CN101665251A - 一种各向同性石墨的制备方法 - Google Patents
一种各向同性石墨的制备方法 Download PDFInfo
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- CN101665251A CN101665251A CN200910068842A CN200910068842A CN101665251A CN 101665251 A CN101665251 A CN 101665251A CN 200910068842 A CN200910068842 A CN 200910068842A CN 200910068842 A CN200910068842 A CN 200910068842A CN 101665251 A CN101665251 A CN 101665251A
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 229910002804 graphite Inorganic materials 0.000 title claims abstract description 16
- 239000010439 graphite Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 9
- 239000003245 coal Substances 0.000 claims abstract description 22
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- RHZUVFJBSILHOK-UHFFFAOYSA-N anthracen-1-ylmethanolate Chemical compound C1=CC=C2C=C3C(C[O-])=CC=CC3=CC2=C1 RHZUVFJBSILHOK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000003830 anthracite Substances 0.000 claims abstract description 8
- 238000005087 graphitization Methods 0.000 claims abstract description 8
- 238000000462 isostatic pressing Methods 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 7
- 230000000630 rising effect Effects 0.000 claims description 7
- 238000007598 dipping method Methods 0.000 claims description 3
- 238000005470 impregnation Methods 0.000 claims description 2
- 235000008373 pickled product Nutrition 0.000 claims description 2
- 238000010792 warming Methods 0.000 claims description 2
- 239000002994 raw material Substances 0.000 abstract description 8
- 238000010298 pulverizing process Methods 0.000 abstract description 2
- 239000010426 asphalt Substances 0.000 abstract 2
- 238000002791 soaking Methods 0.000 abstract 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 12
- 229910052742 iron Inorganic materials 0.000 description 6
- 230000006835 compression Effects 0.000 description 4
- 238000007906 compression Methods 0.000 description 4
- 239000000470 constituent Substances 0.000 description 4
- 241001677738 Aleuron Species 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 239000005864 Sulphur Substances 0.000 description 3
- 239000011294 coal tar pitch Substances 0.000 description 3
- 238000000748 compression moulding Methods 0.000 description 3
- 230000006837 decompression Effects 0.000 description 3
- 239000007770 graphite material Substances 0.000 description 3
- 230000002706 hydrostatic effect Effects 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 239000002931 mesocarbon microbead Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000004576 sand Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 239000011305 binder pitch Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910021383 artificial graphite Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 239000011295 pitch Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
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- Carbon And Carbon Compounds (AREA)
Abstract
Description
阶段 | 升温范围(℃) | 实际升温(℃) | 持续时间(h) | 升温速度(℃/h) |
1 | 100~350 | 250 | 100 | 2.5 |
2 | 350~400 | 50 | 50 | 1 |
3 | 400~500 | 100 | 140 | 0.7 |
4 | 500~600 | 100 | 100 | 1 |
5 | 600~700 | 100 | 70 | 1.4 |
6 | 700~800 | 100 | 50 | 2 |
7 | 800~1100 | 300 | 100 | 3 |
9 | 1100±25 | 保温 | 20 |
体积密度g/cm3 | 抗压强度MPa | 抗折强度MPa | 肖氏硬度HSD | 电阻率μΩ·m |
1.87 | 104 | 42 | 63 | 13 |
阶段 | 升温范围(℃) | 实际升温(℃) | 持续时间(h) | 升温速度(℃/h) |
1 | 100~350 | 250 | 125.0 | 2 |
2 | 350~400 | 50 | 62.5 | 0.8 |
3 | 400~500 | 100 | 142.9 | 0.7 |
4 | 500~600 | 100 | 111.1 | 0.9 |
5 | 600~700 | 100 | 76.9 | 1.3 |
6 | 700~800 | 100 | 58.8 | 1.7 |
7 | 800~1200 | 300 | 133.3 | 3 |
9 | 1200±25 | 保温 | 25 |
体积密度 | 抗压强度 | 抗折强度 | 肖氏硬度 | 电阻率 |
g/cm3 | MPa | MPa | HSD | μΩ·m |
1.91 | 113 | 45 | 70 | 11 |
阶段 | 升温范围(℃) | 实际升温(℃) | 持续时间(h) | 升温速度(℃/h) |
1 | 100~350 | 250 | 104.2 | 2.4 |
2 | 350~400 | 50 | 62.5 | 0.9 |
3 | 400~500 | 100 | 142.9 | 0.7 |
4 | 500~600 | 100 | 100.0 | 1 |
5 | 600~700 | 100 | 83.3 | 1.2 |
6 | 700~800 | 100 | 52.6 | 1.9 |
7 | 800~1200 | 300 | 133.3 | 3 |
9 | 1200±25 | 保温 | 27 |
体积密度g/cm3 | 抗压强度MPa | 抗折强度MPa | 肖氏硬度HSD | 电阻率μΩ·m |
1.89 | 113 | 47 | 65 | 12 |
Claims (5)
Priority Applications (1)
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CN200910068842XA CN101665251B (zh) | 2009-05-15 | 2009-05-15 | 一种各向同性石墨的制备方法 |
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CN200910068842XA CN101665251B (zh) | 2009-05-15 | 2009-05-15 | 一种各向同性石墨的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN101665251A true CN101665251A (zh) | 2010-03-10 |
CN101665251B CN101665251B (zh) | 2012-01-04 |
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CN200910068842XA Active CN101665251B (zh) | 2009-05-15 | 2009-05-15 | 一种各向同性石墨的制备方法 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102241397A (zh) * | 2011-05-16 | 2011-11-16 | 平顶山市开元特种石墨有限公司 | 冷等静压石墨制造方法 |
CN102381700A (zh) * | 2011-07-27 | 2012-03-21 | 中钢集团吉林炭素股份有限公司 | 一种石墨材料的制造方法 |
CN102730672A (zh) * | 2012-06-21 | 2012-10-17 | 湖南省长宇新型炭材料有限公司 | 大规格特种同性石墨材料的生产工艺 |
CN103811758A (zh) * | 2014-02-19 | 2014-05-21 | 新乡市赛日新能源科技有限公司 | 一种合成石墨颗粒负极材料的制备方法 |
CN104386670A (zh) * | 2014-04-23 | 2015-03-04 | 天津锦美碳材科技发展有限公司 | 一种等静压高纯石墨材料及其制备方法 |
CN105215331A (zh) * | 2014-10-22 | 2016-01-06 | 侯玉杰 | 高强高密度各向同性浸银碳/石墨复合材料的制备方法 |
CN112624764A (zh) * | 2020-12-30 | 2021-04-09 | 巴中意科碳素股份有限公司 | 一种防止等静压石墨烧结开裂的方法 |
CN114292106A (zh) * | 2021-12-03 | 2022-04-08 | 曲阜师范大学 | 一种煤炭快速转化高质量石墨的制备方法 |
CN116332650A (zh) * | 2023-03-30 | 2023-06-27 | 青岛正望新材料股份有限公司 | 一种石墨制品的短流程近终形制造方法 |
-
2009
- 2009-05-15 CN CN200910068842XA patent/CN101665251B/zh active Active
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102241397B (zh) * | 2011-05-16 | 2013-03-13 | 平顶山市开元特种石墨有限公司 | 冷等静压石墨制造方法 |
CN102241397A (zh) * | 2011-05-16 | 2011-11-16 | 平顶山市开元特种石墨有限公司 | 冷等静压石墨制造方法 |
CN102381700A (zh) * | 2011-07-27 | 2012-03-21 | 中钢集团吉林炭素股份有限公司 | 一种石墨材料的制造方法 |
CN102381700B (zh) * | 2011-07-27 | 2013-01-23 | 中钢集团吉林炭素股份有限公司 | 一种石墨材料的制造方法 |
CN102730672A (zh) * | 2012-06-21 | 2012-10-17 | 湖南省长宇新型炭材料有限公司 | 大规格特种同性石墨材料的生产工艺 |
CN103811758B (zh) * | 2014-02-19 | 2016-04-20 | 新乡市赛日新能源科技有限公司 | 一种合成石墨颗粒负极材料的制备方法 |
CN103811758A (zh) * | 2014-02-19 | 2014-05-21 | 新乡市赛日新能源科技有限公司 | 一种合成石墨颗粒负极材料的制备方法 |
CN104386670A (zh) * | 2014-04-23 | 2015-03-04 | 天津锦美碳材科技发展有限公司 | 一种等静压高纯石墨材料及其制备方法 |
CN104386670B (zh) * | 2014-04-23 | 2016-08-24 | 天津锦美碳材科技发展有限公司 | 一种等静压高纯石墨材料及其制备方法 |
