CN100543082C - 树脂组合物的组合及其使用方法 - Google Patents
树脂组合物的组合及其使用方法 Download PDFInfo
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- CN100543082C CN100543082C CNB2004800417870A CN200480041787A CN100543082C CN 100543082 C CN100543082 C CN 100543082C CN B2004800417870 A CNB2004800417870 A CN B2004800417870A CN 200480041787 A CN200480041787 A CN 200480041787A CN 100543082 C CN100543082 C CN 100543082C
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- VOZKAJLKRJDJLL-UHFFFAOYSA-N tolylenediamine group Chemical group CC1=C(C=C(C=C1)N)N VOZKAJLKRJDJLL-UHFFFAOYSA-N 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- 125000000725 trifluoropropyl group Chemical group [H]C([H])(*)C([H])([H])C(F)(F)F 0.000 description 1
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 1
- 239000005051 trimethylchlorosilane Substances 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L63/00—Compositions of epoxy resins; Compositions of derivatives of epoxy resins
- C08L63/10—Epoxy resins modified by unsaturated compounds
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- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
- H01L21/50—Assembly of semiconductor devices using processes or apparatus not provided for in a single one of the subgroups H01L21/06 - H01L21/326, e.g. sealing of a cap to a base of a container
- H01L21/56—Encapsulations, e.g. encapsulation layers, coatings
- H01L21/563—Encapsulation of active face of flip-chip device, e.g. underfilling or underencapsulation of flip-chip, encapsulation preform on chip or mounting substrate
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B15/00—Layered products comprising a layer of metal
- B32B15/02—Layer formed of wires, e.g. mesh
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
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- H01L23/00—Details of semiconductor or other solid state devices
- H01L23/28—Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection
- H01L23/29—Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection characterised by the material, e.g. carbon
- H01L23/293—Organic, e.g. plastic
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- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L24/00—Arrangements for connecting or disconnecting semiconductor or solid-state bodies; Methods or apparatus related thereto
- H01L24/01—Means for bonding being attached to, or being formed on, the surface to be connected, e.g. chip-to-package, die-attach, "first-level" interconnects; Manufacturing methods related thereto
- H01L24/26—Layer connectors, e.g. plate connectors, solder or adhesive layers; Manufacturing methods related thereto
- H01L24/28—Structure, shape, material or disposition of the layer connectors prior to the connecting process
- H01L24/29—Structure, shape, material or disposition of the layer connectors prior to the connecting process of an individual layer connector
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2224/00—Indexing scheme for arrangements for connecting or disconnecting semiconductor or solid-state bodies and methods related thereto as covered by H01L24/00
- H01L2224/73—Means for bonding being of different types provided for in two or more of groups H01L2224/10, H01L2224/18, H01L2224/26, H01L2224/34, H01L2224/42, H01L2224/50, H01L2224/63, H01L2224/71
- H01L2224/732—Location after the connecting process
- H01L2224/73201—Location after the connecting process on the same surface
- H01L2224/73203—Bump and layer connectors
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- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
