CN101768536B - Quick-forming process for aged pit mud - Google Patents
Quick-forming process for aged pit mud Download PDFInfo
- Publication number
- CN101768536B CN101768536B CN2010101239609A CN201010123960A CN101768536B CN 101768536 B CN101768536 B CN 101768536B CN 2010101239609 A CN2010101239609 A CN 2010101239609A CN 201010123960 A CN201010123960 A CN 201010123960A CN 101768536 B CN101768536 B CN 101768536B
- Authority
- CN
- China
- Prior art keywords
- mud
- cellar
- gram
- yam
- storing things
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title abstract description 11
- 241000894006 Bacteria Species 0.000 claims abstract description 26
- 239000007788 liquid Substances 0.000 claims abstract description 21
- 239000001963 growth medium Substances 0.000 claims abstract description 8
- 241000193403 Clostridium Species 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 238000012258 culturing Methods 0.000 claims description 11
- 238000011081 inoculation Methods 0.000 claims description 9
- 238000005516 engineering process Methods 0.000 claims description 8
- 235000001674 Agaricus brunnescens Nutrition 0.000 claims description 7
- 239000010802 sludge Substances 0.000 claims description 7
- 229920002472 Starch Polymers 0.000 claims description 6
- 230000004913 activation Effects 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 235000019698 starch Nutrition 0.000 claims description 6
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 5
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 5
- 240000003183 Manihot esculenta Species 0.000 claims description 5
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 5
- 229910019142 PO4 Inorganic materials 0.000 claims description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 5
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 claims description 5
- 239000004202 carbamide Substances 0.000 claims description 5
- 235000013399 edible fruits Nutrition 0.000 claims description 5
- 239000008103 glucose Substances 0.000 claims description 5
- 235000012204 lemonade/lime carbonate Nutrition 0.000 claims description 5
- 239000004571 lime Substances 0.000 claims description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 5
- 239000010452 phosphate Substances 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 239000008107 starch Substances 0.000 claims description 5
- 239000002426 superphosphate Substances 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 238000000386 microscopy Methods 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 235000011837 pasties Nutrition 0.000 claims description 3
- 239000008399 tap water Substances 0.000 claims description 3
- 235000020679 tap water Nutrition 0.000 claims description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 2
- 239000011499 joint compound Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 8
- 238000003756 stirring Methods 0.000 abstract description 3
- 239000003337 fertilizer Substances 0.000 abstract 2
- 230000001580 bacterial effect Effects 0.000 abstract 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 11
- 102000004190 Enzymes Human genes 0.000 description 9
- 108090000790 Enzymes Proteins 0.000 description 9
- 238000000855 fermentation Methods 0.000 description 8
- 230000004151 fermentation Effects 0.000 description 8
- 230000032050 esterification Effects 0.000 description 7
- 238000005886 esterification reaction Methods 0.000 description 7
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 6
- 235000015096 spirit Nutrition 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 230000013368 commensalism Effects 0.000 description 3
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 2
- 230000002053 acidogenic effect Effects 0.000 description 2
- 230000002028 premature Effects 0.000 description 2
- 230000005070 ripening Effects 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- YBCVMFKXIKNREZ-UHFFFAOYSA-N acoh acetic acid Chemical compound CC(O)=O.CC(O)=O YBCVMFKXIKNREZ-UHFFFAOYSA-N 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- -1 carbon organic acid Chemical class 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000013039 cover film Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 150000002895 organic esters Chemical class 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
Images
Landscapes
- Micro-Organisms Or Cultivation Processes Thereof (AREA)
- Fertilizers (AREA)
- Storage Of Fruits Or Vegetables (AREA)
Abstract
The invention discloses a quick-forming process of aged cellar mud, which comprises the following steps: firstly, extracting and purifying clostridium bacterial liquid from old cellar mud; preparing culture medium to activate and culture pure bacteria liquid, preparing culture medium to enlarge culture of inoculated bacteria liquid, curing fertilizer mud, adding the enlarged culture bacteria liquid into the cured fertilizer mud, stirring uniformly and stacking to obtain aged cellar mud. The new process can make the pit mud in the pit wine production mature in advance by more than 10 years, and the pit wine produced by building a pit with the old pit mud cultivated by the method has the quality equivalent to that of the pit wine produced by a pit over 10 years.
Description
[technical field]
The present invention relates to a kind of cellar for storing things mud of storing in the wine production, what be specifically related to is that a kind of old cellar for storing things mud is cultivated new technology.
