CN102379317A - Combination with anticorrosion activity and cosmetic - Google Patents
Combination with anticorrosion activity and cosmetic Download PDFInfo
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- CN102379317A CN102379317A CN2010102662126A CN201010266212A CN102379317A CN 102379317 A CN102379317 A CN 102379317A CN 2010102662126 A CN2010102662126 A CN 2010102662126A CN 201010266212 A CN201010266212 A CN 201010266212A CN 102379317 A CN102379317 A CN 102379317A
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Abstract
The invention relates to a combination with an anticorrosion activity, which is a combination of any two or more than two of Zanthoxylum piperitum extract, Chinese pulsatilla root extract, moss extract and cassia bark extract, wherein the weight ratio of the Zanthoxylum piperitum extract to the Chinese pulsatilla root extract to the moss extract to the cassia bark extract is (0.05-2.0) : (0.05-2.0) : (0.01-0.5) : (0.01-0.5). The invention additionally provides a cosmetic, which contains the combination which contains any two or more than two of Zanthoxylum piperitum extract, Chinese pulsatilla root extract, moss extract and cassia bark extract. The combination not only has an excellent antibacterial activity to fungi such as molds, yeasts and the like, but also has a very high antibacterial generality and has a small impact on the physical and chemical stability of the cosmetic.
Description
Technical field:
The present invention relates to chemical field, relate in particular to a kind of cosmetic additive, is a kind of composition and cosmetics with antiseptic specifically.
Background technology:
Cosmetics preservative is not the additive of the simple corruption that prevents product; Use the commodity process but be fabricated onto the consumer from factory; Suppress the inevitable or accidental microorganism that is present in the middle of the product, prevent the general name of the additive of purposes interpolations such as the cosmetics that cause because of microbial growth are rotten, spoiled, corruption.
The preservative major part is simple to make, the cheap easy mass-produced synthetic material of unit price is main.Representational cosmetics preservative has the methyl p-hydroxybenzoate (Methyl Paraben) of P-hydroxybenzoic acid in this preservative; Ethyl-para-hydroxybenzoate (Ethyl Paraben); Propylparaben (Propyl Paraben); Butyl p-hydroxybenzoate (Butyl Paraben) etc. and quaternary ammonium salt-15 (Quaternium-15); Imidazolidinyl urea (Imidazolidinyl Urea); Two (methylol) imidazolidinyl urea (Diazolidinyl Urea); Phenoxyethanol (Phenoxyethanol); Benzalkonium chloride (Benzalkonium Chloride); Triclosan chemical preservatives such as (Trichlosan).
Though this chemical preservative can suppress the stability that the breeding of microorganism brings cosmetics, also be to bring out skin irritant reason simultaneously.The preservatives such as imidazolidinyl urea and two (methylol) imidazolidinyl ureas of formalin for example can dissociate; Reduce the trend of using in the whole world; Uses of only in hair cleaning and several kinds of washing products, limiting the quantity of is to belong to the preservative that use is forbidden in several countries such as Japan.The preservative of this free formalin is that the formalin group that contains in the structure As time goes on can slow release, and the formalin that dissociates not only brings out skin irritatin, also possibly cause cutaneum carcinoma.
Be considered to safe cosmetics preservative in the past, the widely used hydroxybenzoic acid class of medical science article preservative also can cause allergic and internal secretion is chaotic.The standard of also have to allow using is also doubtful, and has at skin and possibly cause new problems such as acute toxicity and chronic toxicity, sudden change through the accumulation that continues.
As stated, the side effect of preservative can make the consumer reduce the reliability to product, becomes the consumer cosmetics and cosmetics are caused discontented factor.
So constantly reducing the content of preservative or using no protective system in the research and development cosmetics.Also emerge when solving the side effect that preservative brings the avirulent natural antiseptic agent of skin ground stimulation.
But natural antibacterial property part of raw materials has that the color is too dark and the highly seasoned characteristics of raw material, limitation is arranged or is not suitable for using so use.Also have some to reduce the viscosity of cosmetics, influence emulsification system.Also have compared with chemical preservative and do not have antibiotic property widely, the active component in the plant extracts is low to physical stabilities such as light, heat, oxygen compared with chemical preservative, can not keep the problem of its abundant antiseptic at circulation period.
