b07i.html#commomCommen,20131021 *

Also Published As

Publication number Publication date
CN103720619A (en) 2014-04-16

Similar Documents

Publication Publication Date Title
CN103720619B (en) A kind of Sargassum phyllocystum Tseng et Lu,Sargassum horneri (Turn.) C. Ag. (Fucus horneri (Turn.)C.Ag.,Spongocarpus horneri Kutz.) decocting in water algae mud facial film and preparation method thereof
CN103720621B (en) A kind of Entermorpha decocting in water algae mud facial film and preparation method thereof
CN110200875A (en) A kind of antiallergic whitening mask and preparation method thereof
TWI477291B (en) Method for extracting using glacial water and the extract thereof, and cosmetic composition comprising nanoemulsion particles having the extract encapsulated or the glacial water
CN104146925A (en) Facial mask with functions of improving skin barrier and delaying senescence and preparation method thereof
CN103393581A (en) Natural anti-wrinkling anti-aging skin care composition and application thereof in cosmetic
KR102022368B1 (en) Cosmetic compositions for improving wrinkles and skin-lifting and their manufacturing method
CN102688163A (en) Anti-skin aging skin care compound essential oil
CN103976909A (en) Gerbera extracting solution as well as preparation method and application thereof
CN106902030A (en) Skin care compositions and cosmetics with moisturizing, smoothing wrinkle and the elastic effect of recovery
CN103735455B (en) One main laver decocting in water algae mud facial film and preparation method thereof
CN104398435A (en) Mild cutin removing mask and preparation method thereof
CN103361181A (en) Rose compound essential oil for resisting skin aging
CN108888565B (en) Antioxidant toner added with ginseng liposome and preparation method thereof
CN107823001A (en) A kind of moisturizing composition and the skin care item containing said composition
CN103720620B (en) A kind of sargassum horneri alga powder mask and preparation method thereof
CN107753333B (en) A kind of essence that moisturizing is releived dew and preparation method thereof
CN109568553A (en) It is a kind of to eliminate black-eyed Chinese medicine composition and its preparation method and application
CN104257541A (en) Folium artemisiae argyi extract solution as well as preparation method and application of folium artemisiae argyi extract solution
CN103550129B (en) Plant composite polysaccharide, Preparation Method And The Use
CN107648088A (en) A kind of anti-oxidant skin cream and preparation method thereof
KR20080061080A (en) Cosmetic composition comprising tuber melanosporum
CN107174536A (en) A kind of salamander face beautifying skin protection product and preparation method thereof
CN104739715A (en) Facial mask liquid containing flaxseed gum extracting solution and preparation method thereof
CN105125651A (en) Whitening and freckle-lightening composition and preparation method and application method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant