BR112018014841A2 - método de fabricação para álcool de cadeia longa cicloexenona de alta pureza - Google Patents
método de fabricação para álcool de cadeia longa cicloexenona de alta purezaInfo
- Publication number
- BR112018014841A2 BR112018014841A2 BR112018014841-5A BR112018014841A BR112018014841A2 BR 112018014841 A2 BR112018014841 A2 BR 112018014841A2 BR 112018014841 A BR112018014841 A BR 112018014841A BR 112018014841 A2 BR112018014841 A2 BR 112018014841A2
- Authority
- BR
- Brazil
- Prior art keywords
- preparing high
- chain alcohols
- purity
- cyclohexenone long
- formula
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/42—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/16—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of hydrazones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/72—Hydrazones
- C07C251/86—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C281/00—Derivatives of carbonic acid containing functional groups covered by groups C07C269/00 - C07C279/00 in which at least one nitrogen atom of these functional groups is further bound to another nitrogen atom not being part of a nitro or nitroso group
- C07C281/06—Compounds containing any of the groups, e.g. semicarbazides
- C07C281/08—Compounds containing any of the groups, e.g. semicarbazides the other nitrogen atom being further doubly-bound to a carbon atom, e.g. semicarbazones
- C07C281/14—Compounds containing any of the groups, e.g. semicarbazides the other nitrogen atom being further doubly-bound to a carbon atom, e.g. semicarbazones the carbon atom being further bound to a carbon atom of a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
- C07C311/48—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups having nitrogen atoms of sulfonamide groups further bound to another hetero atom
- C07C311/49—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups having nitrogen atoms of sulfonamide groups further bound to another hetero atom to nitrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/516—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of nitrogen-containing compounds to >C = O groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
- C07C49/703—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups
- C07C49/713—Unsaturated compounds containing a keto groups being part of a ring containing hydroxy groups a keto group being part of a six-membered ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/72—Hydrazones
- C07C251/84—Hydrazones having doubly-bound carbon atoms of hydrazone groups being part of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
- C07C49/753—Unsaturated compounds containing a keto groups being part of a ring containing ether groups, groups, groups, or groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyrane Compounds (AREA)
Abstract
a presente invenção refere-se a um método de produção para um composto álcool de cadeia longa de cicloexenona de alta pu-reza representado pela fórmula (i). o método de produção para o com-posto representado pela fórmula (i) adota uma reação de barbier indu-zida por metal. a invenção tem as vantagens de um curso de reação curto, rendimento alto e pureza de produto alta e é adequada para aumento industrialmente.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610044990 | 2016-01-22 | ||
CN201610044990.8 | 2016-01-22 | ||
PCT/CN2017/072078 WO2017125087A1 (zh) | 2016-01-22 | 2017-01-22 | 一种高纯度环己烯酮长链醇的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
BR112018014841A2 true BR112018014841A2 (pt) | 2018-12-18 |
BR112018014841B1 BR112018014841B1 (pt) | 2022-03-03 |
Family
ID=59361489
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR112018014841-5A BR112018014841B1 (pt) | 2016-01-22 | 2017-01-22 | Álcoois de cadeia longa cicloexenona, seus usos e métodos para a produção dos mesmos com alta pureza |
Country Status (12)
Country | Link |
---|---|
US (1) | US11485696B2 (pt) |
EP (1) | EP3406586B1 (pt) |
JP (1) | JP6807396B2 (pt) |
KR (1) | KR102387362B1 (pt) |
AU (1) | AU2017209644B2 (pt) |
BR (1) | BR112018014841B1 (pt) |
CA (1) | CA3011913C (pt) |
ES (1) | ES2849425T3 (pt) |
MX (1) | MX2018008936A (pt) |
RU (1) | RU2729186C2 (pt) |
TW (1) | TWI728042B (pt) |
