CN104622732A - Natural plant preservative containing shampoo for children - Google Patents
Natural plant preservative containing shampoo for children Download PDFInfo
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- CN104622732A CN104622732A CN201410398400.2A CN201410398400A CN104622732A CN 104622732 A CN104622732 A CN 104622732A CN 201410398400 A CN201410398400 A CN 201410398400A CN 104622732 A CN104622732 A CN 104622732A
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Abstract
The invention discloses a natural plant preservative containing shampoo for children, which comprises sodium lauroamphoacetate, cocamidopropyl betaine, propylene glycol, glycol distearate, phenoxyethanol, caprylyl glycol and a preservative; and the shampoo is characterized in that the preservative is a plant preservative, and the plant preservative comprises the following components in parts by weight: 20-40 parts of a rhubarb extracting solution, 5-10 parts of a cassia bark extracting solution, 5-20 parts of a pericarpium granati extracting solution, 10-20 parts of a magnolia biloba extracting solution, 10-35 parts of a saxifraga stolonifera extracting solution, and 10-15 parts of a white ilicifolius extracting solution. The shampoo disclosed by the invention can be applied in the technical field of shampoos for children; and according to the invention, through the addition of the natural plant preservative, the effective reduction of the addition amount of the artificially synthesized preservative is realized, and then the safety of the shampoo for children can be further effectively guaranteed.
Description
Technical field
The present invention relates to hair washing for child water, especially a kind of hair washing for child water containing natural plant preservative.
Background technology
In prior art, the shampoo promoted for child gets more and more; A few money hair washing for child water now for main flow on market contrast as follows:
Contrast 1: shellfish parent hair washing for child essence 500ml, composition: water, cocamido propyl betaine, sodium laureth sulfate, butanediol, LAA, lauryl glucose carboxylic acid sodium, lauryl glucoside, silk gum albumen, polyquaternary ammonium salt-7, sweet leaf of Herba Origani extract (Origanum majorana), beta glucan, glycyrrhizic acid dipotassium, ceteareth-60 myristyl glycol, phenoxyethanol, sodium benzoate, EDETATE SODIUM, citric acid, sodium citrate, essence.
Contrast 2: health shellfish shampoo for children 200ml, composition: water, cocamido propyl betaine, PEG-80 anhydrous sorbitol laurate, LAA, sodium laureth sulfate, lauryl methyl glucitol polyethers-10, Hydroxypropyldimonium Chloride, Polyquaternium-10, PEG-150 distearate, EDTA tetra-sodium, citric acid, sodium chloride, glycerol, betanin, essence, Herba portulacae extract, Aloe extract, Flos Chrysanthemi extract, oat leaf extract, phenoxyethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate, propyl hydroxybenzoate.
For the hair washing for child aquatic products of above-mentioned main flow, be not difficult to find out: the additive that the said goods uses is the synthetic antiseptic of the types such as sodium benzoate, phenoxyethanol, methyl hydroxybenzoate, ethyl hydroxybenzoate, butyl hydroxybenzoate, propyl hydroxybenzoate, there is certain potential safety hazard in actual use.But along with the raising of market demands, consumer wishes to use a certain amount of natural plant preservative in hair washing for child water, to reduce the use amount of synthetic antiseptic; Thus improve the safety of hair washing for child water to a certain extent.
Summary of the invention
The technical problem that the present invention solves is to provide a kind of hair washing for child water containing natural plant preservative, existing problem existing in the art can be solved, can by adding natural plant preservative, realize the addition effectively reducing synthetic antiseptic, effectively can ensure the safety of hair washing for child water further.
For solving the problems of the technologies described above, the invention provides a kind of hair washing for child water containing natural plant preservative, comprise LAA, cocamido propyl betaine, propylene glycol, glycol distearate, phenoxyethanol, caprylyl glycol and antiseptic, it is characterized in that; Described antiseptic is plant antiseptic agent, and described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 20-40 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5-10 weight portion;
Pericarpium Granati extracting solution 5-20 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10-20 weight portion;
Herba Saxifragae extracting solution 10-35 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10-15 weight portion;
The preparation technology of described Radix Et Rhizoma Rhei extract comprises and to be pulverized by Radix Et Rhizoma Rhei dry tablet and to cross 100 mesh sieves, and adds the ethanol extraction agent that concentration is 70%, carries out the ultrasonic Treatment operation of 35min; Carry out the operation of constant temperature reflux, extract, reflux temperature is 60 DEG C, and the time is 1h; Radix Et Rhizoma Rhei extract is obtained after finally extracting liq being carried out vacuum filtration, distilling under reduced pressure concentration operation;
The preparation technology of described Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution comprises and to be pulverized by Cortex cinnamomi japonici (Ramulus Cinnamomi) and to cross 60 mesh sieves, and adds the ethanol extract that concentration is 70%, and solid-liquid ratio is 1g: 10ml; Filter after lixiviate under 60 DEG C of temperature conditions, after extraction time 8h, obtain filtrate, obtain Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution by after filtrate evaporation and concentration;
The preparation technology of described Pericarpium Granati extracting solution comprises and to be pulverized by Pericarpium Granati and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 60%, solid-liquid ratio 1g: 30ml; Filter after lixiviate under 35 DEG C of temperature conditions; Obtain filtrate after extraction time 7h, obtain Pericarpium Granati extracting solution by after filtrate evaporation and concentration;
The preparation technology of described magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution comprises and to be pulverized by magnolia officinalis rehd.et wils.var.biloba rehd.et wils. and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 60%, and solid-liquid ratio is 3g: 50ml; Leaching step is carried out under 27 DEG C of temperature conditions; Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution is obtained after extraction time 10h;
The preparation technology of described Herba Saxifragae extracting solution comprises and to be pulverized by Herba Saxifragae and to cross 50 mesh sieves, and to add concentration be 80% ethanol extract, solid-liquid ratio 1g: 25ml; Under 50 DEG C of temperature conditions, carry out ultrasonic extraction operation, hyperacoustic ultrasonic power is 100W; Herba Saxifragae extracting solution is obtained after extraction time 35min;
The preparation technology of described thorn Acanthopanan trifoliatus (L.) Merr. extracting solution comprises and to be pulverized by thorn Acanthopanan trifoliatus (L.) Merr. and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 80%, and solid-liquid ratio is 1g: 20ml; Carry out microwave extraction operation, microwave power is 200W; Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution is obtained after extraction time 3min.
The above-mentioned hair washing for child water containing natural plant preservative, also can have following features, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 40 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 10 weight portion;
Pericarpium Granati extracting solution 10 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10 weight portion;
Herba Saxifragae extracting solution 20 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10 weight portion.
The above-mentioned hair washing for child water containing natural plant preservative, also can have following features, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 35 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5 weight portion;
Pericarpium Granati extracting solution 10 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10 weight portion;
Herba Saxifragae extracting solution 25 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 15 weight portion.
The above-mentioned hair washing for child water containing natural plant preservative, also can have following features, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 30 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5 weight portion;
Pericarpium Granati extracting solution 15 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10 weight portion;
Herba Saxifragae extracting solution 30 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10 weight portion.
The above-mentioned hair washing for child water containing natural plant preservative, also can have following features, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 25 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 10 weight portion;
Pericarpium Granati extracting solution 20 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 20 weight portion;
Herba Saxifragae extracting solution 10 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 15 weight portion.
The above-mentioned hair washing for child water containing natural plant preservative, also can have following features, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 20 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 10 weight portion;
Pericarpium Granati extracting solution 5 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 15 weight portion;
Herba Saxifragae extracting solution 35 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 15 weight portion.
Technique scheme of the present invention has following beneficial effect:
The present invention has unique function and curative effect by the active ingredient of extracting in Chinese herbal medicine, and makes full use of their good bacteria resistance functions, prepares corresponding plant antiseptic agent and hair washing for child water; Hair washing for child water provided by the invention, by adding natural plant preservative, effectively can reduce the use amount of synthetic antiseptic, effectively can reduce the potential hazard that hair washing for child water exists child.
Other features and advantages of the present invention will be set forth in the following description, and, partly become apparent from description, or understand by implementing the present invention.Object of the present invention and other advantages realize by structure specifically noted in description, claims and obtain.
Detailed description of the invention
For making the object, technical solutions and advantages of the present invention clearly understand, hereinafter will be described in detail to embodiments of the invention.It should be noted that, when not conflicting, the embodiment in the application and the feature in embodiment can combination in any mutually.
The invention provides a kind of hair washing for child water containing natural plant preservative, comprise LAA, cocamido propyl betaine, propylene glycol, glycol distearate, phenoxyethanol, caprylyl glycol and antiseptic, wherein, described antiseptic is plant antiseptic agent;
Concrete, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 20-40 weight portion; Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5-10 weight portion; Pericarpium Granati extracting solution 5-20 weight portion; Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10-20 weight portion; Herba Saxifragae extracting solution 10-35 weight portion; Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10-15 weight portion.
Accordingly, in concrete operations of the present invention, the preparation technology of each extracting solution is as described below:
The preparation technology of described Radix Et Rhizoma Rhei extract comprises and to be pulverized by Radix Et Rhizoma Rhei dry tablet and to cross 100 mesh sieves, and adds the ethanol extraction agent that concentration is 70%, carries out the ultrasonic Treatment operation of 35min; Carry out the operation of constant temperature reflux, extract, reflux temperature is 60 DEG C, and the time is 1h; Radix Et Rhizoma Rhei extract is obtained after finally extracting liq being carried out vacuum filtration, distilling under reduced pressure concentration operation;
The preparation technology of described Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution comprises and to be pulverized by Cortex cinnamomi japonici (Ramulus Cinnamomi) and to cross 60 mesh sieves, and adds the ethanol extract that concentration is 70%, and solid-liquid ratio is 1g: 10ml; Filter after lixiviate under 60 DEG C of temperature conditions, after extraction time 8h, obtain filtrate, obtain Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution by after filtrate evaporation and concentration; Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution also can obtain with Rotary Evaporators is concentrated, and preparation technology is the state of the art, repeats no more herein;
The preparation technology of described Pericarpium Granati extracting solution comprises and to be pulverized by Pericarpium Granati and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 60%, solid-liquid ratio 1g: 30ml; Filter after lixiviate under 35 DEG C of temperature conditions; Obtain filtrate after extraction time 7h, obtain Pericarpium Granati extracting solution by after filtrate evaporation and concentration;
The preparation technology of described magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution comprises and to be pulverized by magnolia officinalis rehd.et wils.var.biloba rehd.et wils. and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 60%, and solid-liquid ratio is 3g: 50ml; Leaching step is carried out under 27 DEG C of temperature conditions; Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution is obtained after extraction time 10h;
The preparation technology of described Herba Saxifragae extracting solution comprises and to be pulverized by Herba Saxifragae and to cross 50 mesh sieves, and to add concentration be 80% ethanol extract, solid-liquid ratio 1g: 25ml; Under 50 DEG C of temperature conditions, carry out ultrasonic extraction operation, hyperacoustic ultrasonic power is 100W; Herba Saxifragae extracting solution is obtained after extraction time 35min;
The preparation technology of described thorn Acanthopanan trifoliatus (L.) Merr. extracting solution comprises and to be pulverized by thorn Acanthopanan trifoliatus (L.) Merr. and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 80%, and solid-liquid ratio is 1g: 20ml; Carry out microwave extraction operation, microwave power is 200W; Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution is obtained after extraction time 3min.