- H01L2924/01—Chemical elements
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- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
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- H01L2924/1025—Semiconducting materials
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- Y10T428/31511—Of epoxy ether
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Abstract
Description
项号# | 前分散体组成 | 最终分散体浓度 | 分散稳定性 |
(PTS<sup>*</sup>/100g SiO2) | (wt%SiO2)/wt%总固体) | (在甲氧基丙醇中) | |
1 | 0.028m/100g | 50%SiO2/63% | 沉淀 |
2 | 0.056m/100g | 47%SiO2/60% | 沉淀 |
3 | 0.13m/100g | 53%SiO2/66% | 稳定,透明 |
4 | 0.13m/100g | 60%SiO2/75% | 稳定,透明 |
5 | 0.19m/100g | 50%SiO2/63% | 稳定,透明 |
(在甲氧基丙醇乙酸酯中) | |||
6 | 0.13m/100g | 50%SiO2/63% | 沉淀 |
7 | 0.19m/100g | 50%SiO2/63% | 稳定,透明 |
项号# | 环氧化物(g)<sup>*</sup> | 硬化剂<sup>**</sup>(g) | 溶剂<sup>***</sup>(g) | 催化剂<sup>****</sup>(g) | FCS量<sup>*****</sup> | Tg<sup>******</sup> |
1 | ECN(3.55) | T758(1.73) | MeOPrOH(2) | TPP(0.12) | 0 | 168 |
2 | ECN(3.55) | T758(1.73) | MeOPrOH(2) | TPP(0.06) | 0 | 165 |
3 | ECN(3.55) | T758(1.73) | MeOPrOH(2) | NMI(0.015) | 0 | 199 |
4 | ECN(3.55) | T758(1.73) | MeOPrOH(2) | NMI(0.018) | 5 | 80 |
5 | ECN(3.55)Epon1002F(0.5) | 758(1.73) | MeOPrOH(2) | TPP(0.06) | 0 | 36 |
6 | ECN(3.55)Epon 1002F(0.5) | T758(1.73) | MeOPrOH(2) | NMI(0.03) | 0 | 84 |
ECN(3.55) | T758(1.73) | BuAc(2) | TPP(0.12) | 5 | 71 | |
8 | ECN(3.55) | 758(1.73) | 二甘醇二甲醚 | TPP(0.12) | 5 | 71 |
9 | ECN(3.55) | T758(1.73) | BuAc(2) | DiBSn(0.12) | 5 | 04 |
项# | T<sub>g</sub>下的CTE(μm/m℃) | T<sub>g</sub>上的CTE(μm/m℃) |
未填充树脂 | 70 | 210 |
表2,项1(TPP含量0.015g) | 46 | 123 |
表3,项3(NMI含量0.0075g) | 40 | 108 |
项号# | 前分散体组成 | 最终分散体浓度(粒度) | 分散稳定性 |
(PTS/100g SiO2) | (wt%SiO2) | (在甲氧基丙醇中) | |
1 | 0.067m/100g | 47%SiO2-50nm | 勉强稳定 |
2 | 0.0838m/100g | 50%SiO2-50nm | 稳定 |
3 | 0.134/100g | 50%SiO2-50nm | 稳定 |
4 | 0.268m/100g | 50%SiO2-50nm | 稳定 |
5 | 0.134/100g | 47%SiO2-50nm | 稳定 |
6 | 0.134/100g | 50%SiO2-20nm | 稳定 |
样品# | 填料*(Wt%SiO2) | EpoxyA(g)<sup>**</sup> | EpoxyB(g)<sup>**</sup> | 硬化剂A(g)<sup>***</sup> | 硬化剂B(g)<sup>***</sup> | 甲氧基丙醇(g) | 催化剂(%)<sup>***</sup><sup>*</sup> |
l | 0 | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
2 | Denka40 | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
3 | 表4,#6(50) | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
4 | 表4,#6(10) | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
5 | 表4,#6(15) | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
6 | 表4,#1(20) | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
7 | 表4,#1(30) | ECN(5.3) | - | Tamanol(2.6) | - | 3 | 0.14 |
8 | 表4,#1(30) | ECN(5.0) | UVR6105(0.475) | HRJ(2.6) | - | 3 | 0.14 |
9 | 表4,#1(60) | ECN(5.0) | UVR6105(0.475) | HRJ(2.6) | - | 3 | 0.14 |
10 | 表4,#1(50) | ECN(4.5) | UVR6105(0.945) | HRJ(2.6) | - | 3 | 0.14 |
11 | 表4,#1(50) | ECN(4.0) | UVR6105(1.52) | HRJ(2.6) | - | 3 | 0.14 |
12 | 表4, | ECN(4.9) | - | Tamanol | - | 2.7 | 0.14 |
#5(10) | (2.4) | - | |||||
13 | 表4,#5(20) | ECN(4.9) | - | Tamanol(2.4) | - | 2.7 | 0.14 |
14 | 表4,#5(30) | ECN(4.9) | - | Tamanol.(2.4) | - | 2.7 | 0.14 |
15 | 表4,#5(40) | ECN(4.9) | - | Tamanol(2.4) | - | 2.7 | 0.14 |
16 | 表4,#5(50) | ECN(4.9) | - | Tamanol(2.4) | - | 2.7 | 0.14 |
17 | 表4,#5(50) | ECN(2.2) | DER732(0.4) | Tamanol(1.2) | - | 1.4 | 0.14 |
18 | 表4,#5(50) | ECN(2.2) | DER736(0.3) | Tamanol(1.2) | - | 1.4 | 0.14 |
19 | 表4,#5(30) | ECN(2.8) | - | Tamanol(1.1) | 氢醌(0.5) | 1.6 | 0.14 |
20 | 表4,#5(40) | ECN(2.4) | - | Tamanol(0.9) | 氢醌(0.5) | 1.3 | 0.14 |
