CN100540542C - 1,2-环氧丙烷的制备方法 - Google Patents

1,2-环氧丙烷的制备方法 Download PDF

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Publication number
CN100540542C
CN100540542C CNB2004800159614A CN200480015961A CN100540542C CN 100540542 C CN100540542 C CN 100540542C CN B2004800159614 A CNB2004800159614 A CN B2004800159614A CN 200480015961 A CN200480015961 A CN 200480015961A CN 100540542 C CN100540542 C CN 100540542C
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China
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zeolite
formed body
catalyst
reactor
obtains
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Expired - Lifetime
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CNB2004800159614A
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English (en)
Chinese (zh)
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CN1802364A (zh
Inventor
U·米勒
G·克鲁格
P·鲁道夫
J·H·特莱斯
H-G·格奥贝尔
P·巴斯勒
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB2004800159614A 2003-05-08 2004-05-10 1,2-环氧丙烷的制备方法 Expired - Lifetime CN100540542C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10320635.3 2003-05-08
DE10320635A DE10320635A1 (de) 2003-05-08 2003-05-08 Verfahren zur Herstellung von Propylenoxid

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2009101516971A Division CN101607211B (zh) 2003-05-08 2004-05-10 成型催化剂体

Publications (2)

Publication Number Publication Date
CN1802364A CN1802364A (zh) 2006-07-12
CN100540542C true CN100540542C (zh) 2009-09-16

Family

ID=33305185

Family Applications (2)

Application Number Title Priority Date Filing Date
CNB2004800159614A Expired - Lifetime CN100540542C (zh) 2003-05-08 2004-05-10 1,2-环氧丙烷的制备方法
CN2009101516971A Expired - Lifetime CN101607211B (zh) 2003-05-08 2004-05-10 成型催化剂体

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN2009101516971A Expired - Lifetime CN101607211B (zh) 2003-05-08 2004-05-10 成型催化剂体

Country Status (17)

Country Link
US (2) US7608728B2 (https=)
EP (2) EP2256110A1 (https=)
JP (1) JP4691016B2 (https=)
KR (1) KR101101016B1 (https=)
CN (2) CN100540542C (https=)
AT (1) ATE488511T1 (https=)
BR (1) BRPI0410145A (https=)
CA (1) CA2524730A1 (https=)
DE (2) DE10320635A1 (https=)
MX (1) MX280551B (https=)
MY (1) MY153225A (https=)
RU (1) RU2332409C2 (https=)
SA (1) SA04250108B1 (https=)
SG (1) SG172482A1 (https=)
TW (1) TW200505886A (https=)
WO (1) WO2004099166A1 (https=)
ZA (1) ZA200508965B (https=)