WO (1) | WO2017125087A1 (pt) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111848552B (zh) * | 2019-04-28 | 2023-12-19 | 南京富润凯德生物医药有限公司 | 一种3-(取代苯基)氧杂环丁烷-3-羧酸及其中间体的制备方法及应用 |
CN111662262B (zh) * | 2020-06-29 | 2023-04-28 | 陕西大美化工科技有限公司 | 6-(4-((2-环己硫基乙基)氨基)苯基)四氢-2h-吡喃-2-酮的合成方法 |
KR20230043923A (ko) | 2020-08-07 | 2023-03-31 | 다이호야쿠힌고교 가부시키가이샤 | 신규 시클로알케논 화합물 또는 그의 염 |
TW202342414A (zh) * | 2022-02-09 | 2023-11-01 | 日商大鵬藥品工業股份有限公司 | 環己烯酮化合物之結晶形 |
CN115353449B (zh) * | 2022-08-12 | 2024-02-20 | 东莞理工学院 | 二价钐单电子还原试剂、制备方法及其应用 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2306918A1 (de) | 1973-02-13 | 1974-08-15 | Bayer Ag | Benzaldehyd-sulfonylhydrazone, verfahren zu ihrer herstellung und ihre verwendung zur bekaempfung von hasenartigen und nagetieren |
DE3924241A1 (de) * | 1989-07-21 | 1991-01-31 | Shell Int Research | Neue glyoxyl-cyclohexendione, verfahren zu ihrer herstellung, diese verbindungen enthaltende formulierungen und ihre verwendung |
JPH1017520A (ja) | 1996-06-26 | 1998-01-20 | Nippon Kayaku Co Ltd | 芳香族化合物のホルミル化法 |
EP1003706B1 (en) * | 1997-08-13 | 2003-03-05 | Meiji Milk Products Company Limited | Cyclohexenone long-chain alcohol and medicament containing same |
JP4469441B2 (ja) * | 1999-02-10 | 2010-05-26 | 明治乳業株式会社 | 神経変性疾患の予防又は治療薬 |
WO2002029014A2 (en) | 2000-10-04 | 2002-04-11 | Meiji Dairies Corporation | Stem cell differentiation-inducing promoter |
JP4861560B2 (ja) | 2001-02-19 | 2012-01-25 | 株式会社明治 | 糖尿病合併症治療剤 |
JP3905340B2 (ja) | 2001-09-13 | 2007-04-18 | 独立行政法人科学技術振興機構 | 有機金属化合物の新規調製法 |
JP4035332B2 (ja) | 2002-01-22 | 2008-01-23 | 明治乳業株式会社 | シクロヘキセノン長鎖アルコールの製造法 |
US7235700B2 (en) * | 2003-03-28 | 2007-06-26 | Meiji Dairies Corporation | Process for producing cyclohexenone long-chain alcohols |
JP2011051904A (ja) | 2009-08-31 | 2011-03-17 | Kansai Electric Power Co Inc:The | 第3級アルコールの製造方法 |
MX2013002981A (es) | 2010-09-16 | 2013-04-05 | Basf Se | Proceso para preparar 2-metil-3-(4-ter-butilfenil)propanal con para-isomericos de alta pureza. |
WO2013147072A1 (ja) | 2012-03-29 | 2013-10-03 | 大鵬薬品工業株式会社 | 3-(15-ヒドロキシペンタデシル)-2,4,4-トリメチル-2-シクロヘキセン-1-オンの共結晶 |
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2017
- 2017-01-22 EP EP17741118.8A patent/EP3406586B1/en active Active
- 2017-01-22 CA CA3011913A patent/CA3011913C/en active Active
- 2017-01-22 RU RU2018130292A patent/RU2729186C2/ru active
- 2017-01-22 US US16/071,709 patent/US11485696B2/en active Active
- 2017-01-22 JP JP2018538103A patent/JP6807396B2/ja active Active
- 2017-01-22 MX MX2018008936A patent/MX2018008936A/es unknown
- 2017-01-22 KR KR1020187023680A patent/KR102387362B1/ko active IP Right Grant
- 2017-01-22 WO PCT/CN2017/072078 patent/WO2017125087A1/zh active Application Filing
- 2017-01-22 AU AU2017209644A patent/AU2017209644B2/en active Active
- 2017-01-22 BR BR112018014841-5A patent/BR112018014841B1/pt active IP Right Grant
- 2017-01-22 ES ES17741118T patent/ES2849425T3/es active Active
- 2017-01-23 TW TW106102506A patent/TWI728042B/zh active
Also Published As
Publication number | Publication date |
---|---|
JP2019504079A (ja) | 2019-02-14 |
KR102387362B1 (ko) | 2022-04-15 |
AU2017209644A2 (en) | 2018-08-30 |
WO2017125087A1 (zh) | 2017-07-27 |
MX2018008936A (es) | 2018-11-09 |
US20210101859A1 (en) | 2021-04-08 |
ES2849425T3 (es) | 2021-08-18 |
JP6807396B2 (ja) | 2021-01-06 |
AU2017209644B2 (en) | 2020-08-13 |
BR112018014841B1 (pt) | 2022-03-03 |
RU2729186C2 (ru) | 2020-08-05 |
EP3406586B1 (en) | 2020-12-30 |
CA3011913C (en) | 2023-02-14 |
EP3406586A4 (en) | 2019-09-11 |
US11485696B2 (en) | 2022-11-01 |
TW201728561A (zh) | 2017-08-16 |
EP3406586A1 (en) | 2018-11-28 |
AU2017209644A1 (en) | 2018-08-09 |
RU2018130292A (ru) | 2020-02-25 |
TWI728042B (zh) | 2021-05-21 |
KR20180108669A (ko) | 2018-10-04 |
RU2018130292A3 (pt) | 2020-03-12 |
CA3011913A1 (en) | 2017-07-27 |
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Legal Events
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B06W | Patent application suspended after preliminary examination (for patents with searches from other patent authorities) chapter 6.23 patent gazette] | ||
B350 | Update of information on the portal [chapter 15.35 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
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