BR9915651B1 - processo para a preparaÇço de Ácidos alcanossulfânicos. - Google Patents

processo para a preparaÇço de Ácidos alcanossulfânicos. Download PDF

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Publication number
BR9915651B1
BR9915651B1 BRPI9915651-2A BR9915651A BR9915651B1 BR 9915651 B1 BR9915651 B1 BR 9915651B1 BR 9915651 A BR9915651 A BR 9915651A BR 9915651 B1 BR9915651 B1 BR 9915651B1
Authority
BR
Brazil
Prior art keywords
nitric acid
dialkyl
oxidation
process according
reactor
Prior art date
Application number
BRPI9915651-2A
Other languages
English (en)
Portuguese (pt)
Other versions
BR9915651A (pt
Inventor
Matthias Eiermann
Christian Tragut
Klaus Ebel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Publication of BR9915651A publication Critical patent/BR9915651A/pt
Publication of BR9915651B1 publication Critical patent/BR9915651B1/pt

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/16Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by oxidation of thiols, sulfides, hydropolysulfides, or polysulfides with formation of sulfo or halosulfonyl groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
BRPI9915651-2A 1998-11-25 1999-11-22 processo para a preparaÇço de Ácidos alcanossulfânicos. BR9915651B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19854428A DE19854428A1 (de) 1998-11-25 1998-11-25 Verfahren zur Herstellung von Alkansulfonsäuren
DE19854428.6 1998-11-25
PCT/EP1999/008994 WO2000031027A1 (de) 1998-11-25 1999-11-22 Verfahren zur herstellung von alkansulfonsäuren

Publications (2)

Publication Number Publication Date
BR9915651A BR9915651A (pt) 2001-08-07
BR9915651B1 true BR9915651B1 (pt) 2011-07-26

Family

ID=7889013

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI9915651-2A BR9915651B1 (pt) 1998-11-25 1999-11-22 processo para a preparaÇço de Ácidos alcanossulfânicos.

Country Status (20)

Country Link
US (1) US6531629B1 (enExample)
EP (1) EP1133470B1 (enExample)
JP (1) JP4294874B2 (enExample)
KR (1) KR100599637B1 (enExample)
CN (1) CN1163479C (enExample)
AT (1) ATE240938T1 (enExample)
AU (1) AU765481B2 (enExample)
BR (1) BR9915651B1 (enExample)
CA (1) CA2350490C (enExample)
DE (2) DE19854428A1 (enExample)
ES (1) ES2200582T3 (enExample)
HU (1) HUP0104484A3 (enExample)
IN (1) IN207425B (enExample)
MX (1) MXPA01004496A (enExample)
PL (1) PL197882B1 (enExample)
RU (1) RU2230735C2 (enExample)
SK (1) SK7152001A3 (enExample)
UA (1) UA66896C2 (enExample)
WO (1) WO2000031027A1 (enExample)
ZA (1) ZA200104256B (enExample)

Families Citing this family (39)

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US7820145B2 (en) * 2003-08-04 2010-10-26 Foamix Ltd. Oleaginous pharmaceutical and cosmetic foam
JP4441726B2 (ja) * 2003-01-24 2010-03-31 石原薬品株式会社 スズ又はスズ合金の脂肪族スルホン酸メッキ浴の製造方法
ES2726013T3 (es) * 2003-05-12 2019-10-01 Arkema Inc Soluciones electrolíticas de ácido sulfónico de pureza elevada
US9399618B2 (en) * 2003-05-12 2016-07-26 Arkema Inc. High purity electrolytic sulfonic acid solutions
OA13183A (en) * 2003-06-21 2006-12-13 Alan K Richards Anhydrous processing of methane into methane-sulfonic acid, methanol, and other compounds.
FR2935142B1 (fr) * 2008-08-20 2010-11-19 Arkema France Dimethyldisulfure issu au moins partiellement de matieres renouvellables
KR101676888B1 (ko) * 2008-12-23 2016-11-16 바스프 에스이 황화수소 함유 기체의 압축 방법
CA2779546C (en) * 2009-11-03 2018-11-06 Basf Se Method for handling aqueous methanesulfonic acid solutions
GB201100531D0 (en) 2011-01-13 2011-03-02 Phosphonics Functionalised materials, processes for the production and uses thereof
MY165223A (en) 2011-04-14 2018-03-13 Basf Se Method of dissolving and/or inhibiting the deposition of scale on a surface of a system
US8648026B2 (en) 2011-11-30 2014-02-11 Basf Se Composition comprising an alkanesulfonic acid for dissolving and/or inhibiting deposition of scale on a surface of a system
WO2013155383A1 (en) 2012-04-12 2013-10-17 Basf Se Cleaning composition for dishwashing
WO2015077737A1 (en) 2013-11-25 2015-05-28 Basf Se Cleaning concentrate for removing scale from a surface of a system
EP3079811B1 (en) 2013-12-11 2017-04-05 Evonik Degussa GmbH A catalyst for oxidation reactions, a method for its preparation and the use thereof
WO2015085522A1 (en) 2013-12-11 2015-06-18 Evonik Industries Ag Process for preparing alkanesulphonic acids
KR20160130421A (ko) 2014-03-04 2016-11-11 바스프 에스이 오일의 탈검 및 에스테르화 방법
AU2015227368B2 (en) 2014-03-04 2018-08-02 Basf Se Method of delinting cotton seeds
EP3035046A1 (de) 2014-12-19 2016-06-22 Evonik Degussa GmbH Verfahren zur Bestimmung eines Dialkyldisulfids
MX2018004011A (es) 2015-09-28 2018-05-23 Basf Se Metodo de neutralizacion de semillas de algodon.
CA3004795A1 (en) * 2015-11-10 2017-05-18 Basf Se Process for purifying alkanesulfonic acids
KR102670176B1 (ko) 2015-11-10 2024-05-28 바스프 에스이 알칸설폰산의 재가공 방법
EP3173405A1 (de) 2015-11-30 2017-05-31 Evonik Degussa GmbH Verfahren zur herstellung einer alkansulfonsäure
EP3472331A1 (en) 2016-06-20 2019-04-24 Basf Se Process for producing ethanol from corn comprising dry-milling and adding alkanesulfonic acid to the separated corn fiber
CA3027739A1 (en) 2016-06-20 2017-12-28 Basf Se Process for producing ethanol from corn comprising dry-milling and adding alkanesulfonic acid to the fermented mash
MX392504B (es) 2016-06-20 2025-03-24 Basf Se Proceso de produccion de etanol a partir de maiz.
KR20190028444A (ko) 2016-07-18 2019-03-18 바스프 에스이 축합 반응을 위한 낮은 부식 알칸 술폰산
TW201841881A (zh) 2017-04-18 2018-12-01 德商巴斯夫歐洲公司 純化烷烴磺酸酐的方法及使用純化的烷烴磺酸酐製造烷烴磺酸的方法
WO2018208701A1 (en) 2017-05-11 2018-11-15 Arkema Inc. Processes and systems for recovering methanesulfonic acid in purified form
US10899705B2 (en) 2017-05-30 2021-01-26 Basf Se Process for the manufacturing of methane sulfonic acid
EP3453447B1 (en) 2017-09-06 2020-12-23 Evonik Operations GmbH Process for the preparation of alkanesulfonic acid
EP3456708B1 (en) * 2017-09-13 2020-07-01 Evonik Operations GmbH Process for operating a plant for preparing an alkanesulfonic acid
CN107698468A (zh) * 2017-10-18 2018-02-16 辽宁省轻工设计院有限公司 甲基磺酸的制备工艺
US11247967B2 (en) 2018-02-07 2022-02-15 Basf Se Process for the manufacturing of alkanesulfonic acids
WO2020126855A1 (en) * 2018-12-21 2020-06-25 Basf Se Mixture comprising methanesulfonic acid and sulfuric acid
MX2022001602A (es) 2019-08-07 2022-03-11 Basf Se Recuperacion de acido metansulfonico libre de agua del flujo de fondo de una columna de destilacion.
CA3156366A1 (en) * 2019-10-01 2021-04-08 Basf Se PROCESS FOR THE PRODUCTION OF ALKANESULPHONIC ACIDS
CN113214120B (zh) * 2021-03-25 2022-10-04 四川上氟科技有限公司 一种全氟己基乙基磺酸盐的制备方法
WO2023156430A1 (en) 2022-02-18 2023-08-24 Basf Se Process for producing alkyl sulfonic acid
CN117924122A (zh) * 2023-12-26 2024-04-26 万华化学集团股份有限公司 一种甲基磺酸的制备方法

Family Cites Families (4)

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Publication number Priority date Publication date Assignee Title
US2697722A (en) * 1951-01-13 1954-12-21 Standard Oil Co Manufacture of sulfonic acids
US2727920A (en) * 1951-04-20 1955-12-20 Standard Oil Co Oxidation of mercaptans to sulfonic acids
RU2062268C1 (ru) * 1993-11-25 1996-06-20 Акционерное общество "Синтез" Способ получения метансульфокислоты
WO1998034914A1 (en) * 1997-02-10 1998-08-13 Innochem Inc. Preparation of alkane sulfonic acids and sulfonyl chlorides by oxidation of alkanethiols and dialkyl disulfides

Also Published As

Publication number Publication date
UA66896C2 (uk) 2004-06-15
HUP0104484A3 (en) 2003-07-28
ZA200104256B (en) 2002-05-24
CA2350490C (en) 2008-03-04
MXPA01004496A (es) 2002-03-01
DE19854428A1 (de) 2000-05-31
CA2350490A1 (en) 2000-06-02
US6531629B1 (en) 2003-03-11
KR100599637B1 (ko) 2006-07-12
KR20010092744A (ko) 2001-10-26
PL347973A1 (en) 2002-05-06
CN1163479C (zh) 2004-08-25
IN2001CH00725A (enExample) 2006-08-25
WO2000031027A1 (de) 2000-06-02
BR9915651A (pt) 2001-08-07
ATE240938T1 (de) 2003-06-15
EP1133470A1 (de) 2001-09-19
SK7152001A3 (en) 2002-01-07
MX217997B (enExample) 2003-12-08
AU765481B2 (en) 2003-09-18
EP1133470B1 (de) 2003-05-21
IN207425B (enExample) 2007-06-29
DE59905681D1 (de) 2003-06-26
ES2200582T3 (es) 2004-03-01
PL197882B1 (pl) 2008-05-30
HUP0104484A2 (hu) 2002-03-28
CN1328544A (zh) 2001-12-26
JP2002530369A (ja) 2002-09-17
AU1859300A (en) 2000-06-13
JP4294874B2 (ja) 2009-07-15
RU2230735C2 (ru) 2004-06-20

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFERIDO O PEDIDO COM BASE NOS ARTIGOS 8O E 13 DA LPI.

B12B Appeal against refusal [chapter 12.2 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 26/07/2011, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE A 19A ANUIDADE.

B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2494 DE 23-10-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.