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KR101183715B1 (ko) 2004-11-18 2012-09-17 에스케이이노베이션 주식회사 과산화수소를 이용한 올레핀의 에폭시화 방법
BRPI0710797A2 (pt) 2006-04-27 2011-08-09 Sumitomo Chemical Co método para produção de óxido de propileno
JP2007314525A (ja) * 2006-04-27 2007-12-06 Sumitomo Chemical Co Ltd プロピレンオキサイドの製造方法
CN102348699A (zh) * 2009-03-13 2012-02-08 住友化学株式会社 生产烯烃氧化物的方法
KR101802535B1 (ko) 2009-07-16 2017-11-28 바스프 에스이 물로부터 아세토니트릴을 분리하는 방법
EP2504098B1 (en) * 2009-11-27 2016-07-06 Basf Se Process for the preparation of a titanium zeolite catalyst
DE102010031060A1 (de) 2010-07-07 2012-01-12 Robert Bosch Gmbh Verfahren zum Betreiben eines Sensorelements
JP5655420B2 (ja) * 2010-08-05 2015-01-21 ナガセケムテックス株式会社 酸化法によるエポキシ化合物の製造方法
MY180180A (en) * 2012-02-07 2020-11-24 Basf Se Micropowder ang molding containing zeolitic material cintaining ti and zn
US9296714B2 (en) 2012-02-07 2016-03-29 Basf Se Micropowder and molding containing a zeolitic material containing Ti and Zn
US10029244B2 (en) 2013-02-05 2018-07-24 Basf Se Process for preparing a titanium-containing zeolitic material having an MWW framework structure
KR102245980B1 (ko) 2013-04-29 2021-04-29 바스프 에스이 부분-스트림 증류
ES2685811T3 (es) 2013-07-24 2018-10-11 Basf Se Un proceso para preparar óxido de propileno
CN105764609B (zh) * 2013-07-24 2018-02-23 巴斯夫欧洲公司 制备环氧丙烷的方法
SG10201803792UA (en) 2013-07-24 2018-06-28 Basf Se Regeneration of a titanium containing zeolite
US9688648B2 (en) 2013-07-24 2017-06-27 Basf Se Process for the preparation of propylene oxide
CN105461661B (zh) * 2014-09-29 2018-07-31 中国石油化工股份有限公司 一种烯烃氧化方法
MY182496A (en) 2014-10-27 2021-01-25 Dow Global Technologies Llc Part-stream distillation
JP6685315B2 (ja) * 2015-02-13 2020-04-22 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ プロピレンのエポキシ化のためのチタンゼオライト触媒の再生方法
ES2877670T3 (es) * 2015-02-13 2021-11-17 Basf Se Procedimiento de regeneración de un catalizador de zeolita de titanio para la epoxidación de propileno
JP7018880B2 (ja) * 2016-07-29 2022-02-14 住友化学株式会社 プロピレンオキサイドの製造方法
EP3558516A1 (en) * 2016-12-20 2019-10-30 Basf Se A process for preparing an extrudable composition comprising a titanium-containing zeolitic material having framework type mww
KR102555075B1 (ko) * 2016-12-20 2023-07-12 바스프 에스이 Mww형 골격을 갖는 티타늄-함유 제올라이트 재료를 포함하는 조성물의 소성도를 감소시키기 위한 산 처리의 용도
KR102500933B1 (ko) 2017-01-18 2023-02-16 바스프 에스이 아연, 및 티타늄 함유 제올라이트를 포함하는 몰딩의 제조 방법
PL3615519T3 (pl) * 2017-04-24 2021-09-27 Basf Se Odzyskiwanie propenu przez przemywanie mieszaniną rozpuszczalnik/woda
WO2019018103A1 (en) * 2017-07-19 2019-01-24 Exxonmobil Research And Engineering Company Alkylation catalyst
CN112500371B (zh) * 2019-09-14 2023-04-11 南京延长反应技术研究院有限公司 一种强化丙烯环氧化制备环氧丙烷的无醚化系统及工艺
ES2938316T3 (es) 2020-10-21 2023-04-10 Evonik Operations Gmbh Un método para aumentar la producción de óxido de propileno de un procedimiento integrado para fabricar óxido de propileno y propilenglicol
EP4673492A2 (en) 2023-03-02 2026-01-07 Basf Se Environmenal friendly ethylene oxide, propylene oxide and downstream products
WO2024213626A1 (en) 2023-04-12 2024-10-17 Basf Se Vinyl acetate having low deuterium content

Citations (5)

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Publication number Priority date Publication date Assignee Title
US3393156A (en) * 1965-09-20 1968-07-16 Union Oil Co Pelleted zeolite compositions
US6008389A (en) * 1996-06-13 1999-12-28 Basf Aktiengesellschaft Oxidation catalyst and process for the production of epoxides from olefines, hydrogen and oxygen using said oxidation catalyst
US6066750A (en) * 1997-07-01 2000-05-23 Arco Chemical Technology, L.P. High efficiency epoxidation process
WO2002028774A2 (en) * 2000-09-29 2002-04-11 Showa Denko K. K. Crystalline mww-type titanosilicate , its preparation and use thereof for producing epoxides
US6491861B1 (en) * 1997-06-06 2002-12-10 Basf Aktiengesellschaft Process for production of a zeolite-containing molding

