CN100478446C - 生物生产1,3-丙二醇的纯化 - Google Patents

生物生产1,3-丙二醇的纯化 Download PDF

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Publication number
CN100478446C
CN100478446C CNB2004800191639A CN200480019163A CN100478446C CN 100478446 C CN100478446 C CN 100478446C CN B2004800191639 A CNB2004800191639 A CN B2004800191639A CN 200480019163 A CN200480019163 A CN 200480019163A CN 100478446 C CN100478446 C CN 100478446C
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CN
China
Prior art keywords
product
ammediol
experience
make
exchange
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Expired - Lifetime
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CNB2004800191639A
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English (en)
Chinese (zh)
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CN1816629A (zh
Inventor
D·M·阿克森
A·W·阿尔索普
T·T·阿姆斯
L·A·楚
J·M·迪斯尼
B·C·德拉维斯
P·费茨吉邦
J·M·加迪
F·G·加拉赫尔
W·F·莱恩哈德特
J·C·利文斯
M·L·卢伊本
M·西潘
R·E·特罗特
G·M·温德特
E·K·于
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Tate And Lyle Combined Ingredients US Ltd
Primary Products Ingredients Americas LLC
EIDP Inc
Original Assignee
Tate And Lyle Combined Ingredients US Ltd
EI Du Pont de Nemours and Co
Tate and Lyle Ingredients Americas LLC
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Publication of CN1816629A publication Critical patent/CN1816629A/zh
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Publication of CN100478446C publication Critical patent/CN100478446C/zh
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/027—Nanofiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
    • B01D3/002—Processes specially adapted for distillation or rectification of fermented solutions by continuous methods
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/145—One step being separation by permeation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
    • B01D61/04—Feed pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/149—Multistep processes comprising different kinds of membrane processes selected from ultrafiltration or microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/58—Multistep processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
    • C12P7/04—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic
    • C12P7/18—Preparation of oxygen-containing organic compounds containing a hydroxy group acyclic polyhydric
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2311/00—Details relating to membrane separation process operations and control
    • B01D2311/04—Specific process operations in the feed stream; Feed pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/145—Ultrafiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/145—Ultrafiltration
    • B01D61/146—Ultrafiltration comprising multiple ultrafiltration steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B01D61/1471—Microfiltration comprising multiple microfiltration steps

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Nanotechnology (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CNB2004800191639A 2003-05-06 2004-05-05 生物生产1,3-丙二醇的纯化 Expired - Lifetime CN100478446C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US46823103P 2003-05-06 2003-05-06
US60/468,231 2003-05-06

Publications (2)

Publication Number Publication Date
CN1816629A CN1816629A (zh) 2006-08-09
CN100478446C true CN100478446C (zh) 2009-04-15

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Country Status (10)

Country Link
