CA2803420C - Process for producing microcapsules - Google Patents

Process for producing microcapsules Download PDF

Info

Publication number
CA2803420C
CA2803420C CA2803420A CA2803420A CA2803420C CA 2803420 C CA2803420 C CA 2803420C CA 2803420 A CA2803420 A CA 2803420A CA 2803420 A CA2803420 A CA 2803420A CA 2803420 C CA2803420 C CA 2803420C
Authority
CA
Canada
Prior art keywords
microcapsules
isocyanate
isocyanates
water
emulsion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA2803420A
Other languages
English (en)
French (fr)
Other versions
CA2803420A1 (en
Inventor
Wolfgang Denuell
Jutta Hotz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cognis IP Management GmbH
Original Assignee
Cognis IP Management GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cognis IP Management GmbH filed Critical Cognis IP Management GmbH
Publication of CA2803420A1 publication Critical patent/CA2803420A1/en
Application granted granted Critical
Publication of CA2803420C publication Critical patent/CA2803420C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B01J13/16—Interfacial polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/71—Monoisocyanates or monoisothiocyanates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L77/00—Compositions of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Compositions of derivatives of such polymers

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Manufacturing & Machinery (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Medicinal Preparation (AREA)
CA2803420A 2010-06-25 2011-03-05 Process for producing microcapsules Expired - Fee Related CA2803420C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10167305.1A EP2399667B1 (en) 2010-06-25 2010-06-25 Process for producing microcapsules
EP10167305.1 2010-06-25
PCT/EP2011/001098 WO2011160733A1 (en) 2010-06-25 2011-03-05 Process for producing microcapsules

Publications (2)

Publication Number Publication Date
CA2803420A1 CA2803420A1 (en) 2011-12-29
CA2803420C true CA2803420C (en) 2018-05-01

Family

ID=43242849

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2803420A Expired - Fee Related CA2803420C (en) 2010-06-25 2011-03-05 Process for producing microcapsules

Country Status (11)

Country Link
US (1) US20130095158A1 (enExample)
EP (1) EP2399667B1 (enExample)
JP (1) JP5934703B2 (enExample)
KR (1) KR101925269B1 (enExample)
CN (1) CN102958597B (enExample)
BR (1) BR112012032634B1 (enExample)
CA (1) CA2803420C (enExample)
ES (1) ES2628087T3 (enExample)
MX (1) MX341671B (enExample)
RU (1) RU2572889C2 (enExample)
WO (1) WO2011160733A1 (enExample)

Families Citing this family (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106268389A (zh) 2011-07-06 2017-01-04 哈佛学院院长等 多重乳剂和用于配制多重乳剂的技术
MX2015002649A (es) * 2012-08-28 2015-05-20 Basf Se Sistema portador para fragancias.
JP6143078B2 (ja) * 2013-05-13 2017-06-07 清水建設株式会社 模擬粉体の製造方法、及び粉体飛散状態評価方法
JP2014221012A (ja) * 2013-05-13 2014-11-27 清水建設株式会社 模擬粉体、粉体飛散状態評価方法、及び粉体取扱い施設
CN103933014B (zh) * 2013-12-31 2016-03-09 杭州师范大学 一种肿瘤细胞靶向载药微胶囊
GB2509431B (en) * 2014-03-26 2016-09-14 Rotam Agrochem Int Co Ltd Herbicidal composition, a method for its preparation and the use thereof
AR100497A1 (es) * 2014-04-29 2016-10-12 Basf Se Proceso para producir microcápsulas
RU2619331C2 (ru) * 2014-10-10 2017-05-15 Александр Александрович Кролевец Способ получения нанокапсул умифеновира (Арбидола) в альгинате натрия
WO2016061095A1 (en) * 2014-10-14 2016-04-21 President And Fellows Of Harvard College Microcapsules and uses thereof
RU2599885C2 (ru) * 2014-11-05 2016-10-20 Александр Александрович Кролевец Способ получения нанокапсул умифеновира (арбидола) в каррагинане
WO2016071152A1 (en) 2014-11-07 2016-05-12 Basf Se Process for preparing microcapsules having a polyurea shell and a lipophilic core material
ES2794652T3 (es) 2014-11-07 2020-11-18 Givaudan Sa Mejoras de o relacionadas con compuestos orgánicos
US10201795B2 (en) 2014-11-07 2019-02-12 Basf Se Microcapsules comprising hydroxyalkyl cellulose
WO2016071151A1 (en) 2014-11-07 2016-05-12 Givaudan Sa Capsule composition
US20180311124A1 (en) * 2015-11-17 2018-11-01 Conopco, Inc., D/B/A Unilever Climbazole microcapsule and hair care composition comprising surfactant and climbazole
WO2017085033A1 (en) 2015-11-18 2017-05-26 Basf Se Improvements in or relating to organic compounds
EP3170552A1 (en) 2015-11-23 2017-05-24 Basf Se Microcapsule comprising a polymeric shell and a hydrophilic or hydrophobic core material
GB201615905D0 (en) * 2016-09-19 2016-11-02 Givaudan Sa Improvements in or relating to organic compounds
EP3295929A1 (en) * 2016-09-19 2018-03-21 S.P.C.M. Sa Use of an ampholyte copolymer as colloidal stabilizer in a process of encapsulating fragrance
CN110121535B (zh) * 2016-12-27 2022-04-29 富士胶片株式会社 水分散物及其制造方法、以及图像形成方法
CN107698865B (zh) * 2017-09-14 2020-04-03 陕西理工大学 一种注塑机螺杆清洗料的制备方法
GB201804038D0 (en) * 2018-03-14 2018-04-25 Givaudan Sa Improvements in or realating to organic compounds
CN111867719A (zh) * 2018-03-23 2020-10-30 富士胶片株式会社 中空粒子的制造方法、以及造孔材料的制造方法、化妆品用粒子的制造方法及轻量化材料的制造方法
WO2019206404A1 (en) * 2018-04-24 2019-10-31 Symrise Ag Core-shell capsules prepared with linear and cyclic aliphatic polyisocyanates
CN109231400B (zh) * 2018-10-08 2021-09-21 华南理工大学 一种用于处理水体富营养化的悬浮木质素微胶囊及制备方法
WO2020164705A1 (de) * 2019-02-13 2020-08-20 Symrise Ag Verfahren zur herstellung von mikrokapseln
EP3845304A1 (en) 2019-12-30 2021-07-07 Bayer AG Capsule suspension concentrates based on polyisocyanates and biodegradable amine based cross-linker
CN111226923B (zh) * 2020-03-09 2022-04-22 上海生农生化制品股份有限公司 一种吡唑醚菌酯·喹啉铜微胶囊悬浮-悬浮剂及其制备方法
GB202003883D0 (en) 2020-03-18 2020-05-06 Givaudan Sa Consumer product
BR112022026484A2 (pt) 2020-06-26 2023-01-31 Bayer Ag Concentrados de suspensão de cápsula aquosa compreendendo grupos éster biodegradáveis
EP4190439A4 (en) * 2020-07-31 2024-08-14 Morishita Jintan Co., Ltd. METHOD FOR PRODUCING MICROCAPSULES
KR20230044009A (ko) 2020-08-06 2023-03-31 시므라이즈 아게 마이크로캡슐을 제조하기 위한 방법
EP3969165B1 (de) 2020-08-06 2024-05-15 Symrise AG Bioabbaubare polyharnstoff/polyurethan-mikrokapseln
JP7546146B2 (ja) 2020-08-06 2024-09-05 シムライズ アーゲー ポリ尿素／ポリウレタンマイクロカプセル
GB202114226D0 (en) 2021-10-05 2021-11-17 Iberchem S A U Microcapsules
WO2023148253A1 (de) 2022-02-02 2023-08-10 Symrise Ag Verfahren zur herstellung von mikrokapseln
WO2023147855A2 (de) 2022-02-02 2023-08-10 Symrise Ag Verfahren zur herstellung von mikrokapseln
WO2024038692A1 (ja) * 2022-08-19 2024-02-22 パナソニックＩｐマネジメント株式会社 リチウムイオン二次電池用の負極スラリー、リチウムイオン二次電池用の負極、およびリチウムイオン二次電池
CN117296839B (zh) * 2023-11-27 2024-02-23 山东华实药业有限公司 免活化稳定性二氧化氯消毒剂及其生产工艺
CN119257955B (zh) * 2024-08-16 2025-09-23 广东丸美生物技术股份有限公司 含美妆功能物质水溶液的微胶囊及其制备方法、化妆品