[background technology]
The existing wine enterprise that stores generally adopts the soil-ripening technology to cultivate artificial distiller's yeast; Build wine cellar with the cellar for storing things mud material and produce cellar for storing things wine; The quality of cellar for storing things wine (product that mainly refers to cellar for storing things wine is fragrant) is closely related with the time length of wine cellar; High-quality cellar for storing things wine, the time in Qi Jiao pond is long more, so the characteristic that how to make the new cellar for storing things mud of cultivation have old cellar for storing things mud is the difficult problem that cellar for storing things wine enterprise needs to be resolved hurrily always.The cellar for storing things wine of producing as for the Lao Jiao pond produces fragrant principle, and theory generally believes at present: wine produces in the fragrant process at the cellar for storing things, has two kinds of different fermentations, and this time length with cellar for storing things mud is directly related.
1. a fermentation is an acidogenic fermentation, and acidogenic fermentation is ubiquitous a kind of fermentation in the wine unstrained spirits of Jiao Chi, and approach is many, and it is also many to produce sour kind, and it is that cellar for storing things wine produces fragrant basis, is example with the butyric fermentation:
Starch
(hydrolysis)→ nC
6H
12O
6 (butyric bacteria, enzyme)→ CH
3(CH
2)
2COOH+2CO
2↑
CH
3CH
2OH+CH
3COOH
(condensing enzyme)→ CH
3(CH
2)
2COOH+H
2O
CH
3CH
2OH+CH
3(CH
2)
2COOH
(condensing enzyme)→ CH
3(CH
2)
4COOH+H
2O
2. a fermentation is to produce the ester fermentation; How esterification of wine unstrained spirits organic acid in the pond, cellar for storing things? Fourth, caproic acid bacteria tunning are that butyric acid, caproic acid are main in the wine unstrained spirits, also have other low carbon organic acid rather than single acetic acid (acetate) in the wine unstrained spirits; Therefore; Can only under corresponding esterification enzyme catalysis, form various low-carbon (LC) organic esters, turn to example with fourth, capronate with ethanol:
CH
3(CH
2)
2COOH+C
2H
5OH
(esterification enzyme)→ CH
3(CH
2)
2COOC
2H
5+ H
2O
CH
3(CH
2)
4COOH+C
2H
5OH
(caproic acid esterification enzyme)→ CH
3(CH
2)
4COOC
2H
5+ H
2O
What specific esterification enzyme produce when Jiao Chi ferments from? From the process of production practice and production test, draw, there is above several ways in the source of esterification enzyme: relevant with aroma-producing yeast, mainly can produce the acid esterification enzyme, and produce ETHYLE ACETATE (light odor type); Relevant with mushroom in the Daqu; Relevant with fourth, caproic acid bacteria commensalism cellar for storing things mud bacterium.
[summary of the invention]
Problem in view of known technology existence at present; The invention provides a kind of novel technique for quickly preparing aged cellar mud; Adopt this novel process can make the cellar for storing things mud in the wine production of cellar for storing things cultivate premature ripening more than 10 years; Old cellar for storing things mud with this novel process is cultivated is built wine cellar production cellar for storing things wine, and the quality of cellar for storing things wine is suitable with the cellar for storing things vinosity amount that wine cellar is produced more than 10 years.
For solving the problems of the technologies described above, the present invention takes following technical scheme to realize:
Mud rapid-result technology in a kind of old cellar for storing things the steps include: 1. to purify: it is some to extract cellar for storing things, Lao Jiao pond mud, puts into test tube, adds zero(ppm) water or tap water, on the wine lamp, boils 2-3 minute, kills other mushroom, remaining active clostridium spp; 2. activation and purebred cultivation: a. preparing culture medium; Get that half-mature yam is cut into small pieces, glucose, potassium primary phosphate, powder lime carbonate, cold boiling water mixes; Ph value of mixture is between 6.8-7.2, and proportioning raw materials is: 5000 milliliters of yam 1000 grams, glucose 3-5 gram, potassium primary phosphate 1-2 gram, powder lime carbonate 4-6 gram, cold boiling water; B. inoculation adds substratum with the bacterium liquid of purifying, and inoculation temp 50-52 ℃, to preserve 24-48 hour at room temperature 30-35 ℃ then, mixed solution produces CO
2Bubble, yam fritter float, and by 5 days-7 days, the yam fritter changed into pasty state gradually, and bacterium liquid microscopy contains just standardization of bacterium more than 100,000,000/milliliter; 3. enlarged culturing: a. preparing culture medium, to get half-mature yam or Tapioca Starch and add water, proportioning raw materials is: yam or Tapioca Starch 50 grams, add 800 milliliters in water; B. cultivate, postvaccinal bacterium liquid is added substratum, proportioning is 1: 100; Under the state of being sick of, cultivate; Inoculation temp 47-52 ℃, can hang down 10 ℃ summer, cultivated 5-6 days down at room temperature 27-30 ℃ then; 4. the fertile mud of slaking: get pond sludge or fertile mud, urea, superphosphate of lime, rotten fruit, rape cake and the some mixing of yellow water; Be sick of, moisture state stacking down; Until mud blackening brown, hear smelly; Proportioning raw materials is: 5000 gram pond sludge or fertile mud, 4-5 gram urea, 1 gram superphosphate of lime, 1 gram rotten fruit, 5 gram rape cakes; 5. rapid-result old cellar for storing things mud: the fertile mud of bacterium liquid adding slaking of enlarged culturing is mixed thoroughly, and the fertile mud of slaking keeps being sick of, the moisture state continuation was stacked more than three months, and the proportioning of the fertile mud of the bacterium liquid of enlarged culturing and slaking is 1: 100.