US (3) US7919658B2 (enExample)
EP (2) EP2239334A1 (enExample)
JP (2) JP4814794B2 (enExample)
KR (1) KR101105957B1 (enExample)
CN (1) CN100478446C (enExample)
BR (1) BRPI0410685B8 (enExample)
CA (1) CA2522928C (enExample)
DE (1) DE602004028359D1 (enExample)
TW (1) TW200506063A (enExample)
WO (1) WO2004101479A2 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI899475B (zh) * 2021-06-02 2025-10-01 日商日本觸媒股份有限公司 用於純化裝置之槽、純化裝置、化合物之製造方法及純化方法

Families Citing this family (141)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7919658B2 (en) * 2003-05-06 2011-04-05 E. I. Du Pont De Nemours And Company Purification of biologically-produced 1,3-propanediol
US20040225107A1 (en) * 2003-05-06 2004-11-11 Sunkara Hari Babu Polytrimethylene ether glycol with excellent quality from biochemically-derived 1,3-propanediol
US7888405B2 (en) 2004-01-30 2011-02-15 E. I. Du Pont De Nemours And Company Aliphatic-aromatic polyesters, and articles made therefrom
US20080103217A1 (en) * 2006-10-31 2008-05-01 Hari Babu Sunkara Polyether ester elastomer composition
US7396896B2 (en) * 2004-12-21 2008-07-08 E.I. Dupont De Nemours And Company Poly(trimethylene terephthalate) composition and shaped articles prepared therefrom
US7629396B2 (en) * 2005-02-23 2009-12-08 E.I. Du Pont De Nemours And Company Silicon-containing polytrimethylene homo- for copolyether composition
US20060189711A1 (en) * 2005-02-23 2006-08-24 Ng Howard C Silicon-containing polytrimethylene homo- or copolyether composition
EP3919543A3 (en) * 2005-04-22 2022-03-16 Mitsubishi Chemical Corporation Biomass-resource-derived polyester and production process thereof
JP5652986B2 (ja) * 2005-04-22 2015-01-14 三菱化学株式会社 ポリエステルペレット及びその貯蔵方法
JP2006328377A (ja) * 2005-04-26 2006-12-07 Mitsubishi Chemicals Corp ポリエステルペレットの貯蔵方法
JP2006328370A (ja) * 2005-04-26 2006-12-07 Mitsubishi Chemicals Corp ポリエステルの製造方法
JP2006328378A (ja) * 2005-04-26 2006-12-07 Mitsubishi Chemicals Corp ポリエステルの製造方法
JP2006328374A (ja) * 2005-04-26 2006-12-07 Mitsubishi Chemicals Corp ポリエステルの製造方法
US7161045B1 (en) 2005-08-16 2007-01-09 E. I. Du Pont De Nemours And Company Process for manufacture of polytrimethylene ether glycol
US7157607B1 (en) 2005-08-16 2007-01-02 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
JP5074678B2 (ja) * 2005-08-26 2012-11-14 株式会社堀場製作所 塩分ミスト除去装置およびこれを用いた分析装置
US7357985B2 (en) * 2005-09-19 2008-04-15 E.I. Du Pont De Nemours And Company High crimp bicomponent fibers
US20070129524A1 (en) * 2005-12-06 2007-06-07 Sunkara Hari B Thermoplastic polyurethanes comprising polytrimethylene ether soft segments
US20070128459A1 (en) * 2005-12-07 2007-06-07 Kurian Joseph V Poly(trimethylene terephthalate)/poly(alpha-hydroxy acid) films
US7666501B2 (en) * 2005-12-07 2010-02-23 E. I. Du Pont De Nemours And Company Poly(trimethylene terephthalate)/poly(alpha-hydroxy acid) bi-constituent filaments
US20070129503A1 (en) * 2005-12-07 2007-06-07 Kurian Joseph V Poly(trimethylene terephthalate)/poly(alpha-hydroxy acid) molded, shaped articles
US7164046B1 (en) 2006-01-20 2007-01-16 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US7388115B2 (en) * 2006-01-20 2008-06-17 E. I. Du Pont De Nemours And Company Manufacture of polytrimethylene ether glycol
US20070203371A1 (en) * 2006-01-23 2007-08-30 Sunkara Hari B Process for producing polytrimethylene ether glycol
TW200732292A (en) * 2006-02-01 2007-09-01 Shell Int Research A method of treating an aldehyde mixture, use of the treated aldehyde, and an alcohol
JP2009525760A (ja) * 2006-02-10 2009-07-16 デユポン・テイト・アンド・ライル・バイオ・プロダクツ・カンパニー・エルエルシー 再生ベースの生分解性１，３−プロパンジオールを含む生分解性組成物
CN105175257A (zh) * 2006-02-10 2015-12-23 杜邦塔特和莱尔生物产品有限责任公司 包括生物学基1,3-丙二醇的单酯和二酯的组合物
JP2009532506A (ja) * 2006-02-10 2009-09-10 デユポン・テイト・アンド・ライル・バイオ・プロダクツ・カンパニー・エルエルシー 生物学的ベースの１，３−プロパンジオールのモノエステルおよびジエステルを含む組成物
US20070275139A1 (en) * 2006-02-10 2007-11-29 Melissa Joerger Food compositions comprising renewably-based, biodegradable1,3-propanediol
CA2647563A1 (en) * 2006-05-17 2007-11-29 E. I. Du Pont De Nemours And Company Personal care compositions
US20080039582A1 (en) * 2006-07-28 2008-02-14 Hari Babu Sunkara Polytrimethylene ether-based polyurethane ionomers
JP5245227B2 (ja) * 2006-08-23 2013-07-24 三菱瓦斯化学株式会社 疎水性化合物の起泡による分離法
US20080175875A1 (en) * 2006-09-25 2008-07-24 Hari Babu Sunkara Cosmetic compositions
WO2008057317A1 (en) * 2006-10-27 2008-05-15 Archer-Daniels-Midland Company Processes for isolating or purifying propylene glycol, ehtylene glycol and products produced therefrom
US7531593B2 (en) 2006-10-31 2009-05-12 E.I. Du Pont De Nemours And Company Thermoplastic elastomer blend composition
US20080108845A1 (en) * 2006-11-07 2008-05-08 Hari Babu Sunkara Polytrimethylene ether glycol esters
WO2008061187A1 (en) * 2006-11-15 2008-05-22 Dupont Tate & Lyle Bio Products Company, Llc Preservative compositions comprising renewably-based, biodegradable 1,3-propanediol
US20080135662A1 (en) * 2006-12-06 2008-06-12 Chang Jing C Melt-spun elastoester multifilament yarns
US20090131625A1 (en) * 2007-11-21 2009-05-21 Kurian Joseph V Processes for making elastomeric polyester esters from post-consumer polyester
CN100999742B (zh) * 2007-01-09 2011-05-11 清华大学 一种发酵生产1，3-丙二醇的高产工艺
US7714174B2 (en) * 2007-03-27 2010-05-11 E. I. Du Pont De Nemours And Company Lower-color polytrimethylene ether glycol using hydride compounds
EP2129737B1 (en) * 2007-04-03 2012-10-17 E. I. Du Pont de Nemours and Company Heat transfer systems using mixtures of polyols and ionic liquids
CN101066906B (zh) * 2007-05-24 2010-09-08 江苏汉邦科技有限公司 四区模拟移动床分离纯化发酵液中的1,3-丙二醇的方法
WO2008156612A1 (en) * 2007-06-15 2008-12-24 Cargill, Incorporated Process for the purification of crude glycerol compositions
JP2009013094A (ja) * 2007-07-03 2009-01-22 Teijin Fibers Ltd グリコールの製造方法
CN101117306B (zh) * 2007-07-20 2011-01-19 三达膜科技（厦门）有限公司 一种1,3-丙二醇发酵液的除杂和脱盐方法
US20090043021A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US20090043017A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US20090043016A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US20090043019A1 (en) * 2007-08-06 2009-02-12 Jing-Chung Chang Flame retardant polytrimethylene terephthalate composition
US7855244B2 (en) * 2007-08-06 2010-12-21 E.I. Du Pont De Nemours And Company Flame retardant polytrimethylene terephthalate composition
BRPI0815314A2 (pt) * 2007-08-24 2017-05-09 Du Pont coposição de óleo lubrificante
BRPI0815293A2 (pt) * 2007-08-24 2017-05-09 Du Pont "composição de óleo lubrificante"
CA2696369A1 (en) * 2007-08-24 2009-03-05 E.I. Du Pont De Nemours And Company Lubrication oil compositions
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US8703681B2 (en) 2007-08-24 2014-04-22 E I Du Pont De Nemours And Company Lubrication oil compositions
DE102007048277A1 (de) * 2007-10-08 2009-04-09 Agraferm Technologies Ag Verfahren und Vorrichtung zur mikrobiellen Herstellung eines bestimmten Produktes und Methan
MX2010003758A (es) * 2007-10-09 2010-04-21 Du Pont Composiciones desodorantes.