Summary of the invention:
The object of the present invention is to provide a kind of composition and cosmetics with antiseptic; Described thisly have the composition of antiseptic and cosmetics preservative antibiotic property that cosmetics will solve employing natural antibacterial raw material of the prior art is limited and physical stability is low, the technical problem that antiseptic effect is not good.
A kind of composition of the present invention with antiseptic; Be long and thin hot pepper extract or Radix Pulsatillae extract or moss extract or Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, perhaps any two kinds or the two or more combinations in long and thin hot pepper extract, Radix Pulsatillae extract, moss extract and the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
Further, described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract is: 0.05-2.0: 0.05-2.0.
Further, described composition is the combination of long and thin hot pepper extract, moss extract, and the weight ratio of described long and thin hot pepper extract, moss extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of Radix Pulsatillae extract, moss extract, and the weight ratio of described Radix Pulsatillae extract, moss extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.01-0.5: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, moss extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5: 0.01-0.5.
Further, described composition is the combination of Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5: 0.01-0.5.
Further; Described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5: 0.01-0.5.
Further, described long and thin hot pepper extract prepares through following method: elder generation cleans long and thin hot pepper and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
Further, described Radix Pulsatillae extract prepares through following method: elder generation cleans the Chinese pulsatilla and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
Further, described moss extract prepares through following method: elder generation cleans moss and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
Further, described Cortex cinnamomi japonici (Ramulus Cinnamomi) extract prepares through following method: elder generation cleans cassia bark and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
The present invention also provides a kind of cosmetics; Contain long and thin hot pepper extract or Radix Pulsatillae extract or moss extract or Cortex cinnamomi japonici (Ramulus Cinnamomi) extract; Perhaps any two kinds or the two or more combinations in long and thin hot pepper extract, Radix Pulsatillae extract, moss extract and the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract; In the gross weight of cosmetics, the percentage by weight of long and thin hot pepper extract in cosmetics is 0.05%-2.0%, and the percentage by weight of Radix Pulsatillae extract in cosmetics is 0.05%-2.0%; The percentage by weight of moss extract in cosmetics is 0.01-0.5%, and the percentage by weight of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract in cosmetics is 0.01-0.5%.
Further, described long and thin hot pepper extract prepares through following method: elder generation cleans long and thin hot pepper and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
Further, described Radix Pulsatillae extract prepares through following method: elder generation cleans the Chinese pulsatilla and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
Further, described moss extract prepares through following method: elder generation cleans moss and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
Further, described Cortex cinnamomi japonici (Ramulus Cinnamomi) extract prepares through following method: elder generation cleans cassia bark and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration, the extract concentrating under reduced pressure after the filtration, freeze drying.
The present invention and prior art are compared, and its effect is actively with tangible.In order to solve the side effect that chemical preservative brings, overcome the problem that natural antiseptic agent brings cosmetics, the present invention is an object with multiple natural plants, studies its antibacterial activity and as the characteristic of cosmetic material.When with the composite long and thin hot pepper extract of suitable concentration, Radix Pulsatillae extract, moss extract and Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, not only fungies such as mould and yeast there is outstanding antibacterial activity, also have very high antibiotic universal.Physical and chemical stability influence to cosmetics is little, stimulates low than general chemical preservative.
Embodiment:
A kind of composition with antiseptic of the present invention is any two kinds or the two or more combinations in long and thin hot pepper extract or Radix Pulsatillae extract or moss extract or the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
Further, described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract is: 0.05-2.0: 0.05-2.0.
Further, described composition is the combination of long and thin hot pepper extract, moss extract, and the weight ratio of described long and thin hot pepper extract, moss extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of Radix Pulsatillae extract, moss extract, and the weight ratio of described Radix Pulsatillae extract, moss extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.01-0.5: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, moss extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5.
Further, described composition is the combination of long and thin hot pepper extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5: 0.01-0.5.
Further, described composition is the combination of Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5: 0.01-0.5.
Further; Described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5: 0.01-0.5.
The present invention also provides a kind of cosmetics; Contain any two kinds or two or more combinations in long and thin hot pepper extract or Radix Pulsatillae extract or moss extract or the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract; Gross weight in cosmetics; The percentage by weight of long and thin hot pepper extract in cosmetics is 0.05%-2.0%; The percentage by weight of Radix Pulsatillae extract in cosmetics is 0.05%-2.0%, and the percentage by weight of moss extract in cosmetics is 0.01-0.5%, and the percentage by weight of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract in cosmetics is 0.01-0.5%.
