CN102958597B - 制备微胶囊的方法 - Google Patents
制备微胶囊的方法 Download PDFInfo
- Publication number
- CN102958597B CN102958597B CN201180031169.8A CN201180031169A CN102958597B CN 102958597 B CN102958597 B CN 102958597B CN 201180031169 A CN201180031169 A CN 201180031169A CN 102958597 B CN102958597 B CN 102958597B
- Authority
- CN
- China
- Prior art keywords
- isocyanates
- premix
- emulsion
- microcapsules
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/14—Polymerisation; cross-linking
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/14—Polymerisation; cross-linking
- B01J13/16—Interfacial polymerisation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/71—Monoisocyanates or monoisothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L77/00—Compositions of polyamides obtained by reactions forming a carboxylic amide link in the main chain; Compositions of derivatives of such polymers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Manufacturing & Machinery (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Manufacturing Of Micro-Capsules (AREA)
- Polyurethanes Or Polyureas (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Medicinal Preparation (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10167305.1A EP2399667B1 (en) | 2010-06-25 | 2010-06-25 | Process for producing microcapsules |
| EP10167305.1 | 2010-06-25 | ||
| PCT/EP2011/001098 WO2011160733A1 (en) | 2010-06-25 | 2011-03-05 | Process for producing microcapsules |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102958597A CN102958597A (zh) | 2013-03-06 |
| CN102958597B true CN102958597B (zh) | 2015-05-13 |
Family
ID=43242849
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201180031169.8A Expired - Fee Related CN102958597B (zh) | 2010-06-25 | 2011-03-05 | 制备微胶囊的方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US20130095158A1 (enExample) |
| EP (1) | EP2399667B1 (enExample) |
| JP (1) | JP5934703B2 (enExample) |
| KR (1) | KR101925269B1 (enExample) |
| CN (1) | CN102958597B (enExample) |
| BR (1) | BR112012032634B1 (enExample) |
| CA (1) | CA2803420C (enExample) |
| ES (1) | ES2628087T3 (enExample) |
| MX (1) | MX341671B (enExample) |
| RU (1) | RU2572889C2 (enExample) |
| WO (1) | WO2011160733A1 (enExample) |
Families Citing this family (40)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103764265A (zh) | 2011-07-06 | 2014-04-30 | 哈佛学院院长等 | 多重乳剂和用于配制多重乳剂的技术 |
| RU2639909C2 (ru) * | 2012-08-28 | 2017-12-25 | Живодан Са | Система носителя для отдушки |
| JP2014221012A (ja) * | 2013-05-13 | 2014-11-27 | 清水建設株式会社 | 模擬粉体、粉体飛散状態評価方法、及び粉体取扱い施設 |
| JP6143078B2 (ja) * | 2013-05-13 | 2017-06-07 | 清水建設株式会社 | 模擬粉体の製造方法、及び粉体飛散状態評価方法 |
| CN103933014B (zh) * | 2013-12-31 | 2016-03-09 | 杭州师范大学 | 一种肿瘤细胞靶向载药微胶囊 |
| GB2509431B (en) * | 2014-03-26 | 2016-09-14 | Rotam Agrochem Int Co Ltd | Herbicidal composition, a method for its preparation and the use thereof |
| US20170042143A1 (en) * | 2014-04-29 | 2017-02-16 | Basf Se | Anionic polyvinyl alcohol copolymer as protective colloid for pesticidal polyurea microcapsules |