In order to check the anti-microbial property of above-mentioned plant antiseptic agent provided by the invention further, the existing antibacterial test experimental technique by commonly using in prior art carries out following corresponding experiment test:
1, the anti-microbial property test of plant antiseptic agent;
Plant antiseptic agent: following several embodiment provided by the invention, in table 1;
The content of table 1: embodiment 1-5 illustrates (unit: weight portion)
| Sequence number | Component | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Component 1 | Radix Et Rhizoma Rhei extract | 40 | 35 | 30 | 25 | 20 |
| Component 2 | Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution | 10 | 5 | 5 | 10 | 10 |
| Component 3 | Pericarpium Granati extracting solution | 10 | 10 | 15 | 20 | 5 |
| Component 4 | Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution | 10 | 10 | 10 | 20 | 15 |
| Component 5 | Herba Saxifragae extracting solution | 20 | 25 | 30 | 10 | 35 |
| Component 6 | Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution | 10 | 15 | 10 | 15 | 15 |
Strain and condition of culture: adopt strain in specific experiment of the present invention, in table 2;
Table 2: strain explanation
| Kind | Culture medium | Condition of culture |
| Staphylococcus aureus | Nutrient agar/PCA | 30℃/48h |
| Escherichia coli | Nutrient agar/PCA | 30℃/48h |
| Pseudomonas | False unit cell agar culture medium | 25℃/48h |
| The dead circumfili bacterium of heat | STAA agar culture medium, | 30℃/48h |
Filter paper experimental procedure is sketched;
Picking cultivates the bacterium colony 2 that 24-48h is of moderate size, and sterile working adds in 9ml physiological saline solution, uses magnetic stirrer 1min, and becoming uniform is 3-5X10 containing bacterium colony
6-10
7cfu.mL
-1outstanding bacterium liquid for subsequent use; The filter paper of thickness 1.5mm being broken into diameter is 6mm disk, and after being wrapped up by filter paper, 160 DEG C of dry heat sterilization 2h are for subsequent use; Be used for each selective medium heating and melting for examination bacterium by what prepare, be poured in too heat-killed culture dish, for subsequent use after flat board solidifies; Drawing 0.2mL respectively respectively for trying bacteria suspension in plate with aseptic straw, being coated with rod with sterile glass triangle and bacteria suspension is carefully coated with evenly; Filter paper is soaked 1min respectively in plant antiseptic agent embodiment 1-5, takes out cool micro-doing and be gently affixed on flat board; Then be inverted in calorstat by plate, each bacterium cultivates 24h according to optimum temperature; The diameter mm of each inhibition zone is measured with micrometer; Bacteria used thereby suspension is down flat plate numeration simultaneously.
Test data analysis; Plant antiseptic agent embodiment 1-5 experimental data is in table 3;
Table 3: embodiment 1-5 experimental data synopsis (unit mm)
| Kind | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Staphylococcus aureus | 19.5 | 19.9 | 20.1 | 19.7 | 17.5 |
| Escherichia coli | 17.8 | 20.1 | 19.8 | 18.3 | 16.8 |
| Pseudomonas | 16.7 | 19.8 | 18.7 | 17.1 | 17.7 |
| The dead circumfili bacterium of heat | 18.6 | 20.1 | 19.6 | 18.1 | 15.6 |
| Blank group | 6.0 | 6.0 | 6.0 | 6.0 | 6.0 |
According to above-mentioned experimental data, can tentatively learn, in plant antiseptic agent embodiment 1-5 provided by the invention, anti-microbial property is embodiment 2 and embodiment 3 preferably.Further, now above-described embodiment 2, enforcement 3 are carried out control comparison experiment with plant antiseptic agent of the prior art.Need to illustrate, during prior art control experiment is analyzed, prior art contrast 1, prior art contrast 2, the embodiment of the present application 2, the application implement 3 and all choose equal-volume and carry out corresponding control experiment.Wherein,
Prior art contrast 1, is selected from application number: 200610042802.4, title: natural-plant food antiseptics; Component: extract 70 weight portion of Flos Caryophylli, extract 25 weight portion of Cortex Cinnamomi, extract 5 weight portion of Corm Eleocharitis skin; Preparation method: Flos Caryophylli, Cortex Cinnamomi, Corm Eleocharitis skin are cleaned respectively and dries, distillation extraction twice, each two hours, merge extractive liquid; Under 60 DEG C of conditions, extracting solution is added at reactor the Tween 80 that gross weight is 3%-5%, carries out fully emulsified, after the easy solubilising of the ethanol with 10%, obtain extracting solution; And then be diluted to concentration 2.0mg/ml with sterilized water, finally obtain antiseptic liquid stand-by.
