CN110559205A - Facial mask liquid capable of controlling oil and shrinking pores and preparation method thereof - Google Patents
Facial mask liquid capable of controlling oil and shrinking pores and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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Abstract
The invention provides a mask liquid for controlling oil and shrinking pores, which is prepared from the following raw materials in parts by weight: 1-2 parts of glycylglycine, 1-3 parts of nicotinamide, 2-5 parts of okra polysaccharide, 1-3 parts of rhodiola rosea extract, 1-5 parts of camellia extract, 2-4 parts of purslane extract, 0.1-0.5 part of buconazole flavone, 2-5 parts of traditional Chinese medicine antibacterial extract, 0.01-1 part of polyglutamic acid, 0.05-2.5 parts of sodium lactate, 0.05-7.5 parts of sodium pyrrolidone carboxylate, 0.05-5 parts of betaine, 0.1-2 parts of hydroxyethyl urea, 0.01-5 parts of thickening agent, 0.01-0.5 part of EDTA disodium, 2-20 parts of polyhydric alcohol and 50-100 parts of deionized water. The facial mask liquid disclosed by the invention is pure natural in raw material components, does not have irritant chemical addition, and has the effects of improving cell tolerance, protecting cell membranes and enhancing the natural barrier function of skin, so that the effect of protecting the skin is achieved.
Description
Technical Field
the invention relates to the technical field of cosmetics, in particular to facial mask liquid for controlling oil and shrinking pores.
background
the facial mask is an important content in skin care, and is applied regularly according to various skin characteristics, so that oily skin can be degreased, large pores can be converged, withered and wrinkled skin can recover luster, and inflammation of pimpled skin can be inhibited. The facial mask makes skin look fresh, smooth, white and tender after being used, because when the facial mask is applied to the skin, the facial mask generates affinity with the skin, the skin temperature rises along with the gradual drying of the facial mask, the blood circulation is accelerated, the skin is tightened and the tension is strengthened, sebum and moisture secreted by the skin reversely permeate into a horny layer, the epidermis is soft and stretched, pores are naturally opened, effective components in the facial mask permeate into the skin to be absorbed by the skin, meanwhile, the facial mask is tightly connected with the skin, and when the facial mask is removed, aged cutin on the skin and deep dirt in the pores are simultaneously leukorrhed, so that the skin is fresh and clean.
with the development of economy and the improvement of living standard, people pay more and more attention to the protection of skin. The mask is also a skin care step which is important in skin care products. 80% -90% of adolescents and most of people with oily skin in the world have skin problems of large pores, face-full pox and dark acne due to the exuberant secretion of skin oil.
The skin problems not only bring skin and flesh pains to the people, but also become a mental obstacle and influence normal work and social activities. The oil control mask is essential for the health and refreshing skin. Some products with quick response to the situations are also available in the market, but most of the products are added with antibiotic medicinal ingredients, and side effects are easy to generate after the products are used.
Disclosure of Invention
In order to solve the technical problems, the invention provides the facial mask liquid for controlling oil and shrinking pores and the preparation method thereof, and aims to provide the facial mask liquid for controlling oil and shrinking pores.
The invention provides a mask liquid for controlling oil and shrinking pores, which is prepared from the following raw materials: glycylglycine, nicotinamide, okra polysaccharide, rhodiola rosea extract, camellia extract, purslane extract, brussels flavonoid, traditional Chinese medicine antibacterial extract, polyglutamic acid, sodium lactate, sodium pyrrolidone carboxylate, betaine, hydroxyethyl urea, a thickening agent, EDTA disodium, polyalcohol and deionized water.
As a further improvement of the invention, the health-care food is prepared from the following raw materials in parts by weight: 1-2 parts of glycylglycine, 1-3 parts of nicotinamide, 2-5 parts of okra polysaccharide, 1-3 parts of rhodiola rosea extract, 1-5 parts of camellia extract, 2-4 parts of purslane extract, 0.1-0.5 part of buconazole flavone, 2-5 parts of traditional Chinese medicine antibacterial extract, 0.01-1 part of polyglutamic acid, 0.05-2.5 parts of sodium lactate, 0.05-7.5 parts of sodium pyrrolidone carboxylate, 0.05-5 parts of betaine, 0.1-2 parts of hydroxyethyl urea, 0.01-5 parts of thickening agent, 0.01-0.5 part of EDTA disodium, 2-20 parts of polyhydric alcohol and 50-100 parts of deionized water.