| RU2619331C2 (ru) * | 2014-10-10 | 2017-05-15 | Александр Александрович Кролевец | Способ получения нанокапсул умифеновира (Арбидола) в альгинате натрия |
| US20170224849A1 (en) * | 2014-10-14 | 2017-08-10 | President And Fellows Of Harvard College | Microcapsules and uses thereof |
| RU2599885C2 (ru) * | 2014-11-05 | 2016-10-20 | Александр Александрович Кролевец | Способ получения нанокапсул умифеновира (арбидола) в каррагинане |
| WO2016071153A1 (en) | 2014-11-07 | 2016-05-12 | Basf Se | Microcapsules comprising hydroxyalkyl cellulose |
| WO2016071149A1 (en) | 2014-11-07 | 2016-05-12 | Givaudan Sa | Improvements in or relating to organic compounds |
| US10307723B2 (en) | 2014-11-07 | 2019-06-04 | Basf Se | Process for preparing microcapsules having a polyurea shell and a lipophilic core material |
| CN107072925B (zh) | 2014-11-07 | 2021-03-12 | 奇华顿股份有限公司 | 胶囊组合物 |
| CN108348783B (zh) * | 2015-11-17 | 2021-05-14 | 荷兰联合利华有限公司 | 氯咪巴唑微囊和包含表面活性剂和氯咪巴唑的毛发护理组合物 |
| EP3377035A1 (en) | 2015-11-18 | 2018-09-26 | Basf Se | Improvements in or relating to organic compounds |
| EP3170552A1 (en) | 2015-11-23 | 2017-05-24 | Basf Se | Microcapsule comprising a polymeric shell and a hydrophilic or hydrophobic core material |
| EP3295929A1 (en) * | 2016-09-19 | 2018-03-21 | S.P.C.M. Sa | Use of an ampholyte copolymer as colloidal stabilizer in a process of encapsulating fragrance |
| GB201615905D0 (en) * | 2016-09-19 | 2016-11-02 | Givaudan Sa | Improvements in or relating to organic compounds |
| JP6656422B2 (ja) * | 2016-12-27 | 2020-03-04 | 富士フイルム株式会社 | 水分散物及びその製造方法、並びに画像形成方法 |
| CN107698865B (zh) * | 2017-09-14 | 2020-04-03 | 陕西理工大学 | 一种注塑机螺杆清洗料的制备方法 |
| GB201804038D0 (en) | 2018-03-14 | 2018-04-25 | Givaudan Sa | Improvements in or realating to organic compounds |
| WO2019181988A1 (ja) * | 2018-03-23 | 2019-09-26 | 富士フイルム株式会社 | 中空粒子の製造方法、並びに、造孔材の製造方法、化粧料用粒子の製造方法、及び軽量化材の製造方法 |
| EP3784713B1 (en) * | 2018-04-24 | 2024-02-21 | Symrise AG | Core-shell capsules prepared with linear and cyclic aliphatic polyisocyanates |
| CN109231400B (zh) * | 2018-10-08 | 2021-09-21 | 华南理工大学 | 一种用于处理水体富营养化的悬浮木质素微胶囊及制备方法 |
| US12220677B2 (en) | 2019-02-13 | 2025-02-11 | Symrise Ag | Process for the preparation of microcapsules |
| EP3845304A1 (en) | 2019-12-30 | 2021-07-07 | Bayer AG | Capsule suspension concentrates based on polyisocyanates and biodegradable amine based cross-linker |
| CN111226923B (zh) * | 2020-03-09 | 2022-04-22 | 上海生农生化制品股份有限公司 | 一种吡唑醚菌酯·喹啉铜微胶囊悬浮-悬浮剂及其制备方法 |
| GB202003883D0 (en) | 2020-03-18 | 2020-05-06 | Givaudan Sa | Consumer product |
| BR112022026484A2 (pt) * | 2020-06-26 | 2023-01-31 | Bayer Ag | Concentrados de suspensão de cápsula aquosa compreendendo grupos éster biodegradáveis |
| US12434215B2 (en) | 2020-07-31 | 2025-10-07 | Morishita Jintan Co., Ltd. | Microcapsule production method |
| JP2023538276A (ja) | 2020-08-06 | 2023-09-07 | シムライズ アーゲー | マイクロカプセルの調製プロセス |
| CN116322326B (zh) | 2020-08-06 | 2025-05-02 | 西姆莱斯股份公司 | 聚脲/聚氨酯微胶囊 |