The manufacturing approach of long and thin hot pepper extract:
Long and thin hot pepper is cleaned and dried, after the oven dry, add 70% (V/V) alcohol reflux and extract three times, each 5 hours, cooling was filtered with the Whatman#5 filter paper.After the extract that filters is lower than 50 ℃ of concentrating under reduced pressure, obtain product through freeze drying.
The manufacturing approach of Radix Pulsatillae extract:
The Chinese pulsatilla is cleaned and dries, after the oven dry, add 70% (V/V) alcohol reflux and extract three times, each 5 hours, cooling was filtered with the Whatman#5 filter paper.After the extract that filters is lower than 50 ℃ of concentrating under reduced pressure, obtain product through freeze drying.
The manufacturing approach of moss extract:
Moss is cleaned and dries, after the oven dry, add 70% (V/V) alcohol reflux and extract three times, each 5 hours, cooling was filtered with the Whatman#5 filter paper.After the extract that filters is lower than 50 ℃ of concentrating under reduced pressure, obtain product through freeze drying.
The manufacturing approach of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract:
Cassia bark is cleaned and dried, after the oven dry, add 70% (V/V) alcohol reflux and extract three times, each 5 hours, cooling was filtered with the Whatman#5 filter paper.After the extract that filters is lower than 50 ℃ of concentrating under reduced pressure, obtain product through freeze drying.
The anti-corrosive properties test
After antiseptic effect is microbe inoculation, confirming to suppress the challenge test (Challenge Test) of effect, is standard with the CTFA experimental technique.
The inoculum concentration of mould and bacterium is respectively 10000cfu/g (ml) and 1000000cfu/g (ml) (CFU is a bacterium colony unit), requires mould reduction by 90% in the time of the 7th day, and bacterium reduces by 99.9%, and the bacterium number continues to descend in 28 days.That is, if the mean value of any micro organism quantity in three parallel tests of single bacterium inoculation dropped to below the 100cfu/g (ml) in the time of the 7th day, 28 days all is 0, and it is good in the challenge test then to be regarded as effect; If drop to below the 1000cfu/g (ml) in the time of the 7th day, then be regarded as scraping; If any microorganism of single bacterium inoculation, any one parallel appearance does not reach above-mentioned standard, and it is invalid that protective system then is assessed as.
Be inoculated into the cosmetics sample to bacterium and fungi, confirm that 1~28 day inhibition microorganism suppresses situation.
The bacterial classification that above-mentioned experiment is used is bacterium, mould
Above-mentioned four kinds of raw materials-long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract were with ratio 49: 49: 1: 1 forms the constituent with antiseptic.Though following instance has been introduced the present invention in detail, not to define the use category.
[instance 1]
[evaluation of product stability]
In order to confirm the stability of above-mentioned instance 1,2,3,4 cosmetic compositions, observe stability in each temperature and estimate stability over 1 month.
Its result is as shown in table 1.Can confirm antiseptic effect according to the preservative free cosmetic composition of the present invention's manufacturing.
Table 1
*NI:No?Increase
Confirm excitant
Skin irritation is through the sealing patch test, selects 20~40 years old N/R healthy men and women of skin as study subject.Being tried the position is that upper arm is inboard.
Excitant test A
The long and thin hot pepper extract, Radix Pulsatillae extract, the moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract was with 49: 49: 1: 1 forms, and contains the above-mentioned additive of 0.5 weight % in the emulsion,
The excitant test b
The long and thin hot pepper extract, Radix Pulsatillae extract, the moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract was with 49: 49: 1: 1 forms, and adds the above-mentioned additive of 0.8 weight % in the emulsion,
Excitant test C
Contain chemical preservative methyl p-hydroxybenzoate 0.2 weight %, nipasol 0.1 weight %, the emulsion of imidazolidinyl urea 0.2 weight %.