Prior art contrast 2, is selected from application number: 200710191998.8, title: the natural plant source antiseptic agent applied in a kind of low-temperature meat product; Component: Flos Caryophylli powder alcohol extract 6.5 parts, Rhizoma Zingiberis Recens powder alcohol extract 1.5 parts, anistree powder extracting solution 2.0 parts.Preparation method: rear mistake 40 mesh sieve pulverized respectively by fragrant, anistree, Rhizoma Zingiberis Recens, gets minus sieve powder and extracts.Flos Caryophylli powder, Rhizoma Zingiberis Recens powder, anistree powder use 60%-95% ethanol extraction 3 hours with the solid-to-liquid ratio of 1: 10 separately, cross and filter residue, the extracting solution of three kinds of spices is concentrated into stock solution, and (stock solution refers to herein: containing the raw-material extract of 1g in 1mL extracting solution, i.e. 1g/1mL), then composite according to the volume ratio of Flos Caryophylli powder alcohol extract 6.5 parts, Rhizoma Zingiberis Recens powder alcohol extract 1.5 parts, anistree powder extracting solution 2.0 parts; Finally obtain antiseptic liquid stand-by
Repeat anti-microbial property experimental procedure, antiseptic check analysis data must be had, in table 4; Table 4: existing antiseptic check analysis table (unit mm)
According to above-mentioned prior art check analysis, known; In the application, its antibacterial effect is obviously due to the antibacterial effect of prior art contrast 1, prior art contrast 2 for the above-mentioned plant antiseptic agent embodiment that the application provides.
The above-mentioned plant antiseptic agent embodiment that the application provides, make use of the anti-microbial property that Radix Et Rhizoma Rhei, Cortex cinnamomi japonici (Ramulus Cinnamomi), Pericarpium Granati, magnolia officinalis rehd.et wils.var.biloba rehd.et wils., Herba Saxifragae and thorn Acanthopanan trifoliatus (L.) Merr. etc. are outstanding cleverly, and the natural performance of plant; In conjunction with existing scientific equipment, and carry out repeatedly creationary experiment and draw preferably extracting solution preparation method and each component ratio relation of antiseptic; Its antibacterial effect finally realized is far superior to the antibacterial effect of plant antiseptic agent of the prior art.
The anti-microbial property test of the hair washing for child water 2, containing this plant antiseptic agent;
Accordingly, the invention provides multiple hair washing for child water specific embodiment containing this plant antiseptic agent, specifically comprise shampoo embodiment 1-8; Each shampoo embodiment parameter is in table 5;
Table 5 is containing natural plant preservative shampoo parameter list
Above-mentioned multiple its preparation process of hair washing for child water provided by the invention is as described later:
By the component A mix homogeneously in parameter list, be heated to 80 DEG C; B component in parameter list is added component A successively, is heated to 85 DEG C and stirring and dissolving, constant temperature stirs 30 minutes simultaneously; Add the component C in parameter list, D successively, and stir 10 minutes; And then when being cooled to 42 DEG C, and add component E, F, G, H successively, and stir; When being cooled to 38 DEG C, sending to inspection, can use after the assay was approved.It should be noted that: above-mentioned hair washing for child water provided by the invention has carried out the examination and test of products according to QB/T 1974-2004 " shampoo (cream) ", and reaches corresponding product standard requirement.It should be noted that: in table 5, give natural plant preservative, and the antiseptic of conventional chemical synthesis, wherein activity extract adds with compound recipe, and the consumption of each material represents with mass fraction.