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3886085A (en) * 1971-08-31 1975-05-27 Fuji Photo Film Co Ltd Process for producing fine oil-containing microcapsules having strong protective shells and microcapsules produced thereby
US4643764A (en) * 1984-01-09 1987-02-17 Stauffer Chemical Company Multiple types of microcapsules and their production
EP0214936B1 (de) * 1985-09-13 1992-07-08 Ciba-Geigy Ag Verfahren zur Herstellung von Mikrokapseln
FR2591124B1 (fr) * 1985-12-10 1988-02-12 Rhone Poulenc Spec Chim Procede de microencapsulation par polyaddition-interfaciale.
EP0267150B1 (de) * 1986-10-23 1991-07-17 Ciba-Geigy Ag Bekämpfung von Ektoparasiten
FR2610537A1 (fr) * 1987-02-11 1988-08-12 Rhone Poulenc Chimie Procede ameliore de microencapsulation par polyaddition interfaciale
JP2929294B2 (ja) * 1989-05-30 1999-08-03 大日本インキ化学工業株式会社 顔料化されたポリウレタンポリ尿素粒子およびその製造方法
US5011885A (en) * 1989-10-27 1991-04-30 The Mead Corporation Methods for the production of microcapsules using functionalized isocyanate
US5225118A (en) * 1990-08-15 1993-07-06 Boise Cascade Corporation Process for manufacturing polyurea microcapsules and product therefrom
DE4130743A1 (de) * 1991-09-16 1993-03-18 Bayer Ag Mikrokapseln aus isocyanaten mit polyethylenoxidhaltigen gruppen
ATE167980T1 (de) * 1993-11-15 1998-07-15 Zeneca Ltd Mikrokapseln, die suspensionen von biologisch aktiven verbindungen enthalten
US5925595A (en) * 1997-09-05 1999-07-20 Monsanto Company Microcapsules with readily adjustable release rates
US6653256B1 (en) * 1999-08-24 2003-11-25 Bayer Aktiengesellschaft Microcapsule formulations
KR100854530B1 (ko) * 2000-06-05 2008-08-26 신젠타 리미티드 신규한 마이크로캡슐
CA2311192A1 (en) * 2000-06-12 2001-12-12 Harald D. H. Stover Encapsulation process using isocyanate moieties
DE10117784A1 (de) * 2001-04-10 2002-10-17 Bayer Ag Mikrokapseln
US6992047B2 (en) * 2001-04-11 2006-01-31 Monsanto Technology Llc Method of microencapsulating an agricultural active having a high melting point and uses for such materials
DE10156672A1 (de) * 2001-11-17 2003-05-28 Creavis Tech & Innovation Gmbh Verfahren zur Herstellung von Mikrokapseln
EP1517746A1 (en) * 2002-05-31 2005-03-30 McMaster University Method of encapsulating hydrophobic organic molecules in polyurea capsules
RU2347608C2 (ru) * 2003-05-11 2009-02-27 Бен-Гурион Юниверсити Оф Дзе Негев Рисерч Энд Дивелопмент Оторити Инкапсулированные эфирные масла
GB0319071D0 (en) * 2003-08-14 2003-09-17 Avecia Ltd Catalyst and process
GB0526416D0 (en) * 2005-12-23 2006-02-08 Syngenta Ltd Formulation
GB0603501D0 (en) * 2006-02-22 2006-04-05 Reaxa Ltd Catalyst
US8143345B2 (en) * 2007-12-06 2012-03-27 Prc Desoto International, Inc. Water dispersible, hydroxyl-terminated, fluorinated polyurethanes and method of preparing the same

Also Published As

Publication number Publication date
US20130095158A1 (en) 2013-04-18
EP2399667B1 (en) 2017-03-08
CN102958597A (zh) 2013-03-06
WO2011160733A1 (en) 2011-12-29
ES2628087T3 (es) 2017-08-01
KR20130121697A (ko) 2013-11-06
KR101925269B1 (ko) 2018-12-05
CA2803420A1 (en) 2011-12-29
BR112012032634B1 (pt) 2018-12-26
EP2399667A1 (en) 2011-12-28
JP5934703B2 (ja) 2016-06-15
RU2013101538A (ru) 2014-07-27
MX341671B (es) 2016-08-30
BR112012032634A2 (pt) 2018-01-23
MX2012015042A (es) 2013-06-28
CN102958597B (zh) 2015-05-13
RU2572889C2 (ru) 2016-01-20
JP2013537472A (ja) 2013-10-03

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EEER Examination request

Effective date: 20160303

MKLA Lapsed

Effective date: 20220307