CN103269978A - 沸石的机械化学生产 - Google Patents

沸石的机械化学生产 Download PDF

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Publication number
CN103269978A
CN103269978A CN2011800573934A CN201180057393A CN103269978A CN 103269978 A CN103269978 A CN 103269978A CN 2011800573934 A CN2011800573934 A CN 2011800573934A CN 201180057393 A CN201180057393 A CN 201180057393A CN 103269978 A CN103269978 A CN 103269978A
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CN
China
Prior art keywords
zeolite
gel rubber
synthesized gel
grinding
template
Prior art date
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Pending
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CN2011800573934A
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English (en)
Chinese (zh)
Inventor
J·舒恩琳娜
J·莱德贝克
J·枯伊
S·外拉什
G·波尔菲斯
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Sued Chemie AG
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Sued Chemie AG
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Publication of CN103269978A publication Critical patent/CN103269978A/zh
Pending legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C01B39/38—Type ZSM-5
    • C01B39/40—Type ZSM-5 using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
CN2011800573934A 2010-12-01 2011-11-28 沸石的机械化学生产 Pending CN103269978A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010053054.9 2010-12-01
DE102010053054A DE102010053054A1 (de) 2010-12-01 2010-12-01 Mechanochemische Herstellung von Zeolithen
PCT/EP2011/071099 WO2012072527A2 (de) 2010-12-01 2011-11-28 Mechanochemische herstellung von zeolithen

Publications (1)

Publication Number Publication Date
CN103269978A true CN103269978A (zh) 2013-08-28

Family

ID=45047780

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2011800573934A Pending CN103269978A (zh) 2010-12-01 2011-11-28 沸石的机械化学生产

Country Status (7)

Country Link
US (1) US20130266507A1 (enExample)
EP (1) EP2646367A2 (enExample)
JP (1) JP2014501683A (enExample)
CN (1) CN103269978A (enExample)
DE (1) DE102010053054A1 (enExample)
WO (1) WO2012072527A2 (enExample)
ZA (1) ZA201303567B (enExample)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104860332A (zh) * 2014-02-21 2015-08-26 中国石油化工股份有限公司 一种制备NaY分子筛的方法
CN108408737A (zh) * 2018-05-29 2018-08-17 王子韩 一种快速制备y型分子筛的方法
CN111001265A (zh) * 2019-12-26 2020-04-14 江苏楚锐环保科技有限公司 高质量沸石转轮生产工艺及其生产设备
WO2020108482A1 (en) * 2018-11-27 2020-06-04 Basf Se Mechanochemical activation in solvent-free zeolite synthesis
CN116102032A (zh) * 2023-02-06 2023-05-12 淄博恒亿化工科技有限公司 一种zsm-5分子筛的制备方法

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102951656B (zh) * 2012-10-16 2014-06-04 大连瑞克科技有限公司 一种颗粒均匀zsm-5分子筛的合成方法
JP6173196B2 (ja) * 2012-12-21 2017-08-02 日揮触媒化成株式会社 ナノサイズゼオライトの合成方法
CN109665541B (zh) * 2017-10-17 2022-04-01 中国石油化工股份有限公司 低硅铝比zsm-12型沸石分子筛的合成方法
EP3825280A4 (en) * 2018-07-27 2021-09-22 SK Innovation Co., Ltd. ZEOLITE MORDENITE WITH EXCELLENT UNIFORMITY OF PARTICLE AND ITS PREPARATION METHOD
KR102020445B1 (ko) 2018-09-21 2019-09-10 에스케이이노베이션 주식회사 입자 크기의 제어가 가능한 모데나이트 제올라이트의 제조방법
WO2020109290A1 (en) 2018-11-27 2020-06-04 Basf Se Solvent-free mechanochemical activation in zeolite synthesis
WO2020109292A1 (en) 2018-11-27 2020-06-04 Basf Se Mechanochemical activation in zeolite synthesis
EP4038041B1 (en) * 2019-09-30 2024-12-04 Dow Global Technologies LLC Methods of etherification
CN110893491B (zh) * 2019-12-13 2021-07-27 湖南中镆科技有限公司 一种铝模板铣槽固定装置
US20240174524A1 (en) * 2022-11-29 2024-05-30 Saudi Arabian Oil Company Method for synthesizing nano-sized zeolite beta

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1089574A (zh) * 1992-06-05 1994-07-20 埃克森化学专利公司 Zsm-5沸石
EP0916056A1 (de) * 1996-08-09 1999-05-19 Uwe Vieregge Teleskoprohr für insbesondere sprinkleranlagen
US7119245B1 (en) * 2001-10-25 2006-10-10 Sandia Corporation Synthesis of an un-supported, high-flow ZSM-22 zeolite membrane

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US4664842A (en) 1983-12-13 1987-05-12 Southern Clay Products, Inc. Process for manufacturing organoclays having enhanced gelling properties
GB8432793D0 (en) * 1984-12-31 1985-02-06 Exxon Research Engineering Co Zeolite beta preparation
DE4405876A1 (de) 1994-02-23 1995-10-05 Sued Chemie Ag Katalysator- bzw. Katalysatorträger-Formkörper
JP3986186B2 (ja) * 1997-11-07 2007-10-03 日本碍子株式会社 高耐熱性β−ゼオライト及びそれを用いた自動車排ガス浄化用吸着材
DE19820515A1 (de) 1998-05-08 1999-11-11 Alsi Penta Zeolithe Gmbh Verfahren zur Herstellung eines Katalysators für die Reinigung von Abgasen, die Stickstoffoxide in Gegenwart von Sauerstoff und Wasser enthalten
ES2160058B1 (es) * 1999-06-17 2002-06-16 Univ Valencia Politecnica Sintesis de zeolitas.
CN101096274B (zh) * 2006-06-29 2010-08-25 中国石油化工股份有限公司 一种富铝beta沸石的制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1089574A (zh) * 1992-06-05 1994-07-20 埃克森化学专利公司 Zsm-5沸石
EP0916056A1 (de) * 1996-08-09 1999-05-19 Uwe Vieregge Teleskoprohr für insbesondere sprinkleranlagen
US7119245B1 (en) * 2001-10-25 2006-10-10 Sandia Corporation Synthesis of an un-supported, high-flow ZSM-22 zeolite membrane

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
KATSUTOSHI YAMAMOTO ET AL.: "Zeolite synthesis using mechanochemical reaction", 《MICROPOROUS AND MESOPOROUS MATERIALS》 *
N.E.GORDINA ET AL.: "Synthesis of NaA Zeolite by Mechanochemical Methods", 《RUSSIAN JOURNAL OF APPLIED CHEMISTRY》 *
XIA Q H ET AL.: "Crystallization kinetics of nanosized Tiβ zeolites with high oxidation activity by a dry-gel conversion technique", 《MATERIALS CHEMISTRY AND PHYSICS》 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104860332A (zh) * 2014-02-21 2015-08-26 中国石油化工股份有限公司 一种制备NaY分子筛的方法
CN108408737A (zh) * 2018-05-29 2018-08-17 王子韩 一种快速制备y型分子筛的方法
WO2020108482A1 (en) * 2018-11-27 2020-06-04 Basf Se Mechanochemical activation in solvent-free zeolite synthesis
CN111001265A (zh) * 2019-12-26 2020-04-14 江苏楚锐环保科技有限公司 高质量沸石转轮生产工艺及其生产设备
CN111001265B (zh) * 2019-12-26 2021-11-12 维珂瑞（北京）环境科技有限公司 高质量沸石转轮生产工艺及其生产设备
CN116102032A (zh) * 2023-02-06 2023-05-12 淄博恒亿化工科技有限公司 一种zsm-5分子筛的制备方法
CN116102032B (zh) * 2023-02-06 2024-09-03 淄博恒亿化工科技有限公司 一种zsm-5分子筛的制备方法

Also Published As

Publication number Publication date
EP2646367A2 (de) 2013-10-09
WO2012072527A2 (de) 2012-06-07
DE102010053054A1 (de) 2012-06-06
ZA201303567B (en) 2014-07-30
US20130266507A1 (en) 2013-10-10
JP2014501683A (ja) 2014-01-23
WO2012072527A3 (de) 2012-10-11

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Application publication date: 20130828