MX2013002981A - Proceso para preparar 2-metil-3-(4-ter-butilfenil)propanal con para-isomericos de alta pureza. - Google Patents
Proceso para preparar 2-metil-3-(4-ter-butilfenil)propanal con para-isomericos de alta pureza.Info
- Publication number
- MX2013002981A MX2013002981A MX2013002981A MX2013002981A MX2013002981A MX 2013002981 A MX2013002981 A MX 2013002981A MX 2013002981 A MX2013002981 A MX 2013002981A MX 2013002981 A MX2013002981 A MX 2013002981A MX 2013002981 A MX2013002981 A MX 2013002981A
- Authority
- MX
- Mexico
- Prior art keywords
- tert
- producing
- propanal
- butylphenyl
- methyl
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/42—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by hydrolysis
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/511—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups
- C07C45/515—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition involving transformation of singly bound oxygen functional groups to >C = O groups the singly bound functional group being an acetalised, ketalised hemi-acetalised, or hemi-ketalised hydroxyl group
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
- C07C45/72—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
- C07C45/74—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups combined with dehydration
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
- C07C45/82—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/85—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to a chemical modification
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
- C25B3/20—Processes
- C25B3/23—Oxidation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La presente invención se relaciona a un proceso para preparar 2-metil-3-(4-ter-butil-fenil)propanal con para-isómeros de alta pureza, y también a un proceso para preparar 4-ter-butilbenzaldehí do con para-isómeros de alta pureza.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP10177074 | 2010-09-16 | ||
PCT/EP2011/065596 WO2012034930A1 (de) | 2010-09-16 | 2011-09-09 | Verfahren zur herstellung von 2-methyl-3-(4-tert-butylphenyl)-propanal mit hoher para-isomerenreinheit |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2013002981A true MX2013002981A (es) | 2013-04-05 |
Family
ID=44584191
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2013002981A MX2013002981A (es) | 2010-09-16 | 2011-09-09 | Proceso para preparar 2-metil-3-(4-ter-butilfenil)propanal con para-isomericos de alta pureza. |
Country Status (7)
Country | Link |
---|---|
US (1) | US8614358B2 (es) |
EP (1) | EP2616424B1 (es) |
JP (1) | JP5869577B2 (es) |
CN (1) | CN103119014B (es) |
ES (1) | ES2553873T3 (es) |
MX (1) | MX2013002981A (es) |
WO (1) | WO2012034930A1 (es) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2012034930A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur herstellung von 2-methyl-3-(4-tert-butylphenyl)-propanal mit hoher para-isomerenreinheit |
JP2015527483A (ja) * | 2012-06-15 | 2015-09-17 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | 求核試薬の存在下での有機基材の陽極酸化 |
CN104151151B (zh) * | 2014-07-30 | 2016-01-20 | 天泽恩源(天津)制药有限公司 | 一种曲前列尼尔(Treprostinil)的合成方法 |
AU2017209644B2 (en) | 2016-01-22 | 2020-08-13 | Taiho Pharmaceutical Co., Ltd. | Manufacturing method for high-purity cyclohexenone long-chain alcohol |
CN110746280B (zh) * | 2019-10-14 | 2022-10-11 | 湖北荆洪生物科技股份有限公司 | 一种4-叔丁基苯甲醛的合成方法 |
WO2023053860A1 (ja) * | 2021-09-29 | 2023-04-06 | 三菱瓦斯化学株式会社 | アルデヒド組成物 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL99111C (es) * | 1956-06-11 | |||
AT337145B (de) * | 1974-12-14 | 1977-06-10 | Ruhrchemie Ag | Verfahren zur gewinnung reiner n-aldehyde |
US4318783A (en) | 1978-11-30 | 1982-03-09 | Bayer Aktiengesellschaft | Process for the preparation of optionally substituted benzaldehyde dialkyl acetals |
JPS5620174A (en) * | 1979-07-27 | 1981-02-25 | Fuso Kagaku Kogyo Kk | Preparation of p-t-butylbenzaldehyde and its acetal |
EP0045571B1 (en) | 1980-07-09 | 1985-06-26 | BUSH BOAKE ALLEN Limited | Process for the production of phenyl substituted aldehydes and of phenyl substituted alcohols |
DE4106661A1 (de) | 1991-03-02 | 1992-09-03 | Basf Ag | 2-methylbenzaldehyddialkylacetale |
DE4327361A1 (de) | 1993-08-14 | 1995-02-16 | Basf Ag | Verfahren zur Herstellung von Benzaldehyddialkylacetalen |
ES2144067T3 (es) * | 1994-05-31 | 2000-06-01 | Firmenich & Cie | Nuevos compuestos aromaticos y utilizacion de los mismos en perfumeria. |
DE19949672A1 (de) | 1999-10-14 | 2001-04-19 | Basf Ag | Kontinuierliches Verfahren zur Herstellung von Zimtaldehydderivaten |
US6686507B2 (en) * | 2002-03-06 | 2004-02-03 | Pfizer Inc | Purification of 2-methoxy-5-trifluoromethoxybenzaldehyde |
DE10223970A1 (de) | 2002-05-29 | 2003-12-24 | Basf Ag | Isolierung von Dihydrozimtaldehyden aus einem Rohgemisch |
DE102004011427A1 (de) | 2004-03-09 | 2005-09-29 | Basf Ag | Absorptionsmittel mit verbesserter Oxidationsbeständigkeit und Verfahren zum Entsäuern von Fluidströmen |
DE102005049568A1 (de) * | 2005-10-17 | 2007-04-19 | Basf Ag | Verfahren zur kontinuierlichen Hydrierung oder hydrierenden Aminierung |
WO2009059944A1 (de) * | 2007-11-06 | 2009-05-14 | Basf Se | Elektrochemisches verfahren zur herstellung von benzaldehyddimethylacetalen |
WO2010108874A1 (de) | 2009-03-27 | 2010-09-30 | Basf Se | Elektrochemisches verfahern zur herstellung von 3-tert.-butylbenzaldehyd-dimethylacetal |
WO2012034930A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur herstellung von 2-methyl-3-(4-tert-butylphenyl)-propanal mit hoher para-isomerenreinheit |
-
2011
- 2011-09-09 WO PCT/EP2011/065596 patent/WO2012034930A1/de active Application Filing
- 2011-09-09 EP EP11754665.5A patent/EP2616424B1/de active Active
- 2011-09-09 ES ES11754665.5T patent/ES2553873T3/es active Active
- 2011-09-09 MX MX2013002981A patent/MX2013002981A/es active IP Right Grant
- 2011-09-09 JP JP2013528611A patent/JP5869577B2/ja active Active
- 2011-09-09 CN CN201180044817.3A patent/CN103119014B/zh active Active
- 2011-09-16 US US13/234,809 patent/US8614358B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
CN103119014B (zh) | 2016-01-20 |
CN103119014A (zh) | 2013-05-22 |
ES2553873T3 (es) | 2015-12-14 |
WO2012034930A1 (de) | 2012-03-22 |
US20120071696A1 (en) | 2012-03-22 |
JP5869577B2 (ja) | 2016-02-24 |
US8614358B2 (en) | 2013-12-24 |
EP2616424A1 (de) | 2013-07-24 |
JP2013538220A (ja) | 2013-10-10 |
EP2616424B1 (de) | 2015-08-26 |
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