| CN116490265B (zh) | 2020-08-06 | 2025-11-21 | 西姆莱斯股份公司 | 可生物降解的聚脲/聚氨酯微胶囊 |
| GB202114226D0 (en) | 2021-10-05 | 2021-11-17 | Iberchem S A U | Microcapsules |
| WO2023147855A2 (de) | 2022-02-02 | 2023-08-10 | Symrise Ag | Verfahren zur herstellung von mikrokapseln |
| JP2025505605A (ja) | 2022-02-02 | 2025-02-28 | シムライズ アーゲー | マイクロカプセルの製造方法 |
| CN119678271A (zh) * | 2022-08-19 | 2025-03-21 | 松下知识产权经营株式会社 | 锂离子二次电池用的负极浆料、锂离子二次电池用的负极和锂离子二次电池 |
| CN117296839B (zh) * | 2023-11-27 | 2024-02-23 | 山东华实药业有限公司 | 免活化稳定性二氧化氯消毒剂及其生产工艺 |
| CN119257955B (zh) * | 2024-08-16 | 2025-09-23 | 广东丸美生物技术股份有限公司 | 含美妆功能物质水溶液的微胶囊及其制备方法、化妆品 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5342556A (en) * | 1991-09-16 | 1994-08-30 | Bayer Aktiengesellschaft | Microcapsules made of isocyanates with groups containing polyethylene oxide |
| WO2005016510A1 (en) * | 2003-08-14 | 2005-02-24 | Reaxa Limited | Microencapsulated catalyst-ligand system, methods of preparation and methods of use thereof |
| WO2007096592A1 (en) * | 2006-02-22 | 2007-08-30 | Reaxa Limited | Microencapsulated catalyst-ligand system |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3886085A (en) * | 1971-08-31 | 1975-05-27 | Fuji Photo Film Co Ltd | Process for producing fine oil-containing microcapsules having strong protective shells and microcapsules produced thereby |
| US4643764A (en) * | 1984-01-09 | 1987-02-17 | Stauffer Chemical Company | Multiple types of microcapsules and their production |
| DE3685920D1 (de) * | 1985-09-13 | 1992-08-13 | Ciba Geigy Ag | Verfahren zur herstellung von mikrokapseln. |
| FR2591124B1 (fr) * | 1985-12-10 | 1988-02-12 | Rhone Poulenc Spec Chim | Procede de microencapsulation par polyaddition-interfaciale. |
| ES2023942B3 (es) * | 1986-10-23 | 1992-02-16 | Ciba-Geigy Ag | Lucha contra los ectoparasitos. |
| FR2610537A1 (fr) * | 1987-02-11 | 1988-08-12 | Rhone Poulenc Chimie | Procede ameliore de microencapsulation par polyaddition interfaciale |
| JP2929294B2 (ja) * | 1989-05-30 | 1999-08-03 | 大日本インキ化学工業株式会社 | 顔料化されたポリウレタンポリ尿素粒子およびその製造方法 |
| US5011885A (en) * | 1989-10-27 | 1991-04-30 | The Mead Corporation | Methods for the production of microcapsules using functionalized isocyanate |
| US5225118A (en) * | 1990-08-15 | 1993-07-06 | Boise Cascade Corporation | Process for manufacturing polyurea microcapsules and product therefrom |
| EP0730406B1 (en) * | 1993-11-15 | 1998-07-08 | Zeneca Limited | Microcapsules containing suspensions of biologically active compounds |
| US5925595A (en) * | 1997-09-05 | 1999-07-20 | Monsanto Company | Microcapsules with readily adjustable release rates |
| US6653256B1 (en) * | 1999-08-24 | 2003-11-25 | Bayer Aktiengesellschaft | Microcapsule formulations |
| ATE309858T1 (de) * | 2000-06-05 | 2005-12-15 | Syngenta Ltd | Neue mikrokapseln |
| CA2311192A1 (en) * | 2000-06-12 | 2001-12-12 | Harald D. H. Stover | Encapsulation process using isocyanate moieties |
| DE10117784A1 (de) * | 2001-04-10 | 2002-10-17 | Bayer Ag | Mikrokapseln |