Now above-mentioned hair washing for child water embodiment 1-8 provided by the invention is carried out validity check by conventional preservation challenge experimental technique; Which kind of it should be noted that, the concrete conventional techniques hands section adopting method to test to be those skilled in the art; Its main purpose analyzes the mutual comparing result between above-mentioned multiple shampoo embodiment, as long as final data can reflect the mutual relation between embodiment.Concrete, preservation challenge experimental technique can be: each embodiment inoculates 6 times, inoculation in 1 week 1 time; 25ml base material adds 0.1ml strain (107-108cfu mL
-1), each embodiment is done one and is not connect the contrast of strain blank experiment simultaneously; Concrete, preservation challenge experimental data is in table 6;
Table 6: preservation challenge experimental data table
Form illustrates:
B:Bacteria antibacterial (staphylococcus aureus, addicted to root cock Salmonella, day ditch dimension enterobacteria, escherichia coli, Klebsiella pneumonia, bacillus pyocyaneus, pseudomonas fluorescens, pseudomonas putida)
M:mold mycete (Aspergillus niger, penicillium)
Y:Yeasts yeast (Candida albicans)
-: do not increase; +: slightly increase; ++: moderate increases; +++: seriously increase;
Known according to the experiment of above-mentioned preservation challenge: the shampoo embodiment 6,7,8 including plant antiseptic agent embodiment 3, ideal relative to the test result of other shampoo embodiments; Further, according to shampoo embodiment 7,8, plant antiseptic agent embodiment 3 1% and 1.2% addition, can the effect of the good bacteriostasis and sterilization of Danone; Drop in conjunction with cost, finally determine that the adding proportion of plant antiseptic agent embodiment 3 is 1%.That is, finally determine that plant antiseptic agent embodiment 3 is for effect preferably plant antiseptic agent embodiment, the hair washing for child water embodiment 7 containing this plant antiseptic agent embodiment 3 is effect preferably hair washing for child water embodiment.
Above-mentioned plant antiseptic agent provided by the invention can be used as a kind of good child care and savors antiseptic, good bacteriostasis is had to skin, hair products, life-time service safety, non-stimulated, free from extraneous odour, avirulence, without anaphylaxis, the viscosity of product can not be made, pH value changes, effectively stable under pH value widely and temperature conditions, there is longer vigor, fungus and bacterium is had to the bactericidal effect of wide spectrum.Accordingly, above-mentioned hair washing for child water provided by the invention, with natural, safety, effect, environmental protection, healthy raw material, has the formula features such as nontoxic, harmless, not carcinogenic.Mild formulation, not containing soap matter, does not stimulate the tender and lovely eyes of baby.Aim at the mild formulation close with skin PH of designed for children, seldom stimulate, with the addition of multiple nutritional components, at clean skin simultaneously, allow the tender skin of baby children remain at water profit state.Its feature is: not containing the antiseptic of chemosynthesis, in the natural plant preservative of interpolation 1%, can reach the antiseptical effect be relatively a good.
Although it is apparent to those skilled in the art that embodiment disclosed by the present invention as above, the embodiment that described content only adopts for ease of understanding the present invention, and be not used to limit the present invention.Those of skill in the art belonging to any the present invention; under the prerequisite not departing from the spirit and scope disclosed by the present invention; any amendment and change can be carried out in the form implemented and details; but scope of patent protection of the present invention, the scope that still must define with appending claims is as the criterion.
Claims (6)
1. the hair washing for child water containing natural plant preservative, comprises LAA, cocamido propyl betaine, propylene glycol, glycol distearate, phenoxyethanol, caprylyl glycol and antiseptic, it is characterized in that; Described antiseptic is plant antiseptic agent, and described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 20-40 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5-10 weight portion;
Pericarpium Granati extracting solution 5-20 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10-20 weight portion;
Herba Saxifragae extracting solution 10-35 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10-15 weight portion;
The preparation technology of described Radix Et Rhizoma Rhei extract comprises and to be pulverized by Radix Et Rhizoma Rhei dry tablet and to cross 100 mesh sieves, and adds the ethanol extraction agent that concentration is 70%, carries out the ultrasonic Treatment operation of 35min; Carry out the operation of constant temperature reflux, extract, reflux temperature is 60 DEG C, and the time is 1h; Radix Et Rhizoma Rhei extract is obtained after finally extracting liq being carried out vacuum filtration, distilling under reduced pressure concentration operation;
The preparation technology of described Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution comprises and to be pulverized by Cortex cinnamomi japonici (Ramulus Cinnamomi) and to cross 60 mesh sieves, and adds the ethanol extract that concentration is 70%, and solid-liquid ratio is 1g: 10ml; Filter after lixiviate under 60 DEG C of temperature conditions, after extraction time 8h, obtain filtrate, obtain Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution by after filtrate evaporation and concentration;
The preparation technology of described Pericarpium Granati extracting solution comprises and to be pulverized by Pericarpium Granati and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 60%, solid-liquid ratio 1g: 30ml; Filter after lixiviate under 35 DEG C of temperature conditions; Obtain filtrate after extraction time 7h, obtain Pericarpium Granati extracting solution by after filtrate evaporation and concentration;
The preparation technology of described magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution comprises and to be pulverized by magnolia officinalis rehd.et wils.var.biloba rehd.et wils. and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 60%, and solid-liquid ratio is 3g: 50ml; Leaching step is carried out under 27 DEG C of temperature conditions; Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution is obtained after extraction time 10h;
The preparation technology of described Herba Saxifragae extracting solution comprises and to be pulverized by Herba Saxifragae and to cross 50 mesh sieves, and to add concentration be 80% ethanol extract, solid-liquid ratio 1g: 25ml; Under 50 DEG C of temperature conditions, carry out ultrasonic extraction operation, hyperacoustic ultrasonic power is 100W; Herba Saxifragae extracting solution is obtained after extraction time 35min;
The preparation technology of described thorn Acanthopanan trifoliatus (L.) Merr. extracting solution comprises and to be pulverized by thorn Acanthopanan trifoliatus (L.) Merr. and to cross 50 mesh sieves, and adds the ethanol extract that concentration is 80%, and solid-liquid ratio is 1g: 20ml; Carry out microwave extraction operation, microwave power is 200W; Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution is obtained after extraction time 3min.