The cellar for storing things wine of producing based on the Lao Jiao pond produces fragrant principle, and the present invention was from the mud of old cellar for storing things, to extract and the distinctive clostridium spp of purifying in one step, then through activation and purebred cultivation, enlarged culturing; One step was to utilize pond sludge or fertile mud to carry out slaking to cultivate, and made it to contain multiple flora, formed common cellar for storing things mud; Then the former is inoculated in the mud of common cellar for storing things; Fully stir, let various mushrooms get along amiably and peacefully, commensalism is in the mud of cellar for storing things; The cellar for storing things mud of cultivation has the characteristic of old cellar for storing things mud by the way; Thereby the cellar for storing things mud premature ripening of realizing cultivating was built wine cellar production cellar for storing things wine with this kind cellar for storing things mud more than 10 years, and the quality of cellar for storing things wine is suitable with the cellar for storing things vinosity amount that wine cellar is produced more than 10 years.Thus, the present invention compared with prior art has outstanding substantive distinguishing features and obvious improvement.
[description of drawings]
The present invention has following accompanying drawing:
Fig. 1 is mushroom activation used in the present invention and purebred culture apparatus figure
[embodiment]
Embodiment: this kind novel technique for quickly preparing aged cellar mud, a step is in the Lao Jiao pond, to extract clostridium spp, carries out activation and purebred cultivation, enlarged culturing; The steps include: 1. to purify: extract cellar for storing things, Lao Jiao pond (selecting best Jiao Chi) mud 3-5 gram, put into test tube, add 5 milliliters in zero(ppm) water or tap water; On the wine lamp, boiled 2-3 minute, and killed other mushroom, remaining active clostridium spp; 2. in culture apparatus shown in Figure 1, carry out activation and purebred cultivation: in the vial 1 zero(ppm) water is housed, in the vial 2 substratum is housed, in the vial 3 aqua calcis is housed; The sealing of three vial bottlenecks, three vials communicate through conduit, a. preparing culture medium; Get that yam (half-mature) 1000 gram is cut into small pieces, glucose 3 grams, potassium primary phosphate 1 gram, powder lime carbonate 4 grams, 5000 milliliters of mixing of cold boiling water, ph value of mixture between 6.8-7.2, the b. inoculation; The bacterium liquid of purifying is added substratum; Inoculation temp 50-52 ℃, to preserve 24-48 hour at room temperature 30-35 ℃ then, the substratum mixed solution produces CO
2Bubble, yam fritter float, and it is muddy that aqua calcis becomes, and by 5 days-7 days, the yam fritter changed into pasty state gradually, and bacterium liquid microscopy contains just standardization of bacterium more than 100,000,000/milliliter; 3. enlarged culturing: a. preparing culture medium, get 50 kilograms of half-mature yam or Tapioca Starchs (half-mature) and add 800 kilograms in water, b. cultivates; Postvaccinal bacterium liquid is added substratum; Proportioning is 1: 100, under the state of being sick of, cultivates inoculation temp 47-52 ℃; Can hang down 10 ℃ summer, cultivate 5-6 days down at room temperature 27-30 ℃ then.One step was to utilize pond sludge or fertile mud to carry out slaking to cultivate, and made it to contain multiple flora, formed common cellar for storing things mud; 4. the fertile mud of slaking: get 500,000 kilograms in pond sludge or fertile mud (is example to build a workshop), add urea 400-500 kilogram, 100 kilograms of superphosphate of lime, 100 kilograms of rotten fruits, 500 kilograms of rape cakes and the some mixing of yellow water, in the state stacking down of being sick of; Cover film; Keep moistening, make the abundant growth and breeding of soil microorganisms flora, standard is that mud blackening brown, news are smelly.At last bacterium liquid is inoculated in the mud of common cellar for storing things, fully stirs, let various mushrooms get along amiably and peacefully; Commensalism is in the mud of cellar for storing things; Promptly 5. rapid-result old cellar for storing things mud: the bacterium liquid of enlarged culturing sprinkled into the fertile mud of slaking mixes thoroughly, the ratio of the bacterium liquid add-on of enlarged culturing and the fertile mud of slaking with 1: 100 for well, the fertile mud of slaking keeps being sick of, moisture state continuation stacking is more than three months; Note management, it is subsequent use to wait to build the pond, cellar for storing things.