US7919017B2 (en) * 2007-11-12 2011-04-05 E. I. Du Pont De Nemours And Company Electrical insulation fluids for use in electrical apparatus
KR101543485B1 (ko) 2007-11-30 2015-08-10 메타볼릭 익스플로러 발효 브로쓰로부터 알콜을 정제하는 방법
US20090197781A1 (en) * 2008-01-31 2009-08-06 Hari Babu Sunkara Wellbore Fluids Comprising Poly(trimethylene ether) glycol Polymers
JP5343628B2 (ja) * 2008-03-04 2013-11-13 東レ株式会社 光透過性に優れたバイオ材料由来グリコールの製造方法及びそれから得られるポリエステルの製造方法
BRPI0907558A2 (pt) 2008-05-07 2017-05-23 Du Pont composição polimérica e processo para a produção de um polímero plastificado
CA2738452C (en) 2008-10-03 2016-06-21 Metabolic Explorer Method for purifying an alcohol from a fermentation broth using a falling film, a wiped film, a thin film or a short path evaporator
CN102186912A (zh) * 2008-10-16 2011-09-14 纳幕尔杜邦公司 阻燃剂聚(对苯二甲酸丙二醇酯)组合物
JP5625334B2 (ja) * 2008-11-28 2014-11-19 東レ株式会社 ジオールまたはトリオールの製造方法
EP2358781A1 (en) 2008-12-15 2011-08-24 E. I. du Pont de Nemours and Company Copolyesters with enhanced tear strength
AU2009330405A1 (en) 2008-12-15 2010-07-01 E. I. Du Pont De Nemours And Company Polymerization of aliphatic-aromatic copolyetheresters
US20110207859A1 (en) 2008-12-15 2011-08-25 E.I.Du Pont De Nemours And Company Copolyesters with enhanced tear strength
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WO2010077905A1 (en) 2008-12-17 2010-07-08 E. I. Du Pont De Nemours And Company Poly(trimethylene terephthalate) polymer blends that have reduced whitening
JP5293157B2 (ja) * 2008-12-22 2013-09-18 東レ株式会社 ブタノールの製造方法
CA2754231A1 (en) 2009-03-03 2010-09-10 E.I. Du Pont De Nemours And Company Poly(trimethylene terephthalate) pellets with reduced oligomers and method to measure oligomer reduction
KR20180042467A (ko) * 2009-06-04 2018-04-25 게노마티카 인코포레이티드 발효액 성분들의 분리 방법
US8349955B2 (en) 2009-09-24 2013-01-08 E I Du Pont De Nemours And Company Poly(hydroxyalkanoic acid) plasticized with poly(trimethylene ether) glycol
US20110112331A1 (en) * 2009-11-09 2011-05-12 E.I. Du Pont De Nemours And Company Method for phase separation of polytrimethylene ether glycol in salt solution
WO2011062600A1 (en) 2009-11-19 2011-05-26 E. I. Du Pont De Nemours And Company Polycondensation with a kneader reactor
WO2011076690A1 (en) 2009-12-22 2011-06-30 Metabolic Explorer Method for purifying 1,2-propanediol from a fermentation broth
TWI500768B (zh) 2010-07-05 2015-09-21 代謝探索公司 由蔗糖製備１，３－丙二醇之方法
CN103119142B (zh) 2010-09-24 2015-12-02 陶氏环球技术有限责任公司 用于润滑剂的非芳族系抗氧化剂
JP2014501810A (ja) 2010-11-22 2014-01-23 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ポリ（１，３−トリメチレンテレフタレート）とポリ（１，３−トリメチレン２，６−ナフタレート）とを含むブロックコポリマー
TR201010403A2 (tr) * 2010-12-13 2012-07-23 Bsh Ev Aletleri̇ San. Ve Ti̇c. A.Ş. BEYAZ EŞYA KAPI İÇ KASASI VE DEKORATİF DlŞ YÜZEY MESAFE ELEMANI
US8247526B2 (en) 2010-12-20 2012-08-21 E I Du Pont De Nemours And Company Process for the preparation of polyalkylene ether glycol
MY163268A (en) * 2011-02-22 2017-08-30 Toray Industries Diol composition and polyester
US9018424B2 (en) 2011-03-30 2015-04-28 Toray Industries, Inc. Method of producing diol or triol
US8558037B2 (en) 2011-03-30 2013-10-15 Toray Industries, Inc. Method of producing butanol
WO2012130316A1 (en) 2011-03-31 2012-10-04 Metabolic Explorer Method for purifying mpg (monopropylene glycol) from a fermentation broth
JP5852732B2 (ja) 2011-04-13 2016-02-03 イーエルシー マネージメント エルエルシー パーソナルケア組成物用コンディショニング剤
EP2697349A4 (en) 2011-04-13 2015-01-07 Elc Man Llc SOFT ANIONIC SURFACTANTS USEFUL IN BODY HYGIENE COMPOSITIONS
WO2012155074A1 (en) * 2011-05-12 2012-11-15 Virent, Inc. Process for purifying lignocellulosic feedstocks
US8629243B2 (en) 2011-08-16 2014-01-14 E I Du Pont De Nemours And Company Variant sucrose transporter polypeptides that enable faster sucrose utilization in bacteria
CN103502303B (zh) 2011-09-06 2015-04-29 东丽株式会社 耐热性优异的聚酯和其制造方法
BR112014008195B1 (pt) 2011-10-14 2021-04-20 Toray Industries, Inc método para produzir 2,3-butanodiol
JP5755995B2 (ja) * 2011-10-26 2015-07-29 株式会社日立製作所 超臨界水を用いた反応プロセス
WO2013086160A1 (en) * 2011-12-08 2013-06-13 Oakwood Foods, Llc (D/B/A Oakwood Technologies) Continuous coolant purification process and device
US8759559B2 (en) 2012-04-18 2014-06-24 E I Du Pont De Nemours And Company Processes for preparing polytrimethylene ether glycol esters
CA2869298C (en) * 2012-04-26 2020-04-07 Toray Industries, Inc. Method for producing sugar solution
CN107602824B (zh) * 2012-06-05 2020-11-13 基因组股份公司 聚酯和聚氨基甲酸酯的制造方法
EP2857377B1 (en) 2012-06-05 2019-05-08 Mitsubishi Chemical Corporation Production method for 1, 4-butanediol
JP2012245519A (ja) * 2012-07-17 2012-12-13 Horiba Ltd 塩分ミスト除去装置およびこれを用いた分析装置
US9174902B2 (en) * 2012-08-29 2015-11-03 Archer Daniels Midland Co. Removal of organic salts from bio-derived glycol products of polyol hydrogenolysis
JP6330659B2 (ja) * 2012-12-19 2018-05-30 東レ株式会社 アルコールの製造方法
JP6048159B2 (ja) * 2013-01-22 2016-12-21 三菱化学株式会社 ポリウレタンの製造方法
CN105209414B (zh) 2013-03-15 2018-04-17 基因组股份公司 用于从发酵肉汤中获得1,4‑丁二醇的方法和系统
JP2015017087A (ja) * 2013-06-13 2015-01-29 三菱化学株式会社 ジオールの製造方法
US10035749B2 (en) * 2013-09-03 2018-07-31 Myriant Corporation Process for manufacturing acrylic acid, acrylonitrile and 1,4-butanediol from 1,3-propanediol
US9309205B2 (en) 2013-10-28 2016-04-12 Wincom, Inc. Filtration process for purifying liquid azole heteroaromatic compound-containing mixtures
PL2896628T3 (pl) 2014-01-20 2019-03-29 Jennewein Biotechnologie Gmbh Sposób wydajnego oczyszczania obojętnych oligosacharydów ludzkiego mleka (HMO) z fermentacji mikrobiologicznej
KR20160125383A (ko) 2014-02-24 2016-10-31 이 아이 듀폰 디 네모아 앤드 캄파니 가소화된 폴리아미드 조성물
JP6486020B2 (ja) * 2014-05-30 2019-03-20 三菱ケミカル株式会社 ２，３−ブタンジオールの製造方法
US10086339B2 (en) 2015-03-10 2018-10-02 The University Of Connecticut Polymers and membranes for separation of polar organic compounds from aqueous mixtures and methods of using
WO2016186122A1 (ja) * 2015-05-20 2016-11-24 東洋紡株式会社 ポリエステル樹脂
US9968531B2 (en) 2015-08-05 2018-05-15 Dupont Tate & Lyle Bio Products Company, Llc Deodorants containing 1,3-propanediol
FR3047171A1 (fr) 2016-01-29 2017-08-04 Plant Advanced Tech Pat Esters de dipropylene glycol des acides dicafeoylquiniques, extrait vegetal les contenant, procede d'obtention et utilisations
CN105777492A (zh) * 2016-04-19 2016-07-20 中石化上海工程有限公司 1,3-丙二醇的精馏提浓方法
CN105732321A (zh) * 2016-04-19 2016-07-06 中石化上海工程有限公司 1,3-丙二醇的精馏提浓装置
FR3059236B1 (fr) 2016-11-25 2019-05-17 Plant Advanced Technologies Pat Extraits de plantes du genre tagetes et leurs utilisations
CN108117481A (zh) * 2016-11-29 2018-06-05 中国石油化工股份有限公司 一种从发酵液中分离提取1,3-丙二醇的方法
CN106748648A (zh) * 2016-12-02 2017-05-31 苏州苏震生物工程有限公司 一种1,3‑丙二醇发酵液脱盐除杂系统及方法
FR3061657B1 (fr) 2017-01-09 2020-01-03 Plant Advanced Technologies Pat Preparation d’un extrait racinaire de filipendula ulmaria et utilisations cosmetiques
EP3600587A1 (en) * 2017-03-31 2020-02-05 Genomatica, Inc. Process and systems for obtaining 1,3-butanediol from fermentation broths
FR3069161B1 (fr) 2017-07-21 2019-08-30 Plant Advanced Technologies Pat Extraits racinaires de polygonum multiflorum et leurs utilisations
FR3072025B1 (fr) 2017-10-06 2019-11-01 Plant Advanced Technologies Pat Extraits racinaires de plantes du genre morus et leurs utilisations
CN107617251A (zh) * 2017-10-19 2018-01-23 苏州苏震生物工程有限公司 一种用于1,3‑丙二醇和2,3‑丁二醇发酵液预处理的设备及工艺
EP3717091A1 (en) * 2017-11-27 2020-10-07 Novamont S.p.A. Process for the production of 1,4-butanediol from renewable sources and polyesters obtained therefrom
JP7797103B2 (ja) 2018-01-30 2026-01-13 イノレックス インベストメント コーポレイション バイオ－１，２－アルカンジオールの合成のためのプロセス
KR20210024618A (ko) 2018-06-28 2021-03-05 듀폰 인더스트리얼 바이오사이언시스 유에스에이, 엘엘씨 폴리에스테르 스테이플 섬유를 포함하는 방적사 및 이를 포함하는 패브릭
DK3853197T3 (da) 2018-09-21 2024-02-12 Versalis Spa Fremgangsmåde til bio-1,3-butandiol-oprensning fra en fermenterinsbouillon
JP2023511473A (ja) 2019-11-01 2023-03-20 プリミエント コベーション エルエルシー 味質及び／又は異味質を改善する１，３－プロパンジオールの使用及び方法
CN112843762B (zh) * 2019-11-26 2024-05-24 南京华基塔业有限公司 一种由寡聚物制备丙交酯的反应系统及方法
CN114075097B (zh) * 2021-04-21 2024-06-14 广州国宏新材料有限公司 膜过滤处理1,3-丙二醇发酵液的方法和装置
CN117500777A (zh) * 2021-06-16 2024-02-02 Gs加德士公司 从发酵液中获得目标化合物的方法
CN113337548B (zh) * 2021-08-02 2022-03-22 苏州苏震生物工程有限公司 一种生物基1,3-丙二醇的制备方法
CN114249633B (zh) * 2022-01-05 2023-10-27 江苏扬农化工集团有限公司 一种分离提纯1,3-丙二醇的方法
CN118987771A (zh) * 2022-02-15 2024-11-22 北京袭明科技有限公司 一种高纯电子级乙二醇生产方法及装置
KR102810479B1 (ko) * 2022-08-04 2025-05-21 씨제이제일제당(주) 색가 모니터링을 통한 정제 공정 제어 방법 및 시스템, 및 폴리하이드록시알카노에이트 수지의 제조 방법
CA3267772A1 (en) 2022-09-16 2024-03-21 Primient Covation Llc Compositions comprising 1,3-propanediol and methods of using it to improve the sweetness and/or reduce the bitterness of sweeteners
WO2025258949A1 (ko) * 2024-06-10 2025-12-18 지에스칼텍스 주식회사 다가 알코올의 정제 방법
US20260151930A1 (en) 2024-12-04 2026-06-04 Primient Covation Llc 1,3-propanediol carrier compositions and methods of use thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6361983B1 (en) * 1999-09-30 2002-03-26 E. I. Du Pont De Nemours And Company Process for the isolation of 1,3-propanediol from fermentation broth
US20020133049A1 (en) * 2000-03-29 2002-09-19 Archer-Daniels-Midland Company Method of recovering 1,3-propanediol from fermentation broth

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4380678A (en) 1981-01-21 1983-04-19 Hydrocarbon Research, Inc. Multi-stage aldoses to polyols process
US5194159A (en) 1989-12-27 1993-03-16 Union Carbide Chemicals & Plastics Technology Corporation Treatment of lower glycol-containing operative fluids
US5034134A (en) 1989-12-27 1991-07-23 Union Carbide Chemicals And Plastics Technology Corporation Treatment of impurity-containing liquid streams in ethylene oxide/glycol processes with semi-permeable membranes
US5223144A (en) 1990-08-08 1993-06-29 First Brands Corporation Process for treatment of aqueous soluions of polyhydric alcohols
US5340909A (en) * 1991-12-18 1994-08-23 Hoechst Celanese Corporation Poly(1,3-propylene terephthalate)
DE4218282A1 (de) 1992-06-03 1993-12-09 Degussa Verfahren zur Herstellung von 1,3-Propandiol
DE4222708A1 (de) * 1992-07-10 1994-01-13 Degussa Verfahren zur Herstellung von 1,3-Propandiol
US5527973A (en) * 1994-12-16 1996-06-18 Kelsey; Donald R. Purification of 1,3-propanediol
US5686276A (en) 1995-05-12 1997-11-11 E. I. Du Pont De Nemours And Company Bioconversion of a fermentable carbon source to 1,3-propanediol by a single microorganism
CA2267198C (en) 1996-11-13 2008-06-17 E.I. Du Pont De Nemours And Company Method for the production of glycerol by recombinant organisms
ID21487A (id) 1996-11-13 1999-06-17 Du Pont Metoda pembuatan 1,3 - propandiol dengan organisme rekombinan
JP4200555B2 (ja) * 1997-10-07 2008-12-24 三菱化学株式会社 高純度エリスリトール結晶の製造方法
DE19840277A1 (de) 1998-09-04 2000-03-09 Degussa Verfahren zur Reduzierung des Gehalts an Acetalen oder Ketalen in alkoholischen Reaktionsgemischen
AU1234400A (en) 1998-10-27 2000-05-15 Cargill Incorporated Method for purifying a polyol product stream
US6245879B1 (en) 1999-01-29 2001-06-12 Shell Oil Company Purification of 1,3-propanediol in carbonyl-containing stream
US20040198965A1 (en) * 1999-04-20 2004-10-07 Cargill B.V. D-galactose isolation system
EP1220939B1 (en) 1999-09-30 2006-07-05 Cognis IP Management GmbH Improved fermentation process
US6538164B1 (en) * 1999-09-30 2003-03-25 E. I. Du Pont De Nemours And Company Recovery process for volatile compounds from solids in aqueous solution
AU2270901A (en) * 1999-12-17 2001-06-25 E.I. Du Pont De Nemours And Company Continuous process for the preparation of polytrimethylene ether glycol
EP1246861B1 (en) * 1999-12-17 2006-05-17 E.I. Du Pont De Nemours And Company Production of polytrimethylene ether glycol and copolymers thereof
WO2001073097A2 (en) 2000-03-29 2001-10-04 Archer-Daniels-Midland Company Method of recovering 1,3-propanediol from fermentation broth
CN1321959C (zh) * 2003-02-24 2007-06-20 国际壳牌研究有限公司 通过蒸馏纯化1,3－丙二醇
US7919658B2 (en) * 2003-05-06 2011-04-05 E. I. Du Pont De Nemours And Company Purification of biologically-produced 1,3-propanediol
BRPI0410686A (pt) 2003-05-06 2006-06-20 Du Pont processo e composição
US20040225107A1 (en) * 2003-05-06 2004-11-11 Sunkara Hari Babu Polytrimethylene ether glycol with excellent quality from biochemically-derived 1,3-propanediol
US7714174B2 (en) * 2007-03-27 2010-05-11 E. I. Du Pont De Nemours And Company Lower-color polytrimethylene ether glycol using hydride compounds

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6361983B1 (en) * 1999-09-30 2002-03-26 E. I. Du Pont De Nemours And Company Process for the isolation of 1,3-propanediol from fermentation broth
US20020133049A1 (en) * 2000-03-29 2002-09-19 Archer-Daniels-Midland Company Method of recovering 1,3-propanediol from fermentation broth

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI899475B (zh) * 2021-06-02 2025-10-01 日商日本觸媒股份有限公司 用於純化裝置之槽、純化裝置、化合物之製造方法及純化方法

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