2. a kind of hair washing for child water containing natural plant preservative according to claim 1, it is characterized in that, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 40 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 10 weight portion;
Pericarpium Granati extracting solution 10 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10 weight portion;
Herba Saxifragae extracting solution 20 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10 weight portion.
3. a kind of hair washing for child water containing natural plant preservative according to claim 1, it is characterized in that, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 35 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5 weight portion;
Pericarpium Granati extracting solution 10 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10 weight portion;
Herba Saxifragae extracting solution 25 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 15 weight portion.
4. a kind of hair washing for child water containing natural plant preservative according to claim 1, it is characterized in that, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 30 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 5 weight portion;
Pericarpium Granati extracting solution 15 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 10 weight portion;
Herba Saxifragae extracting solution 30 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 10 weight portion.
5. a kind of hair washing for child water containing natural plant preservative according to claim 1, it is characterized in that, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 25 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 10 weight portion;
Pericarpium Granati extracting solution 20 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 20 weight portion;
Herba Saxifragae extracting solution 10 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 15 weight portion.
6. a kind of hair washing for child water containing natural plant preservative according to claim 1, it is characterized in that, described plant antiseptic agent comprises:
Radix Et Rhizoma Rhei extract 20 weight portion;
Cortex cinnamomi japonici (Ramulus Cinnamomi) extracting solution 10 weight portion;
Pericarpium Granati extracting solution 5 weight portion;
Magnolia officinalis rehd.et wils.var.biloba rehd.et wils. extracting solution 15 weight portion;
Herba Saxifragae extracting solution 35 weight portion;
Thorn Acanthopanan trifoliatus (L.) Merr. extracting solution 15 weight portion.
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| CN106937926A (en) * | 2017-03-24 | 2017-07-11 | 福建师范大学泉港石化研究院 | A kind of preparation method of the natural shampoo of anti-dandruff and itching-relieving maintenance unification |
| CN110327266A (en) * | 2019-08-09 | 2019-10-15 | 肇庆市凯捷科技有限公司 | A kind of amino acid shampoo with bacterio static itching-relieving and hair care repair function |
| CN115192476A (en) * | 2022-08-31 | 2022-10-18 | 完美（广东）日用品有限公司 | Non-irritant shampoo and shower gel and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106937926A (en) * | 2017-03-24 | 2017-07-11 | 福建师范大学泉港石化研究院 | A kind of preparation method of the natural shampoo of anti-dandruff and itching-relieving maintenance unification |
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| CN110327266A (en) * | 2019-08-09 | 2019-10-15 | 肇庆市凯捷科技有限公司 | A kind of amino acid shampoo with bacterio static itching-relieving and hair care repair function |
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| CN115192476B (en) * | 2022-08-31 | 2023-08-29 | 完美（广东）日用品有限公司 | Non-irritating shampoo bath lotion and preparation method thereof |
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| Publication number | Publication date |
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| CN104622732B (en) | 2016-01-20 |
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