The present invention is applicable to the cellar for storing things wine enterprise of different areas, different cellars for storing things wine producing process, different flavor.We are brewery's embodiment of the present invention in the Congjiang, Guizhou once, test for the first time, and the cellar for storing things mud that utilizes the present invention to cultivate is built three Jiao Chi, and current year's production goes out " from wine ", is cited as intermediate famous brand of wine in Guizhou, wins an immediate success; Embodiment of the present invention is built wine workshop, a cellar for storing things for the second time, also takes effect then, obtains the inside and outside favorable comment of province, produces famous brand of wine " Congjiang Daqu ", " Moon Mountain "; Implement this invention for the third time and set up new workshop, producing " the beautiful alcohol of liquid " influences bigger.
Claims (1)
1. store the rapid-result technology of mud always for one kind, the steps include: 1. to purify: it is some to extract cellar for storing things, Lao Jiao pond mud, puts into test tube, and adding zero(ppm) water or tap water boiled on the wine lamp 2-3 minute, killed other mushroom, were left active clostridium spp; 2. activation and purebred cultivation: a. preparing culture medium; Get that half-mature yam is cut into small pieces, glucose, potassium primary phosphate, powder lime carbonate, cold boiling water mixes; Ph value of mixture is between 6.8-7.2, and proportioning raw materials is: 5000 milliliters of yam 1000 grams, glucose 3-5 gram, potassium primary phosphate 1-2 gram, powder lime carbonate 4-6 gram, cold boiling water; B. inoculation adds substratum with the bacterium liquid of purifying, and inoculation temp 50-52 ℃, to preserve 24-48 hour at room temperature 30-35 ℃ then, mixed solution produces CO
2Bubble, yam fritter float, and by 5 days-7 days, the yam fritter changed into pasty state gradually, and bacterium liquid microscopy contains just standardization of bacterium more than 100,000,000/milliliter; 3. enlarged culturing: a. preparing culture medium, to get half-mature yam or Tapioca Starch and add water, proportioning raw materials is: yam or Tapioca Starch 50 grams, add 800 milliliters in water; B. cultivate, postvaccinal bacterium liquid is added substratum, proportioning is 1: 100; Under the state of being sick of, cultivate; Inoculation temp 47-52 ℃, in low 10 ℃ of summer, cultivated 5-6 days down at room temperature 27-30 ℃ then; 4. the fertile mud of slaking: get pond sludge or fertile mud, urea, superphosphate of lime, rotten fruit, rape cake and the some mixing of yellow water; Be sick of, moisture state stacking down; Until mud blackening brown, hear smelly; Proportioning raw materials is: 5000 gram pond sludge or fertile mud, 4-5 gram urea, 1 gram superphosphate of lime, 1 gram rotten fruit, 5 gram rape cakes; 5. rapid-result old cellar for storing things mud: the fertile mud of bacterium liquid adding slaking of enlarged culturing is mixed thoroughly, and the fertile mud of slaking keeps being sick of, the moisture state continuation was stacked more than three months, and the proportioning of the fertile mud of the bacterium liquid of enlarged culturing and slaking is 1: 100.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101239609A CN101768536B (en) | 2010-02-11 | 2010-02-11 | Quick-forming process for aged pit mud |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010101239609A CN101768536B (en) | 2010-02-11 | 2010-02-11 | Quick-forming process for aged pit mud |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101768536A CN101768536A (en) | 2010-07-07 |
| CN101768536B true CN101768536B (en) | 2012-04-25 |
Family
ID=42501637
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010101239609A Expired - Fee Related CN101768536B (en) | 2010-02-11 | 2010-02-11 | Quick-forming process for aged pit mud |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101768536B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102206565B (en) * | 2011-03-30 | 2014-06-18 | 姚继承 | Culture method for ecological aged cellar mud |