21 | 表4,#5(30) | ECN(2.8) | - | Tamanol(1.1) | 间苯二酚(0.5) | 1.6 | 0.14 |
22 | 表4,#5(40) | ECN(2.4) | - | Tamanol(0.9) | 间苯二酚(0.5) | 1.3 | 0.14 |
祥品# | 材料 | T<sub>g</sub><sup>*</sup> | B-阶段<sup>**</sup> | 透明度<sup>***</sup> | 焊接球的坍塌<sup>****</sup> |
1 | 表5,#1 | 190 | 坚硬 | 透明 | 完全坍塌(极好) |
2 | 表5,#2 | 193 | 坚硬 | 不透明 | 完全坍塌(极好) |
3 | 表5,#3 | 184 | 坚硬 | 透明 | 不坍塌(非常差) |
4 | 表5,#4 | 185 | 坚硬 | 透明 | 完全坍塌(良好) |
5 | 表5,#5 | - | 坚硬 | 透明 | 勉强坍塌(差) |
6 | 表5,#6 | - | 坚硬 | 半透明 | 完全坍塌(极好) |
7 | 表5,#7 | 180 | 坚硬 | 半透明 | 勉强坍塌,可接受 |
8 | 表5,#8 | 158 | 坚硬 | 透明 | 完全坍塌(极好) |
9 | 表5,#9 | 153 | 坚硬 | 透明 | 完全坍塌(极好) |
10 | 表5,#10 | 160 | 坚硬 | 透明 | 完全坍塌(极好) |
11 | 表5,#11 | 157 | 粘性 | 透明 | 完全坍塌(极好) |
12 | 表5,#12 | 183 | 坚硬 | 半透明 | 完全坍塌(极好) |
13 | 表5,#13 | 183 | 坚硬 | 半透明 | 完全坍塌(极好) |
14 | 表5,#14 | 187 | 坚硬 | 半透明 | 完全坍塌(极好) |
15 | 表5,#15 | 190 | 坚硬 | 半透明 | 勉强坍塌,可接受 |
16 | 表5,#16 | 203 | 坚硬 | 半透明 | 勉强坍塌(差) |
17 | 表5,#17 | 163 | 坚硬 | 半透明 | 完全坍塌(极好) |
18 | 表5,#18 | 171 | 坚硬 | 半透明 | 完全坍塌(极好) |
19 | 表5,#19 | 183 | 坚硬 | 半透明 | 完全坍塌(极好) |
20 | 表5,#20 | 180 | 坚硬 | 半透明 | 完全坍塌(极好) |
21 | 表5,#21 | 177 | 坚硬 | 半透明 | 完全坍塌(极好) |
22 | 表5,#22 | 160 | 坚硬 | 半透明 | 完全坍塌(极好) |
Claims (10)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/736,946 | 2003-12-16 | ||
US10/736,946 US7022410B2 (en) | 2003-12-16 | 2003-12-16 | Combinations of resin compositions and methods of use thereof |
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CN100543082C true CN100543082C (zh) | 2009-09-23 |
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US (1) | US7022410B2 (zh) |
EP (1) | EP1697985B1 (zh) |
JP (1) | JP5096744B2 (zh) |
KR (1) | KR101152073B1 (zh) |
CN (1) | CN100543082C (zh) |
DE (1) | DE602004005753T2 (zh) |
MY (1) | MY138890A (zh) |
TW (1) | TWI379864B (zh) |
WO (1) | WO2005062369A1 (zh) |
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CN105482513A (zh) * | 2014-10-11 | 2016-04-13 | 中国科学院宁波材料技术与工程研究所 | 油墨用玻璃粉和颜料的改性分散方法及耐高温油墨 |
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US20050170188A1 (en) * | 2003-09-03 | 2005-08-04 | General Electric Company | Resin compositions and methods of use thereof |
US20060147719A1 (en) * | 2002-11-22 | 2006-07-06 | Slawomir Rubinsztajn | Curable composition, underfill, and method |
US20050181214A1 (en) * | 2002-11-22 | 2005-08-18 | John Robert Campbell | Curable epoxy compositions, methods and articles made therefrom |
US20050266263A1 (en) * | 2002-11-22 | 2005-12-01 | General Electric Company | Refractory solid, adhesive composition, and device, and associated method |
US20050014313A1 (en) * | 2003-03-26 | 2005-01-20 | Workman Derek B. | Underfill method |
US7279223B2 (en) * | 2003-12-16 | 2007-10-09 | General Electric Company | Underfill composition and packaged solid state device |
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CN105482513A (zh) * | 2014-10-11 | 2016-04-13 | 中国科学院宁波材料技术与工程研究所 | 油墨用玻璃粉和颜料的改性分散方法及耐高温油墨 |
CN105482513B (zh) * | 2014-10-11 | 2017-12-26 | 中国科学院宁波材料技术与工程研究所 | 油墨用玻璃粉和颜料的改性分散方法及耐高温油墨 |
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JP5096744B2 (ja) | 2012-12-12 |
EP1697985A1 (en) | 2006-09-06 |
WO2005062369A1 (en) | 2005-07-07 |
TW200533714A (en) | 2005-10-16 |
US20050131106A1 (en) | 2005-06-16 |
TWI379864B (en) | 2012-12-21 |
CN1918703A (zh) | 2007-02-21 |
KR101152073B1 (ko) | 2012-06-11 |
US7022410B2 (en) | 2006-04-04 |
EP1697985B1 (en) | 2007-04-04 |
MY138890A (en) | 2009-08-28 |
DE602004005753T2 (de) | 2008-01-10 |
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JP2007515524A (ja) | 2007-06-14 |
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