As a further improvement of the invention, the health-care food is prepared from the following raw materials in parts by weight: 1.2-1.7 parts of glycylglycine, 1.5-2.5 parts of nicotinamide, 3-4 parts of okra polysaccharide, 1.2-2.7 parts of rhodiola rosea extract, 2-4 parts of camellia extract, 2.5-3.5 parts of purslane extract, 0.2-0.4 part of bruton flavonoid, 2.5-4.5 parts of Chinese medicinal antibacterial extract, 0.05-0.5 part of polyglutamic acid, 0.5-2 parts of sodium lactate, 2-5 parts of sodium pyrrolidone carboxylate, 0.5-3.5 parts of betaine, 0.5-1.5 parts of hydroxyethyl urea, 0.05-3.5 parts of thickening agent, 0.1-0.3 part of EDTA disodium, 5-15 parts of polyhydric alcohol and 70-90 parts of deionized water.
as a further improvement of the invention, the health-care food is prepared from the following raw materials in parts by weight: 1.5 parts of glycylglycine, 2 parts of nicotinamide, 3.5 parts of okra polysaccharide, 2 parts of rhodiola rosea extract, 3 parts of camellia extract, 3 parts of purslane extract, 0.3 part of buconazole flavone, 3 parts of Chinese medicinal bacteriostatic extract, 0.2 part of polyglutamic acid, 1.5 parts of sodium lactate, 3 parts of sodium pyrrolidone carboxylate, 2 parts of betaine, 1 part of hydroxyethyl urea, 1.5 parts of thickening agent, 0.2 part of EDTA disodium, 10 parts of polyalcohol and 80 parts of deionized water.
As a further improvement of the invention, the traditional Chinese medicine bacteriostatic extract is prepared by extracting the following raw materials in parts by weight: 5-10 parts of bighead atractylodes rhizome, 5-10 parts of fructus forsythiae, 5-10 parts of houttuynia cordata, 2-5 parts of radix achyranthis bidentatae, 2-5 parts of honeysuckle, 15-20 parts of mangnolia officinalis, 5-10 parts of semen cuscutae, 2-5 parts of rhizoma cyperi, 5-10 parts of safflower, 15-20 parts of leonurus and 20-25 parts of pseudo-ginseng.
As a further improvement of the invention, the traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning raw materials, oven drying, slicing, placing in the same extraction equipment, adding deionized water, extracting under reduced pressure at low temperature twice, filtering, mixing extractive solutions, and concentrating to obtain antibacterial extract.
as a further improvement of the invention, the reduced pressure low temperature condition is-0.05 MPa, 65 ℃, the mass of the deionized water is 10 times of that of the raw materials, and the density of the Chinese medicinal bacteriostatic extract is 1.5-1.7g/cm3。
As a further improvement of the invention, the thickener is selected from one or more of hydroxyethyl cellulose, xanthan gum, sclerotium gum, carbomer, cross-linked polymers of acrylic acid/alkyl alcohol acrylic acid and gelatin; the polyalcohol is one of butanediol, propylene glycol, glycerol and methyl propylene glycol.
the invention further provides a preparation method of the facial mask liquid for controlling oil and shrinking pores, which is characterized by comprising the following steps of:
(1) weighing the components in parts by weight;
(2) Adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) adding disodium EDTA into deionized water under stirring, mixing thickener, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, maintaining the temperature at 60-75 deg.C, and stirring to dissolve uniformly;
(4) Cooling to 45-50 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukuzuki flavone and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) cooling to 35-45 deg.C, adding glycylglycine, nicotinamide, betaine and polyalcohol, and stirring to dissolve uniformly;
(6) Vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) And (5) removing the vacuum and discharging.