| CN102311902B (en) * | 2011-09-07 | 2013-03-20 | 四川省春之源酒业有限公司 | Novel culture method of Luzhou-flavor liquor pit mud |
| KR101633031B1 (en) * | 2012-03-16 | 2016-06-23 | 산토리 홀딩스 가부시키가이샤 | Method for producing mochi-koji |
| CN103173317A (en) * | 2013-04-08 | 2013-06-26 | 蒋钟璆 | Technology for copying aged pit mud |
| CN103194416A (en) * | 2013-04-24 | 2013-07-10 | 黑龙江大学 | Strong-flavor white wine pit soil caproic acid bacteria proliferation culture medium and preparation method thereof |
| CN104357308B (en) * | 2014-12-01 | 2016-05-11 | 千禾味业食品股份有限公司 | A kind of cellar for storing things vinegar maker skill |
| CN104745393B (en) * | 2015-04-08 | 2017-06-16 | 江苏洋河酒厂股份有限公司 | A kind of production method of storing soft ecology pit mud |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296071A (en) * | 1999-11-12 | 2001-05-23 | 四川沱牌曲酒股份有限公司 | Artificial distiller's yeast culturing process |
| CN1361242A (en) * | 2000-12-29 | 2002-07-31 | 江苏洋河集团有限公司 | Liquor cellar conserving nutrient liquid and its production process |
| CN101503654A (en) * | 2009-01-21 | 2009-08-12 | 江苏双沟酒业股份有限公司 | Aromatic Qu liquor pit mud and preparation thereof |
-
2010
- 2010-02-11 CN CN2010101239609A patent/CN101768536B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1296071A (en) * | 1999-11-12 | 2001-05-23 | 四川沱牌曲酒股份有限公司 | Artificial distiller's yeast culturing process |
| CN1361242A (en) * | 2000-12-29 | 2002-07-31 | 江苏洋河集团有限公司 | Liquor cellar conserving nutrient liquid and its production process |
| CN101503654A (en) * | 2009-01-21 | 2009-08-12 | 江苏双沟酒业股份有限公司 | Aromatic Qu liquor pit mud and preparation thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101768536A (en) | 2010-07-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101768536B (en) | Quick-forming process for aged pit mud | |
| CN103571766B (en) | Liquid microbial leaf fertilizer, and production method and applications thereof | |
| CN102965319B (en) | Microbial agent and bio-organic fertilizer special for winter jujube and preparation methods thereof | |
| CN102154080B (en) | Preparation method of luzhou-flavour white spirit cellar mud added with esterified liquid | |
| CN104447054A (en) | Special biological organic fertilizer for tea | |
| CN103012009B (en) | Organic acid plant soil conditioner and preparation method thereof | |
| CN109006361A (en) | A kind of production method of bio-matrix | |
| CN109180251A (en) | A kind of method of aerobic compost | |
| CN101250066A (en) | Method for producing biological leaf fertilizer by using waste molasses of sugar plant | |
| CN103621385A (en) | Long-acting full-nutritional type culture medium | |
| CN109526552A (en) | A kind of sclerotium industrial planting method of hickory chick | |
| CN104388500A (en) | Method for high density fermentation of spinosad | |
| Barzee et al. | Pilot microalgae cultivation using food waste digestate with minimal resource inputs | |
| CN105858894A (en) | Method for nitrogen abundance transformation treatment of wastewater with high ammonia nitrogen | |
| CN104860732A (en) | Microbial strain organic fertilizer for improving soil alkalinity | |
| CN104387182A (en) | Preparation method of composite nutrient soil for flowers | |
| CN105130698A (en) | Sugarcane special-purpose fertilizer | |
| CN108059562A (en) | One kind cuts leaf plantation bio-organic fertilizer special and preparation method thereof | |
| KR20120092290A (en) | Nutrient agent for plant and manufacturing method the same | |
| CN102146325B (en) | Method for culturing closed cellar mud | |
| CN102010239B (en) | Organic fertilizer and preparation method thereof | |
| CN104446722A (en) | Method for fermenting organic fertilizer | |
| CN104072222A (en) | Bio-organic fertilizer prepared by taking bagasse as major raw material | |
| CN107473907A (en) | The polynary fruit-specific fertilizer of biological organic | |
| CN101638675A (en) | Method for manufacturing citric acid by cane sugar fermentation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20120425 Termination date: 20160211 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |