CA2708595C - Formulation of a metalworking fluid - Google Patents
Formulation of a metalworking fluid Download PDFInfo
- Publication number
- CA2708595C CA2708595C CA2708595A CA2708595A CA2708595C CA 2708595 C CA2708595 C CA 2708595C CA 2708595 A CA2708595 A CA 2708595A CA 2708595 A CA2708595 A CA 2708595A CA 2708595 C CA2708595 C CA 2708595C
- Authority
- CA
- Canada
- Prior art keywords
- acid
- fluid composition
- metalworking fluid
- oil
- volume
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M103/00—Lubricating compositions characterised by the base-material being an inorganic material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/045—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
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- C10M173/00—Lubricating compositions containing more than 10% water
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- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
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- C10M173/00—Lubricating compositions containing more than 10% water
- C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
- C23F11/12—Oxygen-containing compounds
- C23F11/124—Carboxylic acids
- C23F11/126—Aliphatic acids
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- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
- C23F11/08—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids
- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
- C23F11/14—Nitrogen-containing compounds
- C23F11/141—Amines; Quaternary ammonium compounds
- C23F11/143—Salts of amines
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- C10M2201/06—Metal compounds
- C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
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- C10M2207/122—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms monocarboxylic
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/02—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/026—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a nitrile group
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/02—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/028—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds containing monomers having an unsaturated radical bound to a nitrogen-containing hetero ring
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/043—Ammonium or amine salts thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/06—Organic compounds derived from inorganic acids or metal salts
- C10M2227/066—Organic compounds derived from inorganic acids or metal salts derived from Mo or W
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2010/00—Metal present as such or in compounds
- C10N2010/02—Groups 1 or 11
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
- C10N2020/01—Physico-chemical properties
- C10N2020/055—Particles related characteristics
- C10N2020/06—Particles of special shape or size
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
- C10N2020/09—Characteristics associated with water
- C10N2020/091—Water solubility
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/16—Antiseptic; (micro) biocidal or bactericidal
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/24—Emulsion properties
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/01—Emulsions, colloids, or micelles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Lubricants (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/953,502 US20090149359A1 (en) | 2007-12-10 | 2007-12-10 | Formulation of a metal working fluid |
US11/953,502 | 2007-12-10 | ||
PCT/US2008/085483 WO2009076151A1 (en) | 2007-12-10 | 2008-12-04 | Formulation of a metalworking fluid |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2708595A1 CA2708595A1 (en) | 2009-06-18 |
CA2708595C true CA2708595C (en) | 2017-08-15 |
Family
ID=40364329
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2708595A Expired - Fee Related CA2708595C (en) | 2007-12-10 | 2008-12-04 | Formulation of a metalworking fluid |
Country Status (9)
Country | Link |
---|---|
US (1) | US20090149359A1 (ja) |
EP (1) | EP2075319A1 (ja) |
JP (1) | JP5704921B2 (ja) |
KR (2) | KR20100135218A (ja) |
CN (2) | CN101970621A (ja) |
BR (1) | BRPI0822063A2 (ja) |
CA (1) | CA2708595C (ja) |
MX (1) | MX360113B (ja) |
WO (1) | WO2009076151A1 (ja) |
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JP5394691B2 (ja) * | 2008-08-22 | 2014-01-22 | 出光興産株式会社 | 水溶性金属加工油剤および金属加工用クーラント |
WO2010027707A2 (en) * | 2008-08-28 | 2010-03-11 | Basf Corporation | Hydraulic fluid and method of preventing vapor corrosion |
DE102009030409A1 (de) * | 2009-06-25 | 2011-01-05 | Clariant International Limited | Wassergemischte Metallbearbeitungsflüssigkeiten, enthaltend Etherpyrrolidoncarbonsäuren |
JP5420498B2 (ja) * | 2010-08-03 | 2014-02-19 | ユシロ化学工業株式会社 | 固定砥粒ワイヤソー用水溶性加工液 |
CN102191121B (zh) * | 2011-03-22 | 2013-02-06 | 无锡市高润杰化学有限公司 | 一种多功能切削液 |
CN102757852B (zh) * | 2011-04-29 | 2014-04-23 | 中国石油化工股份有限公司 | 轧制润滑剂组合物及其用途 |
CA2835019C (en) | 2011-05-06 | 2018-04-10 | Chemetall Gmbh | Amine-free voc-free metal working fluid |
RU2461610C1 (ru) * | 2011-06-23 | 2012-09-20 | Общество с ограниченной ответственностью "Научное предприятие "Высокие технологии" | Смазочно-охлаждаюшая жидкость |
WO2013086483A1 (en) * | 2011-12-09 | 2013-06-13 | Evans Robert D | Metalworking fluid composition and method for its use in the machining of compacted graphite iron |
CN102585987B (zh) * | 2011-12-28 | 2013-12-25 | 烟台大学 | 一种水晶切割用的水悬浮切割剂 |
CN103361152A (zh) * | 2012-04-06 | 2013-10-23 | 王沛龙 | 水溶性超润滑抗磨剂 |
CN102766517B (zh) * | 2012-07-24 | 2014-01-15 | 东莞市安美润滑科技有限公司 | 全合成水性高硅铝合金切削液、制备方法及其使用方法 |
CN103627491B (zh) * | 2013-11-27 | 2015-02-11 | 常熟市劲力工具有限公司 | 圆盘刀加工用磨削液 |
CN104927998B (zh) * | 2014-03-20 | 2017-12-22 | 中国石油化工股份有限公司 | 微乳化切削液组合物 |
CN105001949B (zh) * | 2015-06-05 | 2018-04-24 | 上海贝能环保科技有限公司 | 一种生物降解环保准干切削液及其制备方法 |
EP3130654A1 (en) * | 2015-08-14 | 2017-02-15 | Sasol Performance Chemicals GmbH | Composition comprising 2-alkyl carboxylic acid salts and use thereof as anti-corrosion additive |
CN105695069A (zh) * | 2016-02-25 | 2016-06-22 | 天津高盛钢丝绳有限公司 | 一种钢丝绳湿式拉丝工艺用润滑剂 |
JP6904979B2 (ja) | 2016-03-01 | 2021-07-21 | エコラボ ユーエスエー インコーポレイティド | 第4級アニオン性界面活性剤の相乗効果に基づく殺菌すすぎ |
CA3031505C (en) | 2016-08-11 | 2021-09-14 | Ecolab Usa Inc. | Interaction between antimicrobial quaternary compounds and anionic surfactants |
CN106279568B (zh) * | 2016-08-31 | 2019-01-08 | 广州米奇化工有限公司 | 长链醇醚聚羧酸及其制备方法和应用 |
WO2019113068A1 (en) * | 2017-12-08 | 2019-06-13 | The Lubrizol Corporation | Maleated soybean oil derivatives as additives in metalworking fluids |
US10640723B2 (en) | 2018-03-16 | 2020-05-05 | Afton Chemical Corporation | Lubricants containing amine salt of acid phosphate and hydrocarbyl borate |
CN108949332B (zh) * | 2018-08-06 | 2021-08-10 | 广州市方川润滑科技有限公司 | 一种汽车空调滤清器盖板的环保型攻丝液的制备方法及环保型攻丝液 |
CN109097176A (zh) * | 2018-08-30 | 2018-12-28 | 江苏欧仕达润滑油有限公司 | 一种微量润滑切削液及其制备方法 |
JP7221479B2 (ja) * | 2018-08-31 | 2023-02-14 | 日化精工株式会社 | ダイシング加工用製剤及び加工処理液 |
CN109370715A (zh) * | 2018-09-07 | 2019-02-22 | 苏州安美润滑科技有限公司 | 一种多效冲压油及其制备方法 |
CN109337733B (zh) * | 2018-11-09 | 2021-06-25 | 上海金兆节能科技有限公司 | 润滑剂组合物及其制备方法和用该组合物制备微量切削液 |
CN109536251B (zh) * | 2018-11-09 | 2021-06-01 | 上海金兆节能科技有限公司 | 润滑油组合物及其制备方法和用该组合物制备微量润滑油 |
CN110305728B (zh) * | 2019-08-07 | 2021-12-17 | 上海工程技术大学 | 一种高分子塑性成形用润滑剂及制备方法 |
CN110846118A (zh) * | 2019-11-29 | 2020-02-28 | 蓝思科技(长沙)有限公司 | 一种环保水基切削液及其制备方法 |
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2007
- 2007-12-10 US US11/953,502 patent/US20090149359A1/en not_active Abandoned
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2008
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- 2008-12-04 JP JP2010538060A patent/JP5704921B2/ja not_active Expired - Fee Related
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- 2008-12-04 BR BRPI0822063-8A patent/BRPI0822063A2/pt not_active IP Right Cessation
- 2008-12-04 KR KR1020107015131A patent/KR20100135218A/ko active Search and Examination
- 2008-12-04 KR KR1020167027230A patent/KR20160120787A/ko not_active Application Discontinuation
- 2008-12-04 CA CA2708595A patent/CA2708595C/en not_active Expired - Fee Related
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MX2010006315A (es) | 2010-10-05 |
CN106635320A (zh) | 2017-05-10 |
EP2075319A1 (en) | 2009-07-01 |
KR20100135218A (ko) | 2010-12-24 |
KR20160120787A (ko) | 2016-10-18 |
BRPI0822063A2 (pt) | 2015-06-23 |
WO2009076151A1 (en) | 2009-06-18 |
JP2011506683A (ja) | 2011-03-03 |
CA2708595A1 (en) | 2009-06-18 |
JP5704921B2 (ja) | 2015-04-22 |
CN101970621A (zh) | 2011-02-09 |
MX360113B (es) | 2018-10-23 |
US20090149359A1 (en) | 2009-06-11 |
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