CN105215331A (zh) * | 2014-10-22 | 2016-01-06 | 侯玉杰 | 高强高密度各向同性浸银碳/石墨复合材料的制备方法 |
CN112624764A (zh) * | 2020-12-30 | 2021-04-09 | 巴中意科碳素股份有限公司 | 一种防止等静压石墨烧结开裂的方法 |
CN112624764B (zh) * | 2020-12-30 | 2022-07-29 | 巴中意科碳素股份有限公司 | 一种防止等静压石墨烧结开裂的方法 |
CN114292106A (zh) * | 2021-12-03 | 2022-04-08 | 曲阜师范大学 | 一种煤炭快速转化高质量石墨的制备方法 |
CN116332650A (zh) * | 2023-03-30 | 2023-06-27 | 青岛正望新材料股份有限公司 | 一种石墨制品的短流程近终形制造方法 |
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CN101665251B (zh) | 2012-01-04 |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
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Owner name: TANGSHAN KIMWAN SPECIAL CARBON+ GRAPHITE CO., LTD. Free format text: FORMER OWNER: TIANJIN KIMWAN SPECIAL CARBON MATERIAL TECHNOLOGY DEVELOPMENT CO., LTD. Effective date: 20111031 |
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Effective date of registration: 20111031 Address after: Nine weft road 300171 Tianjin City Hedong District No. 103 building 11 layer Manhattan Applicant after: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. Address before: Nine weft road 300171 Tianjin City Hedong District No. 103 Street building 11 floor Applicant before: TIANJIN KIMWAN CARBON TECHNOLOGY AND DEVELOPMENT CO.,LTD. |
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Denomination of invention: Preparing method of isotropic graphite Effective date of registration: 20131014 Granted publication date: 20120104 Pledgee: Pudong Shanghai Development Bank Limited by Share Ltd. Tianjin branch Pledgor: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. Registration number: 2013120000044 |
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Date of cancellation: 20150123 Granted publication date: 20120104 Pledgee: Pudong Shanghai Development Bank Limited by Share Ltd. Tianjin branch Pledgor: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. Registration number: 2013120000044 |
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C56 | Change in the name or address of the patentee | ||
CP02 | Change in the address of a patent holder |
Address after: Jin Yong road 300180 Tianjin City Hedong District No. 174 building 201 Patentee after: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. Address before: Nine weft road 300171 Tianjin City Hedong District No. 103 building 11 layer Manhattan Patentee before: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. |
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C56 | Change in the name or address of the patentee | ||
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Address after: 300180 R & D building, No. 174 Jintang Road, Hedong District, Tianjin, 201 Patentee after: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. Address before: Jin Yong road 300180 Tianjin City Hedong District No. 174 building 201 Patentee before: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method for isotropic graphite Granted publication date: 20120104 Pledgee: Tangshan Branch of China Postal Savings Bank Co.,Ltd. Pledgor: TANGSHAN KIMWAN SPECIAL CARBON&GRAPHITE Co.,Ltd. Registration number: Y2024980008260 |
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