The invention has the following beneficial effects:
The glycylglycine added in the invention can inhibit the increase of keratinocyte interleukin-1 alpha (IL-1 alpha) caused by oleic acid, and can stabilize the ion imbalance in cells caused by unsaturated fatty acid, thereby inhibiting the generation of inflammatory cytokines, fundamentally playing a role in shrinking pores, and simultaneously improving the skin state around the pores; the flavonoid compound in the pudding can effectively inhibit skin oil secretion, simultaneously effectively improve the roughness of skin at pore positions, and improve the limitation of the traditional oil-control active ingredient 5 alpha-reductase inhibitor to a certain extent; the okra polysaccharide, rhodiola rosea extract, camellia extract and purslane extract contain abundant amino acids with biological activity, have contraction effect on vascular smooth muscle, have the functions of central and peripheral (different positions with pathological changes), and have the functions of relieving skin and inhibiting skin pruritus caused by dryness. Also has the comprehensive skin improving performances of preventing skin dryness and aging, increasing skin comfort, scavenging free radicals and the like. Is rich in vitamin C and vitamin E, and has effect in resisting skin aging. In addition, vitamin C has a certain effect of eliminating pigmented spots, while vitamin E can protect mitochondrial phospholipid and has an effect of resisting free radicals; the skin absorption channel is opened by matching sodium lactate, sodium pyrrolidone carboxylate, betaine and hydroxyethyl urea with polyhydric alcohol, so that skin absorption is promoted, and the effects of quickly and obviously controlling oil and shrinking pores are generated on the skin;
according to the traditional Chinese medicine antibacterial extract, traditional Chinese medicinal materials with good antibacterial, bacteriostatic, anti-inflammatory and itching relieving functions are added, the extract obtained by extracting the traditional Chinese medicine antibacterial extract has the effects of obviously inhibiting bacteria, relieving itching, resisting allergy, controlling oil, shrinking pores, improving skin state and prolonging the quality guarantee period, and the preservative is not added into the mask liquid, so that the effect of guaranteeing the quality for a long time can be achieved, the allergen is reduced, and the barrier protection of the skin is enhanced;
the oil-control pore-shrinking mask liquid disclosed by the invention is prepared by selecting multiple components for scientific compounding, the cooperativity and compatibility of the components in the formula are fully utilized, the multiple components are mutually cooperated and promoted, the effect of the formula is greatly improved, and the problems of stability, reliability of effect and rapid effect of the product formula are perfectly solved.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is obvious that the embodiments described are only some representative embodiments of the present invention, rather than all embodiments, and all other embodiments obtained by a person skilled in the art without creative efforts belong to the protection scope of the present invention.
Example 1
The raw materials comprise the following components in parts by weight: 1 part of glycylglycine, 1 part of nicotinamide, 2 parts of okra polysaccharide, 1 part of rhodiola rosea extract, 1 part of camellia extract, 2 parts of purslane extract, 0.1 part of bushy flavonoid, 2 parts of Chinese medicinal bacteriostatic extract, 0.01 part of polyglutamic acid, 0.05 part of sodium lactate, 0.05 part of sodium pyrrolidone carboxylate, 0.05 part of betaine, 0.1 part of hydroxyethyl urea, 0.01 part of hydroxyethyl cellulose, 0.01 part of EDTA disodium, 2 parts of butanediol and 50 parts of deionized water.
The traditional Chinese medicine bacteriostatic extract is prepared by extracting the following raw materials in parts by weight: 5 parts of bighead atractylodes rhizome, 5 parts of weeping forsythia, 5 parts of heartleaf houttuynia herb, 2 parts of twotooth achyranthes root, 2 parts of honeysuckle flower, 15 parts of officinal magnolia bark, 5 parts of south dodder seed, 2 parts of nutgrass flatsedge rhizome, 5 parts of safflower, 15 parts of motherwort herb and 20 parts of panax notoginseng.
The traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning raw materials, oven drying, slicing, placing in the same extraction equipment, adding deionized water, extracting twice at-0.05 MPa and 65 deg.C, the mass of deionized water is 10 times of that of raw materials, filteringMixing extractive solutions, and concentrating to obtain antibacterial extract with density of 1.5g/cm3。
the preparation method comprises the following steps:
(1) weighing the components in parts by weight;
(2) Adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) Adding disodium EDTA into deionized water under stirring, mixing hydroxyethyl cellulose, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, maintaining the temperature at 60 deg.C, and stirring to dissolve uniformly;
(4) Cooling to 45 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukul flavonoid and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) cooling to 35 deg.C, adding glycylglycine, nicotinamide, betaine and butanediol, and stirring to dissolve uniformly;
(6) vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) And (5) removing the vacuum and discharging.
Example 2
The raw materials comprise the following components in parts by weight: 2 parts of glycylglycine, 3 parts of nicotinamide, 5 parts of okra polysaccharide, 3 parts of rhodiola rosea extract, 5 parts of camellia extract, 4 parts of purslane extract, 0.5 part of buconazole flavone, 5 parts of Chinese medicinal bacteriostatic extract, 1 part of polyglutamic acid, 2.5 parts of sodium lactate, 7.5 parts of sodium pyrrolidone carboxylate, 5 parts of betaine, 2 parts of hydroxyethyl urea, 5 parts of xanthan gum, 0.5 part of EDTA disodium, 20 parts of propylene glycol and 100 parts of deionized water.
the traditional Chinese medicine bacteriostatic extract is prepared by extracting the following raw materials in parts by weight: 10 parts of bighead atractylodes rhizome, 10 parts of fructus forsythiae, 10 parts of houttuynia cordata, 5 parts of radix achyranthis bidentatae, 5 parts of honeysuckle, 20 parts of mangnolia officinalis, 10 parts of semen cuscutae, 5 parts of rhizoma cyperi, 10 parts of safflower carthamus, 20 parts of leonurus and 25 parts of pseudo-ginseng.
The traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning raw materials, oven drying, slicing, extracting with deionized water twice at-0.05 MPa and 65 deg.C in the same extraction equipment, and removing ionsThe water is 10 times of the raw materials, filtering, mixing extractive solutions, and concentrating to obtain antibacterial extract with density of 1.7g/cm3。
the preparation method comprises the following steps:
(1) weighing the components in parts by weight;
(2) Adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) Adding disodium EDTA into deionized water under stirring, mixing xanthan gum, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, maintaining the temperature at 75 deg.C, and stirring to dissolve uniformly;
(4) cooling to 50 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukul flavonoid and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) Cooling to 45 deg.C, adding glycylglycine, nicotinamide, betaine and propylene glycol, and stirring to dissolve uniformly;
(6) vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) and (5) removing the vacuum and discharging.
Example 3
The raw materials comprise the following components in parts by weight: 1.2 parts of glycylglycine, 1.5 parts of nicotinamide, 3 parts of okra polysaccharide, 1.2 parts of rhodiola rosea extract, 2 parts of camellia extract, 2.5 parts of purslane extract, 0.2 part of bushy flavonoid, 2.5 parts of traditional Chinese medicine antibacterial extract, 0.05 part of polyglutamic acid, 0.5 part of sodium lactate, 2 parts of pyrrolidone carboxylic acid sodium, 0.5 part of betaine, 0.5 part of hydroxyethyl urea, 0.05 part of carbomer, 0.1 part of EDTA disodium, 5 parts of methyl propylene glycol and 70 parts of deionized water.
The traditional Chinese medicine bacteriostatic extract is prepared by extracting the following raw materials in parts by weight: 6 parts of bighead atractylodes rhizome, 6 parts of fructus forsythiae, 6 parts of houttuynia cordata, 3 parts of radix achyranthis bidentatae, 3 parts of honeysuckle, 16 parts of mangnolia officinalis, 6 parts of semen cuscutae, 3 parts of rhizoma cyperi, 6 parts of safflower carthamus, 16 parts of leonurus and 22 parts of panax notoginseng.
The traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning raw materials, oven drying, slicing, placing in the same extraction equipment, adding deionized water at-0.0Extracting twice at 65 deg.C under 5MPa, with deionized water 10 times the weight of the raw materials, filtering, mixing extractive solutions, and concentrating to obtain antibacterial extract with density of 1.55g/cm3。
the preparation method comprises the following steps:
(1) weighing the components in parts by weight;
(2) Adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) adding disodium EDTA into deionized water under stirring, mixing carbomer, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, maintaining the temperature at 65 deg.C, and stirring to dissolve uniformly;
(4) Cooling to 46 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukul flavonoid and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) cooling to 37 deg.C, adding glycylglycine, nicotinamide, betaine and methyl propylene glycol, and stirring to dissolve uniformly;
(6) Vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) And (5) removing the vacuum and discharging.
Example 4
the raw materials comprise the following components in parts by weight: 1.7 parts of glycylglycine, 2.5 parts of nicotinamide, 4 parts of okra polysaccharide, 2.7 parts of rhodiola rosea extract, 4 parts of camellia extract, 3.5 parts of purslane extract, 0.4 part of bushy flavonoid, 4.5 parts of traditional Chinese medicine antibacterial extract, 0.5 part of polyglutamic acid, 2 parts of sodium lactate, 5 parts of pyrrolidone carboxylic acid sodium, 3.5 parts of betaine, 1.5 parts of hydroxyethyl urea, 3.5 parts of gelatin, 0.3 part of EDTA disodium, 15 parts of glycerol and 90 parts of deionized water.
the traditional Chinese medicine bacteriostatic extract is prepared by extracting the following raw materials in parts by weight: 9 parts of bighead atractylodes rhizome, 9 parts of fructus forsythiae, 9 parts of houttuynia cordata, 4 parts of radix achyranthis bidentatae, 4 parts of honeysuckle, 18 parts of mangnolia officinalis, 9 parts of semen cuscutae, 4 parts of rhizoma cyperi, 9 parts of safflower carthamus, 18 parts of motherwort and 24 parts of panax notoginseng.
The traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning raw materials, oven drying, slicing, and extractingAdding deionized water into the equipment, extracting twice at-0.05 MPa and 65 deg.C, the mass of deionized water is 10 times of the raw materials, filtering, mixing extractive solutions, and concentrating to obtain antibacterial extract with density of 1.65g/cm3。
the preparation method comprises the following steps:
(1) weighing the components in parts by weight;
(2) adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) adding disodium EDTA into deionized water under stirring, mixing gelatin, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, maintaining the temperature at 72 deg.C, and stirring to dissolve uniformly;
(4) cooling to 48 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukul flavonoid and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) Cooling to 42 deg.C, adding glycylglycine, nicotinamide, betaine and glycerol, and stirring to dissolve uniformly;
(6) Vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) And (5) removing the vacuum and discharging.
Example 5
the raw materials comprise the following components in parts by weight: 1.5 parts of glycylglycine, 2 parts of nicotinamide, 3.5 parts of okra polysaccharide, 2 parts of rhodiola rosea extract, 3 parts of camellia extract, 3 parts of purslane extract, 0.3 part of buconazole flavone, 3 parts of Chinese medicinal bacteriostatic extract, 0.2 part of polyglutamic acid, 1.5 parts of sodium lactate, 3 parts of sodium pyrrolidone carboxylate, 2 parts of betaine, 1 part of hydroxyethyl urea, 1.5 parts of sclerotium rolfsii, 0.2 part of EDTA disodium, 10 parts of glycerol and 80 parts of deionized water.
the traditional Chinese medicine bacteriostatic extract is prepared by extracting the following raw materials in parts by weight: 7 parts of bighead atractylodes rhizome, 7 parts of fructus forsythiae, 7 parts of houttuynia cordata, 4 parts of radix achyranthis bidentatae, 3 parts of honeysuckle, 17 parts of mangnolia officinalis, 7 parts of semen cuscutae, 4 parts of rhizoma cyperi, 7 parts of safflower, 16 parts of motherwort and 23 parts of pseudo-ginseng.
The traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning the raw materials, drying,Slicing, placing in the same extraction equipment, adding deionized water, extracting at-0.05 MPa and 65 deg.C twice, the deionized water being 10 times of the raw materials, filtering, mixing extractive solutions, and concentrating to obtain antibacterial extract with density of 1.6g/cm3。
The preparation method comprises the following steps:
(1) Weighing the components in parts by weight;
(2) Adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) adding disodium EDTA into deionized water under stirring, mixing sclerotium rolfsii gum, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, keeping the temperature at 67 deg.C, and stirring to dissolve uniformly;
(4) cooling to 48 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukul flavonoid and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) Cooling to 40 deg.C, adding glycylglycine, nicotinamide, betaine and glycerol, and stirring to dissolve uniformly;
(6) Vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) And (5) removing the vacuum and discharging.
test example 1 Performance test
The oil-control pore-shrinking mask solution prepared in the embodiments 1 to 5 of the invention is subjected to various index tests, and the test results are shown in table 1.