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IT1187661B (it) 1985-04-23 1987-12-23 Enichem Sintesi Catalizzatore a base di silicio e titanio ad elevata resistenza meccanica
IT1222868B (it) 1987-10-12 1990-09-12 Montedipe Spa Metodo per la preparazione di titanio silicaliti
GB8906726D0 (en) 1989-03-23 1989-05-10 Shell Int Research Titania extrudates
US5244650A (en) 1989-06-29 1993-09-14 Engelhard Corporation Large-pored molecular sieves with charged octahedral titanium and charged tetrahedral aluminum sites
DE69512204T2 (de) 1994-01-12 2000-05-11 E.I. Du Pont De Nemours And Co., Wilmington Sol-gel poröses mikroverbundderivat von perfluoriertem ionenaustauschpolymer und metalloxyd
US5523426A (en) * 1995-01-04 1996-06-04 Arco Chemical Technology, L.P. Integrated process for epoxidation
DE19607577A1 (de) 1996-02-29 1997-09-04 Basf Ag Netzkatalysator auf Basis von Titan- oder Vanadiumzeolithen und inerten Netzgeweben zur Beschleunigung von Oxidationsreaktionen
DE19723949A1 (de) 1997-06-06 1998-12-10 Basf Ag Verfahren zur Regenerierung eines Zeolith-Katalysators
DE19835907A1 (de) * 1998-08-07 2000-02-17 Basf Ag Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid
DE19939416A1 (de) 1999-08-20 2001-02-22 Basf Ag Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs
DE19954322A1 (de) 1999-11-10 2001-05-17 Basf Ag Oxid und Verfahren zu dessen Herstellung
FR2806084A1 (fr) * 2000-03-10 2001-09-14 Solvay Procede de fabrication d'un oxiranne
DE10135296A1 (de) * 2001-07-19 2003-01-30 Basf Ag Verfahren zur Herstellung von Propylenoxid
JP2003327581A (ja) * 2002-03-04 2003-11-19 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法
DE10232406A1 (de) 2002-07-17 2004-01-29 Basf Ag Verfahren zur Herstellung eines zeolithhaltigen Feststoffes
JP2004285055A (ja) * 2003-03-06 2004-10-14 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法
JP4639606B2 (ja) * 2003-03-06 2011-02-23 住友化学株式会社 プロピレンオキサイドの製造方法
JP2004269380A (ja) * 2003-03-06 2004-09-30 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法
JP2004269379A (ja) * 2003-03-06 2004-09-30 Sumitomo Chem Co Ltd プロピレンオキサイドの製造方法。

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3393156A (en) * 1965-09-20 1968-07-16 Union Oil Co Pelleted zeolite compositions
US6008389A (en) * 1996-06-13 1999-12-28 Basf Aktiengesellschaft Oxidation catalyst and process for the production of epoxides from olefines, hydrogen and oxygen using said oxidation catalyst
US6491861B1 (en) * 1997-06-06 2002-12-10 Basf Aktiengesellschaft Process for production of a zeolite-containing molding
US6066750A (en) * 1997-07-01 2000-05-23 Arco Chemical Technology, L.P. High efficiency epoxidation process
WO2002028774A2 (en) * 2000-09-29 2002-04-11 Showa Denko K. K. Crystalline mww-type titanosilicate , its preparation and use thereof for producing epoxides

Non-Patent Citations (2)

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Title
A novel titanosilicate with......oxidation of alkenes. peng et al.Journal of catalysis,Vol.202 No.2. 2001 *
Extremely high ...... hydrogen peroxide. peng et al.CHEM COMMUN. 2001 *

Also Published As

Publication number Publication date
EP1625118A1 (de) 2006-02-15
JP2006525283A (ja) 2006-11-09
MX280551B (es) 2010-11-03
MXPA05011803A (es) 2006-02-17
KR20060054178A (ko) 2006-05-22
TW200505886A (en) 2005-02-16
RU2005138058A (ru) 2006-06-27
SA04250108B1 (ar) 2009-12-22
US8211822B2 (en) 2012-07-03
CN101607211B (zh) 2013-06-12
CN1802364A (zh) 2006-07-12
EP2256110A1 (de) 2010-12-01
MY153225A (en) 2015-01-29
US20100003173A1 (en) 2010-01-07
WO2004099166A1 (de) 2004-11-18
CA2524730A1 (en) 2004-11-18
ATE488511T1 (de) 2010-12-15
EP1625118B1 (de) 2010-11-17
RU2332409C2 (ru) 2008-08-27
ZA200508965B (en) 2007-02-28
BRPI0410145A (pt) 2006-05-09
US20070043226A1 (en) 2007-02-22
JP4691016B2 (ja) 2011-06-01
DE502004011903D1 (de) 2010-12-30
US7608728B2 (en) 2009-10-27
SG172482A1 (en) 2011-07-28
KR101101016B1 (ko) 2011-12-29
DE10320635A1 (de) 2004-11-18
CN101607211A (zh) 2009-12-23

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