[instance 2]
Composition | A | B | C |
Betain | 2.000 | 2.000 | 2.000 |
Glycerine | 5.000 | 5.000 | 5.000 |
1, the 2-pentanediol | 2.000 | 2.000 | 2.000 |
Butanediol | 4.000 | 4.000 | 4.000 |
Adhesion agent | 8.000 | 8.000 | 8.000 |
Neutralizer | 0.100 | 0.100 | 0.100 |
Stearine | 2.000 | 2.000 | 2.000 |
The PEG-100 stearate | 2.000 | 2.000 | 2.000 |
Cetostearyl alcohol | 1.000 | 1.000 | 1.000 |
Butyrospermum parkii fat | 1.000 | 1.000 | 1.000 |
Dormant oils | 3.000 | 3.000 | 3.000 |
Dimethyl silicone polymer | 2.000 | 2.000 | 2.000 |
Essence | 0.100 | 0.100 | 0.100 |
The antiseptic constituent | 0.500 | 0.800 | - |
Methyl p-hydroxybenzoate | - | 0.2 | |
Nipasol | - | 0.1 | |
Imidazolidinyl urea | - | 0.2 | |
Water | TO?100 | TO?100 | TO?100 |
Above 3 kinds of a certain amount of things that tried are put into spot examination device, and the upper arm that spreads on the experimenter is inboard, continues 48 hours.Confirm excitant according to the erythema degree and to experimenter's enquirement.
Detailed method is following.
Smearing method: closed patch test (upper arm is inboard)
Smear number of times and time limit: sticked 24 hours, and sticked the test back and observed 24 hours.
Observing response: patch test is observed according to the term (terminology) of CTFA criterion after 30 minutes and 24 hours.
Criterion
Evaluation?Criteria:Modified?by?Frosch&Kligman?and?CTFA?guidelines
Grading?Criteria:
The?analysis?of?results?according?to?the?grade?of?mean?score
Grade | Score |
Grade I (non-stimulated scope) | Less than 1 |
Grade II (subexcite scope) | Less than 3 |
Grade III (remising sharp scope) | Less than 5 |
Grade IV (strong stimulation scope) | More than 5 |
Experimental result
Cosmetic composition of the present invention is suitably than the long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, almost non-stimulated to skin that are listed as in three kinds of excitant tests.But methyl hydroxybenzoate, nipasol, the preservative that imidazolidinyl urea is formed has been confirmed as stimulation.
Constituent of the present invention in sum is suitably to form than long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract of row.Outstanding antibacterial activity and antibiotic universal embody outstanding antiseptic effect.Also do not influence the physical and chemical stability of cosmetics, no chemical preservative causes that the possibility of skin irritation is extremely low.
Claims (21)
1. composition with antiseptic; It is characterized in that: described composition is long and thin hot pepper extract or Radix Pulsatillae extract or moss extract or Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, perhaps any two kinds or the two or more combinations in long and thin hot pepper extract, Radix Pulsatillae extract, moss extract and the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
2. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract is: 0.05-2.0: 0.05-2.0.
3. a kind of composition with antiseptic as claimed in claim 1 is characterized in that: described composition is the combination of long and thin hot pepper extract, moss extract, and the weight ratio of described long and thin hot pepper extract, moss extract is: 0.05-2.0: 0.01-0.5.
4. a kind of composition with antiseptic as claimed in claim 1 is characterized in that: described composition is the combination of long and thin hot pepper extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5.
5. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of Radix Pulsatillae extract, moss extract, and the weight ratio of described Radix Pulsatillae extract, moss extract is: 0.05-2.0: 0.01-0.5.
6. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5.
7. a kind of composition with antiseptic as claimed in claim 1 is characterized in that: described composition is the combination of moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.01-0.5: 0.01-0.5.
8. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, moss extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5.
9. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5.
10. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of long and thin hot pepper extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5: 0.01-0.5.
11. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.01-0.5: 0.01-0.5.
12. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described composition is the combination of long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract, and the weight ratio of described long and thin hot pepper extract, Radix Pulsatillae extract, moss extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract is: 0.05-2.0: 0.05-2.0: 0.01-0.5: 0.01-0.5.
13. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described long and thin hot pepper extract prepares through following method: elder generation cleans long and thin hot pepper and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
14. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described Radix Pulsatillae extract prepares through following method: elder generation cleans the Chinese pulsatilla and dries; After the oven dry; Adding alcohol reflux extracts, cools off, filters the extract concentrating under reduced pressure after the filtration, freeze drying.
15. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described moss extract prepares through following method: elder generation cleans moss and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
16. a kind of composition as claimed in claim 1 with antiseptic; It is characterized in that: described Cortex cinnamomi japonici (Ramulus Cinnamomi) extract prepares through following method: elder generation cleans cassia bark and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
17. cosmetics; It is characterized in that: contain long and thin hot pepper extract or Radix Pulsatillae extract or moss extract or Cortex cinnamomi japonici (Ramulus Cinnamomi) extract; Perhaps any two kinds or the two or more combinations in long and thin hot pepper extract, Radix Pulsatillae extract, moss extract and the Cortex cinnamomi japonici (Ramulus Cinnamomi) extract; In the gross weight of cosmetics, the percentage by weight of long and thin hot pepper extract in cosmetics is 0.05%-2.0%, and the percentage by weight of Radix Pulsatillae extract in cosmetics is 0.05%-2.0%; The percentage by weight of moss extract in cosmetics is 0.01-0.5%, and the percentage by weight of Cortex cinnamomi japonici (Ramulus Cinnamomi) extract in cosmetics is 0.01-0.5%.
18. a kind of cosmetics as claimed in claim 1; It is characterized in that: described long and thin hot pepper extract prepares through following method: elder generation cleans long and thin hot pepper and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
19. a kind of cosmetics as claimed in claim 1; It is characterized in that: described Radix Pulsatillae extract prepares through following method: elder generation cleans the Chinese pulsatilla and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
20. a kind of cosmetics as claimed in claim 1; It is characterized in that: described moss extract prepares through following method: elder generation cleans moss and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
21. a kind of cosmetics as claimed in claim 1; It is characterized in that: described Cortex cinnamomi japonici (Ramulus Cinnamomi) extract prepares through following method: elder generation cleans cassia bark and dries, and after the oven dry, adds alcohol reflux extraction, cooling, filtration; Extract concentrating under reduced pressure after the filtration, freeze drying.
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CN102379317B CN102379317B (en) | 2013-12-11 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104622732A (en) * | 2014-08-13 | 2015-05-20 | 广州天源生物科技有限公司 | Natural plant preservative containing shampoo for children |
CN104800894A (en) * | 2015-04-30 | 2015-07-29 | 重庆市海洁消毒卫生用品有限责任公司 | Formula and preparation method of human lubricant |
CN105707139A (en) * | 2014-12-23 | 2016-06-29 | 株式会社韩国人参公社 | Natural preservative composition |
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CN1038920A (en) * | 1989-05-22 | 1990-01-24 | 湖南省塞陵地区制药厂 | A kind of fruit fungus-proof antisepsis emulsion and compound method thereof |
CN1150032A (en) * | 1995-11-16 | 1997-05-21 | 李荣兴 | Composite natural synergic essence and preparing process and use thereof |
CN1220829A (en) * | 1997-12-22 | 1999-06-30 | 大连市环境科学设计研究院 | Traditional Chinese medicine plaster for prevention and treating of diseases of fruit tree scurfskin and method of preparation thereof |
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CN1038920A (en) * | 1989-05-22 | 1990-01-24 | 湖南省塞陵地区制药厂 | A kind of fruit fungus-proof antisepsis emulsion and compound method thereof |
CN1150032A (en) * | 1995-11-16 | 1997-05-21 | 李荣兴 | Composite natural synergic essence and preparing process and use thereof |
CN1220829A (en) * | 1997-12-22 | 1999-06-30 | 大连市环境科学设计研究院 | Traditional Chinese medicine plaster for prevention and treating of diseases of fruit tree scurfskin and method of preparation thereof |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104622732A (en) * | 2014-08-13 | 2015-05-20 | 广州天源生物科技有限公司 | Natural plant preservative containing shampoo for children |
CN104622732B (en) * | 2014-08-13 | 2016-01-20 | 广州天源生物科技有限公司 | A kind of hair washing for child water containing natural plant preservative |
CN105707139A (en) * | 2014-12-23 | 2016-06-29 | 株式会社韩国人参公社 | Natural preservative composition |
CN105707139B (en) * | 2014-12-23 | 2019-01-04 | 株式会社韩国人参公社 | Natural anticorrosion composition |
CN104800894A (en) * | 2015-04-30 | 2015-07-29 | 重庆市海洁消毒卫生用品有限责任公司 | Formula and preparation method of human lubricant |
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