TABLE 1 results of testing various indexes of oil-controlling pore-shrinking mask liquid
Test example 2 bacteriostatic property test
the oil-controlling pore-shrinking mask solutions prepared in examples 1 to 5 and commercially available oil-controlling pore-shrinking mask solutions were filled in dark brown glass bottles, the caps were opened, and the bottles were placed at an ambient temperature of 40 ℃ and a relative humidity of 85%, and continuously observed and tested, and the specific results are shown in table 2. And (3) detecting the level of the microorganisms, wherein specific detection items, detection methods and detection standards are carried out according to QB/T2872-2007.
TABLE 2
| Group of | Phenomenon(s) |
| Example 1 | No abnormality occurs in 60 days, and the temperature is pure. |
| Example 2 | no abnormality occurs in 60 days, and the temperature is pure. |
| Example 3 | no abnormality occurs in 60 days, and the temperature is pure. |
| Example 4 | No abnormality occurs in 60 days, and the temperature is pure. |
| example 5 | No abnormality occurs in 60 days, and the temperature is pure. |
| Is commercially available | Bacterial plaque appears after 7 days, microorganisms exceed the standard, and unpleasant odor is emitted. |
Test example 1 Patch test
1. the test substance: the oil-control pore-shrinking mask solution prepared in example 1.
2. Negative control: deionized water.
3. Subject: the total of 30 people, male 0 person and female 30 people, the age is 19-45 years, and the volunteer enrollment criteria of the subject are met.
4. The spot pasting method comprises the following steps: a qualified spot tester is selected, a closed spot test method is adopted, a test object and a negative control about 0.020-0.025 mL (semifluid) are dripped into the spot tester, a special adhesive tape is externally applied to the back of the test object, the test object is removed after 24 hours, skin reactions are observed after 0.5, 24 and 48 hours after the removal respectively, and the results are recorded according to the skin reaction grading standard in technical Specification for safety of cosmetics (2015 edition). The test results are shown in table 3:
TABLE 3 test results of human skin patches
the result of the human body skin patch test shows that: adverse skin reactions occurred in 0 of 30 people; the anti-allergy mask liquid is safe to use.
test example 2 oil control and pore shrinkage effect test
First, the oil control effect was evaluated as follows.
30 male and female test subjects were selected and divided into two groups, one group of subjects used the product prepared in example 1 of the present invention, and the other group of subjects used a commercially available oil-controlled pore-shrinking product, and applied once a day for 15-20min, and the average sebum reduction (%) after 2 and 4 weeks was measured by using a sebum meter, and the results thereof are shown in table 4, and the results are the average values of the respective groups.
TABLE 4
As can be seen from the data in Table 4, the facial mask solution prepared in example 1 of the present invention is effective in inhibiting the secretion of excess sebum compared to similar products available on the market.
Second, the pore-shrinking effect was evaluated as follows.
25 subjects with enlarged pores between 20 and 35 years old were selected and divided into 5 groups, and the same facial mask fluid containing the above-mentioned example 1 and commercially available facial mask fluid was administered to each group of subjects for 1 week and 2 times for 4 weeks, respectively, and then the change in the number of hair pores was measured by a professional instrument. The number of pores before, after 1 week, after 2 weeks, and after 4 weeks of use was measured using the instrument. The test results are set forth in Table 5, and the result values are the average values of the respective groups.
TABLE 5
According to the data in the table 5, the facial mask liquid for controlling oil and shrinking pores, which is prepared in the embodiment 1 of the invention, has the advantages of quick response, lasting effect and good effect, and is superior to similar products sold in the market.
the anti-allergic mask liquid obtained in examples 2-5 is used as an active effective ingredient to carry out a human body skin patch test and an oil control and pore shrinking effect test according to the method, and similar test results to the test results are obtained.
Compared with the prior art, the glycylglycine added in the invention can inhibit the increase of keratinocyte interleukin-1 alpha (IL-1 alpha) caused by oleic acid, and can stabilize the intracellular ion imbalance caused by unsaturated fatty acid, thereby inhibiting the generation of inflammatory cytokines, fundamentally playing a role in shrinking pores, and simultaneously improving the skin state around the pores; the flavonoid compound in the pudding can effectively inhibit skin oil secretion, simultaneously effectively improve the roughness of skin at pore positions, and improve the limitation of the traditional oil-control active ingredient 5 alpha-reductase inhibitor to a certain extent; the okra polysaccharide, rhodiola rosea extract, camellia extract and purslane extract contain abundant amino acids with biological activity, have contraction effect on vascular smooth muscle, have the functions of central and peripheral (different positions with pathological changes), and have the functions of relieving skin and inhibiting skin pruritus caused by dryness. Also has the comprehensive skin improving performances of preventing skin dryness and aging, increasing skin comfort, scavenging free radicals and the like. Is rich in vitamin C and vitamin E, and has effect in resisting skin aging. In addition, vitamin C has a certain effect of eliminating pigmented spots, while vitamin E can protect mitochondrial phospholipid and has an effect of resisting free radicals; the skin absorption channel is opened by matching sodium lactate, sodium pyrrolidone carboxylate, betaine and hydroxyethyl urea with polyhydric alcohol, so that skin absorption is promoted, and the effects of quickly and obviously controlling oil and shrinking pores are generated on the skin;
according to the traditional Chinese medicine antibacterial extract, traditional Chinese medicinal materials with good antibacterial, bacteriostatic, anti-inflammatory and itching relieving functions are added, the extract obtained by extracting the traditional Chinese medicine antibacterial extract has the effects of obviously inhibiting bacteria, relieving itching, resisting allergy, controlling oil, shrinking pores, improving skin state and prolonging the quality guarantee period, and the preservative is not added into the mask liquid, so that the effect of guaranteeing the quality for a long time can be achieved, the allergen is reduced, and the barrier protection of the skin is enhanced;
The oil-control pore-shrinking mask liquid disclosed by the invention is prepared by selecting multiple components for scientific compounding, the cooperativity and compatibility of the components in the formula are fully utilized, the multiple components are mutually cooperated and promoted, the effect of the formula is greatly improved, and the problems of stability, reliability of effect and rapid effect of the product formula are perfectly solved.
Various modifications may be made to the above without departing from the spirit and scope of the invention as defined by the appended claims. The scope of the invention is therefore intended to be limited not by the above description, but rather by the scope of the appended claims.
Claims (9)
1. The mask liquid capable of controlling oil and shrinking pores is characterized by being prepared from the following raw materials: glycylglycine, nicotinamide, okra polysaccharide, rhodiola rosea extract, camellia extract, purslane extract, brussels flavonoid, traditional Chinese medicine antibacterial extract, polyglutamic acid, sodium lactate, sodium pyrrolidone carboxylate, betaine, hydroxyethyl urea, a thickening agent, EDTA disodium, polyalcohol and deionized water.
2. the mask liquid capable of controlling oil and shrinking pores according to claim 1, which is prepared from the following raw materials in parts by weight: 1-2 parts of glycylglycine, 1-3 parts of nicotinamide, 2-5 parts of okra polysaccharide, 1-3 parts of rhodiola rosea extract, 1-5 parts of camellia extract, 2-4 parts of purslane extract, 0.1-0.5 part of buconazole flavone, 2-5 parts of traditional Chinese medicine antibacterial extract, 0.01-1 part of polyglutamic acid, 0.05-2.5 parts of sodium lactate, 0.05-7.5 parts of sodium pyrrolidone carboxylate, 0.05-5 parts of betaine, 0.1-2 parts of hydroxyethyl urea, 0.01-5 parts of thickening agent, 0.01-0.5 part of EDTA disodium, 2-20 parts of polyhydric alcohol and 50-100 parts of deionized water.