| US6992047B2 (en) * | 2001-04-11 | 2006-01-31 | Monsanto Technology Llc | Method of microencapsulating an agricultural active having a high melting point and uses for such materials |
| DE10156672A1 (de) * | 2001-11-17 | 2003-05-28 | Creavis Tech & Innovation Gmbh | Verfahren zur Herstellung von Mikrokapseln |
| AU2003232543B2 (en) * | 2002-05-31 | 2009-01-29 | Mcmaster University | Method of encapsulating hydrophobic organic molecules in polyurea capsules |
| EP1622713A1 (en) * | 2003-05-11 | 2006-02-08 | Ben Gurion University Of The Negev Research And Development Authority | Encapsulated essential oils |
| GB0526416D0 (en) * | 2005-12-23 | 2006-02-08 | Syngenta Ltd | Formulation |
| US8143345B2 (en) * | 2007-12-06 | 2012-03-27 | Prc Desoto International, Inc. | Water dispersible, hydroxyl-terminated, fluorinated polyurethanes and method of preparing the same |
-
2010
- 2010-06-25 ES ES10167305.1T patent/ES2628087T3/es active Active
- 2010-06-25 EP EP10167305.1A patent/EP2399667B1/en not_active Not-in-force
-
2011
- 2011-03-05 WO PCT/EP2011/001098 patent/WO2011160733A1/en not_active Ceased
- 2011-03-05 KR KR1020127033516A patent/KR101925269B1/ko not_active Expired - Fee Related
- 2011-03-05 MX MX2012015042A patent/MX341671B/es active IP Right Grant
- 2011-03-05 RU RU2013101538/05A patent/RU2572889C2/ru active
- 2011-03-05 JP JP2013515739A patent/JP5934703B2/ja not_active Expired - Fee Related
- 2011-03-05 BR BR112012032634-1A patent/BR112012032634B1/pt not_active IP Right Cessation
- 2011-03-05 US US13/805,549 patent/US20130095158A1/en not_active Abandoned
- 2011-03-05 CN CN201180031169.8A patent/CN102958597B/zh not_active Expired - Fee Related
- 2011-03-05 CA CA2803420A patent/CA2803420C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5342556A (en) * | 1991-09-16 | 1994-08-30 | Bayer Aktiengesellschaft | Microcapsules made of isocyanates with groups containing polyethylene oxide |
| WO2005016510A1 (en) * | 2003-08-14 | 2005-02-24 | Reaxa Limited | Microencapsulated catalyst-ligand system, methods of preparation and methods of use thereof |
| WO2007096592A1 (en) * | 2006-02-22 | 2007-08-30 | Reaxa Limited | Microencapsulated catalyst-ligand system |
Also Published As
| Publication number | Publication date |
|---|---|
| JP5934703B2 (ja) | 2016-06-15 |
| EP2399667B1 (en) | 2017-03-08 |
| CN102958597A (zh) | 2013-03-06 |
| BR112012032634B1 (pt) | 2018-12-26 |
| MX2012015042A (es) | 2013-06-28 |
| CA2803420A1 (en) | 2011-12-29 |
| CA2803420C (en) | 2018-05-01 |
| BR112012032634A2 (pt) | 2018-01-23 |
| RU2572889C2 (ru) | 2016-01-20 |
| EP2399667A1 (en) | 2011-12-28 |
| KR101925269B1 (ko) | 2018-12-05 |
| ES2628087T3 (es) | 2017-08-01 |
| MX341671B (es) | 2016-08-30 |
| RU2013101538A (ru) | 2014-07-27 |
| US20130095158A1 (en) | 2013-04-18 |
| WO2011160733A1 (en) | 2011-12-29 |
| KR20130121697A (ko) | 2013-11-06 |
| JP2013537472A (ja) | 2013-10-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150513 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |