DE102010053054A1 - Mechanochemische Herstellung von Zeolithen - Google Patents

Mechanochemische Herstellung von Zeolithen Download PDF

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Publication number
DE102010053054A1
DE102010053054A1 DE102010053054A DE102010053054A DE102010053054A1 DE 102010053054 A1 DE102010053054 A1 DE 102010053054A1 DE 102010053054 A DE102010053054 A DE 102010053054A DE 102010053054 A DE102010053054 A DE 102010053054A DE 102010053054 A1 DE102010053054 A1 DE 102010053054A1
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Germany
Prior art keywords
grinding
synthesis
mill
zeolite
silicon source
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE102010053054A
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German (de)
English (en)
Inventor
Josef Schönlinner
Dr. Ladebeck Jürgen
Dr. Koy Jürgen
Dr. Wellach Stephan
Dr. Burgfels Götz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sued Chemie IP GmbH and Co KG
Original Assignee
Sued Chemie AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sued Chemie AG filed Critical Sued Chemie AG
Priority to DE102010053054A priority Critical patent/DE102010053054A1/de
Priority to US13/988,598 priority patent/US20130266507A1/en
Priority to EP11788450.2A priority patent/EP2646367A2/de
Priority to CN2011800573934A priority patent/CN103269978A/zh
Priority to PCT/EP2011/071099 priority patent/WO2012072527A2/de
Priority to JP2013541310A priority patent/JP2014501683A/ja
Publication of DE102010053054A1 publication Critical patent/DE102010053054A1/de
Priority to ZA2013/03567A priority patent/ZA201303567B/en
Withdrawn legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7007—Zeolite Beta
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C01B39/38—Type ZSM-5
    • C01B39/40—Type ZSM-5 using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
DE102010053054A 2010-12-01 2010-12-01 Mechanochemische Herstellung von Zeolithen Withdrawn DE102010053054A1 (de)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DE102010053054A DE102010053054A1 (de) 2010-12-01 2010-12-01 Mechanochemische Herstellung von Zeolithen
US13/988,598 US20130266507A1 (en) 2010-12-01 2011-11-28 Mechanochemical production of zeolites
EP11788450.2A EP2646367A2 (de) 2010-12-01 2011-11-28 Mechanochemische herstellung von zeolithen
CN2011800573934A CN103269978A (zh) 2010-12-01 2011-11-28 沸石的机械化学生产
PCT/EP2011/071099 WO2012072527A2 (de) 2010-12-01 2011-11-28 Mechanochemische herstellung von zeolithen
JP2013541310A JP2014501683A (ja) 2010-12-01 2011-11-28 ゼオライトのメカノケミカル製造
ZA2013/03567A ZA201303567B (en) 2010-12-01 2013-05-16 Mechanochemical production of zeolites

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102010053054A DE102010053054A1 (de) 2010-12-01 2010-12-01 Mechanochemische Herstellung von Zeolithen

Publications (1)

Publication Number Publication Date
DE102010053054A1 true DE102010053054A1 (de) 2012-06-06

Family

ID=45047780

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102010053054A Withdrawn DE102010053054A1 (de) 2010-12-01 2010-12-01 Mechanochemische Herstellung von Zeolithen

Country Status (7)

Country Link
US (1) US20130266507A1 (enExample)
EP (1) EP2646367A2 (enExample)
JP (1) JP2014501683A (enExample)
CN (1) CN103269978A (enExample)
DE (1) DE102010053054A1 (enExample)
WO (1) WO2012072527A2 (enExample)
ZA (1) ZA201303567B (enExample)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110893491A (zh) * 2019-12-13 2020-03-20 谢海春 一种铝模板铣槽固定装置
US20210179437A1 (en) * 2018-07-27 2021-06-17 Sk Innovation Co., Ltd. Mordenite Zeolite Having Excellent Particle Uniformity and Method for Preparing Same
US11932545B2 (en) 2018-09-21 2024-03-19 Sk Innovation Co., Ltd. Method for preparing mordenite zeolite having controllable particle size

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102951656B (zh) * 2012-10-16 2014-06-04 大连瑞克科技有限公司 一种颗粒均匀zsm-5分子筛的合成方法
JP6173196B2 (ja) * 2012-12-21 2017-08-02 日揮触媒化成株式会社 ナノサイズゼオライトの合成方法
CN104860332A (zh) * 2014-02-21 2015-08-26 中国石油化工股份有限公司 一种制备NaY分子筛的方法
CN109665541B (zh) * 2017-10-17 2022-04-01 中国石油化工股份有限公司 低硅铝比zsm-12型沸石分子筛的合成方法
CN108408737A (zh) * 2018-05-29 2018-08-17 王子韩 一种快速制备y型分子筛的方法
WO2020108482A1 (en) * 2018-11-27 2020-06-04 Basf Se Mechanochemical activation in solvent-free zeolite synthesis
WO2020109290A1 (en) 2018-11-27 2020-06-04 Basf Se Solvent-free mechanochemical activation in zeolite synthesis
WO2020109292A1 (en) 2018-11-27 2020-06-04 Basf Se Mechanochemical activation in zeolite synthesis
WO2021067077A1 (en) * 2019-09-30 2021-04-08 Dow Global Technologies Llc Methods of etherification
CN111001265B (zh) * 2019-12-26 2021-11-12 维珂瑞（北京）环境科技有限公司 高质量沸石转轮生产工艺及其生产设备
US20240174524A1 (en) * 2022-11-29 2024-05-30 Saudi Arabian Oil Company Method for synthesizing nano-sized zeolite beta
CN116102032B (zh) * 2023-02-06 2024-09-03 淄博恒亿化工科技有限公司 一种zsm-5分子筛的制备方法

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4664842A (en) 1983-12-13 1987-05-12 Southern Clay Products, Inc. Process for manufacturing organoclays having enhanced gelling properties
DE4405876A1 (de) 1994-02-23 1995-10-05 Sued Chemie Ag Katalysator- bzw. Katalysatorträger-Formkörper
EP0187522B2 (en) * 1984-12-31 1999-07-07 Exxon Research And Engineering Company Zeolite beta preparation
EP0955080A1 (de) 1998-05-08 1999-11-10 AlSi-PENTA Zeolithe GmbH Verfahren zur Herstellung eines Katalysators für die Reinigung von Abgasen
US20020090337A1 (en) * 1999-06-17 2002-07-11 Avelino Corma Canos Synthesis of zeolites
US7119245B1 (en) * 2001-10-25 2006-10-10 Sandia Corporation Synthesis of an un-supported, high-flow ZSM-22 zeolite membrane
CN101096274A (zh) * 2006-06-29 2008-01-02 中国石油化工股份有限公司 一种富铝beta沸石的制备方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ZA933879B (en) * 1992-06-05 1993-12-27 Exxon Chemical Patents Inc ZSM-5-zeolite
DE19632133A1 (de) * 1996-08-09 1998-04-09 Uwe Vieregge Teleskoprohr für insbesondere Sprinkleranlagen
JP3986186B2 (ja) * 1997-11-07 2007-10-03 日本碍子株式会社 高耐熱性β−ゼオライト及びそれを用いた自動車排ガス浄化用吸着材

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4664842A (en) 1983-12-13 1987-05-12 Southern Clay Products, Inc. Process for manufacturing organoclays having enhanced gelling properties
EP0187522B2 (en) * 1984-12-31 1999-07-07 Exxon Research And Engineering Company Zeolite beta preparation
DE4405876A1 (de) 1994-02-23 1995-10-05 Sued Chemie Ag Katalysator- bzw. Katalysatorträger-Formkörper
EP0955080A1 (de) 1998-05-08 1999-11-10 AlSi-PENTA Zeolithe GmbH Verfahren zur Herstellung eines Katalysators für die Reinigung von Abgasen
US20020090337A1 (en) * 1999-06-17 2002-07-11 Avelino Corma Canos Synthesis of zeolites
US7119245B1 (en) * 2001-10-25 2006-10-10 Sandia Corporation Synthesis of an un-supported, high-flow ZSM-22 zeolite membrane
CN101096274A (zh) * 2006-06-29 2008-01-02 中国石油化工股份有限公司 一种富铝beta沸石的制备方法

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
DIN 53019
ISO 13320-1
ISO 3219
R. Szostak, Studies in Surface Science Catalysis, 137 (2001) 261-297

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20210179437A1 (en) * 2018-07-27 2021-06-17 Sk Innovation Co., Ltd. Mordenite Zeolite Having Excellent Particle Uniformity and Method for Preparing Same
US11932545B2 (en) 2018-09-21 2024-03-19 Sk Innovation Co., Ltd. Method for preparing mordenite zeolite having controllable particle size
CN110893491A (zh) * 2019-12-13 2020-03-20 谢海春 一种铝模板铣槽固定装置
CN110893491B (zh) * 2019-12-13 2021-07-27 湖南中镆科技有限公司 一种铝模板铣槽固定装置

Also Published As

Publication number Publication date
WO2012072527A3 (de) 2012-10-11
EP2646367A2 (de) 2013-10-09
US20130266507A1 (en) 2013-10-10
CN103269978A (zh) 2013-08-28
ZA201303567B (en) 2014-07-30
WO2012072527A2 (de) 2012-06-07
JP2014501683A (ja) 2014-01-23

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