3. The mask liquid capable of controlling oil and shrinking pores according to claim 2, which is prepared from the following raw materials in parts by weight: 1.2-1.7 parts of glycylglycine, 1.5-2.5 parts of nicotinamide, 3-4 parts of okra polysaccharide, 1.2-2.7 parts of rhodiola rosea extract, 2-4 parts of camellia extract, 2.5-3.5 parts of purslane extract, 0.2-0.4 part of bruton flavonoid, 2.5-4.5 parts of Chinese medicinal antibacterial extract, 0.05-0.5 part of polyglutamic acid, 0.5-2 parts of sodium lactate, 2-5 parts of sodium pyrrolidone carboxylate, 0.5-3.5 parts of betaine, 0.5-1.5 parts of hydroxyethyl urea, 0.05-3.5 parts of thickening agent, 0.1-0.3 part of EDTA disodium, 5-15 parts of polyhydric alcohol and 70-90 parts of deionized water.
4. The mask liquid capable of controlling oil and shrinking pores according to claim 3, which is prepared from the following raw materials in parts by weight: 1.5 parts of glycylglycine, 2 parts of nicotinamide, 3.5 parts of okra polysaccharide, 2 parts of rhodiola rosea extract, 3 parts of camellia extract, 3 parts of purslane extract, 0.3 part of buconazole flavone, 3 parts of Chinese medicinal bacteriostatic extract, 0.2 part of polyglutamic acid, 1.5 parts of sodium lactate, 3 parts of sodium pyrrolidone carboxylate, 2 parts of betaine, 1 part of hydroxyethyl urea, 1.5 parts of thickening agent, 0.2 part of EDTA disodium, 10 parts of polyalcohol and 80 parts of deionized water.
5. the mask liquid capable of controlling oil and shrinking pores according to claim 1, wherein the traditional Chinese medicine bacteriostatic extract is extracted from the following raw materials in parts by weight: 5-10 parts of bighead atractylodes rhizome, 5-10 parts of fructus forsythiae, 5-10 parts of houttuynia cordata, 2-5 parts of radix achyranthis bidentatae, 2-5 parts of honeysuckle, 15-20 parts of mangnolia officinalis, 5-10 parts of semen cuscutae, 2-5 parts of rhizoma cyperi, 5-10 parts of safflower, 15-20 parts of leonurus and 20-25 parts of pseudo-ginseng.
6. The mask liquid capable of controlling oil and shrinking pores according to claim 5, wherein the traditional Chinese medicine bacteriostatic extract is prepared by the following method: cleaning raw materials, oven drying, slicing, placing in the same extraction equipment, adding deionized water, extracting under reduced pressure at low temperature twice, filtering, mixing extractive solutions, and concentrating to obtain antibacterial extract.
7. The mask liquid capable of controlling oil and shrinking pores according to claim 6, wherein the reduced-pressure low-temperature condition is-0.05 MPa, 65 ℃, the mass of deionized water is 10 times of that of the raw materials, and the density of the traditional Chinese medicine bacteriostatic extract is 1.5-1.7g/cm3。
8. The facial mask liquid for controlling oil and shrinking pores according to claim 1, wherein the thickener is one or more selected from the group consisting of hydroxyethyl cellulose, xanthan gum, sclerotium rolfsii gum, carbomer, cross-linked polymers of acrylic acid/alkylol acrylic acid, and gelatin; the polyalcohol is one of butanediol, propylene glycol, glycerol and methyl propylene glycol.
9. A method for preparing an oil-controlling pore-shrinking mask liquid according to any one of claims 1 to 8, which is prepared by the following steps:
(1) weighing the components in parts by weight;
(2) Adding deionized water into a vacuum emulsifying pot, heating to 95 ℃, preserving heat for 20 minutes, and cooling to 75 ℃;
(3) Adding disodium EDTA into deionized water under stirring, mixing thickener, sodium lactate, sodium pyrrolidone carboxylate, hydroxyethyl urea and polyglutamic acid, adding, maintaining the temperature at 60-75 deg.C, and stirring to dissolve uniformly;
(4) cooling to 45-50 deg.C, adding okra polysaccharide, radix Rhodiolae extract, flos Camelliae Japonicae extract, herba Portulacae extract, Bukuzuki flavone and Chinese medicinal antibacterial extract, stirring to dissolve uniformly;
(5) Cooling to 35-45 deg.C, adding glycylglycine, nicotinamide, betaine and polyalcohol, and stirring to dissolve uniformly;
(6) vacuumizing to-0.06 MPa, and stirring for 20 minutes;
(7) And (5) removing the vacuum and discharging.
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